Product Name

  • Name

    C.I. 564100

  • EINECS 230-049-5
  • CAS No. 6925-69-5
  • Article Data17
  • CAS DataBase
  • Density 1.404 g/cm3
  • Solubility Insoluble in water
  • Melting Point 228-230 °C
  • Formula C18H10N2O
  • Boiling Point 522.368 °C at 760 mmHg
  • Molecular Weight 270.29
  • Flash Point 269.719 °C
  • Transport Information
  • Appearance COA
  • Safety
  • Risk Codes
  • Molecular Structure Molecular Structure of 6925-69-5 (C.I. 564100)
  • Hazard Symbols
  • Synonyms 12-Phthaloperinone(6CI,7CI,8CI);10H-Perimidino[2,1-a]isoindol-10-one;Aminoplast Orange LFP;12H-Phthaloperin-12-one;C.I. Disperse Orange 24;C.I. Solvent Orange 60;C.I. SolventOrange 78;Diaresin Orange HS;Disperse Orange 24;KP Plast Orange 8150;KPPlast Orange HG;Macrolex Orange 3G;Oplas Orange 230;Oracet Orange G;Phthaloperinone;Sandoplast Orange 3G;Solvent Orange 78;Sumiplast Orange HRP;
  • PSA 34.89000
  • LogP 3.85840

Synthetic route

phthalic anhydride
85-44-9

phthalic anhydride

naphthalene-1,8-diamine
479-27-6

naphthalene-1,8-diamine

solvent orange 60
6925-69-5

solvent orange 60

Conditions
ConditionsYield
With SA In 1-methyl-pyrrolidin-2-one at 50 - 125℃; Concentration; Large scale;99.2%
With zinc diacetate at 220℃; for 2h; Neat (no solvent);80%
at 160 - 200℃;
3,3-dichlorophthalide
601-70-7

3,3-dichlorophthalide

naphthalene-1,8-diamine
479-27-6

naphthalene-1,8-diamine

A

solvent orange 60
6925-69-5

solvent orange 60

B

1,8-diphthalisoimidonaphthalene
134903-77-8

1,8-diphthalisoimidonaphthalene

Conditions
ConditionsYield
With triethylamine In acetonitrile -5 deg C to r.t.;A 32%
B 65%
3,3-dichlorophthalide
601-70-7

3,3-dichlorophthalide

naphthalene-1,8-diamine
479-27-6

naphthalene-1,8-diamine

A

solvent orange 60
6925-69-5

solvent orange 60

B

N,N'-(1,8-naphthylene)bisphthalisoimide

N,N'-(1,8-naphthylene)bisphthalisoimide

Conditions
ConditionsYield
With triethylamine In acetonitrile for 0.0833333h; Ambient temperature;A n/a
B 65%
1-amino-8-bromonaphthalene
62456-34-2

1-amino-8-bromonaphthalene

potassium phtalimide
1074-82-4

potassium phtalimide

solvent orange 60
6925-69-5

solvent orange 60

Conditions
ConditionsYield
With copper(l) iodide In N,N-dimethyl-formamide at 130℃; for 0.25h;57%
2--benzoic acid

2--benzoic acid

solvent orange 60
6925-69-5

solvent orange 60

Conditions
ConditionsYield
at 185℃;
at 185℃;
4-(di-naphthalene-2-yl-amino)-phenylboronic acid
1232102-18-9

4-(di-naphthalene-2-yl-amino)-phenylboronic acid

solvent orange 60
6925-69-5

solvent orange 60

C44H29N3

C44H29N3

Conditions
ConditionsYield
Stage #1: solvent orange 60 With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h;
Stage #2: 4-(di-naphthalene-2-yl-amino)-phenylboronic acid With potassium carbonate In toluene at 110℃; for 5h;
86%
(4-(di(naphthalene-1-yl)amine)phenyl)boronic acid
889657-98-1

