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Sodium Molybdate Product Name: Sodium Molybdate Molecular Weight: 205.92 CAS NO: 7631-95-0 EC NO: 231-551-7 Molecular Formula: Na2MoO4

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Superiority Product Detail Sodium molybdate Na2MoO4●2H2O Product quality reference standard: Indicator Name Indicator% Na2MoO4●2H2O 98% MOlybdenum (Mo) content 39% Water insoluble matter 0. 0

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Synthetic route

: sodium molybdate decahydrate

: 7631-95-0
sodium molybdate dihydrate

Conditions

Conditions	Yield
In neat (no solvent) decompn. of Na2MoO4*10H2O at ambient temp.;;
In neat (no solvent) decompn. of Na2MoO4*10H2O at room temp. during a few days;;
In neat (no solvent) decompn. of Na2MoO4*10H2O at room temp. during a few days;;
In neat (no solvent) decompn. of Na2MoO4*10H2O at ambient temp.;;

: sodium molybdate

: 7732-18-5
water

: 7631-95-0
sodium molybdate dihydrate

Conditions

Conditions	Yield
In water solving of Na2MoO4 in H2O;; concn. of the soln.; crystn.; filtration; washing with small amt. of H2O; drying between paper and then over CaO and H2SO4 for 24 hours;;
In water solving of Na2MoO4 in H2O;; concn. of the soln.; crystn.; filtration; washing with small amt. of H2O; drying between paper and then over CaO and H2SO4 for 24 hours;;

: 497-19-8
sodium carbonate

: molybdenum(VI) oxide

: 7631-95-0
sodium molybdate dihydrate

Conditions

Conditions	Yield
In water neutralization of an aq. soln. of MoO3 with Na2CO3;; evapn. at ambient temp.;;
In water neutralization of an aq. soln. of MoO3 with Na2CO3;; evapn. at ambient temp.;;

: ammonium molybdate

: 1310-73-2
sodium hydroxide

: 7631-95-0
sodium molybdate dihydrate

Conditions

Conditions	Yield
In sodium hydroxide byproducts: NH3; addn. of an excess of NaOH to a soln. of ammonium molybdate; boiling til formation of NH3 stops;; addn. of alc.; pptn.; washing with alc.; drying; recrystn. from H2O;;
In sodium hydroxide boiling of equival. amts of ammonium molybdate and NaOH;; recrystn.;;
In sodium hydroxide aq. NaOH; boiling of equival. amts of ammonium molybdate and NaOH;; recrystn.;;
In sodium hydroxide byproducts: NH3; aq. NaOH; addn. of an excess of NaOH to a soln. of ammonium molybdate; boiling til formation of NH3 stops;; addn. of alc.; pptn.; washing with alc.; drying; recrystn. from H2O;;

: sodium molybdate

: 7631-95-0
sodium molybdate dihydrate

Conditions

Conditions	Yield
With water In water above 10°C;
With H2O In water above 10°C;

: sodium terbium(III) phosphate molybdate

A: 7631-95-0
sodium molybdate dihydrate

B: 765876-75-3
terbium(III) phosphate

Conditions

Conditions	Yield
In neat (no solvent) heated in alundum crucibles under inert gas flow at a rate of 20 K/min in the range 20-500°C and 10 K/min in the range of 500-900°C; identified by X-ray diffraction;

: sodium thulium phosphate molybdate

A: 7631-95-0
sodium molybdate dihydrate

B: 753426-80-1
thulium(III) phosphate

Conditions

Conditions	Yield
In neat (no solvent) heated in alundum crucibles under inert gas flow at a rate of 20 K/min in the range 20-500°C and 10 K/min in the range of 500-900°C; identified by X-ray diffraction;

: sodium holmium(III) phosphate molybdate

A: 7631-95-0
sodium molybdate dihydrate

B: 791563-17-2
holmium(III) orthophosphate

Conditions

Conditions	Yield
In neat (no solvent) heated in alundum crucibles under inert gas flow at a rate of 20 K/min in the range 20-500°C and 10 K/min in the range of 500-900°C; identified by X-ray diffraction;

