Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:623-79-0
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:623-79-0
Min.Order:0
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Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:623-79-0
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:623-79-0
Min.Order:1 Kilogram
FOB Price: $24.0
Type:Lab/Research institutions
inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
CAS:623-79-0 C5H10OS2Appearance:white poweder Storage:under the cool and dry area Package:Plastic vacuum packaging bag or bucket Application:CAS:623-79-0 C5H10OS2 technical grade or OLED grade Transportation:by express or by sea
We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white crystals powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as
O,S-Diethyl dithiocarbonate cas 623-79-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:623-79-0
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryO,S-Diethyl dithiocarbonate Basic information Product Name: O,S-Diethyl dithiocarbonate
YUYONGMEI was established in Aug,1999, located in the industrial park of Nanjing University of Technology, It is a private enterprises in Jiangsu Province with 1200 square meters’ R&D center. Our R&D center has a well-equipped synthetic laboratory a
Cas:623-79-0
Min.Order:0
Negotiable
Type:Trading Company
inquiryhigh purity Application:Drug intermediates Materials intermediates and active molecules
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water for 1.5h; Ambient temperature; | 93% |
Conditions | Yield |
---|---|
18-crown-6 ether In dichloromethane for 1h; Ambient temperature; | 82% |
In ethanol for 2h; Heating; | 55% |
With ethanol |
Conditions | Yield |
---|---|
In toluene Heating; Irradiation; | 69% |
Zersetzen; | |
In toluene for 0.0833333h; Heating; Irradiation; Yield given; |
Conditions | Yield |
---|---|
In n-heptane for 2.5h; Heating; Irradiation; | 59% |
Heating; Irradiation; | 59% |
In toluene Heating; Irradiation; |
Conditions | Yield |
---|---|
In acetone for 22h; Ambient temperature; Yield given. Further byproducts given; | A 11% B n/a C 30% D 12% |
In acetone for 22h; Ambient temperature; Further byproducts given; | A 11% B n/a C 30% D 12% |
Conditions | Yield |
---|---|
In acetone for 22h; Ambient temperature; Further byproducts given; | A 11% B 1.6% C 30% D 12% |
Conditions | Yield |
---|---|
With 7,8-Dibromobicyclo<4.2.0>octa-2,4-diene In N,N-dimethyl-formamide for 18h; Ambient temperature; Further byproducts given; | A 29% B n/a C 25% D 10% |
Conditions | Yield |
---|---|
With ethanol | |
In ethanol | |
In acetone Heating; | |
With ethanol for 4h; Esterification; Heating; | |
In ethanol for 4h; Heating; |
Conditions | Yield |
---|---|
With ethanol |
bis-ethoxythiocarbonyldisulfane
A
carbon disulfide
B
O,S-Diethyl dithiocarbonate
C
thiocarbonic acid O,O'-diethyl ester
D
methylammonium carbonate
Conditions | Yield |
---|---|
bei der Destillation; Produkt 5:Schwefel; |
Conditions | Yield |
---|---|
at 200 - 210℃; | |
Zersetzen; |
bis-ethoxythiocarbonyldisulfane
A
O,S-Diethyl dithiocarbonate
B
thiocarbonic acid O,O'-diethyl ester
Conditions | Yield |
---|---|
bei der Destillation; |
Conditions | Yield |
---|---|
at 135℃; Zersetzen; |
Conditions | Yield |
---|---|
at 135℃; Zersetzen; |
2-methyl-5-nitrobenzene-1-sulfonyl chloride
potassium ethyl xanthogenate
A
O,S-Diethyl dithiocarbonate
B
bis-ethoxythiocarbonyldisulfane
Conditions | Yield |
---|---|
Erhitzen unter vermindertem Druck; |
Conditions | Yield |
---|---|
With benzenesulfonyl chloride | |
With p-toluenesulfonyl chloride | |
With 2-Naphthalenesulfonyl chloride | |
With 2-Naphthalenesulfonyl chloride at 100℃; | |
With 5-diazonio-6-nitroindan chloride |
potassium ethyl xanthogenate
benzenesulfonyl chloride
A
O,S-Diethyl dithiocarbonate
B
diphenyl disulfone
C
potassium benzenesulfonate
Conditions | Yield |
---|---|
at 0℃; analoge Reaktion mit anderen Sulfonsaeurechloriden; |
diethyl dibromomalonate
potassium ethyl xanthogenate
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
With 2,3-dimethyl-buta-1,3-diene |
bis(ethoxythiocarbonyl) sulfide
bis-(2,2,2-trimethylethyl) xanthic anhydride
A
O,S-Diethyl dithiocarbonate
D
O,S-di-(2,2,2-trimethylethyl) dithiocarbonate
Conditions | Yield |
---|---|
In toluene Irradiation; Title compound not separated from byproducts; |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
