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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone Manufacturer/High quality/Best price/In stock

Cas:66346-01-8

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Wuhan Fortuna Chemical Co.,Ltd

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone CAS 66346-01-8 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additives,

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone CAS 66346-01-8

Cas:66346-01-8

Min.Order:10 Kilogram

FOB Price: $10.0

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory supply 1-(4-Chlorophenyl)-4,4-Dimethyl-3-Pentanone

Cas:66346-01-8

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

huge stock TC Fungicide 1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone 66346-01-8 GLP Manufacturer

Cas:66346-01-8

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone Basic information Product Name: 1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone Synonyms: 1-(4-chlorophenyl)-4,4-dimethyl-3-pentanon;hwg1608-alkyl

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Hot productCAS 66346-01-8 with best price

Cas:66346-01-8

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name 1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone Synonyms 1-(4-chlorophenyl)-4,4-dimethyl-3-pentanon;hwg1608-alkylketon;1-(4-CHLOROPHENYL)-4,4-DIMETHYL-3-PENTANONE;1-(4-CHLORO-PHENYL)-4,4-DIMETHY

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

1-(4-Chlorophenyl)-4,4-Dimethyl-3-Pentanone

Cas:66346-01-8

Min.Order:0

Negotiable

Type:Manufacturers

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanoneCAS NO.: 66346-01-8

Cas:66346-01-8

Min.Order:1 Gram

FOB Price: $2.0

Type:Lab/Research institutions

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Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:1 Milligram

Negotiable

Type:Trading Company

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Shanghai Minstar Chemical Co., Ltd

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone Basic information Product Name: 1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone Synonyms: 1-(4-chlorophenyl)-4,4-dimethyl-3-pentanon;hwg1608-alkylketon;1-(4-CHLOROPHENYL)-4,4-DIMETHYL-3-PENTANONE;1-(4-CHLORO-P

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

low price 1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Siwei Development Group Ltd.

Product name: 1-(4-Chlorophenyl)-4,4-Dimethyl-3-Pentanone CAS No.:66346-01-8 Molecule Formula:C13H17ClO Molecule Weight:224.73 Purity: 99.0% Package: 200kg/drum Description:Yellow liquid Manufacture Standards:Enterprise Standard

High Quality 1-(4-Chlorophenyl)-4,4-Dimethyl-3-Pentanone

Cas:66346-01-8

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

66346-01-8 CAS NO.66346-01-8

Cas:66346-01-8

Min.Order:1 Metric Ton

FOB Price: $7.0 / 8.0

Type:Trading Company

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone cas no. 66346-01-8 98%

Cas:66346-01-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

4,4-Dimethyl-1-(p-chlorophenyl)-3-pentanone

Cas:66346-01-8

Min.Order:0

Negotiable

Type:Other

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DB BIOTECH CO., LTD

Q1: Are you a manufacturer Answer: Yes, we are factory founded on 2012.Q2: How to contact with us Click "contact supplier" And then send us message the product you interest in, you will get reply within 12 hours.Q3:Which kind of payment terms do you

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:0

Negotiable

Type:Trading Company

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Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:0

Negotiable

Type:Manufacturers

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Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

1-(4-Chlorophenyl)-4,4-Dimethyl-3-Pentanone

Cas:66346-01-8

Min.Order:0

Negotiable

Type:Manufacturers

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Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

1-(4-Chlorophenyl)-4,4-dimethylpentan-3-one

Cas:66346-01-8

Min.Order:0

Negotiable

Type:Manufacturers

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Wuxi TAA Chemical Industry Co.,LTD.

