Sodium 1-naphthalenesulfonate supplier

Name
Sodium 1-naphthalenesulfonate
EINECS 204-976-0
CAS No. 130-14-3
Article Data5
CAS DataBase
Density 1.423g/cm3
Solubility Soluble in water.
Melting Point 299-301 °C
Formula C₁₀H₇NaO₃S
Boiling Point
Molecular Weight 230.22
Flash Point
Transport Information
Appearance
Safety 26-36
Risk Codes 36/37/38
Molecular Structure
Hazard Symbols Xi
Synonyms 1-Naphthalenesulfonicacid, sodium salt (8CI,9CI);Alpha salt;Sodium1-naphthylsulfonate;Sodium a-naphthalenesulfonate;Sodium a-naphthalenesulfonic acid;Sodium a-naphthylsulfonate;a-Naphthalenesulfonic acid sodium salt;
PSA 65.58000
LogP 2.82470

Synthetic route

: 81292-93-5
Naphthalinsulfonsaeure-trimethylsilylester

: 130-14-3
sodium 1-naphthalenesulfonate

Conditions

Conditions	Yield
With sodium hydrogencarbonate In tetrachloromethane for 0.333333h; Yield given;

: 130-14-3
sodium 1-naphthalenesulfonate

: 85-46-1
1-Naphthalenesulfonyl chloride

Conditions

Conditions	Yield
With trichlorophosphate In sulfolane; acetonitrile at 68 - 72℃; for 0.666667h;	94%
With phosphorus pentachloride
With phosphorus pentachloride at 125℃; aus bei 180grad getrocknetem Edukt1 und Behandeln nach dem Abkuehlen mit Eis und mit Wasser;
With chlorine-triphenylphosphine In acetonitrile for 15h; Ambient temperature;

: (1R,2R,4S)-2-(3-chlorophenyl)-1-(4-chlorophenyl)-4-((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)-4-methylhept-6-en-1-ol

: 130-14-3
sodium 1-naphthalenesulfonate

: 108-88-3
toluene

: 7143-01-3
Methanesulfonic anhydride

A: C27H33Cl2NO4S

B: C33H37Cl2NO4S

C: C26H30Cl2NO(1+)*C10H7O3S(1-)*0.5C7H8

Conditions

Conditions	Yield
Stage #1: (1R,2R,4S)-2-(3-chlorophenyl)-1-(4-chlorophenyl)-4-((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)-4-methylhept-6-en-1-ol; toluene; Methanesulfonic anhydride With 2,6-dimethylpyridine at 75℃; for 12h; Stage #2: With sulfuric acid In dichloromethane; water at 20℃; for 0.5h; Stage #3: sodium 1-naphthalenesulfonate In dichloromethane; water	A n/a B n/a C 90%

...Expand

: 290-37-9
1,4-pyrazine

: 130-14-3
sodium 1-naphthalenesulfonate

: silver nitrate

: [Ag(1-naphthalenesulfonate)(pyrazine)]*H2O

Conditions

Conditions	Yield
In ethanol; water High Pressure; mixt. sodium 1-naphthalenesulfonate and AgNO3 in water was stirred for 5min and filtered, pyrazine in EtOH was added, transferred to Teflon-lin ed stainless steel autoclave and heated at 140°C for 1 day; cooling to room temp. at 10°C/h; elem. anal.;	85%

...Expand

: 292638-84-7
styrene

: 130-14-3
sodium 1-naphthalenesulfonate

: 63536-46-9
1-ethylquinoxaline-2(1H)-one

: 1-ethyl-3-(2-(naphthalene-1-sulfonyl)-1-phenylethyl)quinoxaline-2(1H)-one

Conditions

Conditions	Yield
With dipotassium peroxodisulfate In water at 70℃; for 24h; Green chemistry;	85%

...Expand

: 130-14-3
sodium 1-naphthalenesulfonate

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 27331-33-5
1-(4-methoxyphenyl)naphthalene

Conditions

Conditions	Yield
With bis(tricyclohexylphosphine)nickel(II) dichloride In tetrahydrofuran at 20℃; for 20h; Sealed tube; Inert atmosphere;	83%

: 130-14-3
sodium 1-naphthalenesulfonate

: 529-36-2
1-Naphthalenethiol

Conditions

Conditions	Yield
With triphenylphosphine; 18-crown-6 ether; iodine In benzene for 35h; Heating;	70%
With 18-crown-6 ether; iodine; triphenylphosphine In benzene for 35h; Heating;	70 % Chromat.
Multi-step reaction with 2 steps 1: PCl5 / 125 °C / aus bei 180grad getrocknetem Edukt1 und Behandeln nach dem Abkuehlen mit Eis und mit Wasser 2: zinc dust; water / 60 °C / dann bei 70grad, anschliessend Behandeln mit verd. Salzsaeure und Zinkstaub View Scheme

: 108-99-6
3-Methylpyridine

: 130-14-3
sodium 1-naphthalenesulfonate

: silver nitrate

: [Ag(1-naphthalenesulfonate)(β-picoline)2]