: sodium dysprosium(III) phosphate molybdate

A: 7631-95-0
sodium molybdate dihydrate

B: 785025-30-1
dysprosium(III) orthophosphate

Conditions

Conditions	Yield
In neat (no solvent) heated in alundum crucibles under inert gas flow at a rate of 20 K/min in the range 20-500°C and 10 K/min in the range of 500-900°C; identified by X-ray diffraction;

: sodium erbium(III) molybdophosphate

A: 7631-95-0
sodium molybdate dihydrate

B: 775556-30-4
erbium(III) orthophosphate

Conditions

Conditions	Yield
In neat (no solvent) heated in alundum crucibles under inert gas flow at a rate of 20 K/min in the range 20-500°C and 10 K/min in the range of 500-900°C; identified by X-ray diffraction;

: sodium lutetium(III) phosphate molybdate

A: 733719-76-1
lutetium(III) orthophosphate

B: 7631-95-0
sodium molybdate dihydrate

Conditions

Conditions	Yield
In neat (no solvent) heated in alundum crucibles under inert gas flow at a rate of 20 K/min in the range 20-500°C and 10 K/min in the range of 500-900°C;

: 3Na(1+)*Rb(1+)*2MoO4(2-)*9H2O=Na3Rb(MoO4)2*9H2O

: 7631-95-0
sodium molybdate dihydrate

Conditions

Conditions	Yield
In neat (no solvent, solid phase) byproducts: NaRbMoO4*2H2O, H2O; storage for 1-2h at room temp.; not isolated; X-ray diffraction;

: 7631-95-0
sodium molybdate dihydrate

: K9[A,α-PW9O34]*16H2O

: K7[α-PW9Mo2O39]

Conditions

Conditions	Yield
With lithium chloride; hydrochloric acid; potassium bromide In water to a soln. of sodium molybdate was added LiCl, water and dropwise hydrochloric acid until pH 4.5 to 5, K9(A,α-PW9O34)*16H2O was added slowly and pH kept between 4.5 and 5 (HCl), KBr was added; ppt. was filtered off, dried;	99%

: 7631-95-0
sodium molybdate dihydrate

: 25005-97-4
2,3,5,6-tetrakis(2-pyridyl)pyrazine

: 7732-18-5
water

: 34946-82-2
copper(II) bis(trifluoromethanesulfonate)

: [Cu4(2,3,5,6-tetrakis(2-pyridyl)pyrazine)4(H2O)4(molybdateate)2](triflate)4*7H2O

Conditions

Conditions	Yield
In water; acetone Cu salt and ligand dissolved in H2O-acetone under stirring and heating at 75°C; diluted aq. Na2MoO4*2H2O carefully added; filtered; filtrate evapd. slowly in air at room temp. for 1 mo; crystalscollected; washed with very small amt. of cold H2O and acetone; second crop obtained by evapn. of the soln.; elem. anal.;	99%

...Expand

: 7446-07-3
tellurium(IV) oxide

: 7631-95-0
sodium molybdate dihydrate

: Na2MoTe4O12

Conditions

Conditions	Yield
In water molar ratio Mo:Te=3:1, acid digestion bomb, 225°C, 4 d; then cooling to room temp. over 36 h;	98%
In neat (no solvent, solid phase) stoich. amts., heating in air (450°C, 6 h; then 625°C, 2 d; intermittent grinding);

: 7631-95-0
sodium molybdate dihydrate

: 32646-21-2
2-formylpyridine-N(4)-methylthiosemicarbazone

: (C6H4NCHN2HCSNHCH3)4(pyridine-2-carboxaldehyde N4-methylthiosemicarbazone)2(β-octamolybdate)*2H2O

