hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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Cas:107-06-2
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inquiryChemical name: Dichloroethane Molecular formula: C2H4Cl2 Structural formula: Molecular weight: 98.97 CAS No.: 107-06-2 Physicochemical property: colorless or light yellow transparent liquid; melting point -35.7℃; boiling point 83.5℃; den
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inquiry1,2-Dichloroethane CAS:107-06-2 Specification mp -35 °C bp 83 °C(lit.) density 1.256 g/mL at 25 °C(lit.) vapor density 3.4 (20 °C, vs air) vapor pressure 87 mm Hg (
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inquiryAppearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:As customer request Port:Qingda
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inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat
Product Name: 1,2-Dichloroethane Synonyms: 1,2-Bichloroethane;1,2-DCE;1,2-Dichloorethaan;1,2-Dichlor-aethan;1,2-Dichlorethan;1,2-Dichlorethane;1,2-dichloro-ethan;1,2-dichloroethane (ethylene dichloride) CAS: 107-06-2 MF: C2
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Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
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inquiry1,2-DichloroethaneAppearance:powder Storage:200MT Package:as your requirement Application:Pharmaceutical Intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/FCL for
in stock Application:107-06-2
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inquiryoxirane
trichlorodistyrylphosphorane
A
Bis-((E)-styryl)-phosphinic acid 2-chloro-ethyl ester
B
1,2-dichloro-ethane
Conditions | Yield |
---|---|
With titanium tetrachloride In benzene at 40℃; | A 91% B n/a |
oxirane
Styryl-phosphortetrachlorid
A
bis(2-chloroethyl) styrylphosphonate
B
1,2-dichloro-ethane
Conditions | Yield |
---|---|
With titanium tetrachloride In benzene at 40℃; | A 90% B n/a |
Conditions | Yield |
---|---|
With chlorotrifluoromethane; hydrogen iodide Product distribution; Mechanism; Irradiation; var. pressure; labeling (38)Cl; | A 0.76% B 78% |
ethene
tetrabutylammonium p-toluenesulfonate
A
2-chloroethyl tosylate
B
1,2-dichloro-ethane
Conditions | Yield |
---|---|
With chlorine In dichloromethane at 20℃; for 0.25h; Product distribution; Mechanism; | A 43% B 57 % Spectr. |
With chlorine In dichloromethane at 20℃; for 0.25h; | A 43% B 57 % Spectr. |
With chlorine In dichloromethane Ambient temperature; |
Conditions | Yield |
---|---|
With tetrabutylammonium p-toluenesulfonate; chlorine In dichloromethane at 20℃; for 0.25h; | A 43% B 57 % Spectr. |
dichloromethane
aniline
A
N-methylenebenzenamine
B
methylene chloride
C
1,2-dichloro-ethane
D
Azobenzene
E
N-phenylphenylene-1,4-diamine
F
N-phenyl-1,2-benzenediamine
Conditions | Yield |
---|---|
at 15℃; for 24h; Product distribution; Mechanism; Irradiation; | A n/a B n/a C n/a D 18.6% E 15.6% F 25.8% G n/a |
chloromethyl-methyl-diphenyl-silane
A
Methyltrichlorosilane
B
biphenyl
C
chloromethyldiphenylsilane
D
Phenyltrichlorosilane
E
1,2-dichloro-ethane
Conditions | Yield |
---|---|
iron(III) chloride at 70℃; for 0.5h; Product distribution; other conditions: other catalyst, other temperature; | A 8% B 10% C 17% D 14% E 22% |
1,3-dioxolane-2-spirocyclohexane
A
6-(1-cyclohexenyl)caproic acid β-chloroethyl ester
B
ethylene glycol
C
