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inquiryUnique advantages for 4-Isopropylaniline Cas 99-88-7 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Colorless liquid Storage:Store below +30°C Package:1kg/foil bag;25kg/drum
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Appearance:colorless liquid Storage:room temperature Package:200kg/Drum Application:4-Isopropylaniline was used in the hydroamination of phenylacetylene. Transportation:Express/Sea/Air Port:Any port in China
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Product Name: 4-Isopropylaniline CAS: 99-88-7 MF: C9H13N MW: 135.21 EINECS: 202-797-2 Product Categories: 4-Isopropylaniline Structure 4-Isopropylaniline Chemical Properties Melting point -63 °C Boiling point 226-227 &
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Conditions | Yield |
---|---|
With triethylamine In water at 80℃; for 2h; Inert atmosphere; Green chemistry; chemoselective reaction; | 99% |
With borane-ammonia complex In methanol; water at 49.84℃; for 0.1h; Catalytic behavior; | 99% |
With nickel; ammonium chloride In water at 80 - 90℃; for 1.5h; | 96% |
(4-isopropylphenyl)boronic acid
4-Isopropylaniline
Conditions | Yield |
---|---|
With copper(I) oxide; ammonium hydroxide; air In methanol at 20℃; for 12h; | 88% |
1,2-Bis(4-isopropylphenyl)diazene
4-Isopropylaniline
Conditions | Yield |
---|---|
With perchloric acid In isopropyl alcohol; acetonitrile at 25℃; for 0.8h; pH=2; Inert atmosphere; Irradiation; | 88% |
Conditions | Yield |
---|---|
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In tetrahydrofuran -78 deg C, 10 min, reflux, 24 h; | 87% |
Conditions | Yield |
---|---|
With aluminum oxide; aluminium trichloride for 0.0583333h; microwave irradiation; | 87% |
Conditions | Yield |
---|---|
With ammonium hydroxide; L-2-O-methyl-chiro-inositol; copper(II) acetate monohydrate In 1-methyl-pyrrolidin-2-one at 110℃; for 20h; | 87% |
Conditions | Yield |
---|---|
With ammonium sulfate; bis(1,5-cyclooctadiene)nickel (0); sodium t-butanolate at 100 - 110℃; for 12h; | 81% |
4-isopropylphenylhydrazine
4-Isopropylaniline
Conditions | Yield |
---|---|
With 4,4'-di-tert-butylbiphenyl; lithium; nickel dichloride In tetrahydrofuran at 20℃; Reduction; | 72% |
Isopropylbenzene
A
4-Isopropylaniline
B
meta-iso-propyl aniline
C
2-isopropylaniline
Conditions | Yield |
---|---|
With tris-(2-chloro-ethyl)-amine; trifluorormethanesulfonic acid; trifluoroacetic acid In chloroform at 25℃; for 5h; | A 37% B 9% C 48% |
aniline
isopropyl alcohol
A
propene
B
4-Isopropylaniline
C
N-Isopropylaniline
D
2-isopropylaniline
Conditions | Yield |
---|---|
With Ce-Y zeolite at 300℃; Product distribution; var. zeolites, temp., and flow rate; | A n/a B 1.9% C 4% D 10.7% |
Conditions | Yield |
---|---|
With nitric acid man faellt mit Wasser das rohe Nitrocumol als Oel aus und reduziert es mit Schwefelammon in alkoh. Loesung; | |
With sulfuric acid; nitric acid man faellt mit Wasser das rohe Nitrocumol als Oel aus und reduziert es mit Zink und Salzsaeure; | |
Stage #1: Isopropylbenzene With nitric acid at 10℃; for 0.166667h; Flow reactor; Stage #2: In toluene at 100℃; under 30003 Torr; Flow reactor; Overall yield = 76.79 %Chromat.; | A 59.4 %Chromat. B 16.7 %Chromat. |
Conditions | Yield |