Conditions

Conditions	Yield
With HCl In water aq. soln. of Na2MoO4*2H2O acidified with 2 drops of HCl, treated with solid ligand (0.5 equiv.) under vigorous stirring, reacted for 2 h; filtered, washed (H2O, EtOH, acetone), dried (vac.), elem. anal.;	98%

: 7631-95-0
sodium molybdate dihydrate

: 17356-08-0
thiourea

: molybdenum(IV) disulfide

Conditions

Conditions	Yield
With hydrogenchloride; 1-butyl-3-methylimidazolium chloride In water at 180℃; for 24h; pH=< 1; High pressure; Inert atmosphere;	98%
In water at 210℃; for 24h; Autoclave;
With Rochelle's salt In water at 200℃; for 24h; Temperature; Autoclave;

: 7647-01-0
hydrogenchloride

: 7631-95-0
sodium molybdate dihydrate

: 68-12-2, 33513-42-7
N,N-dimethyl-formamide

: 21356-99-0, 18078-67-6
bis(N,N-dimethylformamide)dichloridodioxidomolybdenum(VI)

Conditions

Conditions	Yield
Stage #1: hydrogenchloride; sodium molybdate dihydrate In water at 20℃; Green chemistry; Stage #2: N,N-dimethyl-formamide In diethyl ether for 0.0833333h; Green chemistry;	97.5%

...Expand

: 3608-75-1
pyridine-2-carbaldehyde thiosemicarbazone

: 7631-95-0
sodium molybdate dihydrate

: copper(II) perchlorate hexahydrate

: [Cu(C5H5NHCHN2CSNH2)(H2O)]2(β-octamolybdate)

Conditions

Conditions	Yield
With HClO4 In water solid ligand added to aq. soln. of Cu(ClO4)6H2O (L:Cu=1:1), reacted for30 min, filtered, soln. added to aq. soln. of Na2MoO42H2O (4 equiv.), pH adjusted to 3 (HClO4), reacted for 2 h; filtered, washed (acidified H2O), dried (vac.), crystd. for 20 d, elem. anal.;	97%

...Expand

: 280-57-9
1,4-diaza-bicyclo[2.2.2]octane

: 7647-01-0
hydrogenchloride

: iron(III) chloride hexahydrate

: 7631-95-0
sodium molybdate dihydrate

: (H2-1,4-diazabicyclo[2.2.2]octane)(H-1,4-diazabicyclo[2.2.2]octane)[Fe(OH)6Mo6O18]*4H2O

Conditions

Conditions	Yield
In water aq. soln. Na2MoO42H2O at 0°C was adjusted to pH 6 with 5 M HCl, FeCl36H2O was added, pH was adjusted to 4, stirred for 2 h at low temp., soln. aq. DABCO (pH 4, HCl) was added, stirred at room temp. for 1 h; ppt. was filtered, washed with water and EtOH and dried in air; elem. anal.;	97%
In water High Pressure; aq. soln. Na2MoO42H2O, FeCl36H2O and DABCO (pH 4, HCl) was heated in Teflon-lined autoclave at 130°C for 2 days; soln. was filtered and left at room temp. for a few days;

...Expand

: 7647-01-0
hydrogenchloride

: 7631-95-0
sodium molybdate dihydrate

: 67-68-5
dimethyl sulfoxide

: dichlorobis(dimethylsulfoxide)dioxomolybdenum(VI)

Conditions

Conditions	Yield
Stage #1: hydrogenchloride; sodium molybdate dihydrate In water at 20℃; Green chemistry; Stage #2: dimethyl sulfoxide In diethyl ether for 0.0833333h; Green chemistry;	97%

...Expand

: 7631-95-0
sodium molybdate dihydrate

: 25310-12-7
N-phenylhexanohydroxamic acid

: MoO2(CH3(CH2)4C(O)N(C6H5)O)2

Conditions

Conditions	Yield
With HCl In ethanol; water addn. of 2 equiv. ligand (in EtOH) to aq. molybdate (stirring), pptn. onpH-adjustment to 3 (HCl); recrystn. (hot EtOH);	96%