1,2-dichloro-ethane
D
2-chloro-ethanol
Conditions | Yield |
---|---|
With hydrogenchloride at 150℃; for 2h; | A 15% B n/a C n/a D n/a |
1,4-dioxaspiro[4.4]nonane
A
5-(1-cyclopentenyl)valeric acid β-chloroethyl ester
B
ethylene glycol
C
1,2-dichloro-ethane
D
2-chloro-ethanol
Conditions | Yield |
---|---|
With hydrogenchloride at 150℃; for 2h; | A 14% B n/a C n/a D n/a |
oxirane
Methanesulfenyl chloride
A
Dimethyldisulphide
B
methanesulfinic acid-(2-chloro-ethyl ester)
C
1,2-dichloro-ethane
Conditions | Yield |
---|---|
With disulfur dichloride |
Conditions | Yield |
---|---|
Einw. dunkler elektrischer Entladungen; |
Conditions | Yield |
---|---|
bei der Einwirkung dunkler elektrischer Entladungen; |
chloroethyl chlorosulfate
sulfurous acid bis-(2-chloro-ethyl ester)
A
sulfuric acid bis-(2-chloroethyl) ester
B
1,2-dichloro-ethane
Conditions | Yield |
---|---|
at 130 - 175℃; | |
at 130 - 175℃; | |
With zinc(II) chloride at 130 - 175℃; |
sulfurous acid bis-(2-chloro-ethyl ester)
A
2-chloroethyl chlorosulphite
B
1,2-dichloro-ethane
Conditions | Yield |
---|---|
With tetrachloromethane; phosphorus pentachloride |
Conditions | Yield |
---|---|
With hydrogenchloride; alkali chloride |
Conditions | Yield |
---|---|
erfolgt Zersetzung; |
ethanol
dichloro-(2-chloro-ethoxy)-acetyl chloride
A
chloroethane
B
1,2-dichloro-ethane
C
oxalic acid diethyl ester
Conditions | Yield |
---|---|
zuletzt in der Siedehitze; reagiert analog mit Methanol und Isopropylalkohol; |
Conditions | Yield |
---|---|
With hydrogenchloride; aluminum oxide; air; water; sodium chloride; copper dichloride at 225℃; unter Druck; | |
With hydrogenchloride; aluminum oxide; air; water; sodium chloride; copper dichloride at 280 - 290℃; |
Conditions | Yield |
---|---|
With sulfuric acid; copper dichloride at 0℃; |
Conditions | Yield |
---|---|
With chlorine | |
With chlorine at -78℃; | |
With chlorine; ethylene dibromide at 40 - 100℃; ueber poroeses Material; |
Conditions | Yield |
---|---|
With sulfuryl dichloride at 20℃; | |
With disulfur dichloride; sulfuryl dichloride; sulfur dichloride at 20℃; |
Conditions | Yield |
---|---|
With water; Iodine monochloride |
Conditions | Yield |
---|---|
With chlorine; 2-chloro-ethanol | |
With oxirane; chlorine | |
With oxirane; chlorine; 2-chloro-ethanol |
Conditions | Yield |
---|---|
With chlorine | |
With chlorine im Licht; | |
With antimonypentachloride at 100℃; | |
With water Chlorierung; |
Conditions | Yield |
---|---|
at 0℃; Einfluss des Loesungsmittels auf die Photochlorierung; | |
With chlorine In chlorobenzene Mechanism; Kinetics; other solvent; object of study: solvents effects vs. the reaction selectivity; | |
With chlorine In gas at 8 - 94℃; Kinetics; Thermodynamic data; Mechanism; ΔE(excit); |
Conditions | Yield |
---|---|
at 180℃; | |
at 180℃; Gleichgewicht; |
Conditions | Yield |
---|---|
With potassium hydroxide; tetrabutylammomium bromide for 0.333333h; Ambient temperature; | 100% |
4-((3-chloro-2-fluorophenyl)amino)-7-methoxyquinazolin-6-ol
1,2-dichloro-ethane
C17H14Cl2FN3O2
Conditions | Yield |
---|---|
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 60℃; for 48h; | 100% |
trans-4-(2,4-Bis{[tert-butyl(dimethyl)silyl]oxy}phenyl)cyclohexylamine
methanesulfonyl chloride
1,2-dichloro-ethane
trans-N-[4-(2,4-Bis{[tert-butyl(dimethyl)silyl]oxy}phenyl)cyclohexyl] Methane Sulfonamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane; water | 100% |
