As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so o
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Cas:87333-19-5
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Product Name: Ramipril Synonyms: PRAMACE;RAMIPRIL;RAMACE;UNIPRIL;TRITACE;(2s-(1(r*(r*)),2-alpha,3a-beta,6a-beta))-henylpropyl)amino)-1-oxopropyl;cyclopenta(b)pyrrole-2-carboxylicacid,octahydro-1-(2-((1-(ethoxycarbonyl)-3-p;[2S,3AS,6AS]-1-[(2S)-2-[
Cas:87333-19-5
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:87333-19-5
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inquiryRamipril CAS:87333-19-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates, s
Cas:87333-19-5
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:87333-19-5
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:87333-19-5
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryRamipril CAS: 87333-19-5 Specification Items Specifications Results Appearance White or almost white crystalline powder White crystalline powder Specific rotation +32°~+38° +34.5° Pa
1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
We can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need C
Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater
Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-
Cas:87333-19-5
Min.Order:5 Gram
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Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Hubei Yuanmeng Biological Technology Co., Ltd., which is located in Wuhan, China. We are specializing in the exportation of APIs, and plant extracts ect. Our products has been exported to America, Australia, Brazil, the Europe, Middle East and other
Cas:87333-19-5
Min.Order:1 Kilogram
FOB Price: $3.0 / 5.0
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
2--L-alanyl>-(1S,3S,5S)-2-azabicyclo<3.3.0>octane-3-carboxylic acid benzylester
Ramipril
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol at 0 - 10℃; under 1838.94 - 2206.73 Torr; | 95% |
With hydrogen; palladium 10% on activated carbon In methanol at 20℃; under 760.051 Torr; for 1.5h; Product distribution / selectivity; | 80% |
With hydrogen; 3% Pd/C In ethanol at 20 - 25℃; under 760.051 Torr; for 1 - 3h; Product distribution / selectivity; | 78% |
Ramipril
Conditions | Yield |
---|---|
at 40℃; under 2 Torr; for 10 - 12h; Product distribution / selectivity; | 94% |
N-[(S)-1-carbethoxy-3-phenyl-propyl]-S-alaninoyl chloride hydrochloride
(2S,3aS,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[b]pyrrole-2-carboxylic acid
Ramipril
Conditions | Yield |
---|---|
Stage #1: (2S,3aS,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[b]pyrrole-2-carboxylic acid With sodium ethanolate; triethylamine In ethanol at -40℃; Stage #2: N-[(S)-1-carbethoxy-3-phenyl-propyl]-S-alaninoyl chloride hydrochloride In ethanol; dichloromethane at -50 - 20℃; for 1.08333h; Stage #3: With hydrogenchloride In water pH=4.2; Acidic aqueous solution; | 88% |
N-[1-(S)-ethoxycarbonyl-3-phenylpropyl]-L-alanine N-carboxyanhydride
Ramipril
Conditions | Yield |
---|---|
With sodium hydroxide In water at 10 - 15℃; pH=8.5 - 9.5; | 74% |
benzyl (2S,3AS,6AS)-octahydrocyclopenta[b]pyrrole-2-carboxylate hydrochloride
N-[1-(S)-ethoxycarbonyl-3-phenylpropyl]-L-alanine N-carboxyanhydride
Ramipril
Conditions | Yield |
---|---|
With acetic acid; triethylamine In ethyl acetate at 5 - 20℃; for 4h; | 74% |
[1(S)-(ethoxycarbonyl)-3-phenylpropyl]-(S)-alanine
