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HUBEI RISON CHEMICAL CO.,LTD.

Appearance:White powder Storage:keep in cool and dry place Package:25kg/drum Application:used for pharmeceutical industry Transportation:By sea or by air Port:Shanghai port, china

1-Phenyl-1H-tetrazole-5-thiol/ 1-Phenyltetrazole-5-thiol

Cas:86-93-1

Min.Order:1 Kilogram

Negotiable

Type:Other

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Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products 1-Phenyltetrazole-5-thiol(86-93-1)

Cas:86-93-1

Min.Order:100 Gram

Negotiable

Type:Other

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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

1-Phenyltetrazole-5-thiol Manufacturer/High quality/Best price/In stock

Cas:86-93-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 1-Phenyl-5-Mercaptotetrazole supplier in China

Cas:86-93-1

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Henan Allgreen Chemical Co.,Ltd

he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality se T rvice Appearance:Whit

1-Phenyltetrazole-5-thiol

Cas:86-93-1

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 1-phenyltetrazole-5-thiol

Cas:86-93-1

Min.Order:1

Negotiable

Type:Other

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Beijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)

Capability on chemical synthesis 1. Beijing High-Tech Enterprises 2. Strong R&D Team 3. 8 years of experiences in R & D of high-tech Catalyst; 4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sal

1-Phenyltetrazole-5-thiol

Cas:86-93-1

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1,2-Dihydro-1-phenyl-5H-tetrazole-5-thione

Cas:86-93-1

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hubei DiBo chemical co., LTD

Name:1-Phenyl-1H-tetrazole-5-thiol CAS NO:86-93-1 Grade:Medical scientific research and export Molecular formula:C7H6N4S Molecular weight:178 Product Quality 12 years of chemical raw materials Mature operation of the industry System stabil

1-Phenyl-1H-tetrazole-5-thiol/ CAS:86-93-1/ raw material/ high-quality

Cas:86-93-1

Min.Order:25 Kilogram

FOB Price: $2.0 / 3.0

Type:Other

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com/pro01en/id/1537.html Product Name 1-Phenyltetrazole-5-thiol CAS No. 86-93-1

1-Phenyltetrazole-5-thiol

Cas:86-93-1

Min.Order:1 Gram

FOB Price: $2.0

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

1-Phenyl-1H-tetrazole-5-thiol CAS 86-93-1

Cas:86-93-1

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

1-Phenyltetrazole-5-thiol 86-93-1

Cas:86-93-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

New production CAS 86-93-1 with best quality

Cas:86-93-1

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name 1-Phenyltetrazole-5-thiol Synonyms 1-Phenyltetrazole-5-thiol;1-Phenyl-5-mercaptotetrazole CAS: 86-93-1 MF: - MW: -

1-Phenyltetrazole-5-thiol CAS:86-93-1

Cas:86-93-1

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Hangzhou Sartort Biopharma Co., Ltd

Appearance:white fluffy or crystalline powder or crystals Storage:Store at +15°C to +25°C. Package:25kg/Barrel Application:pharmaceutical intermediates Transportation:Express/Sea/Air Port:Any port in china

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

5H-Tetrazole-5-thione,1,2-dihydro-1-phenyl- 86-93-1

Cas:86-93-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

1-Phenyltetrazole-5-thiol Chemical Properties Melting point 145 °C (dec.)(lit.) Boiling point 342°C (rough estimate) density 1.3046 (rough estimate) refractive index 1.5500 (estimate) Fp 138°C storage temp. Store a

1-Phenyltetrazole-5-thiol.

Cas:86-93-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Leader Biochemical Group

About Product Details 1-Phenyltetrazole-5-thiol Basic information Product Name: 1-Pheny

China Biggest Factory Manufacturer Supply 1-Phenyltetrazole-5-thiol CAS 86-93-1

Cas:86-93-1

Min.Order:500 Kilogram

FOB Price: $1.0 / 2.0

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

1-Phenyltetrazole-5-thiol CAS:86-93-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in

1-Phenyltetrazole-5-thiol CAS:86-93-1

Cas:86-93-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1-Phenyltetrazole-5-thiol

Cas:86-93-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:86-93-1

Cas:86-93-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Ocean Chemical Co., Ltd.