: 7631-95-0
sodium molybdate dihydrate

: 1643-19-2
tetrabutylammomium bromide

: bis(tetrabutylammonium) hexamolybdate

Conditions

Conditions	Yield
With hydrogenchloride In water; acetone for 5h;	96%
With hydrogenchloride In water at 75 - 80℃; for 0.75h;	78%

: 7631-95-0
sodium molybdate dihydrate

: 7732-18-5
water

: [tris(ethylendiamine)cobalt(III) chloride]*1.5H2O

: [tris(ethylendiamine)cobalt(III)]2[Mo7O24]*8H2O

Conditions

Conditions	Yield
With hydrogenchloride; succinic acid at 20℃; for 168h; pH=4; Temperature; Concentration;	95.3%

...Expand

: 7631-95-0
sodium molybdate dihydrate

: tris(ethylenediamine)nickel(II) nitrate

: nickel(II) tris(ethylene diamine) molybdate

Conditions

Conditions	Yield
In water	95%
In ethanol; water react. of alc. Na2MoO4*2H2O-soln. with very concd. aq. (Ni(NH2C2H4NH2)3)(NO3)2-soln.;; pptn., washing with 96% alc. and with ether;;
In ethanol; water react. of alc. Na2MoO4*2H2O-soln. with very concd. aq. (Ni(NH2C2H4NH2)3)(NO3)2-soln.;; pptn., washing with 96% alc. and with ether;;

: 7631-95-0
sodium molybdate dihydrate

: 40783-15-1
O,O-di(2-tolyl)dithiophosphoric acid ammonium salt

: Mo2O3[O,O-di(2-tolyl)dithiophosphoric acid(-H)]4

Conditions

Conditions	Yield
In water aq. soln. of 2 equiv. organic ligand added dropwise to aq. Mo-compound with constant stirring; filtered; washed with ether; dried over P2O5; recrystallized from benzene:Et2O 1:2 mixt.; elem. anal.;	95%

: 280-57-9
1,4-diaza-bicyclo[2.2.2]octane

: 7647-01-0
hydrogenchloride

: 7631-95-0
sodium molybdate dihydrate

: 506-59-2
N,N-dimethylammonium chloride

: (1,4-diazabicyclo[2.2.2]octane(+2H))2(dimethylammonium)0.5Na0.75(H3O)0.75[Mo8O27]*3H2O

Conditions

Conditions	Yield
In water diazabicyclooctane and hydrochloride were added to aq. soln. of Mo compd.; aq. HCl was added to pH 4; stirred at room temp. for 3 h; filtered; washed (H2O, EtOH, Et2O); elem. anal.;	95%

...Expand

: 280-57-9
1,4-diaza-bicyclo[2.2.2]octane

: 7631-95-0
sodium molybdate dihydrate

: 7732-18-5
water

: 506-59-2
N,N-dimethylammonium chloride

: (H2DABCO)2(HDMA)0.5Na0.8(H3O)0.7[Mo8O27].3H2O

Conditions

Conditions	Yield
Stage #1: 1,4-diaza-bicyclo[2.2.2]octane; sodium molybdate dihydrate; water; N,N-dimethylammonium chloride Stage #2: With hydrogenchloride In water pH=4;	95%

...Expand

: 7631-95-0
sodium molybdate dihydrate

: 506-59-2
N,N-dimethylammonium chloride

: 2C2H7N*2H(1+)*Mo7O22(2-)

Conditions

Conditions	Yield
With hydrogenchloride In water at 120℃; for 6h; pH=1; Autoclave; High pressure;	95%

: 7631-95-0
sodium molybdate dihydrate

: 188713-27-1
N,N-bis(3,5-di-t-butyl-2-hydroxybenzyl)-N',N'-dimethylethylenediamine

: [MoO2((((CH3)3C)2(O)C6H2CH2)2NCH2CH2N(CH3)2)]