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: triphenylphosphine / CH2Cl2 / 0.75 h 1.2: 45 percent / CH2Cl2 / 2.5 h / 25 - 30 °C 2.1: triethylamine / CH2Cl2 / 4 h / -15 - -10 °C 3.1: hydrogen / Pd/C View Scheme |
N-[1(S)-ethoxycarbonyl-3-phenylpropyl]-(S)-alanine-2'-benzothiazolylthio ester
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / CH2Cl2 / 4 h / -15 - -10 °C 2: hydrogen / Pd/C View Scheme |
ethyl (E)-4-oxo-4-phenyl-2-butenoate
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 1.) 2N NaOH, 2.) N(C2H5)3 / 1.) methylene chloride, 2.) ethanol, 2 h 2: 90 percent / H2, 1.6percent H2SO4 / 10percent Pd/C / acetic acid / 7 h / 30002.4 Torr / Ambient temperature 3: 95 percent / K2CO3, 25percent ethylmethylphosphinic anhydride / H2O; CH2Cl2 4: H2 / 10percent Pd/C / methanol / 0.5 h / 750.06 - 3750.3 Torr / Ambient temperature View Scheme |
benzyl (2S,3AS,6AS)-octahydrocyclopenta[b]pyrrole-2-carboxylate hydrochloride
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 95 percent / K2CO3, 25percent ethylmethylphosphinic anhydride / H2O; CH2Cl2 2: H2 / 10percent Pd/C / methanol / 0.5 h / 750.06 - 3750.3 Torr / Ambient temperature View Scheme |
(1RS,3RS,5RS)-2-Azabicyclo<3.3.0>octan-3-carbonsaeurebenzylester-hydrochlorid
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 67.8 g / 1.) 10percent NaOH 2.) 6N HCl / CH2Cl2; ethyl acetate 2: 95 percent / K2CO3, 25percent ethylmethylphosphinic anhydride / H2O; CH2Cl2 3: H2 / 10percent Pd/C / methanol / 0.5 h / 750.06 - 3750.3 Torr / Ambient temperature View Scheme |
(1'S,2S)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 90 percent / H2, 1.6percent H2SO4 / 10percent Pd/C / acetic acid / 7 h / 30002.4 Torr / Ambient temperature 2: 95 percent / K2CO3, 25percent ethylmethylphosphinic anhydride / H2O; CH2Cl2 3: H2 / 10percent Pd/C / methanol / 0.5 h / 750.06 - 3750.3 Torr / Ambient temperature View Scheme |
N-[(1S)-1-ethoxycarbonyl-3-phenyl-3-oxopropyl]-L-alanine
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 95 percent / K2CO3, 25percent ethylmethylphosphinic anhydride / H2O; CH2Cl2 2: H2 / 10percent Pd/C / methanol / 0.5 h / 750.06 - 3750.3 Torr / Ambient temperature View Scheme |
(1RS,3RS,5RS)-2-Azabicyclo<3.3.0>octan-3-carbonsaeure-hydrochlorid
N-[1-(S)-ethoxycarbonyl-3-phenylpropyl]-L-alanine N-carboxyanhydride
A
ramipril
B
Ramipril
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; |
(S,S,S)-2-azabicyclo<3.3.0>octane-3-carboxylic acid hydrochloride
N-[1-(S)-ethoxycarbonyl-3-phenylpropyl]-L-alanine N-carboxyanhydride
Ramipril
Conditions | Yield |
---|---|
Stage #1: (2S)-2,3,3a,4,5,6-hexahydrocyclopenta[b]pyrrole-2-carboxylic acid; (S,S,S)-2-azabicyclo<3.3.0>octane-3-carboxylic acid hydrochloride With sodium hydroxide; hydrogenation catalyst In water at 20 - 25℃; pH=10 - 11; Stage #2: N-[1-(S)-ethoxycarbonyl-3-phenylpropyl]-L-alanine N-carboxyanhydride In water at 20 - 25℃; for 3 - 4h; pH=10 - 11; Stage #3: With hydrogenchloride In water at 15 - 20℃; for 2.5 - 2.75h; pH=4.4 - 5.2; Product distribution / selectivity; |
benzyl (1S,3S,5S)-2-azabicyclo<3.3.0>octane-3-carboxylate
[1(S)-(ethoxycarbonyl)-3-phenylpropyl]-(S)-alanine
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: hydrogenchloride; (chloromethylene)dimethyliminium chloride / N,N-dimethyl-formamide; dichloromethane / 0.42 h / -10 °C / Inert atmosphere 1.2: Inert atmosphere 2.1: hydrogen; palladium 10% on activated carbon / methanol / 20 °C / Inert atmosphere View Scheme |
