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inquiryName: 4-tert-Butylbenzaldehyde Synonyms: p-Tertbutyl Benzaldehyde CAS:939-97-9 MF: C11H14O Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application:Organic synthesis Transportation:By sea
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inquiry4-tert-Butylbenzaldehyde Chemical Properties Melting point 245-246 °C Boiling point 130 °C25 mm Hg(lit.) density 0.97 g/mL at 25 °C(lit.) refractive index n20/D 1.53(lit.) Fp 214 °F storage temp. Keep in dark p
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inquiry1. ISO AVALIABLE ; 2. IN STOCK 3. FAST REPLY QUALIFED ; EFFICIENCY; RESPONSIBLE Appearance:white crystalline powder Storage:in cool Package:as request Application:active pharmaceutical ingredient Transportation:Air / SEA BOTH OK Port:any po
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Conditions | Yield |
---|---|
With 1H-imidazole; sodium periodate; manganese(III)-porphyrin complex immobilized on polystyrene In water; acetonitrile at 20℃; for 1.16667h; | 100% |
With oxygen In 1,3,5-trimethyl-benzene at 60℃; under 760.051 Torr; for 7h; Solvent; Reagent/catalyst; | 100% |
With titanium(IV) oxide; oxygen at 29.84℃; under 760.051 Torr; for 6h; Sealed tube; Irradiation; | 99% |
Conditions | Yield |
---|---|
With polymethylhydrosiloxane; trifuran-2-yl-phosphane; tetrabutyl ammonium fluoride; potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0) In tetrahydrofuran; water at 20℃; for 1h; | 99% |
With diethylene glycol dimethyl ether; lithium tri-t-butoxyaluminum hydride | |
With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal In ethyl acetate at 25℃; under 760 Torr; for 1.75h; Yield given; | |
Multi-step reaction with 2 steps 1: dichloromethane / 0.5 h / 20 °C / Cooling with ice 2: Schwartz's reagent / tetrahydrofuran / 0.5 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
With p-PPh2-C6H4-(OCH2CH2)n-O-C6H4-PPh2-p; ozone Product distribution; various catalysts; | 98% |
Stage #1: 4-tert-Butylstyrene With oxygen; ozone In dichloromethane at -78℃; Stage #2: With poly(ethylene glycol)-triphenylphosphine In dichloromethane at -78 - 20℃; | 98% |
With oxygen; benzoic acid; sodium nitrite In toluene at 80℃; for 20h; Reagent/catalyst; Solvent; Temperature; | 82% |
4-tert-butyl benzene carbaldehyde oxime
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With iron(III) chloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In water; toluene at 60℃; under 760.051 Torr; for 3h; | 98% |
(4-tert-butylbenzyloxy)trimethylsilane
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With trinitratocerium(IV) bromate for 0.7h; Heating; | 97% |
With copper(II) nitrate trihydrate; water; silica gel; potassium bromide at 90℃; for 0.5h; Neat (no solvent); | 87% |
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; hydrogen; palladium diacetate; propyl di-tert-butylphosphinite In toluene at 100℃; under 3750.38 Torr; for 20h; Inert atmosphere; | 97% |
4-tert-butylbenzyl chloride
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With 1-dodecyl-3-methylimidazolium iron chloride; periodic acid at 30℃; for 1.5h; | 96% |
With potassium hydroxide; cetyltrimethylammonim bromide; potassium nitrate In water for 4h; pH=10 - 11; Reflux; | 90% |
With potassium nitrite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; potassium bromide In water for 4h; Reflux; | 90% |
With sodium nitrate; acetic acid In water for 3.5h; Reflux; | 90% |
With hexamethylenetetramine; sulfuric acid; sodium carbonate In ethanol; water; toluene | 11.8 g (60%) |
Conditions | Yield |
---|---|
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In fluorobenzene; dimethyl sulfoxide at 80℃; for 8h; | 95% |