Conditions

Conditions	Yield
With acetic acid In methanol for 2h; Reflux;	95%

: 7631-95-0
sodium molybdate dihydrate

: Mg4.27Al2(OH)1254*C6H4(CO2)2(2-)*99H2O

: 12Mg(2+)*6Al(3+)*36OH(1-)*Mo7O24(6-)*99H2O=Mg12Al6(OH)36(Mo7O24)*99H2O

Conditions

Conditions	Yield
	94%

: potassium cyanide

: 7631-95-0
sodium molybdate dihydrate

: 7732-18-5
water

: tetrapotassium octacyanomolybdate(IV) dihydrate

Conditions

Conditions	Yield
With NaBH4; H2O2; acetic acid In water; acetic acid byproducts: H2; aq. acetic acid; Na2MoO4*2H2O (0.149 mol), KCN (1.31 mol), NaBH4 (0.264 mol) dissolved inH2O; 40% acetic acid (120 ml) added dropwise (2 h, vigorous stirring); small excess of 30% H2O2 added slowly; pptd. with EtOH; recrystd. from H2O by pptn. with EtOH;	94%

...Expand

: 7631-95-0
sodium molybdate dihydrate

: hexaammonium heptamolybdate tetrahydrate

: 119-44-8
xanthopterin hydrate

: 105227-46-1
2Na(1+)*4(CH3)2SO*[Mo2O5(O2N5C6H3)2](2-) = [Na((CH3)2SO)2]2[Mo2O5(O2N5C6H3)2]

Conditions

Conditions	Yield
With dimethylsulfoxide In dimethyl sulfoxide added DMSO; heated to 80°C; stirred for 50 min at 85-90°Cor at 80°C for <1 h; cooled; DMSO removed in vacuo; redissolved in DMF; pptd. with Et2O; filtered; elem. anal.;	94%

...Expand

: 7631-95-0
sodium molybdate dihydrate

: cis-diaqua(2,2',2''-triaminotriethylamine)cobalt(III) perchlorate

: molybdato(2,2',2''-triaminotriethylamine)cobalt(III) perchlorate

Conditions

Conditions	Yield
In water portionwise addn. of small excess Co-complex to molybdate; cooling in ice bath (30 min), collection (filtration), washing (95% EtOH, ether); elem. anal.;	93.26%

: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer

: 7631-95-0
sodium molybdate dihydrate

: ((η(5)-pentamethylcyclopentadienyl)Rh)4Mo4O16 * 2 H2O

Conditions

Conditions	Yield
In water aq. soln. (pH 7.3) of Na2MoO4*2H2O added dropwise to suspn. of {C5Me5RhCl2}2 in water (pH 3.8); stirred for 3 h at 25°C;; recrystn. from CH2Cl2:C6H5Me (1:1); elem. anal.;;	93%

: lithium tetrafluoroborate

: 7631-95-0
sodium molybdate dihydrate

: K(7-x)Na(x)[α-PW11O39]*14H2O

: 1643-19-2
tetrabutylammomium bromide

: (Bu4N)3[α-PW11O39(Mo(VI)O)]

Conditions

Conditions	Yield
With hydrochloric acid In 1,4-dioxane; water byproducts: potassium tetrafluoroborate; to a soln. of LiBF4 in water was added KNa(α-PW11O39)14H2O, to this suspn. was added a soln. of Na2MoO42H2O in water-dioxane and hydrochloric acid, filtered, a soln. of N(C4H9)4Br in H2O-dioxane-HCl was added; ppt. was filtered off, washed with ethanol and diethyl ether;	93%

...Expand

: 7631-95-0
sodium molybdate dihydrate

: C5H4NHCHN2HCSNH2(1+)*Cl(1-)*H2O=C5H4NHCHN2HCSNH2Cl*H2O

: (C6H4NHCHN2HCSNH2)4(β-octamolybdate)(H2O)4

Conditions

Conditions	Yield
With HCl In water aq. soln. of Na2MoO4*2H2O acidified with 2 drops of HCl, treated with solid ligand (0.5 equiv.) under vigorous stirring, reacted for 2 h; filtered, washed (H2O, EtOH, acetone), dried (vac.), elem. anal.;	93%

