Product Name

  • Name

    1,9-Nonanediol

  • EINECS 223-517-5
  • CAS No. 3937-56-2
  • Article Data58
  • CAS DataBase
  • Density 0.931 g/cm3
  • Solubility 5.7g/L at 20℃
  • Melting Point 45-47 °C
  • Formula C9H20O2
  • Boiling Point 292.4 °C at 760 mmHg
  • Molecular Weight 160.257
  • Flash Point 137 °C
  • Transport Information
  • Appearance white fused crystalline solid
  • Safety 22-24/25
  • Risk Codes
  • Molecular Structure Molecular Structure of 3937-56-2 (1,9-Nonanediol)
  • Hazard Symbols
  • Synonyms a,w-Nonanediol;NSC 5416;1,9-Dihydroxynonane;
  • PSA 40.46000
  • LogP 1.70170

Synthetic route

9-hydroxynonyl-1-triphenylmethylether
82777-72-8

9-hydroxynonyl-1-triphenylmethylether

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
Stage #1: 9-hydroxynonyl-1-triphenylmethylether With n-butyllithium In hexane at 0℃;
Stage #2: With naphthalene; lithium In tetrahydrofuran; hexane at 0 - 20℃; for 20h;
99%
1,9-di(trityloxy)nonane
634902-05-9

1,9-di(trityloxy)nonane

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With naphthalene; lithium In tetrahydrofuran at -30℃; for 3.5h;99%
9-(triphenylsilyloxy)-1-nonanol
109027-55-6

9-(triphenylsilyloxy)-1-nonanol

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With naphthalene; lithium In tetrahydrofuran; methanol at 20℃; for 1h;98%
9-<(2H-tetrahydropyran-2-yl)oxy>nonan-1-ol
98847-00-8

9-<(2H-tetrahydropyran-2-yl)oxy>nonan-1-ol

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With copper dichloride In methanol at 20℃; Hydrolysis;95%
With CuCl2*2H2O In methanol at 20℃; for 1.25h;95%
1,3-Dioxa-cyclododecane-4,12-dione

1,3-Dioxa-cyclododecane-4,12-dione

A

azelaic acid
123-99-9

azelaic acid

B

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

C

9-hydroxynonanoic acid
3788-56-5

9-hydroxynonanoic acid

Conditions
ConditionsYield
With sodium tetrahydroborate In tetrahydrofuran at 23℃; for 120h;A n/a
B 2%
C 92%
With sodium tetrahydroborate In tetrahydrofuran at 65℃; for 6h;A n/a
B 6%
C 87%
azelaic acid
123-99-9

azelaic acid

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 4h; Reflux;91%
With zirconium(IV) borohydride In tetrahydrofuran at 25℃; for 1h; Reduction;90%
With samarium diiodide; water; triethylamine In tetrahydrofuran at 20℃; for 18h; Inert atmosphere;88%
1-[dimethyl(phenyl)silyloxy]-9-(triphenylsilyloxy)nonane
862249-29-4

1-[dimethyl(phenyl)silyloxy]-9-(triphenylsilyloxy)nonane

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With naphthalene; lithium In tetrahydrofuran; methanol at 20℃; for 3h;79%
octadec-9-enoic acid methyl ester
112-62-9

octadec-9-enoic acid methyl ester

A

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

B

nonyl alcohol
143-08-8

nonyl alcohol

Conditions
ConditionsYield
With lithium aluminium tetrahydride multistep reaction, other substrates;A 74%
B 64%
With lithium aluminium tetrahydride 1) CH2Cl2; Yield given. Multistep reaction. Yields of byproduct given;
With lithium aluminium tetrahydride Yield given. Multistep reaction. Yields of byproduct given;
With lithium aluminium tetrahydride Yield given. Multistep reaction. Yields of byproduct given;
nona-1,8-diene
4900-30-5

nona-1,8-diene

A

nonane-1,5-diol
13686-96-9

nonane-1,5-diol

B

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With 9-borabicyclo[3.3.1]nonane dimer; dimethylsulfide borane complex Product distribution;A 71%
B 15%
9-benzylsulfonyloxynonyl benzylsulfonate
61801-07-8