With ammonium cerium(IV) nitrate In water; acetic acid at 85 - 95℃; for 1.5h; | 94% |
With carbon tetrabromide; oxygen In acetonitrile at 20℃; for 3h; Irradiation; Green chemistry; | 90% |
1,1-bis(4-t-butylphenyl)methane
1-azidononane
A
4-tert-Butylbenzaldehyde
B
4-tert-butyl-N-nonylaniline
Conditions | Yield |
---|---|
With water; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride at 60℃; for 5h; | A 85% B 94% |
Conditions | Yield |
---|---|
Stage #1: N-(4-tert-butylbenzyl)-4-tert-butylaniline With oxygen; toluene-4-sulfonic acid; dimethyl sulfoxide In toluene at 100℃; for 119h; Green chemistry; Stage #2: With hydrogenchloride In water at 20℃; for 1h; Reagent/catalyst; Temperature; Green chemistry; | A 93% B 94% |
Conditions | Yield |
---|---|
Stage #1: formic acid; 1-tert-butyl-4-iodobenzene With palladium diacetate; acetic anhydride; tricyclohexylphosphine In N,N-dimethyl-formamide at 30℃; for 1h; Inert atmosphere; Green chemistry; Stage #2: With triethylamine In N,N-dimethyl-formamide at 80℃; for 6h; Inert atmosphere; Green chemistry; | 93% |
With palladium diacetate; triethylamine; dicyclohexyl-carbodiimide; tricyclohexylphosphine In N,N-dimethyl-formamide at 80℃; for 10h; Inert atmosphere; Sealed tube; | 72% |
4-tert-butyltoluene
A
4-tert-Butylbenzaldehyde
B
4-(1,1-dimethylethyl)benzoic acid
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; oxygen; cobalt(II) acetate In acetic acid at 25℃; under 760 Torr; for 20h; | A 2% B 91% |
With N-hydroxyphthalimide; oxygen; cobalt(II) acetate In acetonitrile at 25℃; under 760 Torr; for 20h; | A 4% B 77% |
With oxygen; acetic acid; N-hydroxyphthalimide at 100℃; for 6h; Product distribution / selectivity; | A 3.8% B 66.5% |
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; nickel(II) bis(2,2,6,6-tetramethylheptane-3,5-dionate); Ir(dF(CF3)ppy)2(bpy)PF6; zinc dibromide In N,N-dimethyl acetamide at 27℃; for 48h; Inert atmosphere; Irradiation; | 91% |
1-(bromomethyl)-4-(1,1-dimethylethyl)benzene
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With potassium hydrogencarbonate; dimethyl sulfoxide for 0.0583333h; Microwave irradiation; | 90% |
With carbon dioxide; copper(II) nitrate | |
With ethanol; carbon dioxide; hexamethylenetetramine | |
With 4-methylmorpholine N-oxide at 20℃; for 4h; Reflux; | 246.6 mg |
Multi-step reaction with 2 steps 1: eosin y; oxygen / dimethyl sulfoxide / 12 h / 25 °C / Irradiation 2: eosin y / dimethyl sulfoxide / 24 h / 80 °C / Irradiation View Scheme |
4-(1,1-dimethylethyl)-benzenemethanamine
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With cercosporin; oxygen In methanol at 20℃; Schlenk technique; Irradiation; Green chemistry; chemoselective reaction; | 89% |
With copper(I) 2-hydroxy-3-methylbenzoate; oxygen; ascorbic acid In N,N-dimethyl acetamide at 45℃; for 2h; chemoselective reaction; | 70% |
With dipotassium peroxodisulfate; tris(bipyridine)ruthenium(II) dichloride hexahydrate; water In acetonitrile at 20℃; for 12h; Sealed tube; Irradiation; Green chemistry; |
tert-butylisonitrile
1-tert-butyl-4-iodobenzene
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
Stage #1: tert-butylisonitrile; 1-tert-butyl-4-iodobenzene With triethylsilane; palladium diacetate; sodium carbonate; CyJohnPhos In N,N-dimethyl-formamide at 65℃; for 8h; Inert atmosphere; Sealed tube; Green chemistry; Stage #2: With water Green chemistry; | 88% |
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With eosin y In water; acetonitrile at 20℃; for 4h; Irradiation; | 88% |
4-t-butylphenylacetic acid