: 7631-95-0
sodium molybdate dihydrate

: tetraoxo-μ-oxobis(pentamethylcyclopentadienyl)dimolybdenum(VI)

: 874-80-6
1-butylpyridinium bromide

: C4H9NC5H5(1+)*(C5(CH3)5)Mo6O18(1-)=C4H9NC5H5(C5(CH3)5)Mo6O18

Conditions

Conditions	Yield
With HNO3 In methanol; water byproducts: H2O; (C5(CH3)5)Mo2O5 in methanol was mixed with an aq. soln. of Na2MoO4*2H2O,aq. HNO3 was added, stirring for 2 h, bromide salt in water was added; ppt. was filtered off, washed with small portions of water, methanol anddiethyl ether, dried under vac. at 70°C; elem. anal.;	93%

...Expand

: 110-86-1
pyridine

: 7647-01-0
hydrogenchloride

: 7631-95-0
sodium molybdate dihydrate

: 6MoOCl4H2O(1-)*10C5H6N(1+)*4Cl(1-)=(C5H6N)10(MoOCl4(OH2))6Cl4

Conditions

Conditions	Yield
With hydrazine hydrate In neat (no solvent) byproducts: NaCl; (under Ar); hydrazine hydrate added dropwise to HCl, stirred, added to Na2MoO4*2H2O, heated to 80°C for 3 h, cooled to room temp., placedin freezer overnight, filtered, pyridine added dropwise at room temp., cooled to 0°C; ppt. dried under vac.; elem. anal.;	92.7%

...Expand

: 7631-95-0
sodium molybdate dihydrate

: 5922-92-9
tetrahexylammonium chloride

: 2N((CH2)5CH3)4(1+)*Mo2O3(O2)4(2-)=(N((CH2)5CH3)4)2[Mo2O3(O2)4]

Conditions

Conditions	Yield
With hydrogenchloride; dihydrogen peroxide In water treatment of Na2MoO4 soln. with 30% H2O2, pH adjustment to 4.2 (diltd. HCl), dropwise addn. of (C6H13)4NCl (pptn.); filtration, washing (H2O, Et2O), drying in air; elem. anal.;	92%

: 7631-95-0
sodium molybdate dihydrate

: tetraoxo-μ-oxobis(pentamethylcyclopentadienyl)dimolybdenum(VI)

: 1643-19-2
tetrabutylammomium bromide

: N(C4H9)4(1+)*(C5(CH3)5)Mo6O18(1-) = [N(C4H9)4][(C5(CH3)5)Mo6O18]

Conditions

Conditions	Yield
With HNO3 In methanol; water byproducts: H2O; (C5(CH3)5)Mo2O5 in methanol was mixed with an aq. soln. of Na2MoO4*2H2O,aq. HNO3 was added, stirring for 2 h, bromide salt in water was added; ppt. was filtered off, washed with small portions of water, methanol anddiethyl ether, dried under vac. at 70°C; elem. anal.;	92%

...Expand

: 7631-95-0
sodium molybdate dihydrate

: tetraoxo-μ-oxobis(pentamethylcyclopentadienyl)dimolybdenum(VI)

: 2751-90-8
tetraphenylphosphonium bromide

: P(C6H5)4(1+)*(C5(CH3)5)Mo6O18(1-)=P(C6H5)4(C5(CH3)5)Mo6O18

Conditions

Conditions	Yield
With HNO3 In methanol; water byproducts: H2O; (C5(CH3)5)Mo2O5 in methanol was mixed with an aq. soln. of Na2MoO4*2H2O,aq. HNO3 was added, stirring for 2 h, bromide salt in water was added; ppt. was filtered off, washed with small portions of water, methanol anddiethyl ether, dried under vac. at 70°C; elem. anal.;	92%

...Expand

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