9-benzylsulfonyloxynonyl benzylsulfonate

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With 4,4'-di-tert-butylbiphenyl; lithium In tetrahydrofuran at 0℃; for 2.5h;67%

A

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

B

1,7-nonanediol
4469-84-5

1,7-nonanediol

C

1,8-dihydroxynonane
61448-29-1

1,8-dihydroxynonane

D

nonyl alcohol
143-08-8

nonyl alcohol

Conditions
ConditionsYield
With acetylacetonatodicarbonylrhodium(l); 1-hydroxytetraphenylcyclopentadienyl(tetraphenyl-2,4-cyclopentadien-1-one)-μ-hydrotetracarbonyldiruthenium(II); carbon monoxide; C70H72O2P2; hydrogen In 1,4-dioxane at 120℃; under 3750.38 Torr; for 36h; Inert atmosphere; Autoclave;A 62%
B n/a
C n/a
D 24 %Chromat.
Dimethyl azelate
1732-10-1

Dimethyl azelate

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With ethanol; sodium
With ethanol; sodium
With i-Amyl alcohol; sodium
With hydrogenchloride; cerium monofluoride; Triethoxysilane 1. 12 h, 25 deg C; 2. acetone, 30 min; Yield given. Multistep reaction;
Dimethyl azelate
1732-10-1

Dimethyl azelate

A

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

B

9-hydroxynonanoic acid
3788-56-5

9-hydroxynonanoic acid

Conditions
ConditionsYield
With ethanol; sodium
diethyl azelate
624-17-9

diethyl azelate

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With ethanol; sodium
With copper chromite at 270℃; under 154457 Torr; Hydrogenation;
With i-Amyl alcohol; sodium
oleoyl alcohol
143-28-2

oleoyl alcohol

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
(i) O3, AcOEt, (ii) LiAlH4, Py; Multistep reaction;
undecanedioic acid diethyl ester
22543-29-9

undecanedioic acid diethyl ester

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With sodium In ethanol
(Sp)-2,12-dioxa-1(1,4)-benzena-cyclododecaphane-12-carboxylic acid

(Sp)-2,12-dioxa-1(1,4)-benzena-cyclododecaphane-12-carboxylic acid

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
(i) H2, Al2O3, Rh, AcOH, (ii) KOH, EtOH; Multistep reaction;
oxecan-2-one
6008-27-1

oxecan-2-one

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With lithium triethylborohydride In various solvent(s) for 0.416667h; Thermodynamic data; ΔH;
1-acetoxy-9-octadecene
136934-14-0

1-acetoxy-9-octadecene

A

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

B

nonyl alcohol
143-08-8

nonyl alcohol

Conditions
ConditionsYield
With lithium aluminium tetrahydride 1) CH2Cl2; Yield given. Multistep reaction. Yields of byproduct given;
(E)-Octadec-15-ene-1,9,10,13-tetraol

(E)-Octadec-15-ene-1,9,10,13-tetraol

A

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

B

(E)-Non-6-ene-1,4-diol

(E)-Non-6-ene-1,4-diol

Conditions
ConditionsYield
With sodium tetrahydroborate; periodic acid 1.) ether, 1 h, 2.) overnight; Multistep reaction;
azelaic acid amide

azelaic acid amide

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With pentan-1-ol; sodium
diethyl azelate
624-17-9

diethyl azelate

barium oxide

barium oxide

copper oxide-chromium oxide

copper oxide-chromium oxide

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
at 300℃; under 198587 Torr; Hydrogenation;
pentan-1-ol
71-41-0

pentan-1-ol

1,7-heptanedicarboxamide
1842-72-4

1,7-heptanedicarboxamide

sodium

sodium

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Dimethyl azelate
1732-10-1

Dimethyl azelate

ethanol
64-17-5

ethanol

sodium

sodium

A

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

B

9-hydroxynonanoic acid
3788-56-5

9-hydroxynonanoic acid

diethyl azelate
624-17-9

diethyl azelate

barium oxide

barium oxide

copper oxide-chromium oxide

copper oxide-chromium oxide

A

nonane
111-84-2

nonane

B

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

C

nonyl alcohol
143-08-8

nonyl alcohol

Conditions
ConditionsYield
at 400℃; under 198587 Torr; Hydrogenation;
nona-1,8-diene
4900-30-5

