CAS No.62396-98-9,α-Oxo-1,3-benzodioxole-5-acetic Acid Suppliers

Qingdao Beluga Import and Export Co., LTD

α-Oxo-1,3-benzodioxole-5-acetic Acid CAS:62396-98-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in hi

α-Oxo-1,3-benzodioxole-5-acetic Acid CAS:62396-98-9

Cas:62396-98-9

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

1,3-Benzodioxole-5-acetic acid, a-oxo- CAS NO.62396-98-9

Cas:62396-98-9

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

α-Oxo-1,3-benzodioxole-5-acetic Acid

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists，engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

1,3-Benzodioxole-5-acetic acid, a-oxo-

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Antimex Chemical Limied

Our own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin

1,3-Benzodioxole-5-acetic acid, a-oxo-

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

α-Oxo-1,3-benzodioxole-5-acetic Acid

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Topbatt Chemical Co., Ltd.

Topbatt Chemical Co., Ltd., Established in 2019, located in Shenzhen, Guangdong Province, is a Manufacturer and Trading company which specialized in fine chemicals like Pharmaceutical Reference Standards and Stable Isotopes. Our Stable Isotopes produ

alfa-Oxo-1,3-Benzodioxole-5-Acetic Acid

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NUTROCHEM- MANUFACTURE PLACE

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α-Oxo-1,3-benzodioxole-5-acetic Acid

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TOSUN PHARM

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α-Oxo-1,3-benzodioxole-5-acetic Acid

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Synthetic route

: 86358-30-7
benzo[1,3]dioxol-5-ylglyoxylic acid ethyl ester

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions

Conditions	Yield
Stage #1: benzo[1,3]dioxol-5-ylglyoxylic acid ethyl ester With methanol; sodium hydroxide at 0℃; for 2h; Stage #2: In water pH=~ 3 - 4;	70%
With water; lithium hydroxide In tetrahydrofuran at 20℃; for 3h; Inert atmosphere;	32%
With water; sodium hydroxide In tetrahydrofuran for 6h; Reflux;
With sodium hydroxide In water at 0 - 20℃; for 6h;

: 3162-29-6
1-(benzo[d][1,3]dioxol-6-yl)ethanone

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions

Conditions	Yield
With pyridine; selenium(IV) oxide at 90 - 110℃; for 4h; Inert atmosphere;	39%
With potassium permanganate
With pyridine; selenium(IV) oxide

: 2-(benzo[d][1,3]dioxol-5-yl)-N-methyl-2-oxoacetamide

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions

Conditions	Yield
With sodium hydroxide

: 120-58-1
isosafrole

A: 94-53-1
Piperonylic acid

B: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions

Conditions	Yield
With potassium permanganate; water

: 3162-29-6
1-(benzo[d][1,3]dioxol-6-yl)ethanone

alkaline potassium permanganate: alkaline potassium permanganate

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 90843-60-0
2-(3,4-dioxymethylenephenyl)propionaldehyde

alkaline potassium permanganate: alkaline potassium permanganate

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions

Conditions	Yield
in der Kaelte;

: 3162-29-6
1-(benzo[d][1,3]dioxol-6-yl)ethanone

alkaline potassium permanganate: alkaline potassium permanganate

A: 94-53-1
Piperonylic acid

B: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

...Expand

: 120-58-1
isosafrole

aqueous potassium permanganate: aqueous potassium permanganate

A: 94-53-1
Piperonylic acid

B: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

...Expand

: 120-58-1
isosafrole

aqueous potassium permanganate: aqueous potassium permanganate

A: 94-53-1
Piperonylic acid

B: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

C 3.4-methylenedioxy-mandelic acid: 3.4-methylenedioxy-mandelic acid

...Expand

: 25054-53-9
3,4-(methylenedioxy)benzoyl chloride

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 90 °C / Durchleiten von Wasserdampf durch das in Chloroform und Benzol geloeste Reaktionsprodukt 2: NaOH-solution View Scheme

: 2635-13-4
1,2-(methylenedioxy)-4-bromobenzene

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: magnesium / tetrahydrofuran / 1 h / 20 °C 1.2: 1 h / -78 - -10 °C 2.1: sodium hydroxide; water / tetrahydrofuran / 6 h / Reflux View Scheme

: 274-09-9
Methylenedioxybenzene

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: aluminum (III) chloride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere 1.2: 2.17 h / 0 - 20 °C / Inert atmosphere 2.1: water; lithium hydroxide / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme

: 5876-51-7
5-iodo-1,3-benzodioxole

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: copper(I) bromide; isopropylmagnesium chloride / tetrahydrofuran / 0.5 h / -15 - -10 °C / Inert atmosphere 2: sodium hydroxide / water / 6 h / 0 - 20 °C View Scheme

: 1076-38-6
4-hydroxy[1]benzopyran-2-one

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 3-(benzo[d][1,3]dioxol-5-yl)-3-[2-(2-hydroxyphenyl)-2-oxoethyl]-2H-furo[3,2-c]chromene-2,4(3H)-dione

Conditions

Conditions	Yield
With silver(l) oxide In acetonitrile at 110℃; for 0.166667h; Sealed tube; Microwave irradiation;	84%

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 1-[(triisopropylsilyl)ethynyl]-1,2-benziodoxol-3(1H)-one

: 1-(benzo[d][1,3]dioxol-5-yl)-3-(triisopropylsilyl)prop-2-yn-1-one

Conditions

Conditions	Yield
With dipotassium peroxodisulfate In water; acetonitrile at 50℃; for 12h; Inert atmosphere; Schlenk technique; Sealed tube;	82%

: 3682-71-1
2-phenyl-2H-indazole

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: benzo[d][1,3]dioxol-5-yl(2-phenyl-2H-indazol-3-yl)methanone

Conditions

Conditions	Yield
With sodium persulfate; silver nitrate In water; acetone at 23℃; for 24h; Inert atmosphere;	81%

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 1029649-48-6
tert-butyl (2-isocyanophenyl)carbamate

: C15H10N2O3

Conditions

Conditions	Yield
Stage #1: benzo[1,3]dioxol-5-yl-oxo-acetic acid; tert-butyl (2-isocyanophenyl)carbamate In 1,2-dichloro-ethane at 150℃; for 10h; Microwave irradiation; Stage #2: With trifluoroacetic acid In 1,2-dichloro-ethane at 100℃; for 0.166667h; Microwave irradiation;	80%

: 914785-45-8
N-(4-methoxyphenyl)-N-methyl-3-phenylprop-2-ynamide

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 3-(benzo[d][1,3]dioxole-5-carbonyl)-1-methyl-4-phenyl-1-azaspiro[4.5]deca-3,6,9-triene-2,8-dione

Conditions

Conditions	Yield
With dipotassium peroxodisulfate In water; acetone at 120℃; for 12h; Sealed tube;	80%

: 61-54-1
tryptamine

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: N-(2-(1H-indol-3-yl)ethyl)-2-(1,3-benzodioxol-5-yl)-2-oxoacetamide

Conditions

Conditions	Yield
With 1,1'-carbonyldiimidazole	79%

: (9H-β-carbolin-1-yl)-phenyl-methanone

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: (2-(9H-pyrido[3,4-b]indole-1-carbonyl)phenyl)(benzo[d][1,3]dioxol-5-yl)methanone

Conditions

Conditions	Yield
With dipotassium peroxodisulfate; palladium diacetate In 1,2-dichloro-ethane at 80℃; for 16h; regioselective reaction;	79%

: 1942-45-6
4-Octyne

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: (Z)-3-(benzo[d][1,3]dioxol-5-yl)-4-propyl-5-propylidenefuran-2(5H)-one

Conditions

Conditions	Yield
With tetrakis(acetonitrile)copper(I)tetrafluoroborate In 1,1,2-trichloroethane at 130℃; for 20h; Inert atmosphere; Sealed tube; diastereoselective reaction;	79%

: 928-49-4
hex-3-yne

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: C14H14O4

Conditions

Conditions	Yield
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; copper diacetate; Trimethylacetic acid In N,N-dimethyl-formamide at 120℃; for 12h;	77%

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 3102-33-8
trans-3-penten-2-one

: 1-(furan-2-yl)-2-methylpentane-1,4-dione

Conditions

Conditions	Yield
With dipotassium hydrogenphosphate; [Ir(dF(CF3)ppy)2(phen)]PF6 In dichloromethane; water at 20℃; for 9h; Schlenk technique; Irradiation;	77%

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 93-55-0
1-phenyl-propan-1-one

: 1-oxo-1-phenylpropan-2-yl 2-(benzo[d][1,3]dioxol-5-yl)-2-oxoacetate

Conditions

Conditions	Yield
With copper(l) iodide; oxygen; acetic acid In dimethyl sulfoxide at 120℃; for 12h;	76%