under 15 Torr; bei der Destillation; |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
at 350℃; |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
at 50 - 60℃; im Hochvakuum; |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
at 350℃; |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
at 350℃; |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
at 350℃; |
ethyl isothiocyanate
sulfuric acid
A
O,S-Diethyl dithiocarbonate
B
carbon dioxide
C
ammonia
ethyl isothiocyanate
sulfuric acid
A
O,S-Diethyl dithiocarbonate
B
carbon dioxide
C
ammonia
Conditions | Yield |
---|---|
beim Erhitzen; |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
In neat (no solvent) decompn. at 350°C;; |
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride In methanol; water at 20 - 25℃; |
Conditions | Yield |
---|---|
Aliquat 336 at 100℃; for 1h; | 85% |
With boron trifluoride diethyl etherate In diethyl ether for 1.5h; Heating; | 65% |
With aluminium trichloride In carbon disulfide Heating; | |
With boron trifluoride diethyl etherate | |
With 4-(dimethylamino)pyridine N-oxide In dimethylsulfoxide-d6 at 80℃; for 3h; | 88 % Spectr. |
O,S-Diethyl dithiocarbonate
rac-Ala-OH
N-ethoxythioxomethyl-D,L-alanine
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 72h; Heating; | 82% |
O,S-Diethyl dithiocarbonate
benzylamine
benzylthiocarbamic acid O-ethyl ester
Conditions | Yield |
---|---|
for 8h; Heating; | 81% |
Conditions | Yield |
---|---|
With sodium hydride In 1,2-dimethoxyethane 1) room temp., 1 h, 2) reflux, 4 h.; | 80% |
Conditions | Yield |
---|---|
for 8h; Heating; | 75% |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
With cobalt(II) 5,10,15,20-tetraphenylporphyrin In toluene at 120℃; Schlenk technique; Inert atmosphere; | 58% |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
With cobalt(II) 5,10,15,20-tetraphenylporphyrin In toluene at 120℃; Schlenk technique; Inert atmosphere; | 54% |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
With cobalt(II) 5,10,15,20-tetraphenylporphyrin In toluene at 120℃; Schlenk technique; Inert atmosphere; | 47% |
O,S-Diethyl dithiocarbonate
chloro(chlorosulfanyl)methanone
A
(Ethyldithio)carbonyl Chloride
B
(((Ethylthio)carbonyl)dithio)carbonyl Chloride
Conditions | Yield |
---|---|
at 0℃; for 10h; Title compound not separated from byproducts; | A 2% B 46% |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
With cobalt(II) 5,10,15,20-tetraphenylporphyrin In toluene at 120℃; Schlenk technique; Inert atmosphere; | 46% |
O,S-Diethyl dithiocarbonate
Conditions | Yield |
---|---|
With cobalt(II) 5,10,15,20-tetraphenylporphyrin In toluene at 120℃; Schlenk technique; Inert atmosphere; | 43% |
O,S-Diethyl dithiocarbonate
3-ethoxycarbonyltriazolo<1,5-a>pyridine
ethyl 3-oxo-3H-thiazolo[3,4-a]pyridine-1-carboxylate
Conditions | Yield |
---|---|
With cobalt(II) 5,10,15,20-tetraphenylporphyrin In toluene at 120℃; Schlenk technique; Inert atmosphere; | 36% |
O,S-Diethyl dithiocarbonate
A
S,S-diethyl dithiocarbonate
B
S-Ethyl S'-methyl dithiocarbonate
Conditions | Yield |
---|---|
In dimethylsulfoxide-d6 at 80℃; for 30h; Mechanism; Product distribution; | A 31.75% B 4.7% |
O,S-Diethyl dithiocarbonate
A
S,S-diethyl dithiocarbonate
B
S-Ethyl S'-methyl dithiocarbonate
Conditions | Yield |
---|---|
1-methoxy-4-dimethylaminopyridinium iodide In dimethylsulfoxide-d6 at 80℃; for 30h; Title compound not separated from byproducts; | A 31.75% B 4.7% |
O,S-Diethyl dithiocarbonate
ethylenediamine
N-butylamine
A
N,N'-ethylenethiourea
B
2-(2'-Aminoethylamino)-Δ2-imidazoline
Conditions | Yield |
---|---|
for 6h; Mechanism; Heating; | A 17.5% B 18% |
sarcosine
O,S-Diethyl dithiocarbonate
N-(ethoxycarbonothioyl)-N-methylglycine
Conditions | Yield |
---|---|
With potassium hydroxide; ethanol |
O,S-Diethyl dithiocarbonate
chloroamine-T
N,N'-bis-(toluene-4-sulfonyl)-ethanesulfinamidyne
Conditions | Yield |
---|---|
With water |
O,S-Diethyl dithiocarbonate
5-aminomethyl-2-methyl-3H-pyrimidin-4-one; hydrochloride
Conditions | Yield |
---|---|
With sodium ethanolate |
Conditions | Yield |
---|---|
With water; hydrazine und anschliessenden Erhitzen mit wss.HCl; |
Conditions | Yield |
---|---|
With ammonia |
O,S-Diethyl dithiocarbonate
ethoxy(potassiosulfanyl)methanethione
Conditions | Yield |
---|---|
With potassium hydroxide; ethanol |
Conditions | Yield |
---|---|
With ethanol; hydrazine hydrate |
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