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 5%-palladium/activated carbon; hydrogen / acetic acid / 40 - 60 °C / 3750.38 - 4500.45 Torr 2: thionyl chloride / 0 - 30 °C 3: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / toluene / 1 h / 0 - 5 °C 4: 5%-palladium/activated carbon; hydrogen / ethanol / 20 - 22 °C / 2327.23 - 2585.81 Torr View Scheme |
(S,S,S)-2-azabicyclo<3.3.0>octane-3-carboxylic acid hydrochloride
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: thionyl chloride / 0 - 30 °C 2: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / toluene / 1 h / 0 - 5 °C 3: 5%-palladium/activated carbon; hydrogen / ethanol / 20 - 22 °C / 2327.23 - 2585.81 Torr View Scheme |
[1(S)-(ethoxycarbonyl)-3-phenylpropyl]-(S)-alanine
benzyl (2S,3AS,6AS)-octahydrocyclopenta[b]pyrrole-2-carboxylate hydrochloride
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / toluene / 1 h / 0 - 5 °C 2: 5%-palladium/activated carbon; hydrogen / ethanol / 20 - 22 °C / 2327.23 - 2585.81 Torr View Scheme |
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: hydrogen / water / 55 - 60 °C / 4125.41 - 4500.45 Torr 2.1: water / 1 h / 15 - 55 °C 2.2: 0 - 5 °C 3.1: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / toluene / 1 h / 0 - 5 °C 4.1: 5%-palladium/activated carbon; hydrogen / ethanol / 20 - 22 °C / 2327.23 - 2585.81 Torr View Scheme |
(±)-methyl 2-(acetylamino)-3-(2-oxocyclopentyl)-propionate
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: immozyme alkaline serine endopeptidase; sodium carbonate / water / 20 h / 24 - 26 °C / pH 6.2 - 6.8 / Enzymatic reaction 2: hydrogenchloride / water / 3 h / Reflux 3: 5%-palladium/activated carbon; hydrogen / acetic acid / 40 - 60 °C / 3750.38 - 4500.45 Torr 4: thionyl chloride / 0 - 30 °C 5: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / toluene / 1 h / 0 - 5 °C 6: 5%-palladium/activated carbon; hydrogen / ethanol / 20 - 22 °C / 2327.23 - 2585.81 Torr View Scheme |
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: water / 1 h / 15 - 55 °C 1.2: 0 - 5 °C 2.1: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / toluene / 1 h / 0 - 5 °C 3.1: 5%-palladium/activated carbon; hydrogen / ethanol / 20 - 22 °C / 2327.23 - 2585.81 Torr View Scheme |
(2S,3aS,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[b]pyrrole-2-carboxylic acid
N-[1-(S)-ethoxycarbonyl-3-phenylpropyl]-L-alanine N-carboxyanhydride
Ramipril
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: water / Reflux 2.1: hydrogen / water / 55 - 60 °C / 4125.41 - 4500.45 Torr 3.1: water / 1 h / 15 - 55 °C 3.2: 0 - 5 °C 4.1: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / toluene / 1 h / 0 - 5 °C 5.1: 5%-palladium/activated carbon; hydrogen / ethanol / 20 - 22 °C / 2327.23 - 2585.81 Torr View Scheme |
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: hydrogenchloride / water / 3 h / Reflux 2: 5%-palladium/activated carbon; hydrogen / acetic acid / 40 - 60 °C / 3750.38 - 4500.45 Torr 3: thionyl chloride / 0 - 30 °C 4: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / toluene / 1 h / 0 - 5 °C 5: 5%-palladium/activated carbon; hydrogen / ethanol / 20 - 22 °C / 2327.23 - 2585.81 Torr View Scheme |
N-[1-(S)-ethoxycarbonyl-3-phenylpropyl]-L-alanine N-carboxyanhydride
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydrogencarbonate / water; ethyl acetate / 0.08 h / 15 °C 1.2: 1.08 h / 20 °C 2.1: hydrogen; palladium 10% on activated carbon / methanol / 15 - 20 °C / 760.05 Torr View Scheme |