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 100-61-8
N-methylaniline

: N-(2-(benzo[d][1,3]dioxole-5-carbonyl)phenyl)-N-methylnitrous amide

Conditions

Conditions	Yield
With tert.-butylnitrite; palladium diacetate In 1,2-dichloro-ethane at 40℃; for 20h; regioselective reaction;	75%

: 123-32-0
2,5-dimethyl-pyrazine

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: (benzo[d][1,3]dioxol-5-yl)(3,6-dimethylpyrazin-2-yl)methanone

Conditions

Conditions	Yield
With dipotassium peroxodisulfate; silver orthophosphate In dichloromethane; water at 40℃; for 24h;	72%

: 5-fluoro-2-phenyl-2H-indazole

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: benzo[d][1,3]dioxol-5-yl(5-fluoro-2-phenyl-2H-indazol-3-yl)methanone

Conditions

Conditions	Yield
With sodium persulfate; silver nitrate In water; acetone at 23℃; for 24h; Inert atmosphere;	68%

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 932-87-6
1-Bromo-2-phenylacetylene

: 38395-09-4
1-(benzo[d][1,3]dioxol-5-yl)-3-phenylprop-2-yn-1-one

Conditions

Conditions	Yield
With [bis(acetoxy)iodo]benzene In toluene at 20℃; for 8h; Reagent/catalyst; Irradiation;	64%

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 2417-77-8
9-bromoethylanthracene

: anthracene-9-ylmethyl 2-(benzo[d][1,3]dioxol-5-yl)-2-oxoacetate

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 3h;	60%

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: N-(2-cyanophenyl)-N-methylmethacrylamide

: 3-(2-(benzo[d][1,3]dioxol-5-yl)-2-oxoethyl)-1,3-dimethylquinoline-2,4(1H,3H)-dione

Conditions

Conditions	Yield
With ammonium peroxydisulfate; silver nitrate In water; acetone at 120℃; for 12h; Inert atmosphere;	54%

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 2861-28-1
1,3-benzodioxole-5-acetic acid

Conditions

Conditions	Yield
Stage #1: benzo[1,3]dioxol-5-yl-oxo-acetic acid With hydrazine hydrate; potassium hydroxide at 0 - 110℃; Stage #2: With hydrogenchloride at 0℃; pH=3 - 4;	45%

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 106-49-0
p-toluidine

: N-(p-tolyl)benzo[d][1,3]dioxole-5-carboxamide

Conditions

Conditions	Yield
With water; oxygen In 1,4-dioxane at 20℃; for 48h; Schlenk technique; Irradiation;	44%

: 67-56-1
methanol

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 157530-74-0
methyl 2-(benzo[d][1,3]dioxol-5-yl)-2-oxoacetate

Conditions

Conditions	Yield
With hydrogenchloride

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 59-88-1
phenylhydrazine hydrochloride

: benzo[1,3]dioxol-5-yl-phenylhydrazono-acetic acid

Conditions

Conditions	Yield
With water

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 120-57-0
piperonal

Conditions

Conditions	Yield
With Dimethyl-p-toluidine at 160℃;

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: benzo[1,3]dioxol-5-yl-hydroxyimino-acetic acid

Conditions

Conditions	Yield
With hydroxylamine hydrochloride; water at 60 - 70℃;

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 872265-57-1
dichloro-(2,2-dichloro-benzo[1,3]dioxol-5-yl)-acetyl chloride

Conditions

Conditions	Yield
With phosphorus pentachloride at 160℃;

: 62396-98-9
benzo[1,3]dioxol-5-yl-oxo-acetic acid

: 79-19-6
thiosemicarbazide

: 16562-29-1
6-benzo[1,3]dioxol-5-yl-3-thioxo-3,4-dihydro-2H-[1,2,4]triazin-5-one

Conditions

Conditions	Yield
(i), (ii) aq. KOH; Multistep reaction;

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Qingdao Beluga Import and Export Co., LTD

Zibo Hangyu Biotechnology Development Co., Ltd

Shandong Mopai Biotechnology Co., LTD

Bluecrystal chem-union

Antimex Chemical Limied

ZHEJIANG JIUZHOU CHEM CO.,LTD

Topbatt Chemical Co., Ltd.

NUTROCHEM- MANUFACTURE PLACE

TOSUN PHARM

Synthetic route

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