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With oxygen; copper diacetate In dimethyl sulfoxide at 120℃; for 18h; Sealed tube; | 87% |
With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20 - 25℃; for 6h; Irradiation; | 76% |
With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; N,N,N',N'-tetramethylguanidine In acetonitrile at 20℃; for 6h; Irradiation; | 55% |
With water; copper dichloride at 250℃; under 30003 Torr; for 0.17h; Sealed tube; Green chemistry; | 94 %Chromat. |
4-tert-butylbenzyl mercaptan
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; tetrakis(pyridine)silver(II) peroxodisulfate; oxygen In N,N-dimethyl-formamide at 23℃; under 760.051 Torr; Irradiation; | 87% |
Conditions | Yield |
---|---|
With nitric acid In dichloromethane at 20℃; for 1h; | 86% |
1-tert-butyl-4-iodobenzene
9-methyl-9H-fluorene-9-carbonyl chloride
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With dichloro(1,5-cyclooctadiene)palladium(II); N-Methyldicyclohexylamine; potassium formate; tetra-(n-butyl)ammonium iodide; tricyclohexylphosphine tetrafluoroborate; bis(dibenzylideneacetone)-palladium(0); tri tert-butylphosphoniumtetrafluoroborate In acetonitrile at 80℃; for 18h; Sealed tube; Glovebox; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With rhodium(III) iodide; dichloro [1,1'-bis(diphenylphosphino)propane]palladium(II); hydrogen; acetic anhydride; triethylamine; triphenylphosphine In N,N-dimethyl acetamide at 100℃; for 24h; Autoclave; | 85% |
With dichloro [1,1'-bis(diphenylphosphino)propane]palladium(II); 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 100℃; under 7500.75 Torr; for 20h; Autoclave; Green chemistry; | 81% |
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With triethylsilane; palladium diacetate; tricyclohexylphosphine In toluene at 100℃; for 20h; Inert atmosphere; Sealed tube; | 85% |
1-tert-butoxymethyl-4-tert-butylbenzene
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; nitrogen(II) oxide In acetonitrile at 60℃; for 10h; | 84% |
84% |
methanol
(E)-1,1'-(1,2-ethenediyl)bis(4-butyl)benzene
A
4-tert-Butylbenzaldehyde
B
methyl 4-tert-butylbenzoate
Conditions | Yield |
---|---|
With iodine; oxygen; trifluoroacetic acid In ethyl acetate for 20h; Solvent; Reagent/catalyst; Irradiation; | A 84% B 7 %Spectr. |
3-(4-(tert-butyl)phenyl)acrylaldehyde
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With pyrrolidine; water In acetonitrile at 20℃; for 12h; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
In 1,4-dioxane for 12h; Heating; | A 82% B 66% |
Conditions | Yield |
---|---|
With rhodium(III) chloride trihydrate; hydrogen; triethylamine; triphenylphosphine In N,N-dimethyl acetamide at 90℃; under 7500.75 Torr; for 12h; Autoclave; | 81% |
Conditions | Yield |
---|---|
With hydrogen bromide; oxygen In acetonitrile at 20℃; for 5h; UV-irradiation; | 100% |
With tert.-butylhydroperoxide; potassium tert-butylate In water at 60℃; for 5h; | 96% |
With N-Bromosuccinimide; oxygen In ethyl acetate at 20℃; Irradiation; | 93% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol at 25℃; for 0.5h; | 100% |
With sodium tetrahydroborate In ethanol at 20℃; for 0.5h; Inert atmosphere; | 100% |
With sodium tetrahydroborate In ethanol at 20℃; for 0.5h; Inert atmosphere; | 100% |
4-tert-Butylbenzaldehyde
diethylzinc
1-(4-tert-butylphenyl)propan-1-ol
Conditions | Yield |
---|---|
With (R,R)-(2,4,6-Me3C6H2-CH=N-CH(Ph))2; (R)-(+)-3,3'-diphenyl-[1,1'-binaphthalene]-2,2'-diol In hexane; dichloromethane 1.) -78 deg C, 4 h, 2.) -20 deg, 1 h; | 100% |
With (1R,2R)-N,N'-bis[(2,4,6-trimethylphenyl)methylene]-1,2-cyclohexane-diamine; (R)-(+)-3,3'-diphenyl-[1,1'-binaphthalene]-2,2'-diol In hexane; dichloromethane at -78 - -20℃; for 5h; | 100% |