1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re

Cartoon Ingredients Co., Ltd

Cartoon Ingredients Co.,Ltd.is located in NanJing, the capital of Jiangsu Province.with Convenient traffic As a manufacturer, the company mainly engaged in providing Food ingredients, Herbal extracts, Vitamins, APIs and Fine chemicals &a

1-(4-Chlorophenyl)-4,4-dimethyl-3-pentanone

Cas:66346-01-8

Min.Order:0

Negotiable

Type:Trading Company

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Synthetic route

1-(4-chlorophenyl)-4,4-dimethylpent-1-en-3-one
1577-03-3

1-(4-chlorophenyl)-4,4-dimethylpent-1-en-3-one

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

Conditions
ConditionsYield
With sulfolane; hydrogen In methanol at 50 - 60℃; under 750.075 Torr; Temperature; Pressure; Reagent/catalyst; Autoclave;99%
With sodium phosphite; hydrogen; ethanolamine In methanol at 70℃; under 6750.68 Torr; Reagent/catalyst; Temperature; Pressure; Autoclave;97.8%
With hydrogen In ethanol at 80℃; under 22502.3 Torr; for 2h;
1,3-diphenyl-propen-3-one
614-47-1

1,3-diphenyl-propen-3-one

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

Conditions
ConditionsYield
With hydrogen; aluminum nickel In ethyl acetate
2,2'-thiobis-ethanol
111-48-8

2,2'-thiobis-ethanol

(E)-1-(4-chlorophenyl)-4,4-dimethylpent-1-en-3-one
41564-62-9

(E)-1-(4-chlorophenyl)-4,4-dimethylpent-1-en-3-one

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

Conditions
ConditionsYield
aluminum nickel In methanol
4-chlorobenzaldehyde
104-88-1

4-chlorobenzaldehyde

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydroxide / ethanol / 2.5 h / 60 °C / Cooling with ice
2: hydrogen / ethanol / 2 h / 80 °C / 22502.3 Torr
View Scheme
3,3-dimethyl-butan-2-one
75-97-8

3,3-dimethyl-butan-2-one

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydroxide / ethanol / 2.5 h / 60 °C / Cooling with ice
2: hydrogen / ethanol / 2 h / 80 °C / 22502.3 Torr
View Scheme
2-(4-chlorobenzyl)-4,4-dimethyl-3-carbonylvaleric acid methyl ester

2-(4-chlorobenzyl)-4,4-dimethyl-3-carbonylvaleric acid methyl ester

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

Conditions
ConditionsYield
With isopropyl alcohol; sodium hydroxide at 85℃; for 1h; Reagent/catalyst; Temperature;38 g
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

dimethyl sulfate
77-78-1

dimethyl sulfate

2-[2-(4-chlorophenyl)ethyl]-2-(1,1-dimethylethyl)ethylene oxide
80443-63-6

2-[2-(4-chlorophenyl)ethyl]-2-(1,1-dimethylethyl)ethylene oxide

Conditions
ConditionsYield
Stage #1: dimethyl sulfate With p-propoxybenzyl sulfide at 90℃; for 2h;
Stage #2: 1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one With potassium hydroxide In toluene at 50℃; for 4h; Reagent/catalyst; Concentration; Temperature;
99.6%
With dimethylsulfide; potassium hydroxide In toluene at 25 - 50℃; for 5h; Reagent/catalyst; Temperature; Solvent;98.8%
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

methyl iodide
74-88-4

methyl iodide

2-[2-(4-chlorophenyl)ethyl]-2-(1,1-dimethylethyl)ethylene oxide
80443-63-6

2-[2-(4-chlorophenyl)ethyl]-2-(1,1-dimethylethyl)ethylene oxide

Conditions
ConditionsYield
Stage #1: methyl iodide With p-propoxybenzyl sulfide at 90℃; for 2h;
Stage #2: 1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one With potassium hydroxide In toluene at 0℃; for 4h;
99.2%
trimethylsulfonium chloride
3086-29-1

trimethylsulfonium chloride

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

2-[2-(4-chlorophenyl)ethyl]-2-(1,1-dimethylethyl)ethylene oxide
80443-63-6

2-[2-(4-chlorophenyl)ethyl]-2-(1,1-dimethylethyl)ethylene oxide

Conditions
ConditionsYield
Stage #1: trimethylsulfonium chloride; 1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one With potassium hydroxide In dimethyl sulfoxide at 20℃; for 0.5h;
Stage #2: 1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one In toluene at 80℃; for 10h; Solvent; Temperature;
95%
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