---|---|
With cobalt(II) chloride at 250℃; | |
With zinc dibromide at 250℃; | |
With cadmium(II) chloride at 250℃; |
4,4'-(1-methyl-ethane-1,1-diyl)-bis-aniline
A
4-Isopropylaniline
B
aniline
Conditions | Yield |
---|---|
With nickel at 200℃; under 36775.4 Torr; Hydrogenation; | |
With nickel; cyclohexanol at 200℃; |
Conditions | Yield |
---|---|
With zinc(II) chloride at 260℃; |
propane
aniline
A
4-Isopropylaniline
B
meta-iso-propyl aniline
C
2-isopropylaniline
Conditions | Yield |
---|---|
With oxygen In gaseous matrix at 80℃; Irradiation; | A 35 % Spectr. B 2 % Spectr. C 63 % Spectr. |
With oxygen In gaseous matrix at 80℃; Irradiation; | A 35 % Spectr. B n/a C n/a |
propane
aniline
A
4-Isopropylaniline
B
meta-iso-propyl aniline
C
N-Isopropylaniline
D
2-isopropylaniline
Conditions | Yield |
---|---|
at 40℃; Mechanism; Product distribution; Irradiation; intramolecular selectivity in the gas-phase alkylation and acetylation of aniline by charged electrophiles; |
4,4'-(1-methyl-ethane-1,1-diyl)-bis-aniline
A
4-Isopropylaniline
B
aniline
Conditions | Yield |
---|---|
at 200℃; under 36775.4 Torr; Hydrogenation; |
4,4'-(1-methyl-ethane-1,1-diyl)-bis-aniline
cyclohexanol
A
4-Isopropylaniline
B
aniline
Conditions | Yield |
---|---|
at 225℃; |
4-Isopropylaniline
Conditions | Yield |
---|---|
With nickel; isopropyl alcohol at 100℃; under 58840.6 Torr; Hydrogenation; | |
With hydrogenchloride; tin | |
With hydrogenchloride; iron |
Conditions | Yield |
---|---|
at 250℃; |
Conditions | Yield |
---|---|
at 250℃; |
Conditions | Yield |
---|---|
at 250℃; |
hydrogenchloride
N-(4-iso-propylphenyl)benzamide
A
4-Isopropylaniline
B
benzoic acid
Conditions | Yield |
---|---|
at 150℃; |
N-Isopropylaniline
A
propene
B
4-Isopropylaniline
C
aniline
D
2-isopropylaniline
Conditions | Yield |
---|---|
Ce-Y zeolite In hexane at 30℃; Product distribution; Further Variations:; Catalysts; Temperatures; other alkyl aniline; Isomerization; dealkylation; |
N-(4-isopropylphenyl)-N',N'-dimethylurea
A
4-Isopropylaniline
B
dimethyl amine
Conditions | Yield |
---|---|
With sulfuric acid In methanol; water at 80 - 90℃; Kinetics; Further Variations:; Temperatures; |
N-(4-isopropylphenyl)-N',N'-dimethylurea
A
N,N-dimethylcarbamic acid
B
4-Isopropylaniline
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water at 90℃; Kinetics; Further Variations:; Temperatures; pH-values; |
N-(4-isopropylphenyl)-N',N'-dimethylurea
4-Isopropylaniline
Conditions | Yield |
---|---|
With Arthrobacter sp. N2 In various solvent(s) pH=6.6; Kinetics; |
aniline
isopropyl alcohol
A
4-Isopropylaniline
B
N-Isopropylaniline
C
2-isopropylaniline
Conditions | Yield |
---|---|
Li-Y zeolite at 350℃; Product distribution; Further Variations:; Catalysts; Temperatures; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. HNO3, H2SO4 / nitromethane 2: H2 / PtO2 / ethanol View Scheme |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; Inert atmosphere; | 100% |
With ZnAl2O4 nanoparticles at 20℃; for 0.05h; Neat (no solvent); | 96% |
In neat (no solvent) at 20℃; for 0.05h; | 96% |
dimethoxyacetaldehyde
4-Isopropylaniline
N-[(2,2-dimethoxyethyl)amino]-4-(2-propyl)aniline
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol under 760 Torr; for 18h; | 100% |
4-Isopropylaniline
diethyl 2-ethoxymethylenemalonate