With titanium(IV) isopropylate at 80℃; for 1h; Time; Inert atmosphere; | 60 %Chromat. |
With magnesium chloride at 80℃; for 0.5h; Reagent/catalyst; Inert atmosphere; | 24.2 %Chromat. |
Conditions | Yield |
---|---|
With sodium hydroxide for 1.5h; | 100% |
4-tert-Butylbenzaldehyde
1-amino-2-propene
Allyl-[1-(4-tert-butyl-phenyl)-meth-(E)-ylidene]-amine
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; for 20h; | 100% |
N-[3-fluoro-4-(4-morpholinyl)phenyl]-N-(4-piperidinylmethyl)-N'-(tetrahydro-2H-pyran-4-yl)urea
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With MP-triacetoxyborohydride In dichloromethane at 20℃; for 18h; MP-triacetoxyborohydride; | 100% |
4-tert-Butylbenzaldehyde
vinyl magnesium bromide
1-(4-(tert-butyl)phenyl)prop-2-en-1-ol
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; for 1h; Inert atmosphere; | 100% |
Stage #1: 4-tert-Butylbenzaldehyde; vinyl magnesium bromide In tetrahydrofuran at 20℃; for 20h; Heating / reflux; Stage #2: With water; ammonium chloride | |
In tetrahydrofuran at 0℃; for 1h; |
Conditions | Yield |
---|---|
Stage #1: 4-tert-Butylbenzaldehyde; 2-(3-methoxyphenyl)-1-ethanamine With potassium carbonate In methanol at 20℃; for 2h; Heating / reflux; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 3h; Heating / reflux; Stage #3: With hydrogenchloride In methanol; water | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-tert-Butylbenzaldehyde; 2-(3-Fluorophenyl)ethylamine In methanol at 20℃; for 2.5h; Heating / reflux; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 3.08h; Heating / reflux; Stage #3: With hydrogenchloride In methanol; water at 20℃; | 100% |
4-tert-Butylbenzaldehyde
2-(3-chlorophenyl)ethylamine
(4-tert-butyl-benzyl)-[2-(3-chloro-phenyl)-ethyl]-amine
Conditions | Yield |
---|---|
Stage #1: 4-tert-Butylbenzaldehyde; 2-(3-chlorophenyl)ethylamine In methanol at 20℃; for 3h; Heating / reflux; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 4.08h; Heating / reflux; Stage #3: With hydrogenchloride In methanol; water at 20℃; | 100% |
4-tert-Butylbenzaldehyde
4-fluoro-2-phenethylamine
(4-tert-butyl-benzyl)-[2-(4-fluoro-phenyl)-ethyl]-amine
Conditions | Yield |
---|---|
Stage #1: 4-tert-Butylbenzaldehyde; 4-fluoro-2-phenethylamine In methanol at 20℃; for 4.5h; Heating / reflux; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 2.08h; Heating / reflux; Stage #3: With hydrogenchloride In methanol; water at 20℃; | 100% |
4-tert-Butylbenzaldehyde
2-(p-tolyl)ethylamine
(4-tert-butyl-benzyl)-(2-p-tolyl-ethyl)-amine
Conditions | Yield |
---|---|
Stage #1: 4-tert-Butylbenzaldehyde; 2-(p-tolyl)ethylamine In methanol at 20℃; for 3h; Heating / reflux; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 2.38h; Heating / reflux; Stage #3: With hydrogenchloride In methanol; water at 20℃; | 100% |
2-(2-fluoro-5-trifluoromethyl-phenyl)-ethylamine hydrochloride
4-tert-Butylbenzaldehyde
(4-tert-butyl-benzyl)-[2-(2-fluoro-5-trifluoromethyl-phenyl)-ethyl]-amine
Conditions | Yield |
---|---|
Stage #1: 2-(2-fluoro-5-trifluoromethyl-phenyl)-ethylamine hydrochloride; 4-tert-Butylbenzaldehyde With potassium carbonate In methanol at 20℃; for 3h; Heating / reflux; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 2.58h; Heating / reflux; | 100% |
4-tert-Butylbenzaldehyde
cis, trans-1,3-dimethylaminocyclohexane
C30H42N2
Conditions | Yield |
---|---|
In methanol at 20℃; Molecular sieve; | 100% |
In methanol at 20℃; Molecular sieve; |
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
2-(4-Chloro-3-Ethyl-Phenyl)-Ethyl-Amine-Hydrochloride
4-tert-Butylbenzaldehyde
[1-(4-tert-butyl-phenyl)-meth-(E)-ylidene]-[2-(4-chloro-3-ethyl-phenyl)-ethyl]-amine