nona-1,8-diene

A

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

B

non-8-en-1-ol
13038-21-6

non-8-en-1-ol

C

non-7-en-1-ol
63768-13-8

non-7-en-1-ol

D

nonyl alcohol
143-08-8

nonyl alcohol

Conditions
ConditionsYield
Stage #1: nona-1,8-diene With triisobutylaluminum; bis-triphenylphosphine-palladium(II) chloride In dichloromethane at 25℃; for 12h;
Stage #2: With sodium hydroxide; oxygen In dichloromethane
A 14 % Spectr.
B 12 % Spectr.
C 24 % Spectr.
D 25 % Spectr.
benzyl 9-(allyloxycarbonyl)-1-nonyl carbonate

benzyl 9-(allyloxycarbonyl)-1-nonyl carbonate

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With naphthalen-1-yl-lithium In tetrahydrofuran at 0℃; for 2h;
9-(2,2-dimethylpropanoyloxy)nonyl pivalate

9-(2,2-dimethylpropanoyloxy)nonyl pivalate

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
With naphthalene; lithium In tetrahydrofuran at 0℃; for 1h;99 % Chromat.
9-Trimethylsilanyloxy-9-[3-((E)-2-trimethylsilanyloxy-hept-4-enyl)-oxiranyl]-nonanoic acid methyl ester

9-Trimethylsilanyloxy-9-[3-((E)-2-trimethylsilanyloxy-hept-4-enyl)-oxiranyl]-nonanoic acid methyl ester

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: LiAlH4 / tetrahydrofuran / Heating
2: 1.) H5IO6, 2.) NaBH4 / 1.) ether, 1 h, 2.) overnight
View Scheme
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

1,9-Dibromononane
4549-33-1

1,9-Dibromononane

Conditions
ConditionsYield
With carbon tetrabromide; Cu(tmp)(BINAP)BF4; sodium bromide In N,N-dimethyl-formamide for 24h; Appel Halogenation; UV-irradiation; Inert atmosphere;99%
With water; hydrogen bromide
With hydrogen bromide
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

1,9-nonanedioldiisopropyl ether
200499-47-4

1,9-nonanedioldiisopropyl ether

Conditions
ConditionsYield
With hydrogen; Pd-C In acetone99%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

nonane-1,9-diyl bis(4-methylbenzenesulfonate)
73992-42-4

nonane-1,9-diyl bis(4-methylbenzenesulfonate)

Conditions
ConditionsYield
With pyridine In dichloromethane at 5 - 15℃; for 0.333333h;98.6%
With pyridine at 0℃; for 2.5h;88%
With trimethylamine hydrochloride; triethylamine In dichloromethane at 20℃; for 1h;85%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

trityl chloride
76-83-5

trityl chloride

9-hydroxynonyl-1-triphenylmethylether
82777-72-8

9-hydroxynonyl-1-triphenylmethylether

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide98%
With dmap; triethylamine In N,N-dimethyl-formamide at 25℃; for 12h;43%
With pyridine at 0 - 20℃; for 16.5h;
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

acetic acid 1-(tert-butyl-dimethyl-silanyloxymethyl)-4-hydroxy-3-oxo-1,3-dihydro-isobenzofuran-1-ylmethyl ester
721448-82-4

acetic acid 1-(tert-butyl-dimethyl-silanyloxymethyl)-4-hydroxy-3-oxo-1,3-dihydro-isobenzofuran-1-ylmethyl ester

acetic acid 4-{9-[1-acetoxymethyl-1-(tert-butyl-dimethyl-silanyloxymethyl)-3-oxo-1,3-dihydro-isobenzofuran-4-yloxy]-nonyloxy}-1-(tert-butyl-dimethyl-silanyloxymethyl)-3-oxo-1,3-dihydro-isobenzofuran-1-ylmethyl ester

acetic acid 4-{9-[1-acetoxymethyl-1-(tert-butyl-dimethyl-silanyloxymethyl)-3-oxo-1,3-dihydro-isobenzofuran-4-yloxy]-nonyloxy}-1-(tert-butyl-dimethyl-silanyloxymethyl)-3-oxo-1,3-dihydro-isobenzofuran-1-ylmethyl ester