(4-(di(naphthalene-1-yl)amine)phenyl)boronic acid

solvent orange 60
6925-69-5

solvent orange 60

C44H29N3

C44H29N3

Conditions
ConditionsYield
Stage #1: solvent orange 60 With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h;
Stage #2: (4-(di(naphthalene-1-yl)amine)phenyl)boronic acid With potassium carbonate In toluene at 110℃; for 5h;
84%
solvent orange 60
6925-69-5

solvent orange 60

4-(diphenylamino)phenyl boronic acid
201802-67-7

4-(diphenylamino)phenyl boronic acid

C36H25N3

C36H25N3

Conditions
ConditionsYield
Stage #1: solvent orange 60 With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h;
Stage #2: 4-(diphenylamino)phenyl boronic acid With potassium carbonate In toluene at 110℃; for 5h;
82%
methyl magnesium iodide
917-64-6

methyl magnesium iodide

diethyl ether
60-29-7

diethyl ether

solvent orange 60
6925-69-5

solvent orange 60

10-oxy-10-methyl-phthaloperine

10-oxy-10-methyl-phthaloperine

hydrogenchloride
7647-01-0

hydrogenchloride

solvent orange 60
6925-69-5

solvent orange 60

2--benzoic acid

2--benzoic acid

solvent orange 60
6925-69-5

solvent orange 60

acetic acid
64-19-7

acetic acid

zinc dust

zinc dust

di--ether

di--ether

solvent orange 60
6925-69-5

solvent orange 60

acetic acid
64-19-7

acetic acid

x.x-dibromo-phthaloperinone-(10)

x.x-dibromo-phthaloperinone-(10)

Conditions
ConditionsYield
beim Bromieren;
solvent orange 60
6925-69-5

solvent orange 60

nitric acid
7697-37-2

nitric acid

x.x-dinitro-phthaloperinone-(10)

x.x-dinitro-phthaloperinone-(10)

solvent orange 60
6925-69-5

solvent orange 60

Reaxys ID: 32394263

Reaxys ID: 32394263

Reaxys ID: 32394254

Reaxys ID: 32394254

Conditions
ConditionsYield
Stage #1: solvent orange 60 With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h;
Stage #2: With potassium carbonate at 110℃; for 5h;

Solvent Orange 60 Chemical Properties


Systematic Name: 12H-Isoindolo[2,1-a]perimidin-12-one
Moleculer Formula: C18H10N2O
Molecular Weight: 270.29
Canonical SMILES: O=C1N2c3c4c(cccc4N=C2c2ccccc12)ccc3
InChI: InChI=1/C18H10N2O/c21-18-13-8-2-1-7-12(13)17-19-14-9-3-5-11-6-4-10-15(16(11)14)20(17)18/h1-10H
EINECS: 230-049-5
Product Categories: Solvent Dyestuff
XLogP3-AA: 3.4
H-Bond Donor: 0
H-Bond Acceptor: 2Index of Refraction: 1.777 
Molar Refractivity: 80.61 cm3 
Molar Volume: 192.5 cm3 
Polarizability: 31.95×10-24 cm3 
Surface Tension: 59.5 dyne/cm 
Density: 1.4 g/cm3 
Flash Point: 269.7 °C 
Enthalpy of Vaporization: 79.58 kJ/mol 
Boiling Point: 522.4 °C at 760 mmHg  
Melting Point: 231 °C
Solubility: Insoluble in water
Vapour Pressure of Solvent Orange 60 (CAS NO.6925-69-5): 5.21E-11 mmHg at 25 °C

Solvent Orange 60 Uses

 Solvent Orange 60 (CAS NO.6925-69-5) is supposed to be used as dye.

Solvent Orange 60 Specification

 Solvent Orange 60 (CAS NO.6925-69-5), its Synonyms are 12H-Phthaloperin-12-one ; 12-Phthaloperinone ; C.I. Disperse Orange 24 ; C.I. Solvent Orange 60 ; C.I. Solvent Orange 78 ; Solvaperm Orange 3G .

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