Our advantages: Sales term: Has a strong chemical professional quality and strong sense of responsibilit.In the sales field of fine chemicals and the market development of new products, we have a strong foresight and pertinence to provide custo

1-Phenyltetrazole-5-thiol

Cas:86-93-1

Min.Order:1 Kilogram

FOB Price: $10.0

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

1-Phenyl-5-Mercaptotetrazole

Cas:86-93-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

1-Phenyltetrazole-5-thiol

Cas:86-93-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures

1-Phenyl-5-mercaptotetrazole

Cas:86-93-1

Min.Order:1 Kilogram

FOB Price: $80.0 / 100.0

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

1-Phenyl-1H-tetrazole-5-thiol

Cas:86-93-1

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1-Phenyltetrazole-5-thiol

Cas:86-93-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

1-Phenyl-5-mercaptotetrazole

Cas:86-93-1

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 1-Phenyl-5-Mercaptotetrazole

Cas:86-93-1

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Hangzhou Lingrui Chemical Co.,Ltd.

1-Phenyltetrazole-5-thiolAppearance:White or Almost White crystalline powder Storage:Store in refrigerator Package:according to customers' requirements Application:Steroids injection For Body building Transportation:By air(EMS or EUB or FedEx or TNT

1-Phenyltetrazole-5-thiol

Cas:86-93-1

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Synthetic route

phenyl isothiocyanate
103-72-0

phenyl isothiocyanate

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With sodium azide; zinc(II) chloride In acetonitrile at 80℃; for 1h;99%
With sodium azide In water at 90℃; for 16h; Inert atmosphere;75%
With sodium azide In ethanol at 70℃; for 3h; Cyclization;
phenyl-dithiocarbamic acid; sodium salt
18418-42-3

phenyl-dithiocarbamic acid; sodium salt

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
Stage #1: phenyl-dithiocarbamic acid; sodium salt With sodium azide; sodium carbonate In water at 92℃; for 10h; Large scale;
Stage #2: With sulfuric acid In water for 0.5h; pH=3; Reagent/catalyst; Temperature; pH-value; Large scale;
93.7%
S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
32276-00-9

S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate

2-hydroxy-5-chloro-aniline
95-85-2

2-hydroxy-5-chloro-aniline

A

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

B

5-chloro-2-benzoxazolinone
95-25-0

5-chloro-2-benzoxazolinone

Conditions
ConditionsYield
In acetonitrile for 12h;A n/a
B 92%
1-phenyl-4-(tetrahydro-2H-pyran-2-yl)-1H-tetrazole-5(4H)-thione

1-phenyl-4-(tetrahydro-2H-pyran-2-yl)-1H-tetrazole-5(4H)-thione

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With hydrogenchloride In water; isopropyl alcohol at 40℃;92%
S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
32276-00-9

S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate

2-amino-phenol
95-55-6

2-amino-phenol

A

2-Benzoxazolinone
59-49-4

2-Benzoxazolinone

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
In acetonitrile for 12h;A 89%
B n/a
S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
32276-00-9

S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate

1,2-diamino-benzene
95-54-5

1,2-diamino-benzene

A

1,3-dihydro-2H-benzimidazol-2-one
615-16-7

1,3-dihydro-2H-benzimidazol-2-one

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
In acetonitrile for 12h;A 87%
B n/a
5-bromo-1-phenyl-1H-tetrazole
18233-34-6

5-bromo-1-phenyl-1H-tetrazole

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
Stage #1: 5-bromo-1-phenyl-1H-tetrazole With thiourea In ethanol at 60℃; for 10h;
Stage #2: With sodium hydroxide In ethanol at 25 - 50℃; for 3h; Reagent/catalyst; Temperature;
86.4%
N-methyl-2-dimethylamino-acetohydroxamic acid
65753-93-7

N-methyl-2-dimethylamino-acetohydroxamic acid

3-(1-Phenyl-1H-tetrazol-5-ylsulfanyl)-3H-isobenzofuran-1-one
84598-74-3

3-(1-Phenyl-1H-tetrazol-5-ylsulfanyl)-3H-isobenzofuran-1-one

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
In tetrahydrofuran; water; N,N-dimethyl-formamide at 40℃; for 3h; 0.1M aq. phosphate buffer pH 7.6;86%
5-Chloro-1-phenyltetrazole
14210-25-4