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran Mitsunobu reaction;98%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

1,9-dichlorononane
821-99-8

1,9-dichlorononane

Conditions
ConditionsYield
With Ethyl trichloroacetate; triphenylphosphine In acetonitrile at 10 - 15℃; for 3h;97%
With thionyl chloride In dichloromethane; N,N-dimethyl-formamide65%
With pyridine; thionyl chloride
With thionyl chloride
3,4-dihydro-2H-pyran
110-87-2

3,4-dihydro-2H-pyran

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

9-<(2H-tetrahydropyran-2-yl)oxy>nonan-1-ol
98847-00-8

9-<(2H-tetrahydropyran-2-yl)oxy>nonan-1-ol

Conditions
ConditionsYield
With 1-butyl-3-methylimidazolium hydrogen sulfate In hexane for 0.0333333h; Microwave irradiation;97%
With tin(ll) chloride In chloroform for 24h; Ambient temperature;80%
With toluene-4-sulfonic acid In dichloromethane for 1.5h;60%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

9-bromononan-1-ol
55362-80-6

9-bromononan-1-ol

Conditions
ConditionsYield
With hydrogen bromide In toluene for 7.5h; Time; Reflux;95%
With hydrogen bromide In toluene for 30h; Dean-Stark; Reflux;94%
With hydrogen bromide In n-heptane at 150℃;93%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

p-Methoxybenzyl bromide
2746-25-0

p-Methoxybenzyl bromide

9-((4-methoxybenzyl)oxy)nonan-1-ol
267005-80-1

9-((4-methoxybenzyl)oxy)nonan-1-ol

Conditions
ConditionsYield
With sodium hydride; tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide at 0 - 20℃; for 1h;95%
With tetra-(n-butyl)ammonium iodide; sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h;95%
With sodium hydride In N,N-dimethyl-formamide at 0 - 25℃; for 1h;90%
With sodium hydride In tetrahydrofuran at 0 - 20℃; for 4h;76%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

9-iodononan-1-ol
76334-30-0

9-iodononan-1-ol

Conditions
ConditionsYield
With iodine In acetonitrile at 120℃; for 0.0666667h; Microwave irradiation; chemoselective reaction;93%
Multi-step reaction with 2 steps
1: 47percent HBr / toluene / Heating
2: NaI / acetone / Ambient temperature
View Scheme
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

acetic acid
64-19-7

acetic acid

9-hydroxyl nonanyl acetate
103109-24-6

9-hydroxyl nonanyl acetate

Conditions
ConditionsYield
With HY-Zeolite In chloroform for 3.5h; Heating;92%
With sulfuric acid In hexane; cyclohexane; water for 36h; Heating;90%
82%
With sulfuric acid In water56%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

nonanedial
51651-40-2

nonanedial

Conditions
ConditionsYield
With Dess-Martin periodane In dichloromethane at 20℃; for 0.583333h;92%
With 2,6-dimethylpyridine; silica gel; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate In dichloromethane at 20℃; for 48h;83%
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In ethyl acetate for 2h; Heating;77%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

3-vinylbenzoic acid
28447-20-3

3-vinylbenzoic acid

nonane-1,9-diyl bis(3-vinylbenzoate)

nonane-1,9-diyl bis(3-vinylbenzoate)

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 15h; Steglich Esterification; Inert atmosphere;92%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

acetophenone
98-86-2

acetophenone

C25H32O2
116223-42-8

C25H32O2

Conditions
ConditionsYield
With potassium hydroxide; bis(1,5-cyclooctadiene)diiridium(I) dichloride; triphenylphosphine at 100℃; for 15h; Inert atmosphere;91%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

methyl 5-(chlorocarbonyl)furan-2-carboxylate

methyl 5-(chlorocarbonyl)furan-2-carboxylate

2-(9-hydroxynonyl) 5-methyl furan-2,5-dicarboxylate

2-(9-hydroxynonyl) 5-methyl furan-2,5-dicarboxylate

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane; triethylamine In tetrahydrofuran at 25℃; for 10h;91%
With 1,4-diaza-bicyclo[2.2.2]octane; triethylamine In tetrahydrofuran at 20℃;
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