1-(4'-chlorophenyl)-2-bromo-4,4-dimethylpentan-3-one
66346-02-9

1-(4'-chlorophenyl)-2-bromo-4,4-dimethylpentan-3-one

Conditions
ConditionsYield
With 1-butyl-3-methylpyridinium tribromide for 0.2h; Inert atmosphere; Cooling; regioselective reaction;94.2%
With 1-butyl-3-methylimidazolium tribromide for 0.166667h; Ionic liquid;92.7%
With copper(ll) bromide In ethanol for 4h; Reflux;
trimethylsulphonium bromide
3084-53-5

trimethylsulphonium bromide

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

2-[2-(4-chlorophenyl)ethyl]-2-(1,1-dimethylethyl)ethylene oxide
80443-63-6

2-[2-(4-chlorophenyl)ethyl]-2-(1,1-dimethylethyl)ethylene oxide

Conditions
ConditionsYield
With potassium hydroxide In toluene at 40 - 45℃; for 5h;92%
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

(R)-2-[2-(4-Chloro-phenyl)-ethyl]-2-hydroxy-3,3-dimethyl-butyraldehyde
120687-96-9

(R)-2-[2-(4-Chloro-phenyl)-ethyl]-2-hydroxy-3,3-dimethyl-butyraldehyde

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1) 1.98 M BuLi / 1) n-hexane, THF, -78 to 0 deg C, 2) THF, 30 min, 25 deg C
2: NCS, AgNO3 / acetonitrile / 15 h / 40 - 50 °C
View Scheme
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

(R)-1-p-chlorophenyl-4,4-dimethyl-3-(1H-1,2,4-triazol-1-ylmethyl)pentan-3-ol
80443-41-0, 107534-96-3, 119364-85-1, 120786-56-3

(R)-1-p-chlorophenyl-4,4-dimethyl-3-(1H-1,2,4-triazol-1-ylmethyl)pentan-3-ol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 1) 1.98 M BuLi / 1) n-hexane, THF, -78 to 0 deg C, 2) THF, 30 min, 25 deg C
2: NCS, AgNO3 / acetonitrile / 15 h / 40 - 50 °C
3: LiAlH4 / diethyl ether / 3 h / 35 °C
4: NEt3 / CH2Cl2 / 4 h / 25 °C
5: dimethylformamide / 6 h / 120 °C
View Scheme
Multi-step reaction with 5 steps
1: 1) 1.98 M BuLi / 1) n-hexane, THF, -78 to 0 deg C, 2) THF, 30 min, 25 deg C
2: NCS, AgNO3 / acetonitrile / 0.25 h / 40 - 50 °C
3: LiAlH4 / diethyl ether / 3 h / 35 °C
4: NEt3 / CH2Cl2 / 4 h / 25 °C
5: dimethylformamide / 6 h / 120 °C
View Scheme
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

(S)-1-p-chlorophenyl-4,4-dimethyl-3-(1H-1,2,4-triazol-1-ylmethyl)pentan-3-ol
119364-85-1

(S)-1-p-chlorophenyl-4,4-dimethyl-3-(1H-1,2,4-triazol-1-ylmethyl)pentan-3-ol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 1) 1.98 M BuLi / 1) n-hexane, THF, -78 to 0 deg C, 2) THF, 30 min, 25 deg C
2: NCS, AgNO3 / acetonitrile / 15 h / 40 - 50 °C
3: LiAlH4 / diethyl ether / 3 h / 35 °C
4: NEt3 / CH2Cl2 / 4 h / 25 °C
5: dimethylformamide / 6 h / 120 °C
View Scheme
Multi-step reaction with 5 steps
1: 1) 1.98 M BuLi / 1) n-hexane, THF, -78 to 0 deg C, 2) THF, 30 min, 25 deg C
2: NCS, AgNO3 / acetonitrile / 0.25 h / 40 - 50 °C
3: LiAlH4 / diethyl ether / 3 h / 35 °C
4: NEt3 / CH2Cl2 / 4 h / 25 °C
5: 49 percent / dimethylformamide / 6 h / 120 °C
View Scheme
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

Methanesulfonic acid (R)-2-[2-(4-chloro-phenyl)-ethyl]-2-hydroxy-3,3-dimethyl-butyl ester
120687-98-1

Methanesulfonic acid (R)-2-[2-(4-chloro-phenyl)-ethyl]-2-hydroxy-3,3-dimethyl-butyl ester

