Appearance:White powder Storage:keep in cool and dry place Package:25kg/drum Application:used for pharmeceutical industry Transportation:By sea or by air Port:Shanghai port, china
Cas:86-93-1
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inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:86-93-1
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryhe company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality se T rvice Appearance:Whit
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Capability on chemical synthesis 1. Beijing High-Tech Enterprises 2. Strong R&D Team 3. 8 years of experiences in R & D of high-tech Catalyst; 4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sal
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:86-93-1
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inquiryName:1-Phenyl-1H-tetrazole-5-thiol CAS NO:86-93-1 Grade:Medical scientific research and export Molecular formula:C7H6N4S Molecular weight:178 Product Quality 12 years of chemical raw materials Mature operation of the industry System stabil
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1537.html Product Name 1-Phenyltetrazole-5-thiol CAS No. 86-93-1
Cas:86-93-1
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:86-93-1
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:86-93-1
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct Name 1-Phenyltetrazole-5-thiol Synonyms 1-Phenyltetrazole-5-thiol;1-Phenyl-5-mercaptotetrazole CAS: 86-93-1 MF: - MW: -
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inquiryAppearance:white fluffy or crystalline powder or crystals Storage:Store at +15°C to +25°C. Package:25kg/Barrel Application:pharmaceutical intermediates Transportation:Express/Sea/Air Port:Any port in china
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry1-Phenyltetrazole-5-thiol Chemical Properties Melting point 145 °C (dec.)(lit.) Boiling point 342°C (rough estimate) density 1.3046 (rough estimate) refractive index 1.5500 (estimate) Fp 138°C storage temp. Store a
Cas:86-93-1
Min.Order:1 Gram
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inquiryAbout Product Details 1-Phenyltetrazole-5-thiol Basic information Product Name: 1-Pheny
Cas:86-93-1
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inquiry1-Phenyltetrazole-5-thiol CAS:86-93-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
Cas:86-93-1
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Our advantages: Sales term: Has a strong chemical professional quality and strong sense of responsibilit.In the sales field of fine chemicals and the market development of new products, we have a strong foresight and pertinence to provide custo
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Cas:86-93-1
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
Cas:86-93-1
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:86-93-1
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:86-93-1
Min.Order:4 Kilogram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:86-93-1
Min.Order:10 Gram
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inquiry1-Phenyltetrazole-5-thiolAppearance:White or Almost White crystalline powder Storage:Store in refrigerator Package:according to customers' requirements Application:Steroids injection For Body building Transportation:By air(EMS or EUB or FedEx or TNT
Conditions | Yield |
---|---|
With sodium azide; zinc(II) chloride In acetonitrile at 80℃; for 1h; | 99% |
With sodium azide In water at 90℃; for 16h; Inert atmosphere; | 75% |
With sodium azide In ethanol at 70℃; for 3h; Cyclization; |
phenyl-dithiocarbamic acid; sodium salt
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
Stage #1: phenyl-dithiocarbamic acid; sodium salt With sodium azide; sodium carbonate In water at 92℃; for 10h; Large scale; Stage #2: With sulfuric acid In water for 0.5h; pH=3; Reagent/catalyst; Temperature; pH-value; Large scale; | 93.7% |
S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