4-nitro-phenol
oxalyl dichloride
1,2-dichloro-ethane
4-nitrophenyl 4-acetylbenzoate
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane; chloroform; 4-acetyl-benzoic acid | 100% |
1,2-dichloro-ethane
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane Ar atmosphere; removement of excess solvent (vacuum); elem. anal.; | 100% |
Conditions | Yield |
---|---|
at 110℃; for 17h; Darkness; | 100% |
In chloroform at 60℃; under 14251400 Torr; for 24h; Pressure; Menshutkin Reaction; High pressure; | 95% |
at 110℃; for 6h; neat (no solvent); | 91% |
1,2-dichloro-ethane
1-Phenyl-1H-tetrazole-5-thiol
5-((2-chloroethyl)thio)-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile at 60℃; for 72h; | 100% |
With potassium carbonate for 48h; Reflux; |
(1R,3aS,5aR,5bR,7aR,11aR,11bR,13aR,13bR)-3a-amino-5a,5b,8,8,11a-pentamethyl-1-(prop-1-en-2-yl)octadecahydro-1H-cyclopenta[a]chrysen-9(5bH)-one hydrochloride
1,2-dichloro-ethane
(1R,3aS,5aR,5bR,7aR,11aR,11bR,13aR,13bR)-3a-(aziridin-1-yl)-5a,5b,8,8,11a-pentamethyl-1-(prop-1-en-2-yl)octadecahydro-1H-cyclopenta[a]chrysen-9(5bH)-one
Conditions | Yield |
---|---|
With potassium phosphate In acetonitrile at 130℃; for 36h; Concentration; Time; Inert atmosphere; Sealed tube; | 100% |
4'-(4-pyridin-4-ylethynyl-phenyl)[2,2';6',2'']terpyridine
2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline
zinc trifluoromethanesulfonate
1,2-dichloro-ethane
Conditions | Yield |
---|---|
In acetonitrile for 2h; Reflux; | 100% |
Conditions | Yield |
---|---|
With copper(I) bromide at 90℃; for 0.5h; Microwave irradiation; | 100% |
4-Chloro-3,5-dimethylpyrazole
1,2-dichloro-ethane
Conditions | Yield |
---|---|
With tetrabutyl-ammonium chloride; sodium hydroxide In water | 100% |
Conditions | Yield |
---|---|
With tetrabutyl-ammonium chloride; sodium hydroxide In water | 100% |
Conditions | Yield |
---|---|
at 450 - 550℃; under 10501.1 - 26252.6 Torr; for 0.00416667 - 0.00833333h; | A n/a B 99.52% |
at 362 - 485℃; eine nahezu homogene Reaktion erster Ordnung, die wahrscheinlich von Chloratomen und 1.2-Dichlor-aethyl-Radikalen unterhalten wird.Thermolysis; | |
at 600℃; Conversion of starting material; | |
at 615℃; Rate constant; | |
at 650℃; Rate constant; |
Conditions | Yield |
---|---|
With triethylbenzylammonium ethanolate at -20 - 20℃; | 99% |
75% | |
With polyacrylonitrile-based active carbon fiber at 350℃; under 760 Torr; for 2h; other catalyst, var. reaction time; | 57% |
theophylline
1,2-dichloro-ethane
7-(2-chloroethyl)-3,7-dihydro-1,3-dimethyl-1H-purine-2,6-dione
Conditions | Yield |
---|---|
With sodium hydroxide; Aliquat 336 for 4h; Heating; | 99% |
With sodium hydroxide In water; isopropyl alcohol at 78 - 80℃; for 76.5h; Heating; | 90% |
In water; dimethyl sulfoxide |
(1,1'-biphenyl)-4,4'-dithiol
1,2-dichloro-ethane
4,4'-Bis-(2-chloro-ethylsulfanyl)-biphenyl
Conditions | Yield |
---|---|
With potassium hydroxide; tetrabutylammomium bromide for 0.333333h; Ambient temperature; | 99% |
Conditions | Yield |
---|---|
With pyridine | 99% |
2,3-Dihydrobenzofuran
1,2-dichloro-ethane
2,3-dihydrobenzofuran-5-sulfonyl chloride
Conditions | Yield |
---|---|
With thionyl chloride In water | 99% |
Methylenedioxybenzene
1,2-dichloro-ethane
6-chlorosulfonyl-1,4-benzodioxane
Conditions | Yield |
---|---|
With thionyl chloride In water | 99% |
