tetraacetyl thioglucose
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
With sodium methylate In methanol for 0.25h; Ambient temperature; |
O2,O3,O4,O6,S-Pentaacetyl-1-thio-β-D-glucopyranose
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
With sodium methylate In methanol at 0 - 20℃; |
D-glucose
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 2-chloro-1,3-dimethylimidazolinium chloride; triethylamine / water-d2; acetonitrile / 0.05 h / 0 °C 1.2: 1.5 h / 0 °C 2.1: sodiumsulfide nonahydrate / water-d2 / 1 h / 20 °C View Scheme |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
With sodiumsulfide nonahydrate In water-d2 at 20℃; for 1h; Solvent; |
1-iodo-butane
sodium 1-thio-β-D-glucopyranoside
n-butyl 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol at 20℃; for 1h; | 100% |
D,L-2-amino-5-hexenoic acid
sodium 1-thio-β-D-glucopyranoside
2-amino-6-(1-thio-β-D-glucopyranosyl)hexanoic acid
Conditions | Yield |
---|---|
With 2,2’-azobis[2-(2-imidazolin-2-yl)propane]dihydrochloride at 20℃; pH=4; aq. acetate buffer; regioselective reaction; | 98% |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 0.333333h; | 98% |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol; acetone at 20℃; for 5h; | 96% |
C14H13ClO4
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol; acetone at 20℃; for 5h; | 96% |
sodium 1-thio-β-D-glucopyranoside
(4S)-2,2-dioxo-1,2,3-oxathiazolidinone-4-carboxylic acid
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water at 20℃; for 4h; | 95% |
With sodium hydrogencarbonate at 20℃; for 4h; |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol; acetone at 20℃; for 18h; | 95% |
2,3-dichloro-5,8-dimethoxynaphthalene-1,4-dione
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol; acetone at 20℃; for 1.5h; | 94% |
2,3-Dichloro-1,4-naphthoquinone
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol; acetone at 20℃; for 1.5h; | 93% |
sodium 1-thio-β-D-glucopyranoside
methyl iodide
methyl 1-deoxy-1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol | 91% |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 0.25h; | 91% |
In N,N-dimethyl-formamide at 20℃; for 0.25h; | 91% |
Conditions | Yield |
---|---|
With hydrogenchloride; 2,2-dimethoxy-2-phenylacetophenone In water at 20℃; UV-irradiation; | 90% |
Conditions | Yield |
---|---|
With hydrogenchloride; 2,2-dimethoxy-2-phenylacetophenone In water at 20℃; UV-irradiation; | 90% |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 0.333333h; | 90% |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol; acetone at 20℃; for 1.5h; | 89% |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; | 88% |
In N,N-dimethyl-formamide at 20℃; for 0.25h; | 88% |
3,5-di-tert-butyl-o-benzoquinone
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In water; acetic acid for 4h; | 87% |
sodium 1-thio-β-D-glucopyranoside
ditetradecyl maleate
ditetradecyl (R,S)-2-(β-D-glucopyranosylthio)succinate
Conditions | Yield |
---|---|
With acetic acid In isopropyl alcohol at 55℃; for 1h; pH=8; | 85% |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; Darkness; | 85% |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol; acetone at 20℃; for 1.5h; | A 5% B 5.5% C 84% |
Conditions | Yield |
---|---|
With triethylamine In dimethyl sulfoxide at 20℃; for 0.5h; Darkness; | 83% |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; Darkness; | 83% |
dichloro(2,2'-bipyridine)platinum(II)
water
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
at 60℃; for 1h; | 81% |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
Stage #1: sodium 1-thio-β-D-glucopyranoside With N,N,N',N'-tetramethylguanidine In tetrahydrofuran at 24℃; for 0.0833333h; Stage #2: 1-[(triisopropylsilyl)ethynyl]-1,2-benziodoxol-3(1H)-one In tetrahydrofuran at 24℃; for 0.0833333h; | 81% |
Conditions | Yield |
---|---|
With hydrogenchloride; 2,2-dimethoxy-2-phenylacetophenone In water at 20℃; UV-irradiation; | 81% |
sodium 1-thio-β-D-glucopyranoside
heptakis(6-deoxy-6-iodo)cyclomaltoheptaose
Conditions | Yield |
---|---|
With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone at 70℃; for 7h; | 80% |
3-chloro-2,5,8-trimethoxynaphthalene-1,4-dione
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol; acetone at 20℃; for 0.6h; | 80% |
2-chloro-5,8-dihydroxy-3-methoxynaphthalene-1,4-dione
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol; acetone at 20℃; for 1.5h; | 80% |
sodium 1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Darkness; | 78% |
sodium 1-thio-β-D-glucopyranoside
1,6,19,24-Tetraoxa-2,5,20,23-tetraoxocyclohexatriconta-3,21-diene
Conditions | Yield |
---|---|
With acetic acid In isopropyl alcohol at 50℃; for 3h; pH=8; | 77% |
IUPAC Name: Sodium (2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxane-2-thiolate
Systematic of 1-Thio-β-D-glucose sodium salt (CAS NO.10593-29-0): EINECS 234-200-6 ; Sodium glucopyranosyl sulphide
CAS NO: 10593-29-0
Molecular Formula of 1-Thio-β-D-glucose sodium salt (CAS NO.10593-29-0): C6H11NaO5S
Molecular Weight: 218.2033
Molecular Structure:
Melting Point: 173 °C
H bond acceptors: 5
H bond donors: 4
Freely Rotating Bonds: 6
Polar Surface Area: 84.95 Å2
Flash Point of 1-Thio-β-D-glucose sodium salt (CAS NO.10593-29-0): 215.5 °C
Enthalpy of Vaporization: 79.48 kJ/mol
Boiling Point: 432.6 °C at 760 mmHg
Vapour Pressure: 2.66E-09 mmHg at 25°C
Safety Statements: 6
S6: Keep under ... (there follows the name of an inert gas).
WGK Germany: 3
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