[1(S)-(ethoxycarbonyl)-3-phenylpropyl]-(S)-alanine
Ramipril
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: hydrogenchloride; thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 0 h / -10 - -5 °C / Inert atmosphere 1.2: 0.01 h 2.1: hydrogen; palladium 10% on activated carbon / methanol / 15 - 20 °C / 760.05 Torr View Scheme |
Conditions | Yield |
---|---|
In water; isopropyl alcohol at 20℃; for 0.5h; | 98% |
In butanone for 0.5h; Product distribution / selectivity; Heating / reflux; |
Ramipril
Conditions | Yield |
---|---|
With water In di-isopropyl ether for 1 - 1.5h; Product distribution / selectivity; | 86% |
With water for 1 - 1.5h; Product distribution / selectivity; | 86% |
With water In formaldehyde diethyl acetal for 1 - 1.5h; Product distribution / selectivity; | 85% |
Conditions | Yield |
---|---|
In water; ethyl acetate at 20 - 40℃; | 79% |
In ethyl acetate at 10℃; for 1h; | 67% |
In ethyl acetate at 50 - 70℃; |
Ramipril
2-amino-2-hydroxymethyl-1,3-propanediol
ramipril tris(hydroxymethyl)aminomethane salt
Conditions | Yield |
---|---|
In ethanol; water at 20 - 40℃; | 75% |
1,1-Diphenylethylene
Ramipril
Conditions | Yield |
---|---|
With [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; cesium fluoride In N,N-dimethyl acetamide at 25 - 30℃; for 8h; Irradiation; Inert atmosphere; Schlenk technique; Molecular sieve; regioselective reaction; | 72% |
Ramipril
Conditions | Yield |
---|---|
With platinum(IV) oxide; hydrogen; acetic acid In ethanol at 30℃; under 1292.9 - 1551.49 Torr; for 24h; Temperature; | 66% |
Ramipril
ramipril-ammonia
Conditions | Yield |
---|---|
With ammonia In ethanol; ethyl acetate at 32.5 - 37.5℃; for 1h; | 57% |
Ramipril
Conditions | Yield |
---|---|
With [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; caesium carbonate In N,N-dimethyl acetamide; water for 24h; Sealed tube; Irradiation; Inert atmosphere; | 31% |
Ramipril
ramiprilate
Conditions | Yield |
---|---|
at 37℃; esterase from various rat tissue homogenates or plasma; | |
With porcine liver esterase In phosphate buffer at 37℃; pH=8.6; | |
Stage #1: Ramipril With sodium hydroxide In methanol; water at 60℃; for 0.0833333h; Stage #2: In methanol; water Acidic conditions; | |
With recombinant human carboxylesterase 1; water In aq. phosphate buffer at 37℃; for 0.133333h; Kinetics; Enzymatic reaction; |
Ramipril
Conditions | Yield |
---|---|
In isopropyl alcohol Heating; Yield given; | |
Stage #1: Ramipril With hydrogenchloride; water In methanol at 80℃; for 30h; Stage #2: In methanol Acidic conditions; |
Conditions | Yield |
---|---|
In butanone for 0.5h; Heating / reflux; |
Ramipril
(2S,3aS,6aS)-1[(S)-N-[(S)-1-carboxy-3-phenylpropyl]alanyl]octahydrocyclopenta[b]pyrrole-2-carboxylic acid 1-ethyl ester sodium salt
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water at 20℃; for 1h; |
Ramipril
Conditions | Yield |
---|---|
With calcium hydroxide In butanone for 1h; Heating / reflux; |
Ramipril
(R)-2-[(2-aminoethoxy)methyl]4-(2-chlorophenyl)-1,4-dihydro-6-methyl-3,5-pyridinedicarboxylic acid 3-ethyl 5-methyl ester
ramipril-amlodipine salt
Conditions | Yield |
---|---|
In ethyl acetate at 20℃; for 0.0333333h; |
Conditions | Yield |
---|---|
In ethyl acetate at 20℃; for 0.0333333h; |
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