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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

1,3,4,6,7,9,9b-Heptaazaphenalene,2,5,8- trichloro-

Cas:6710-92-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1,3,4,6,7,9,9b-Heptaazaphenalene,2,5,8- trichloro-

Cas:6710-92-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

1,3,4,6,7,9,9b-Heptaazaphenalene,2,5,8- trichloro-

Cas:6710-92-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

1,3,4,6,7,9,9b-Heptaazaphenalene,2,5,8- trichloro-

Cas:6710-92-5

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Antimex Chemical Limied

Our own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin

1,3,4,6,7,9,9b-Heptaazaphenalene,2,5,8- trichloro-

Cas:6710-92-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1,3,4,6,7,9,9b-Heptaazaphenalene,2,5,8- trichloro-

Cas:6710-92-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

6710-92-5

Cas:6710-92-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

home-produced Application:medicine

1,3,4,6,7,9,9b-Heptaazaphenalene,2,5,8- trichloro-

Cas:6710-92-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1,3,4,6,7,9,9b-Heptaazaphenalene,2,5,8- trichloro-

Cas:6710-92-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

LEAP CHEM Co., Ltd.

Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP

2,5,8-Trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

Cas:6710-92-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

1,3,4,6,7,9,9b-Heptaazaphenalene,2,5,8-trichloro

Cas:6710-92-5

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Changzhou Extraordinary Pharmatech co.,LTD

Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa

heptazine chloride

Cas:6710-92-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

phosphorus pentachloride
10026-13-8, 874483-75-7

phosphorus pentachloride

cyameluric acid tripotassium salt

cyameluric acid tripotassium salt

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

Conditions
ConditionsYield
In neat (no solvent) at 220℃; for 24h; Sealed tube;92%
cyameluric acid tripotassium salt

cyameluric acid tripotassium salt

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

Conditions
ConditionsYield
With phosphorus pentachloride at 130℃; under 0.075006 Torr; for 10h;91%
With phosphorus pentachloride at 130℃; for 8h; Schlenk technique;82%
With phosphorus pentachloride; trichlorophosphate at 110℃; for 6h; Inert atmosphere;68%
cyamelluric acid
1502-46-1

cyamelluric acid

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

Conditions
ConditionsYield
With phosphorus pentachloride at 218℃;
With phosphorus pentachloride; trichlorophosphate for 6h; Product distribution / selectivity; Heating / reflux;
With phosphorus pentachloride; trichlorophosphate
melem
1502-47-2

melem

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium hydroxide / water / 6 h / 160 °C / Schlenk technique
2: phosphorus pentachloride / 31 h / 100 - 140 °C / Sealed tube
View Scheme
2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

diphenylphosphane
829-85-6

diphenylphosphane

2,5,8-tris(diphenylphosphanyl)-tri-s-triazine

2,5,8-tris(diphenylphosphanyl)-tri-s-triazine

Conditions
ConditionsYield
In 1,3,5-trimethyl-benzene Inert atmosphere;100%
2-ethylhexyl 4-aminobenzoate
26218-04-2

2-ethylhexyl 4-aminobenzoate

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

2,5,8-tris-(4-(2-ethylhexyloxycarbonyl)phenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

2,5,8-tris-(4-(2-ethylhexyloxycarbonyl)phenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

Conditions
ConditionsYield
In toluene for 1h; Heating / reflux;97%
In toluene for 1h; Heating / reflux;97%
4-amino-benzoic acid butyl ester
94-25-7

4-amino-benzoic acid butyl ester

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

2,5,8-tris-(4-(butoxycarbonyl)phenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

2,5,8-tris-(4-(butoxycarbonyl)phenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

Conditions
ConditionsYield
In toluene at 110℃; for 0.5h; Heating / reflux;96%
In toluene at 110℃; for 0.5h; Heating / reflux;96%
2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

5-aminoisophthalic acid
99-31-0

5-aminoisophthalic acid

2,5,8-tris-(3,5-dicarboxylphenylamino)-s-heptazine acid

2,5,8-tris-(3,5-dicarboxylphenylamino)-s-heptazine acid

Conditions
ConditionsYield
With hydrogenchloride; sodium hydrogencarbonate; sodium hydroxide In 1,4-dioxane; water at 100℃; for 24h; pH=2;94%
2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

chlorobenzene
108-90-7

chlorobenzene

2,5,8-tris(4-chlorophenyl)-1,3,4,6,7,9,9b-heptaazaphenalene

2,5,8-tris(4-chlorophenyl)-1,3,4,6,7,9,9b-heptaazaphenalene

Conditions
ConditionsYield
With aluminum (III) chloride In neat (no solvent) at 0 - 20℃; for 12.5h; Friedel-Crafts Alkylation;89%
2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

2,4,6-tribromophenol
118-79-6

2,4,6-tribromophenol

C24H6Br9N7O3

C24H6Br9N7O3

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane at 120℃; for 24h; Concentration; Reagent/catalyst; Temperature;87.1%
iodoacetonitrile
624-75-9

iodoacetonitrile

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

C12H6N10

C12H6N10

Conditions
ConditionsYield
Stage #1: 2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 1.75h;
Stage #2: iodoacetonitrile With iodine In tetrahydrofuran at -78℃;
86.4%
2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

diethylamine
109-89-7

diethylamine

2,5,8-tris(diethylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

2,5,8-tris(diethylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 2h;86%
at 100℃; for 72h;15%
diisobutylamine
110-96-3

diisobutylamine

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

C22H36ClN9

C22H36ClN9

Conditions
ConditionsYield
In tetrahydrofuran at -95℃;85%
di-p-tolylamine
620-93-9

di-p-tolylamine

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

hexa-4-tolylmelem
1256354-13-8

hexa-4-tolylmelem

Conditions
ConditionsYield
In xylene at 80℃; for 15h;84%
1,1,1-trifluoro-2-iodoethane
353-83-3

1,1,1-trifluoro-2-iodoethane

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

C12H6F9N7

C12H6F9N7

Conditions
ConditionsYield
Stage #1: 2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 1.75h;
Stage #2: 1,1,1-trifluoro-2-iodoethane With iodine In tetrahydrofuran at -78℃;
83.5%
2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

toluene
108-88-3

toluene

2,5,8-tri(p-methylbenzene)-1,3,4,6,7,9,9b-heptaazaphenalene

2,5,8-tri(p-methylbenzene)-1,3,4,6,7,9,9b-heptaazaphenalene

Conditions
ConditionsYield
With aluminum (III) chloride at 60℃; for 0.5h;83%
Stage #1: 2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene; toluene With aluminum (III) chloride at 65℃;
Stage #2: With water In toluene
22%
2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene
6710-92-5

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

naphthalen-2-ylamine
91-59-8

naphthalen-2-ylamine

2,5,8-tris-(naphthalen-2-ylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

2,5,8-tris-(naphthalen-2-ylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In 1,4-dioxane at 120℃; for 0.166667h;79%
With diisopropylamine In 1,4-dioxane at 120℃; for 0.166667h; Microwave oven;79%

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