Conditions | Yield |
---|---|
With SA In 1-methyl-pyrrolidin-2-one at 50 - 125℃; Concentration; Large scale; | 99.2% |
With zinc diacetate at 220℃; for 2h; Neat (no solvent); | 80% |
at 160 - 200℃; |
3,3-dichlorophthalide
naphthalene-1,8-diamine
A
solvent orange 60
B
1,8-diphthalisoimidonaphthalene
Conditions | Yield |
---|---|
With triethylamine In acetonitrile -5 deg C to r.t.; | A 32% B 65% |
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 0.0833333h; Ambient temperature; | A n/a B 65% |
Conditions | Yield |
---|---|
With copper(l) iodide In N,N-dimethyl-formamide at 130℃; for 0.25h; | 57% |
solvent orange 60
Conditions | Yield |
---|---|
at 185℃; | |
at 185℃; |
Conditions | Yield |
---|---|
Stage #1: solvent orange 60 With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h; Stage #2: 4-(di-naphthalene-2-yl-amino)-phenylboronic acid With potassium carbonate In toluene at 110℃; for 5h; | 86% |
Conditions | Yield |
---|---|
Stage #1: solvent orange 60 With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h; Stage #2: (4-(di(naphthalene-1-yl)amine)phenyl)boronic acid With potassium carbonate In toluene at 110℃; for 5h; | 84% |
Conditions | Yield |
---|---|
Stage #1: solvent orange 60 With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h; Stage #2: 4-(diphenylamino)phenyl boronic acid With potassium carbonate In toluene at 110℃; for 5h; | 82% |
Conditions | Yield |
---|---|
beim Bromieren; |
solvent orange 60
Conditions | Yield |
---|---|
Stage #1: solvent orange 60 With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h; Stage #2: With potassium carbonate at 110℃; for 5h; |
Systematic Name: 12H-Isoindolo[2,1-a]perimidin-12-one
Moleculer Formula: C18H10N2O
Molecular Weight: 270.29
Canonical SMILES: O=C1N2c3c4c(cccc4N=C2c2ccccc12)ccc3
InChI: InChI=1/C18H10N2O/c21-18-13-8-2-1-7-12(13)17-19-14-9-3-5-11-6-4-10-15(16(11)14)20(17)18/h1-10H
EINECS: 230-049-5
Product Categories: Solvent Dyestuff
XLogP3-AA: 3.4
H-Bond Donor: 0
H-Bond Acceptor: 2Index of Refraction: 1.777
Molar Refractivity: 80.61 cm3
Molar Volume: 192.5 cm3
Polarizability: 31.95×10-24 cm3
Surface Tension: 59.5 dyne/cm
Density: 1.4 g/cm3
Flash Point: 269.7 °C
Enthalpy of Vaporization: 79.58 kJ/mol
Boiling Point: 522.4 °C at 760 mmHg
Melting Point: 231 °C
Solubility: Insoluble in water
Vapour Pressure of Solvent Orange 60 (CAS NO.6925-69-5): 5.21E-11 mmHg at 25 °C
Solvent Orange 60 (CAS NO.6925-69-5) is supposed to be used as dye.
Solvent Orange 60 (CAS NO.6925-69-5), its Synonyms are 12H-Phthaloperin-12-one ; 12-Phthaloperinone ; C.I. Disperse Orange 24 ; C.I. Solvent Orange 60 ; C.I. Solvent Orange 78 ; Solvaperm Orange 3G .
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View