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hydroxide; sodium chloride; hydroxylamine hydrochloride In methanol; dichloromethane; chloroform; water | 99% |
With hydrogenchloride; sodium hydroxide; sodium chloride; hydroxylamine hydrochloride In methanol; dichloromethane; chloroform; water | 99% |
1,2-dichloro-ethane
silver(l) oxide
3-(N,N-diethylcarbamoylmethyl)-1-mesitylimidazolium bromide
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane heating of excess of Ag2O and C18H26BrN3O in 1,2-dichloroethane at 90°C for 4 h in the presence of molecular sieves; filtration, removal of solvent in vacuo, washing with ether with hygroscopic solid; elem. anal.; | 99% |
Yb(2,6-di-tert-butylphenolate)2(THF)3
1,2-dichloro-ethane
chlorobis(2,6-di-tert-butylphenolato)bis(tetrahydrofuran)ytterbium(III)
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: C2H4, THF; under Ar or N2, 0.5 equiv. of halogen-compd. was added to Yb-compd. soln. in THF, stirring for 24 h at room temp.; volatiles were removed in vac., solid was dried in vac. at room temp., elem. anal.; | 99% |
tris(tetrahydrofuran)bis(2,4,6-tri-t-butylphenolato)ytterbium(II)
1,2-dichloro-ethane
chlorobis(2,4,6-tri-tert-butylphenolato)bis(tetrahydrofuran)ytterbium(III)
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: C2H4, THF; under Ar or N2, 0.5 equiv. of halogen-compd. was added to Yb-compd. soln. in THF, stirring for 24 h at room temp.; volatiles were removed in vac., solid was dried in vac. at room temp., elem. anal.; | 99% |
Yb(2,6-di-tert-butyl-4-methylphenolate)2(THF)3
1,2-dichloro-ethane
chlorobis(2,6-di-tert-butyl-4-methylphenolato)bis(tetrahydrofuran)ytterbium(III)
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: C2H4, THF; under Ar or N2, 0.5 equiv. of halogen-compd. was added to Yb-compd. soln. in THF, stirring for 24 h at room temp.; volatiles were removed in vac., solid was dried in vac. at room temp., elem. anal.; | 99% |
chloro(trimethylamine-isocyanoborane)gold(I)
1,2-dichloro-ethane
potassium iodide
Conditions | Yield |
---|---|
In dichloromethane; water (Ar); a soln. of Au complex in CH2Cl2 poured into an aq. soln. of KI, stirred for 18 h; phases sepd., the aq. phase extd. (CH2Cl2), the org. exts. combined, recrystd. (1,2-dichloroethane and pentane); elem. anal.; | 99% |
1,2-dichloro-ethane
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) Irradiation (UV/VIS); treated for 25 h; crystd. (CH2Cl2/Et2O), elem. anal.; | 99% |
Conditions | Yield |
---|---|
In sulfur dioxide under Ar atm. SO2 was condensed onto mixt. Ph3CCl and Li2(B12Cl12), warmed and stirred at room temp. for 1 h; volatiles were removed in vacuo, residue was extd. with 1,2-C2H4Cl2; | 99% |
N,N'-dimethyl-N,N'-hexamethylenebis(5-tert-butyl-2-hydroxy-3-hydroxyiminomethyl)benzylamine
copper(II) acetate monohydrate
1,2-dichloro-ethane
Conditions | Yield |
---|---|
In ethanol; 1,2-dichloro-ethane soln. of Cu salt and ligand (1:1) in 1,2-dichloroethane and EtOH (1:4 v/v) stirred at 40°C for 24 h; evapd.(vac.), took with C2H4Cl2, filtered, crystd. for a few d, elem. anal.; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 35℃; for 4h; | 99% |
trimethylsilyl cyanide
2,2-diphenyl-4-pentyn-1-amine
1,2-dichloro-ethane
Conditions | Yield |
---|---|
With water; copper(I) bromide In acetonitrile at 90℃; for 0.666667h; Inert atmosphere; Microwave irradiation; | 99% |
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