2-hydroxy-5-chloro-aniline
A
1-Phenyl-1H-tetrazole-5-thiol
B
5-chloro-2-benzoxazolinone
Conditions | Yield |
---|---|
In acetonitrile for 12h; | A n/a B 92% |
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With hydrogenchloride In water; isopropyl alcohol at 40℃; | 92% |
S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
2-amino-phenol
A
2-Benzoxazolinone
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
In acetonitrile for 12h; | A 89% B n/a |
S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
1,2-diamino-benzene
A
1,3-dihydro-2H-benzimidazol-2-one
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
In acetonitrile for 12h; | A 87% B n/a |
5-bromo-1-phenyl-1H-tetrazole
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
Stage #1: 5-bromo-1-phenyl-1H-tetrazole With thiourea In ethanol at 60℃; for 10h; Stage #2: With sodium hydroxide In ethanol at 25 - 50℃; for 3h; Reagent/catalyst; Temperature; | 86.4% |
N-methyl-2-dimethylamino-acetohydroxamic acid
3-(1-Phenyl-1H-tetrazol-5-ylsulfanyl)-3H-isobenzofuran-1-one
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
In tetrahydrofuran; water; N,N-dimethyl-formamide at 40℃; for 3h; 0.1M aq. phosphate buffer pH 7.6; | 86% |
5-Chloro-1-phenyltetrazole
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
Stage #1: 5-Chloro-1-phenyltetrazole With thiourea In ethanol at 60℃; for 10h; Stage #2: With sodium hydroxide In ethanol at 30 - 50℃; for 3h; Temperature; | 77% |
2-amino-3-hydroxypyridine
S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
A
2,3-dihydro[1,3]oxazolo[4,5-b]pyridin-2-one
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
In acetonitrile for 12h; | A 68% B n/a |
S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
2-amino-benzenethiol
A
2(3H)-Benzothiazolone
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
In acetonitrile for 12h; | A 60% B n/a |
5-anilino-1,2,3,4-thiatriazole
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With sodium hydroxide In water for 0.5h; Heating; | 50% |
With sodium hydroxide |
(E)-1-<1-phenyl-5(1H)-tetrazolylthio>propan-2-one oxime
A
1-hydroxy-2-propanone oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.); |
A
1,3-dihydroxyacetone oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.); |
(E)-3-<1-phenyl-5(1H)-tetrazolylthio>butan-2-one oxime
A
3-hydroxybutan-2-one oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; |
2-<1-phenyl-5(1H)-tetrazolylthio>cyclopentanone oxime
A
2-Hydroxy-cyclopentan-1-on-oxim
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.); |
2-<1-phenyl-5(1H)-tetrazolylthio>cyclohexanone oxime
A
2-hydroxycyclohexanonoxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.); |
A
2,4-dihydroxy-pentan-3-one oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; |
(E)-2-phenyl-2-<1-phenyl-5(1H)-tetrazolylthio>propanal oxime
A
2-hydroxy-2-phenyl-propionaldehyde-oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; |
1-phenyl-1-<1-phenyl-5(1H)-tetrazolylthio>propan-2-one oxime
A
1-Hydroxy-1-phenyl-2-propanone oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; |
α-<1-phenyl-5(1H)-tetrazolylthio>-4-methoxyacetophenone oxime
A
2-hydroxy-1-(4-methoxyphenyl)ethanone oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.); |
1,3-bis<1-phenyl-5(1H)-tetrazolylthio>propan-2-one oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Equilibrium constant; Thermodynamic data; ΔH(excit.), ΔS(excit.); |
2,4-Bis-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-pentan-3-one oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; |
(Z)-2-acetaldehyde oxime
A
hydroxyacetaldehyde oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Mechanism; other substituted oximes; |
(E)-2-acetaldehyde oxime
A
hydroxyacetaldehyde oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; |
(Z)-2-<1-phenyl-5(1H)-tetrazolylthioacetyl>phenol oxime
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; |
S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