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 1) 1.98 M BuLi / 1) n-hexane, THF, -78 to 0 deg C, 2) THF, 30 min, 25 deg C
2: NCS, AgNO3 / acetonitrile / 15 h / 40 - 50 °C
3: LiAlH4 / diethyl ether / 3 h / 35 °C
4: NEt3 / CH2Cl2 / 4 h / 25 °C
View Scheme
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

Methanesulfonic acid (S)-2-[2-(4-chloro-phenyl)-ethyl]-2-hydroxy-3,3-dimethyl-butyl ester
119298-84-9

Methanesulfonic acid (S)-2-[2-(4-chloro-phenyl)-ethyl]-2-hydroxy-3,3-dimethyl-butyl ester

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 1) 1.98 M BuLi / 1) n-hexane, THF, -78 to 0 deg C, 2) THF, 30 min, 25 deg C
2: NCS, AgNO3 / acetonitrile / 0.25 h / 40 - 50 °C
3: LiAlH4 / diethyl ether / 3 h / 35 °C
4: NEt3 / CH2Cl2 / 4 h / 25 °C
View Scheme
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

A

1-(4'-chlorophenyl)-2-bromo-4,4-dimethylpentan-3-one
66346-02-9

1-(4'-chlorophenyl)-2-bromo-4,4-dimethylpentan-3-one

Conditions
ConditionsYield
With bromine In tetrachloromethane
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

4-(tert-butyl)-5-(4-chlorobenzyl)thiazol-2-aminenitrate
1239339-35-5

4-(tert-butyl)-5-(4-chlorobenzyl)thiazol-2-aminenitrate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1-butyl-3-methylimidazolium tribromide / 0.17 h / Ionic liquid
2: ethanol / 3 h / Reflux
3: silver nitrate / ethanol / 0.5 h / 35 °C
View Scheme
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

2-amino-4-(tert-butyl)-5-(4-chlorobenzyl)thiazol-3-ium bromide
1068658-48-9

2-amino-4-(tert-butyl)-5-(4-chlorobenzyl)thiazol-3-ium bromide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1-butyl-3-methylimidazolium tribromide / 0.17 h / Ionic liquid
2: ethanol / 3 h / Reflux
View Scheme
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

4-tert-butyl-5-[4-chlorobenzyl]-1,3-thiazol-2-amine

4-tert-butyl-5-[4-chlorobenzyl]-1,3-thiazol-2-amine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: copper(ll) bromide / ethanol / 4 h / Reflux
2: ethanol / 7.5 h / Reflux
View Scheme
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

N-(4-(tert-butyl)-5-(4-chlorobenzyl)thiazol-2-yl)-2-methoxybenzamide

N-(4-(tert-butyl)-5-(4-chlorobenzyl)thiazol-2-yl)-2-methoxybenzamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: copper(ll) bromide / ethanol / 4 h / Reflux
2.1: ethanol / 7.5 h / Reflux
3.1: dmap / dichloromethane / 0.5 h / 20 °C
3.2: 20 °C
View Scheme
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

N-(4-(tert-butyl)-5-(4-chlorobenzyl)thiazol-2-yl)-2-chlorobenzamide

N-(4-(tert-butyl)-5-(4-chlorobenzyl)thiazol-2-yl)-2-chlorobenzamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: copper(ll) bromide / ethanol / 4 h / Reflux
2.1: ethanol / 7.5 h / Reflux
3.1: dmap / dichloromethane / 0.5 h / 20 °C
3.2: 20 °C
View Scheme
1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one
66346-01-8

1-(4-chlorophenyl)-4,4-dimethyl-pentan-3-one

N-(4-(tert-butyl)-5-(4-chlorobenzyl)thiazol-2-yl)-4-chlorobenzamide

N-(4-(tert-butyl)-5-(4-chlorobenzyl)thiazol-2-yl)-4-chlorobenzamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: copper(ll) bromide / ethanol / 4 h / Reflux
2.1: ethanol / 7.5 h / Reflux
3.1: dmap / dichloromethane / 0.5 h / 20 °C
3.2: 20 °C
View Scheme

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