Conditions | Yield |
---|---|
Stage #1: 2-(4-Chloro-3-Ethyl-Phenyl)-Ethyl-Amine-Hydrochloride With sodium hydroxide In water; ethyl acetate Stage #2: 4-tert-Butylbenzaldehyde In ethyl acetate at 20℃; for 2h; | 100% |
With sodium hydroxide In water; ethyl acetate at 20℃; for 2h; | 100% |
Conditions | Yield |
---|---|
In ethanol at 20℃; | 100% |
4-tert-Butylbenzaldehyde
allylmagnesium bromide
1-(4-(tert-butyl)phenyl)but-3-en-1-ol
Conditions | Yield |
---|---|
In tetrahydrofuran; diethyl ether at 0 - 20℃; | 100% |
With indium In tetrahydrofuran; diethyl ether at 0℃; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: malonic acid; 4-tert-Butylbenzaldehyde With piperidine; pyridine Knoevenagel-Doebner reaction; Reflux; Stage #2: With hydrogenchloride In water Cooling with ice; optical yield given as %de; | 99% |
With piperidine; pyridine for 2h; Knoevenagel condensation; Reflux; | 88% |
With piperidine; pyridine | 87% |
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In ethanol; water for 5.5h; Heating; | 99% |
With potassium carbonate |
Conditions | Yield |
---|---|
Stage #1: ethyl 2-diethoxyphosphorylpropionate With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.5h; Inert atmosphere; Stage #2: 4-tert-Butylbenzaldehyde In tetrahydrofuran; hexane at 0 - 20℃; Inert atmosphere; | 99% |
Stage #1: ethyl 2-diethoxyphosphorylpropionate With sodium hydride In tetrahydrofuran at 0 - 25℃; Stage #2: 4-tert-Butylbenzaldehyde In tetrahydrofuran for 1h; Heating; | |
With sodium hydride In tetrahydrofuran; mineral oil at -78 - 20℃; for 3h; |
Conditions | Yield |
---|---|
With ammonium sulfate; sodium carbonate; sulfur In dimethyl sulfoxide at 120℃; for 10h; Sealed tube; | 99% |
With pyridine; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; ammonium peroxydisulfate; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; ammonium carbamate In water; acetonitrile at 20℃; for 24h; Irradiation; Sealed tube; | 98% |
Stage #1: 4-tert-Butylbenzaldehyde With pyridine; 1,1,1,3,3,3-hexamethyl-disilazane In dichloromethane at 26℃; for 0.0833333h; Stage #2: With 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate In dichloromethane at 26℃; for 18h; | 97% |
3-(diethoxyphosphorylmethyl)-4-methoxybenzamide
4-tert-Butylbenzaldehyde
Conditions | Yield |
---|---|
With sodium tert-pentoxide In N,N-dimethyl-formamide at 20℃; for 1h; Horner-Wadsworth-Emmons olefination; | 99% |
4-tert-Butylbenzaldehyde
girard's reagent T
diisopropyl (2-oxo-2-(pyrrolidin-1-yl)ethyl)phosphonate
B
C17H23NO
Conditions | Yield |
---|---|
Stage #1: 4-tert-Butylbenzaldehyde; diisopropyl (2-oxo-2-(pyrrolidin-1-yl)ethyl)phosphonate With potassium tert-butylate In tetrahydrofuran at 20℃; for 6h; Horner-Wadsworth-Emmons Olefination; Stage #2: girard's reagent T In tetrahydrofuran; methanol stereoselective reaction; | A n/a B 99% C n/a |
Conditions | Yield |
---|---|
With palladium on activated charcoal; hydrogen In methanol at 25℃; under 760.051 Torr; for 0.833333h; | 99% |
Conditions | Yield |
---|---|
With silica gel; toluene-4-sulfonic acid In dichloromethane Reflux; | 99% |
With boron trifluoride diethyl etherate In dichloromethane Inert atmosphere; | |
With boron trifluoride diethyl etherate In dichloromethane at 0 - 25℃; |
Conditions | Yield |
---|---|
In neat (no solvent) at 60℃; for 0.0666667h; Microwave irradiation; | 99% |
Conditions | Yield |
---|---|
Stage #1: pentanonitrile; 4-tert-Butylbenzaldehyde With hydrogen In 2-methyltetrahydrofuran at 100℃; under 11251.1 Torr; for 20h; High pressure; Autoclave; Stage #2: With hydrogenchloride In diethyl ether | 99% |
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