benzoic acid
benzylamine
A
N-benzylbenzamide
B
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With triethylamine Product distribution; multistep reaction; var. carboxylic acid and amines; |
5,5'-dithiobis(1-phenyl-1H-tetrazole)
A
phenyl-1H-tetrazole
B
1-Phenyl-1H-tetrazole-5-thiol
5,5'-dithiobis(1-phenyl-1H-tetrazole)
sodium methylate
A
1-Phenyl-1H-tetrazole-5-thiol
1-Phenyl-1H-tetrazole-5-thiol
Benzoic acid (2S,3R,4R,5R,6R)-5-hydroxy-6-((E)-3-hydroxy-propenyl)-4-methanesulfonyloxy-5-methyl-2-triisopropylsilanyloxy-tetrahydro-pyran-3-yl ester
Benzoic acid (2S,3R,4R,5R,6R)-5-hydroxy-4-methanesulfonyloxy-5-methyl-6-[(E)-3-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-propenyl]-2-triisopropylsilanyloxy-tetrahydro-pyran-3-yl ester
Conditions | Yield |
---|---|
With tributylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0℃; for 0.5h; Mitsunobu reaction; | 100% |
7-(2-heptyl-[1,3]dithian-2-yl)-heptan-1-ol
1-Phenyl-1H-tetrazole-5-thiol
5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine for 0.166667h; | 100% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 25℃; | 100% |
With tetrabutylammomium bromide; sodium hydroxide In water; toluene for 3h; Reflux; | 84% |
With potassium carbonate In acetone at 70℃; for 2h; | 75% |
With triethylamine In tetrahydrofuran for 6h; Heating; |
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran; toluene at 0 - 20℃; for 0.5h; Inert atmosphere; | 100% |
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; for 1h; | 95% |
1-Phenyl-1H-tetrazole-5-thiol
methyl iodide
5-methylsulfanyl-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 25℃; | 100% |
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 2h; | 99% |
With triethylamine In tetrahydrofuran at 0 - 20℃; for 2h; Inert atmosphere; | 78% |
Stage #1: 1-Phenyl-1H-tetrazole-5-thiol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.5h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran; mineral oil at 0 - 20℃; Inert atmosphere; |
propargyl alcohol
1-Phenyl-1H-tetrazole-5-thiol
1-phenyl-5-(prop-2-yn-1-ylsulfanyl)-1H-tetrazole
Conditions | Yield |
---|---|
With bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; triphenylphosphine In dichloromethane at 20℃; for 1.5h; Mitsunobu reaction; | 100% |
With bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; triphenylphosphine for 1.5h; Mitsunobu reaction; | 100% |
With DMAB; triphenylphosphine In toluene at 20℃; Solvent; Reagent/catalyst; Mitsunobu Displacement; | 99% |
8-iodomethyl-1,4-dioxa-spiro[4.5]decane
1-Phenyl-1H-tetrazole-5-thiol
5-(1,4-dioxaspiro[4.5]dec-8-ylmethylsulfanyl)-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol at 80℃; for 2.5h; | 100% |
tert-butyl ((3R,6S)-6-(iodomethyl)tetrahydro-2H-pyran-3-yl)carbamate
1-Phenyl-1H-tetrazole-5-thiol
tert-butyl ((3R,6S)-6-(((1-phenyl-1H-tetrazol-5-yl)thio)methyl)-tetrahydro-2H-pyran-3-yl)carbamate
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 1h; Heating / reflux; | 100% |
Stage #1: 1-Phenyl-1H-tetrazole-5-thiol With potassium hydroxide In ethanol for 1h; Heating / reflux; Stage #2: tert-butyl ((3R,6S)-6-(iodomethyl)tetrahydro-2H-pyran-3-yl)carbamate In ethanol Heating / reflux; |
(diphenylphosphoryl)methyl p-toluenesulfonate
1-Phenyl-1H-tetrazole-5-thiol
α-(diphenylphosphoryl)methyl 5-(1-phenyl)-1H-tetrazolyl sulfide
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 4h; | 100% |
(4S,6R)-4-benzyloxymethyl-6-(2-iodoethyl)-2,2-dimethyl-1,3-dioxane
1-Phenyl-1H-tetrazole-5-thiol
5-(2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethylthio)-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With potassium sulfite; 18-crown-6 ether In dichloromethane at 20℃; for 24h; | 100% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran Inert atmosphere; | 100% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 12h; | 87% |
((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methanol
1-Phenyl-1H-tetrazole-5-thiol