9-bromononanal
124388-97-2

9-bromononanal

Conditions
ConditionsYield
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In ethyl acetate at 60℃;90%
Multi-step reaction with 2 steps
1: 7.8 g / HBr / benzene / 24 h / Heating
2: 7.18 g / PCC / CH2Cl2 / 0.5 h
View Scheme
Multi-step reaction with 2 steps
1: 60 percent / 48percent HBr / toluene; H2O / 48 h / 90 - 95 °C
2: 85 percent / pyridiniumchlorochromate, MgSO4 / CH2Cl2 / 1.5 h
View Scheme
Multi-step reaction with 2 steps
1: HBr / benzene
2: 60 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 2 h / Ambient temperature
View Scheme
(Z)-9-octadecenoyl chloride
112-77-6

(Z)-9-octadecenoyl chloride

1,9-Nonanediol
3937-56-2

1,9-Nonanediol

6-[(Z)-octadec-9-enoyl]oxynonyl-(Z)-octadec-9-enoate
1494679-01-4

6-[(Z)-octadec-9-enoyl]oxynonyl-(Z)-octadec-9-enoate

Conditions
ConditionsYield
With pyridine In chloroform at 20℃; Inert atmosphere;90%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

3-(4-chloro-1,2,5-thiadiazol-3-yl)pyridine
131986-28-2

3-(4-chloro-1,2,5-thiadiazol-3-yl)pyridine

1,9-bis[3-(pyrid-3-yl)-1,2,5-thiadiazol-4-yloxy]nonane
274688-26-5

1,9-bis[3-(pyrid-3-yl)-1,2,5-thiadiazol-4-yloxy]nonane

Conditions
ConditionsYield
Stage #1: 1,9-Nonanediol With sodium hydride In tetrahydrofuran
Stage #2: 3-(4-chloro-1,2,5-thiadiazol-3-yl)pyridine In tetrahydrofuran for 20h; Heating; Further stages.;
88%
With sodium hydride In tetrahydrofuran Substitution; Heating;
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

aniline
62-53-3

aniline

N,N'-diphenyl-nonanediyldiamine

N,N'-diphenyl-nonanediyldiamine

Conditions
ConditionsYield
With Pt-Sn/γ-Al2O3 In o-xylene at 145℃; for 24h; Inert atmosphere;88%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

p-methoxybenzyl chloride
824-94-2

p-methoxybenzyl chloride

9-((4-methoxybenzyl)oxy)nonan-1-ol
267005-80-1

9-((4-methoxybenzyl)oxy)nonan-1-ol

Conditions
ConditionsYield
Stage #1: 1,9-Nonanediol With sodium hydride In tetrahydrofuran; dimethyl sulfoxide; mineral oil at 0℃; for 1h;
Stage #2: p-methoxybenzyl chloride With tetra-(n-butyl)ammonium iodide In tetrahydrofuran; dimethyl sulfoxide; mineral oil at 0 - 20℃; for 18.5h;
84%
Stage #1: 1,9-Nonanediol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 1h; Inert atmosphere;
Stage #2: p-methoxybenzyl chloride With tetra-(n-butyl)ammonium iodide In tetrahydrofuran; mineral oil at 23℃; Inert atmosphere;
83%
With sodium hydride In N,N-dimethyl-formamide at 25℃; for 12h;71%
With tetra-(n-butyl)ammonium iodide; sodium hydride In tetrahydrofuran; mineral oil at 0 - 60℃; Inert atmosphere;46%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

9-((tert-butyldimethylsilyl)oxy)nonan-1-ol
157730-99-9

9-((tert-butyldimethylsilyl)oxy)nonan-1-ol

Conditions
ConditionsYield
With 1H-imidazole In tetrahydrofuran at 20℃; for 3h;83%
With 1H-imidazole In tetrahydrofuran at 0 - 20℃; for 65.67h;83%
Stage #1: 1,9-Nonanediol With sodium hydride In tetrahydrofuran; mineral oil at 20℃; Inert atmosphere; Schlenk technique;
Stage #2: tert-butyldimethylsilyl chloride In tetrahydrofuran; mineral oil at 0℃; for 2h; Inert atmosphere; Schlenk technique;
73%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