Conditions

Conditions	Yield
In water High Pressure; mixt. sodium 1-naphthalenesulfonate and AgNO3 in water was stirred for 5min and filtered, picoline was added, react. mixt. was transferred to T eflon-lined stainless steel autoclave and heated at 140°C for 1 day; cooling to room temp. at 10°C/h; elem. anal.;	70%

...Expand

: 100-97-0
hexamethylenetetramine

: 130-14-3
sodium 1-naphthalenesulfonate

: silver nitrate

: [Ag(1-naphthalenesulfonate)(hexamethylenetetramine)]*H2O

Conditions

Conditions	Yield
With NH4OH In water; acetonitrile aq. soln. hexamethylenetetramine was added dropwise to soln. AgNO3 and sodium 1-naphthalenesulfonate in aq. MeCN (1:1) for 10 min; aq. soln. NH3 was added and kept in the dark for several days; elem. anal.;	70%

...Expand

: 130-14-3
sodium 1-naphthalenesulfonate

: silver nitrate

: 603-35-0
triphenylphosphine

: 895139-18-1
tris(triphenylphosphine)(1-naphthalenesulfonato)silver(I)

Conditions

Conditions	Yield
In methanol; water mixt. of Na salt of ligand and AgNO3 in H2O stirred for 5 min; filtered;PPh3 in MeOH added to filtrate; ppt. dissolved in min. MeCN; crystd. by slow evapn. in the dark for several d; elem. anal.;	67%

...Expand

: 124-38-9
carbon dioxide

: 130-14-3
sodium 1-naphthalenesulfonate

: 86-55-5
1-naphthalenecarboxylic acid

Conditions

Conditions	Yield
Stage #1: carbon dioxide; sodium 1-naphthalenesulfonate With copper(l) iodide; potassium tert-butylate; o-phenanthroline In dimethyl sulfoxide at 140℃; under 760.051 Torr; for 12h; Schlenk technique; Stage #2: With hydrogenchloride In water; dimethyl sulfoxide Schlenk technique;	65%

: 130-14-3
sodium 1-naphthalenesulfonate

: 317-55-5
naphthalene-1-sulfonyl fluoride

Conditions

Conditions	Yield
Stage #1: sodium 1-naphthalenesulfonate With 1,3,5-trichloro-2,4,6-triazine; tetrabutylammomium bromide In acetonitrile at 60 - 70℃; for 15h; Stage #2: With potassium hydrogen difluoride In acetone; acetonitrile at 20℃; for 12h;	64%

: 130-14-3
sodium 1-naphthalenesulfonate

: 2633-66-1
2-mesitylmagnesium bromide

: 22187-05-9
1-(2,4,6-trimethylphenyl)naphthalene

Conditions

Conditions	Yield
With bis(tricyclohexylphosphine)nickel(II) dichloride In tetrahydrofuran at 60℃; for 20h; Sealed tube; Inert atmosphere;	52%

: 4Co(2+)*6(C6H4CH2C3H2N2C5H4N)2*8BF4(1-)=[Co4((C6H4CH2C3H2N2C5H4N)2)6](BF4)8

: 130-14-3
sodium 1-naphthalenesulfonate

: 4Co(2+)*6(C6H4CH2C3H2N2C5H4N)2*6BF4(1-)*2C10H7SO3(1-)*12H2O=Co4((C6H4CH2C3H2N2C5H4N)2)6(BF4)6(C10H7SO3)2*12H2O

Conditions

Conditions	Yield
In acetonitrile NaC10H7SO3 added to MeCN soln. of Co-complex; Et2O diffused; elem. anal.;	16%

: 130-14-3
sodium 1-naphthalenesulfonate

: 90-15-3
α-naphthol

Conditions

Conditions	Yield
With sodium hydroxide at 300 - 320℃; in einem gusseisernen Kessel, man loest in Wasser, faellt das α-Naphthol mit Saeure aus und destilliert es;
With water; methyllithium; sodium carbonate; calcium carbonate
With sodium hydroxide at 300℃;

: 130-14-3
sodium 1-naphthalenesulfonate

: 89108-43-0
5-chloronaphthalene-1-sulfonic acid

Conditions

Conditions	Yield
With hydrogenchloride; sodium chlorate und Erhitzen nach mehrstuendigem Stehen langsam bis fast zum Kochen;

: 130-14-3
sodium 1-naphthalenesulfonate

: 77-78-1
dimethyl sulfate

: 5138-52-3
naphthalene-1-sulfonic acid methyl ester

Conditions

Conditions	Yield
With benzene at 150 - 160℃;

: 829-83-4
diphenylarsane

: 130-14-3
sodium 1-naphthalenesulfonate

: 21498-52-2
naphthalen-1-yl-diphenyl-arsane

Conditions

Conditions	Yield
(i) K, EtO(CH2CH2O)2Et, (ii) /BRN= 3639038/; Multistep reaction;