diethyl 4-i-propylanilinomethylenemalonate
Conditions | Yield |
---|---|
at 130℃; for 2h; | 100% |
at 120℃; for 4h; Inert atmosphere; |
2-(1H-pyrrol-1-yl)benzaldehyde
4-Isopropylaniline
Conditions | Yield |
---|---|
at 20℃; | 100% |
4-Isopropylaniline
[(2-{6-[(methyloxy)carbonyl]-3-phenyl-1H-indol-1-yl}ethyl)oxy]acetic acid
methyl 1-{2-[(2-{[4-(1-methylethyl)phenyl]amino}-2-oxoethyl)oxy]ethyl}-3-phenyl-1H-indole-6-carboxylate
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 16h; | 100% |
4-Isopropylaniline
3-oxobenzo[d]isothiazole-2(3H)-carbaldehyde 1,1-dioxide
N-[4-(propan-2-yl)phenyl]formamide
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.25h; chemoselective reaction; | 100% |
2-chloro-6-methoxyquinazoline
4-Isopropylaniline
N-(4-isopropylphenyl)-6-methoxyquinazolin-2-amine
Conditions | Yield |
---|---|
In ethanol at 80℃; for 16h; | 100% |
4-Isopropylaniline
2-chloro-5-methoxyquinoline
Conditions | Yield |
---|---|
In neat (no solvent) at 160℃; | 100% |
In neat (no solvent) at 160℃; |
4-Isopropylaniline
bis(pinacol)diborane
(4-isopropylphenyl)boronic acid
Conditions | Yield |
---|---|
With tert.-butylnitrite In acetonitrile at 0 - 80℃; for 2h; | 99.8% |
With tert.-butylnitrite In acetonitrile at 0 - 80℃; for 2h; | 99.8% |
Conditions | Yield |
---|---|
for 16h; Reflux; | 99% |
With choline chloride*2SnCl2 at 70℃; for 0.333333h; | 97% |
With choline chloride*2SnCl2 at 70℃; | 97% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 99% |
With TEA In dichloromethane at 0 - 25℃; for 3h; Acylation; | |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; Trimethylacetic acid In dichloromethane at 20℃; for 18h; |
Conditions | Yield |
---|---|
[(Me3Si)2N]3Yb(μ-Cl)Li(THF)3 In dichloromethane at 40℃; for 4h; | 99% |
With C23H40AlN In toluene at 25℃; for 1h; Inert atmosphere; Schlenk technique; | 92% |
With [Cp*2(Me)Zr(μ-O)Zr(NMe2)2(μ-O)Zr(Me)Cp*2] In benzene-d6 at 110℃; for 12h; Temperature; Reagent/catalyst; Time; Inert atmosphere; |
cis,trans-2,5-dimethoxytetrahydrofuran
4-Isopropylaniline
1-(4-(iso-propyl)phenyl)-1H-pyrrole
Conditions | Yield |
---|---|
In acetic acid; ethyl acetate | 99% |
In acetic acid; ethyl acetate | 99% |
In acetic acid for 1.5h; Heating / reflux; | 99% |
4-Trifluoromethylbenzaldehyde
4-Isopropylaniline
(4-isopropylphenyl){(E)-[4-(trifluoromethyl)phenyl]methylene}amine
Conditions | Yield |
---|---|
Stage #1: 4-Trifluoromethylbenzaldehyde; 4-Isopropylaniline In water at 20℃; for 2h; Stage #2: In dichloromethane; water for 0.333333h; | 99% |
4-Isopropylaniline
2-Iodobenzoyl chloride
2-iodo-N-(4-isopropylphenyl)benzamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 3h; | 99% |
With triethylamine In dichloromethane | |
With pyridine In dichloromethane at 0 - 20℃; |
diazoacetic acid ethyl ester
4-Isopropylaniline
ethyl 2-((4-isopropylphenyl)amino)acetate
Conditions | Yield |
---|---|
With sodium dithionite; myoglobin mutant H64V,V68A In aq. phosphate buffer pH=8.0; Reagent/catalyst; chemoselective reaction; | 99% |
With sodium dithionite; Bacillus megaterium cytochrome P450 variant H2-5-F10 In aq. phosphate buffer at 20℃; for 12h; pH=8; Enzymatic reaction; | 59% |
Conditions | Yield |
---|---|
In methanol Reflux; | 99% |
Conditions | Yield |
---|---|