(S)-(-)-3,3,3-Trifluormilchsaeure
125995-00-8

(S)-(-)-3,3,3-Trifluormilchsaeure

1,9-nonanediol mono-(S)-3,3,3-trifluorolactate

1,9-nonanediol mono-(S)-3,3,3-trifluorolactate

Conditions
ConditionsYield
With sulfuric acid In toluene Heating;82%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

tert-butylchlorodiphenylsilane
58479-61-1

tert-butylchlorodiphenylsilane

A

9-(tert-butyldiphenylsilyloxy)-nonan-1-ol
139258-85-8

9-(tert-butyldiphenylsilyloxy)-nonan-1-ol

B

1,9-di-(tert-butyldiphenylsilyloxy)-nonane

1,9-di-(tert-butyldiphenylsilyloxy)-nonane

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 28h; Substitution;A 81%
B 8.5%
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 40h;A 55%
B 25%
1,9-Nonanediol
3937-56-2

1,9-Nonanediol

ethyl acetate
141-78-6

ethyl acetate

9-hydroxyl nonanyl acetate
103109-24-6

9-hydroxyl nonanyl acetate

Conditions
ConditionsYield
With HY-Zeolite for 6h; Heating;81%

1,9-Nonanediol Specification

The IUPAC name of 1,9-Nonanediol is nonane-1,9-diol. With the CAS registry number 3937-56-2 and EINECS 223-517-5, it is also named as alpha,omega-Nonanediol. The product's categories are alpha,omega-Alkanediols; alpha,omega-Bifunctional Alkanes; Monofunctional & alpha,omega-Bifunctional Alkanes; Linear Hydrocarbon Series. It is white fused crystalline solid which is easily soluble in alcohol, ether, soluble in hot benzene and slightly soluble in water. Additionally, this chemical should be sealed in the container and stored in the cool and dry place.

The other characteristics of this product can be summarized as: (1)ACD/LogP: 1.53; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): 1.53; (4)ACD/LogD (pH 7.4): 1.53; (5)ACD/BCF (pH 5.5): 8.51; (6)ACD/BCF (pH 7.4): 8.51; (7)ACD/KOC (pH 5.5): 161.18; (8)ACD/KOC (pH 7.4): 161.18; (9)#H bond acceptors: 2; (10)#H bond donors: 2; (11)#Freely Rotating Bonds: 10; (12)Polar Surface Area: 18.46 Å2; (13)Index of Refraction: 1.456; (14)Molar Refractivity: 46.81 cm3; (15)Molar Volume: 172.1 cm3; (16)Surface Tension: 36.7 dyne/cm; (17)Enthalpy of Vaporization: 61.71 kJ/mol; (18)Vapour Pressure: 0.000196 mmHg at 25°C; (19)Rotatable Bond Count: 8; (20)Exact Mass: 160.14633; (21)MonoIsotopic Mass: 160.14633; (22)Topological Polar Surface Area: 40.5; (23)Heavy Atom Count: 11; (24)Complexity: 56.6.

Preparation of 1,9-Nonanediol: It can be obtained by nonanedioic acid. This reaction which is a kind of Reduction needs reagent Zr(BH4)4 and solvent tetrahydrofuran at temperature of 25 °C. The reaction time is 1 hours. The yield is 90%.

Uses of 1,9-Nonanediol: It is in organic synthesis. It also can react with 3,4-dihydro-2H-pyran and 9-(tetrahydropyrane-2-yloxy)nonan-1-ol. This reaction needs reagent p-toluenesulfonic acid and solvent CH2Cl2. The reaction time is 1.5 hours. The yield is 60%.

People can use the following data to convert to the molecule structure. 
1. SMILES:OCCCCCCCCCO
2. InChI:InChI=1/C9H20O2/c10-8-6-4-2-1-3-5-7-9-11/h10-11H,1-9H2
3. InChIKey:ALVZNPYWJMLXKV-UHFFFAOYAQ

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