5-Chloro-1-phenyltetrazole

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
Stage #1: 5-Chloro-1-phenyltetrazole With thiourea In ethanol at 60℃; for 10h;
Stage #2: With sodium hydroxide In ethanol at 30 - 50℃; for 3h; Temperature;
77%
2-amino-3-hydroxypyridine
16867-03-1

2-amino-3-hydroxypyridine

S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
32276-00-9

S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate

A

2,3-dihydro[1,3]oxazolo[4,5-b]pyridin-2-one
60832-72-6

2,3-dihydro[1,3]oxazolo[4,5-b]pyridin-2-one

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
In acetonitrile for 12h;A 68%
B n/a
S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
32276-00-9

S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate

2-amino-benzenethiol
137-07-5

2-amino-benzenethiol

A

2(3H)-Benzothiazolone
934-34-9

2(3H)-Benzothiazolone

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
In acetonitrile for 12h;A 60%
B n/a
5-anilino-1,2,3,4-thiatriazole
13078-30-3

5-anilino-1,2,3,4-thiatriazole

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With sodium hydroxide In water for 0.5h; Heating;50%
With sodium hydroxide
(E)-1-<1-phenyl-5(1H)-tetrazolylthio>propan-2-one oxime
145614-22-8

(E)-1-<1-phenyl-5(1H)-tetrazolylthio>propan-2-one oxime

A

1-hydroxy-2-propanone oxime
134252-16-7

1-hydroxy-2-propanone oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.);
1-Hydroxy-3-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-propan-2-one oxime

1-Hydroxy-3-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-propan-2-one oxime

A

1,3-dihydroxyacetone oxime
37110-18-2

1,3-dihydroxyacetone oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.);
(E)-3-<1-phenyl-5(1H)-tetrazolylthio>butan-2-one oxime
145614-23-9

(E)-3-<1-phenyl-5(1H)-tetrazolylthio>butan-2-one oxime

A

3-hydroxybutan-2-one oxime
37110-17-1

3-hydroxybutan-2-one oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant;
2-<1-phenyl-5(1H)-tetrazolylthio>cyclopentanone oxime
145614-30-8

2-<1-phenyl-5(1H)-tetrazolylthio>cyclopentanone oxime

A

2-Hydroxy-cyclopentan-1-on-oxim
14352-55-7

2-Hydroxy-cyclopentan-1-on-oxim

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.);
2-<1-phenyl-5(1H)-tetrazolylthio>cyclohexanone oxime
145614-34-2

2-<1-phenyl-5(1H)-tetrazolylthio>cyclohexanone oxime

A

2-hydroxycyclohexanonoxime
3307-35-5

2-hydroxycyclohexanonoxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.);
2-Hydroxy-4-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-pentan-3-one oxime

2-Hydroxy-4-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-pentan-3-one oxime

A

2,4-dihydroxy-pentan-3-one oxime
98137-61-2

2,4-dihydroxy-pentan-3-one oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant;
(E)-2-phenyl-2-<1-phenyl-5(1H)-tetrazolylthio>propanal oxime
145614-21-7

(E)-2-phenyl-2-<1-phenyl-5(1H)-tetrazolylthio>propanal oxime

A

2-hydroxy-2-phenyl-propionaldehyde-oxime
115051-47-3

2-hydroxy-2-phenyl-propionaldehyde-oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant;
1-phenyl-1-<1-phenyl-5(1H)-tetrazolylthio>propan-2-one oxime
145614-27-3

1-phenyl-1-<1-phenyl-5(1H)-tetrazolylthio>propan-2-one oxime

A

1-Hydroxy-1-phenyl-2-propanone oxime
26226-58-4

1-Hydroxy-1-phenyl-2-propanone oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant;
α-<1-phenyl-5(1H)-tetrazolylthio>-4-methoxyacetophenone oxime
145614-26-2

α-<1-phenyl-5(1H)-tetrazolylthio>-4-methoxyacetophenone oxime

A

2-hydroxy-1-(4-methoxyphenyl)ethanone oxime
86790-89-8, 86790-91-2

2-hydroxy-1-(4-methoxyphenyl)ethanone oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.);
1,3-bis<1-phenyl-5(1H)-tetrazolylthio>propan-2-one oxime
115786-72-6