: 130-14-3
sodium 1-naphthalenesulfonate

: 62-53-3
aniline

: 90-30-2
N-phenyl-1-naphthylamine

Conditions

Conditions	Yield
With sodium; copper 1.) 180 deg C, 3 h, 2.) 250 deg C, 15 h;; Yield given. Multistep reaction;

: 130-14-3
sodium 1-naphthalenesulfonate

: 1950-75-0
naphthalene-1-sulfonyl bromide

Conditions

Conditions	Yield
With triphenylphosphine dibromide 1:1 addition complex In acetonitrile for 5h; Ambient temperature;

: 130-14-3
sodium 1-naphthalenesulfonate

potassium ferro cyanide: potassium ferro cyanide

: 86-53-3
1-Cyanonaphthalene

: 130-14-3
sodium 1-naphthalenesulfonate

: 71862-35-6
naphthalene-1-sulfonic acid benzylamide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: Ph3P*Br2 / acetonitrile / 5 h / Ambient temperature 2: Et3N / acetonitrile / 0 - 20 °C View Scheme
Multi-step reaction with 2 steps 1: Ph3P*Cl2 / acetonitrile / 15 h / Ambient temperature 2: Et3N / acetonitrile / 0 - 20 °C View Scheme

: 130-14-3
sodium 1-naphthalenesulfonate

: 606-25-7
naphthalene-1-sulfonamide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: PCl5 2: water; ammonia View Scheme

: 130-14-3
sodium 1-naphthalenesulfonate

: 67199-40-0
naphthalene-1-sulfonic acid ethyl ester

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: PCl5 View Scheme

: 130-14-3
sodium 1-naphthalenesulfonate

: 85-47-2
1-naphthalenesulfonic acid

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: PCl5 2: alcohol; zinc 3: water View Scheme

: 130-14-3
sodium 1-naphthalenesulfonate

: 39178-11-5
1,2-di(naphthalen-1-yl)disulfane

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: PCl5 2: alcohol; zinc 3: water 4: KOH-solution View Scheme

: 130-14-3
sodium 1-naphthalenesulfonate

: 607-33-0
naphthalene-1-sulphinic acid

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: PCl5 2: alcohol; zinc View Scheme

: 130-14-3
sodium 1-naphthalenesulfonate

: 49833-22-9
S-(naphthalen-1-yl) naphthalene-1-sulfonothioate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: PCl5 2: alcohol; zinc 3: water View Scheme

: 130-14-3
sodium 1-naphthalenesulfonate

: 17316-47-1
Diphenyl-naphthyl-(1)-arsin-sulfid

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: (i) K, EtO(CH2CH2O)2Et, (ii) /BRN= 3639038/ 2: sulfur / benzene / Heating View Scheme

Sodium 1-naphthalenesulfonate Specification

The Sodium 1-naphthalenesulfonate, with the CAS registry number 130-14-3 and EINECS registry number 204-976-0, has the systematic name of sodium naphthalene-1-sulfonate. It belongs to the product category of Intermediates of Dyes and Pigments. And the molecular formula of the chemical is C₁₀H₇NaO₃S.

The characteristics of this chemical are as followings: (1)H-Bond Donor 0; (2)H-Bond Acceptor 3; (3)Rotatable Bond Count 1; (4)Exact Mass 230.001359; (5)MonoIsotopic Mass 230.001359; (6)Topological Polar Surface Area 65.6; (7)Heavy Atom Count 15; (8)Formal Charge 0; (9)Complexity 296; (10)Isotope Atom Count 0; (11)Defined Atom StereoCenter Count 0; (12)Undefined Atom StereoCenter Count 0; (13)Defined Bond StereoCenter Count 0; (14)Undefined Bond StereoCenter Count 0; (15)Covalently-Bonded Unit Count 2.

Uses of Sodium 1-naphthalenesulfonate: It can be used to produce naphthalene-1-sulfonyl chloride. This reaction will need reagent POCl₃, menstruum acetonitrile and tetrahydrothiophene 1,1-dioxide. The reaction time is 40 minutes with temperature of 68-72°C, and the yield is about 94%.

You should be cautious while dealing with this chemical. It irritates to eyes, respiratory system and skin. Therefore, you had better take the following instructions: Wear suitable protective clothing, and if in case of contacting with eyes, rinse immediately with plenty of water and seek medical advice.

Addtionally, the following datas could be converted into the molecular structure:
(1)SMILES: [Na+].[O-]S(=O)(=O)c2cccc1ccccc12
(2)InChI: InChI=1/C10H8O3S.Na/c11-14(12,13)10-7-3-5-8-4-1-2-6-9(8)10;/h1-7H,(H,11,12,13);/q;+1/p-1
(3)InChIKey: HIEHAIZHJZLEPQ-REWHXWOFAJ

Product Name

Sodium 1-naphthalenesulfonate

Synthetic route

Sodium 1-naphthalenesulfonate Specification

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