5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)thio)-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 1h; Mitsunobu Displacement; Inert atmosphere; | 100% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 1h; Mitsunobu reaction; Inert atmosphere; | 85% |
1,2-dichloro-ethane
1-Phenyl-1H-tetrazole-5-thiol
5-((2-chloroethyl)thio)-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile at 60℃; for 72h; | 100% |
With potassium carbonate for 48h; Reflux; |
(R)-2-methyl-1,4-butanediol 4-benzyl ether
1-Phenyl-1H-tetrazole-5-thiol
5-[(2R)-4-benzoxy-2-methylbutylsulfanyl]-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 1h; Inert atmosphere; | 100% |
8-(tert-butyldiphenylsilyloxy)-(3S,7R)-3,7-dimethyl-1-octanol
1-Phenyl-1H-tetrazole-5-thiol
5-[8-(tert-butyldiphenylsilyloxy)-(3S,7R)-3,7-dimethyloctylsulfanyl]-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 1h; Inert atmosphere; | 100% |
13-benzoxy-(2R,6S,10S)-2,6,10-trimethyl-1-tridecanol
1-Phenyl-1H-tetrazole-5-thiol
5-[13-benzoxy-(2R,6R,10S)-2,6,10-trimethyl-1-tridecylsulfanyl]-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 0.5h; Inert atmosphere; | 100% |
4-bromoethylbutanoate
1-Phenyl-1H-tetrazole-5-thiol
ethyl-4-[(1-phenyl-1H-tetrazole-5-yl)thio]butanoate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 100% |
With potassium carbonate In acetone at 20℃; for 12h; Inert atmosphere; |
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 2.5h; Inert atmosphere; | 100% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 6h; | 92% |
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 2h; Mitsunobu Displacement; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; | 100% |
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran; toluene at 0 - 20℃; for 24h; Mitsunobu Displacement; Inert atmosphere; | 100% |
1-bromo-6-hexanol
1-Phenyl-1H-tetrazole-5-thiol
6-(1-phenyl-1H-tetrazole-5-ylsulfanyl)hexane-1-ol
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20 - 40℃; for 18h; | 99.5% |
trans-5,6-dihydro-6-(hydroxymethyl)-2-methoxy-2H-pyran
1-Phenyl-1H-tetrazole-5-thiol
5-(6-methoxy-3,6-dihydro-2H-pyran-2-ylmethylsulfanyl)-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 12h; | 99% |
1-Phenyl-1H-tetrazole-5-thiol
(S)-5-(4-methoxyphenoxy)-hexan-1-ol
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 12h; Mitsunobu coupling; | 99% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 91% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran Mitsunobu coupling; |
1-[(3-bromopropoxy)methyl]-benzene
1-Phenyl-1H-tetrazole-5-thiol
5-(3-benzyloxypropylsulfanyl)-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 18h; | 99% |
With sodium hydride In N,N-dimethyl-formamide |
1-Phenyl-1H-tetrazole-5-thiol
(4R,6S)-4-(2-iodoethyl)-2,2-dimethyl-6-phenethyl-[1,3]dioxane
5-{2-[(4R,6S)-2,2-dimethyl-6-phenethyl-[1,3]dioxan-4-yl]-ethylsulfanyl}-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
Stage #1: 1-Phenyl-1H-tetrazole-5-thiol With sodium hydride In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: (4R,6S)-4-(2-iodoethyl)-2,2-dimethyl-6-phenethyl-[1,3]dioxane In tetrahydrofuran; N,N-dimethyl-formamide Williamson etherification; | 99% |
1-Phenyl-1H-tetrazole-5-thiol
(R)-2-{(4R,5S)-5-[(S)-1-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-4,5-dihydro-isoxazol-3-yl}-propan-1-ol
5-((R)-2-{(4R,5S)-5-[(S)-1-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-4,5-dihydro-isoxazol-3-yl}-propylsulfanyl)-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran for 1.5h; | 99% |
pentadecanol
1-Phenyl-1H-tetrazole-5-thiol
5-pentadecylsulfanyl-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine for 0.166667h; | 99% |
1-Phenyl-1H-tetrazole-5-thiol
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 99% |
(16S,17S)-1-bromo-16-methoxy-17-methylpentatriacontane
1-Phenyl-1H-tetrazole-5-thiol
5-((16S,17S)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20 - 40℃; for 18h; | 99% |
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