1,3-bis<1-phenyl-5(1H)-tetrazolylthio>propan-2-one oxime

A

1-Hydroxy-3-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-propan-2-one oxime

1-Hydroxy-3-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-propan-2-one oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Equilibrium constant; Thermodynamic data; ΔH(excit.), ΔS(excit.);
2,4-Bis-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-pentan-3-one oxime
145614-24-0

2,4-Bis-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-pentan-3-one oxime

A

2-Hydroxy-4-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-pentan-3-one oxime

2-Hydroxy-4-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-pentan-3-one oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant;
(Z)-2-acetaldehyde oxime
145614-42-2

(Z)-2-acetaldehyde oxime

A

hydroxyacetaldehyde oxime
37110-02-4

hydroxyacetaldehyde oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant; Mechanism; other substituted oximes;
(E)-2-acetaldehyde oxime
145614-19-3

(E)-2-acetaldehyde oxime

A

hydroxyacetaldehyde oxime
37110-02-4

hydroxyacetaldehyde oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant;
(Z)-2-<1-phenyl-5(1H)-tetrazolylthioacetyl>phenol oxime
145614-46-6

(Z)-2-<1-phenyl-5(1H)-tetrazolylthioacetyl>phenol oxime

A

2-Hydroxy-1-(2-hydroxy-phenyl)-ethanone oxime

2-Hydroxy-1-(2-hydroxy-phenyl)-ethanone oxime

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With potassium hydroxide In water; acetonitrile at 22℃; Rate constant;
S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate
32276-00-9

S,S"-bis(1-phenyl-1H-tetrazol-5-yl) dithiocarbonate

benzoic acid
65-85-0

benzoic acid

benzylamine
100-46-9

benzylamine

A

N-benzylbenzamide
1485-70-7

N-benzylbenzamide

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Conditions
ConditionsYield
With triethylamine Product distribution; multistep reaction; var. carboxylic acid and amines;
5,5'-dithiobis(1-phenyl-1H-tetrazole)
5117-07-7

5,5'-dithiobis(1-phenyl-1H-tetrazole)

alkaline solution

alkaline solution

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5,5'-dithiobis(1-phenyl-1H-tetrazole)
5117-07-7

5,5'-dithiobis(1-phenyl-1H-tetrazole)

diluted NaOH-solution

diluted NaOH-solution

A

phenyl-1H-tetrazole
5378-52-9

phenyl-1H-tetrazole

B

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5,5'-dithiobis(1-phenyl-1H-tetrazole)
5117-07-7

5,5'-dithiobis(1-phenyl-1H-tetrazole)

sodium methylate
124-41-4

sodium methylate

A

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

B

compound of triphenyl-isomelamine with phenyl cyanamide

compound of triphenyl-isomelamine with phenyl cyanamide

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

Benzoic acid (2S,3R,4R,5R,6R)-5-hydroxy-6-((E)-3-hydroxy-propenyl)-4-methanesulfonyloxy-5-methyl-2-triisopropylsilanyloxy-tetrahydro-pyran-3-yl ester
359766-31-7

Benzoic acid (2S,3R,4R,5R,6R)-5-hydroxy-6-((E)-3-hydroxy-propenyl)-4-methanesulfonyloxy-5-methyl-2-triisopropylsilanyloxy-tetrahydro-pyran-3-yl ester

Benzoic acid (2S,3R,4R,5R,6R)-5-hydroxy-4-methanesulfonyloxy-5-methyl-6-[(E)-3-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-propenyl]-2-triisopropylsilanyloxy-tetrahydro-pyran-3-yl ester
359766-38-4

Benzoic acid (2S,3R,4R,5R,6R)-5-hydroxy-4-methanesulfonyloxy-5-methyl-6-[(E)-3-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-propenyl]-2-triisopropylsilanyloxy-tetrahydro-pyran-3-yl ester

Conditions
ConditionsYield
With tributylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0℃; for 0.5h; Mitsunobu reaction;100%
7-(2-heptyl-[1,3]dithian-2-yl)-heptan-1-ol
861997-60-6