With C55H43ClN5P2Ru(1+)*Cl(1-); potassium hydroxide In toluene at 140℃; for 2h; Sealed tube; | 99% |
With C17H18IrN3O; caesium carbonate at 120℃; for 20h; Inert atmosphere; | 93% |
With tetrakis[3,5-bis(trifluoromethyl)phenyl]boric acid bis(diethyl ether) complex; C32H63CoNP2Si(2+) In toluene for 48h; Molecular sieve; Reflux; Inert atmosphere; chemoselective reaction; | 90% |
With 9-N-methylamino-1-oxophenalene; potassium tert-butylate In toluene at 130℃; for 18h; Inert atmosphere; | 81% |
With [(NH-C3H5)Tr(NHP(iPr)2)2CoCl2]; potassium tert-butylate In toluene at 80℃; for 24h; | 76% |
Conditions | Yield |
---|---|
With hydrogenchloride In water at 20℃; for 2h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: 3-bromo-3-methyl-2-indolinone With nickel(II) tetrafluoroborate hexahydrate; C42H66N4O8 In ethyl acetate at 35℃; for 0.583333h; Stage #2: With N-ethyl-N,N-diisopropylamine In ethyl acetate at 0℃; for 0.166667h; Stage #3: 4-Isopropylaniline In ethyl acetate at 0℃; for 24h; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
at 140℃; for 2h; | 98.35% |
bis(trichloromethyl) carbonate
4-Isopropylaniline
4-isopropylphenylisocyanate
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane at 70 - 83℃; | 98.2% |
With triethylamine In benzene Substitution; dehydrochlorination; Heating; | 66.2% |
With triethylamine In dichloromethane at 0 - 20℃; for 0.0833333h; |
Conditions | Yield |
---|---|
With pyridine for 24h; Ambient temperature; | 98% |
di-tert-butyl dicarbonate
4-Isopropylaniline
4-isopropyl-N-tert-butoxycarbonylaniline
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 25℃; for 17h; Inert atmosphere; | 98% |
With choline chloride; urea at 50℃; Green chemistry; | 95% |
With 3a,6a-diphenylglycoluril In ethanol at 25 - 30℃; for 0.333333h; Catalytic behavior; Reagent/catalyst; | 95% |
With triethylamine In tetrahydrofuran at 25℃; for 17h; Inert atmosphere; | 67% |
With dmap In dichloromethane at 20℃; for 0.5h; |
4-Isopropylaniline
Conditions | Yield |
---|---|
Stage #1: 4-Isopropylaniline With hydrogenchloride; sodium nitrite In water; ethyl acetate at 0℃; for 1h; Stage #2: With sodium azide In water; ethyl acetate at 20℃; for 4h; | 98% |
With tert.-butylnitrite; trimethylsilylazide In acetonitrile at 20℃; for 1h; | 96% |
Stage #1: 4-Isopropylaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 2h; Stage #2: With sodium azide In water at 0 - 20℃; | 94% |
Conditions | Yield |
---|---|
[(Me3Si)2N]3Yb(μ-Cl)Li(THF)3 In tetrahydrofuran at 60℃; for 4h; | 98% |
With C23H40AlN In toluene at 25℃; for 1h; Inert atmosphere; Schlenk technique; | 89% |
4-Isopropylaniline
p-chlorobenzoylphenylacetylene
(Z)-3-(4-isopropylphenylamino)-1-(4-chlorophenyl)-3-phenylprop-2-en-1-one
Conditions | Yield |
---|---|
at 80℃; for 1h; Michael addition; | 98% |
4-Isopropylaniline
N,N-Dimethylcarbamoyl chloride
N-(4-isopropylphenyl)-N',N'-dimethylurea
Conditions | Yield |
---|---|
With sodium carbonate; sodium iodide In hexane at 50℃; for 16h; pH=7; | 98% |
With triethylamine In dichloromethane at 0 - 20℃; for 24h; |
4-Isopropylaniline
o-phthalic dicarboxaldehyde
1-p-isopropylphenylimino-2-p-isopropylphenylisoindoline
Conditions | Yield |
---|---|
With formic acid In diethyl ether at 20℃; for 12h; Inert atmosphere; | 98% |
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