7-(2-heptyl-[1,3]dithian-2-yl)-heptan-1-ol

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole
861997-61-7

5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine for 0.166667h;100%
benzyl bromide
100-39-0

benzyl bromide

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

BI-83B3
3206-48-2

BI-83B3

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 0 - 25℃;100%
With tetrabutylammomium bromide; sodium hydroxide In water; toluene for 3h; Reflux;84%
With potassium carbonate In acetone at 70℃; for 2h;75%
With triethylamine In tetrahydrofuran for 6h; Heating;
1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

hexan-1-ol
111-27-3

hexan-1-ol

5-hexylthio-1-phenyl-1H-tetrazole

5-hexylthio-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran; toluene at 0 - 20℃; for 0.5h; Inert atmosphere;100%
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; for 1h;95%
1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

methyl iodide
74-88-4

methyl iodide

5-methylsulfanyl-1-phenyl-1H-tetrazole
1455-92-1

5-methylsulfanyl-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 0 - 25℃;100%
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 2h;99%
With triethylamine In tetrahydrofuran at 0 - 20℃; for 2h; Inert atmosphere;78%
Stage #1: 1-Phenyl-1H-tetrazole-5-thiol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.5h; Inert atmosphere;
Stage #2: methyl iodide In tetrahydrofuran; mineral oil at 0 - 20℃; Inert atmosphere;
propargyl alcohol
107-19-7

propargyl alcohol

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

1-phenyl-5-(prop-2-yn-1-ylsulfanyl)-1H-tetrazole
53918-41-5

1-phenyl-5-(prop-2-yn-1-ylsulfanyl)-1H-tetrazole

Conditions
ConditionsYield
With bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; triphenylphosphine In dichloromethane at 20℃; for 1.5h; Mitsunobu reaction;100%
With bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; triphenylphosphine for 1.5h; Mitsunobu reaction;100%
With DMAB; triphenylphosphine In toluene at 20℃; Solvent; Reagent/catalyst; Mitsunobu Displacement;99%
8-iodomethyl-1,4-dioxa-spiro[4.5]decane
625114-56-9

8-iodomethyl-1,4-dioxa-spiro[4.5]decane

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-(1,4-dioxaspiro[4.5]dec-8-ylmethylsulfanyl)-1-phenyl-1H-tetrazole
1010815-07-2

5-(1,4-dioxaspiro[4.5]dec-8-ylmethylsulfanyl)-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With potassium hydroxide In ethanol at 80℃; for 2.5h;100%
tert-butyl ((3R,6S)-6-(iodomethyl)tetrahydro-2H-pyran-3-yl)carbamate
881657-58-5

tert-butyl ((3R,6S)-6-(iodomethyl)tetrahydro-2H-pyran-3-yl)carbamate

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

tert-butyl ((3R,6S)-6-(((1-phenyl-1H-tetrazol-5-yl)thio)methyl)-tetrahydro-2H-pyran-3-yl)carbamate
881657-48-3

tert-butyl ((3R,6S)-6-(((1-phenyl-1H-tetrazol-5-yl)thio)methyl)-tetrahydro-2H-pyran-3-yl)carbamate

Conditions
ConditionsYield
With potassium hydroxide In ethanol for 1h; Heating / reflux;100%
Stage #1: 1-Phenyl-1H-tetrazole-5-thiol With potassium hydroxide In ethanol for 1h; Heating / reflux;
Stage #2: tert-butyl ((3R,6S)-6-(iodomethyl)tetrahydro-2H-pyran-3-yl)carbamate In ethanol Heating / reflux;
(diphenylphosphoryl)methyl p-toluenesulfonate
33730-69-7

(diphenylphosphoryl)methyl p-toluenesulfonate

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

α-(diphenylphosphoryl)methyl 5-(1-phenyl)-1H-tetrazolyl sulfide
1021879-80-0

α-(diphenylphosphoryl)methyl 5-(1-phenyl)-1H-tetrazolyl sulfide

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 4h;100%
(4S,6R)-4-benzyloxymethyl-6-(2-iodoethyl)-2,2-dimethyl-1,3-dioxane
1067185-78-7

(4S,6R)-4-benzyloxymethyl-6-(2-iodoethyl)-2,2-dimethyl-1,3-dioxane

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-(2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethylthio)-1-phenyl-1H-tetrazole
1067185-77-6

5-(2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethylthio)-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With potassium sulfite; 18-crown-6 ether In dichloromethane at 20℃; for 24h;100%
C27H50O5Si
1186073-80-2

C27H50O5Si

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

C34H54N4O4SSi
1186073-96-0

C34H54N4O4SSi

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran Inert atmosphere;100%
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 12h;87%
((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methanol
1333237-38-9

((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methanol

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)thio)-1-phenyl-1H-tetrazole
1333237-39-0

5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)thio)-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 1h; Mitsunobu Displacement; Inert atmosphere;100%
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 1h; Mitsunobu reaction; Inert atmosphere;85%
1,2-dichloro-ethane
107-06-2

1,2-dichloro-ethane

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-((2-chloroethyl)thio)-1-phenyl-1H-tetrazole
1153358-38-3

5-((2-chloroethyl)thio)-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With caesium carbonate In acetonitrile at 60℃; for 72h;100%
With potassium carbonate for 48h; Reflux;
(R)-2-methyl-1,4-butanediol 4-benzyl ether
96154-47-1

(R)-2-methyl-1,4-butanediol 4-benzyl ether

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-[(2R)-4-benzoxy-2-methylbutylsulfanyl]-1-phenyl-1H-tetrazole
1443232-98-1

5-[(2R)-4-benzoxy-2-methylbutylsulfanyl]-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 1h; Inert atmosphere;100%
8-(tert-butyldiphenylsilyloxy)-(3S,7R)-3,7-dimethyl-1-octanol
1443233-18-8

8-(tert-butyldiphenylsilyloxy)-(3S,7R)-3,7-dimethyl-1-octanol

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-[8-(tert-butyldiphenylsilyloxy)-(3S,7R)-3,7-dimethyloctylsulfanyl]-1-phenyl-1H-tetrazole
1443233-26-8

5-[8-(tert-butyldiphenylsilyloxy)-(3S,7R)-3,7-dimethyloctylsulfanyl]-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 1h; Inert atmosphere;100%
13-benzoxy-(2R,6S,10S)-2,6,10-trimethyl-1-tridecanol
1443233-29-1

13-benzoxy-(2R,6S,10S)-2,6,10-trimethyl-1-tridecanol

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-[13-benzoxy-(2R,6R,10S)-2,6,10-trimethyl-1-tridecylsulfanyl]-1-phenyl-1H-tetrazole
1443233-30-4

5-[13-benzoxy-(2R,6R,10S)-2,6,10-trimethyl-1-tridecylsulfanyl]-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 0.5h; Inert atmosphere;100%
4-bromoethylbutanoate
2969-81-5

4-bromoethylbutanoate

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

ethyl-4-[(1-phenyl-1H-tetrazole-5-yl)thio]butanoate
1173997-34-6

ethyl-4-[(1-phenyl-1H-tetrazole-5-yl)thio]butanoate

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere;100%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere;100%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere;100%
With potassium carbonate In acetone at 20℃; for 12h; Inert atmosphere;
(2R,3R,E)-5-iodo-3-((4-methoxybenzyl)oxy)-2-methylpent-4-en-1-ol

(2R,3R,E)-5-iodo-3-((4-methoxybenzyl)oxy)-2-methylpent-4-en-1-ol

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-(((2S,3R,E)-5-iodo-3-((4-methoxybenzyl)oxy)-2-methylpent-4-en-1-yl)thio)-1-phenyl-1H-tetrazole

5-(((2S,3R,E)-5-iodo-3-((4-methoxybenzyl)oxy)-2-methylpent-4-en-1-yl)thio)-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 2.5h; Inert atmosphere;100%
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 6h;92%
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 2h; Mitsunobu Displacement; Inert atmosphere;91%
1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

epichlorohydrin
106-89-8

epichlorohydrin

(+/-)-3-chloro-1-(1-phenyl-1H-1,2,3,4-tetrazol-5-ylthio)-2-propanol

(+/-)-3-chloro-1-(1-phenyl-1H-1,2,3,4-tetrazol-5-ylthio)-2-propanol

Conditions
ConditionsYield
In neat (no solvent) at 20℃;100%
1,3-dimethoxy-5-(5-hydroxypentyl)benzene
836-27-1

1,3-dimethoxy-5-(5-hydroxypentyl)benzene

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

C20H24N4O2S

C20H24N4O2S

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran; toluene at 0 - 20℃; for 24h; Mitsunobu Displacement; Inert atmosphere;100%
1-bromo-6-hexanol
4286-55-9

1-bromo-6-hexanol

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

6-(1-phenyl-1H-tetrazole-5-ylsulfanyl)hexane-1-ol
934502-98-4

6-(1-phenyl-1H-tetrazole-5-ylsulfanyl)hexane-1-ol

Conditions
ConditionsYield
With potassium carbonate In acetone at 20 - 40℃; for 18h;99.5%
trans-5,6-dihydro-6-(hydroxymethyl)-2-methoxy-2H-pyran
63358-55-4

trans-5,6-dihydro-6-(hydroxymethyl)-2-methoxy-2H-pyran

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-(6-methoxy-3,6-dihydro-2H-pyran-2-ylmethylsulfanyl)-1-phenyl-1H-tetrazole
343764-60-3

5-(6-methoxy-3,6-dihydro-2H-pyran-2-ylmethylsulfanyl)-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; for 12h;99%
1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

(S)-5-(4-methoxyphenoxy)-hexan-1-ol
457100-61-7

(S)-5-(4-methoxyphenoxy)-hexan-1-ol

5-[(S)-5-(4-methoxyphenoxy)-hexylsulfanyl]-1-phenyl-1H-tetrazole

5-[(S)-5-(4-methoxyphenoxy)-hexylsulfanyl]-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 12h; Mitsunobu coupling;99%
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; Inert atmosphere;91%
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran Mitsunobu coupling;
1-[(3-bromopropoxy)methyl]-benzene
54314-84-0

1-[(3-bromopropoxy)methyl]-benzene

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-(3-benzyloxypropylsulfanyl)-1-phenyl-1H-tetrazole
1023306-27-5

5-(3-benzyloxypropylsulfanyl)-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 18h;99%
With sodium hydride In N,N-dimethyl-formamide
1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

(4R,6S)-4-(2-iodoethyl)-2,2-dimethyl-6-phenethyl-[1,3]dioxane
745058-38-2

(4R,6S)-4-(2-iodoethyl)-2,2-dimethyl-6-phenethyl-[1,3]dioxane

5-{2-[(4R,6S)-2,2-dimethyl-6-phenethyl-[1,3]dioxan-4-yl]-ethylsulfanyl}-1-phenyl-1H-tetrazole
485321-90-2

5-{2-[(4R,6S)-2,2-dimethyl-6-phenethyl-[1,3]dioxan-4-yl]-ethylsulfanyl}-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
Stage #1: 1-Phenyl-1H-tetrazole-5-thiol With sodium hydride In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 0.5h;
Stage #2: (4R,6S)-4-(2-iodoethyl)-2,2-dimethyl-6-phenethyl-[1,3]dioxane In tetrahydrofuran; N,N-dimethyl-formamide Williamson etherification;
99%
1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

(R)-2-{(4R,5S)-5-[(S)-1-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-4,5-dihydro-isoxazol-3-yl}-propan-1-ol
735317-63-2

(R)-2-{(4R,5S)-5-[(S)-1-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-4,5-dihydro-isoxazol-3-yl}-propan-1-ol

5-((R)-2-{(4R,5S)-5-[(S)-1-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-4,5-dihydro-isoxazol-3-yl}-propylsulfanyl)-1-phenyl-1H-tetrazole
735317-66-5

5-((R)-2-{(4R,5S)-5-[(S)-1-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-4,5-dihydro-isoxazol-3-yl}-propylsulfanyl)-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran for 1.5h;99%
pentadecanol
629-76-5

pentadecanol

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-pentadecylsulfanyl-1-phenyl-1H-tetrazole
861997-80-0

5-pentadecylsulfanyl-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine for 0.166667h;99%
1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

2-halo-1-naphthalen-2-yl-ethanone

2-halo-1-naphthalen-2-yl-ethanone

1-naphthalen-2-yl-2-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-ethanone

1-naphthalen-2-yl-2-(1-phenyl-1H-tetrazol-5-ylsulfanyl)-ethanone

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃;99%
(16S,17S)-1-bromo-16-methoxy-17-methylpentatriacontane
934503-46-5

(16S,17S)-1-bromo-16-methoxy-17-methylpentatriacontane

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

5-((16S,17S)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole
934503-48-7

5-((16S,17S)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole

Conditions
ConditionsYield
With potassium carbonate In acetone at 20 - 40℃; for 18h;99%
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