2-Bromoethyl methyl ether
2,8,9-trioxa-5-aza-1-borabicyclo[3.3.3]undecane
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
With tetrabutyl-ammonium chloride; sodium hydroxide In sulfolane at 60 - 120℃; Reagent/catalyst; | 92.7% |
2-chloroethyl methyl ether
2,8,9-trioxa-5-aza-1-borabicyclo[3.3.3]undecane
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; potassium hydroxide In dimethyl sulfoxide at 60 - 120℃; Catalytic behavior; Reagent/catalyst; Solvent; Inert atmosphere; Autoclave; Large scale; | 86.3% |
1-chloro-2-(2-methoxyethoxy)ethane
2-(2-methoxyethoxy)ethanamine
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
With sodium carbonate at 110℃; for 24h; Temperature; | 85.48% |
1-chloro-2-(2-methoxyethoxy)ethane
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
With ammonia In methanol |
2-(2-methoxyethoxy)ethyl alcohol
A
8-aza-2,5,11,14-tetraoxa-pentadecane
B
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
With ammonia; hydrogen; nickel at 185℃; 1.) 3h, 2.) 2h; | A 3241 % B 15125 g |
With ammonia; hydrogen; nickel at 185℃; 1.) 3h, 2.) 2h; | A 3241 g B 15125 g |
2-(2-methoxyethoxy)ethyl alcohol
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2, Py 2: NH3 / methanol View Scheme | |
aluminum nickel | |
Multi-step reaction with 2 steps 1: thionyl chloride / N,N-dimethyl-formamide / 3 h / 28 - 60 °C 2: sodium carbonate / 24 h / 110 °C View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide / 3 h / 28 - 60 °C 2: ammonia / 6 h / 130 °C / 11251.1 Torr / Autoclave 3: sodium carbonate / 24 h / 110 °C View Scheme |
triethanolamine
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: toluene / 1 h / Reflux; Inert atmosphere; Large scale 2: potassium hydroxide; tetrabutylammomium bromide / dimethyl sulfoxide / 60 - 120 °C / Inert atmosphere; Autoclave; Large scale View Scheme | |
Multi-step reaction with 2 steps 1: toluene / 1 h / Reflux 2: potassium hydroxide; tetrabutylammomium bromide / dimethyl sulfoxide / 60 - 120 °C / Inert atmosphere; Autoclave; Large scale View Scheme | |
Multi-step reaction with 2 steps 1: toluene / 1 h / Reflux 2: potassium hydroxide; tetrabutylammomium bromide / dimethyl sulfoxide / 60 - 120 °C / Inert atmosphere; Autoclave; Large scale View Scheme | |
Multi-step reaction with 2 steps 1: toluene / 1 h / Reflux; Inert atmosphere; Large scale 2: sodium hydroxide; tetrabutyl-ammonium chloride / sulfolane / 60 - 120 °C View Scheme | |
Multi-step reaction with 2 steps 1: toluene / 1 h / Reflux 2: sodium hydroxide; tetrabutyl-ammonium chloride / sulfolane / 60 - 120 °C View Scheme |
Conditions | Yield |
---|---|
In acetone at 35 - 45℃; | 100% |
2-acrylamido-2-methylpropanesulfonic acid
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
at 25℃; for 8h; | 99% |
3-Acryloyloxypropane-1-sulfonic acid
Tris(3,6-dioxaheptyl)amine
C15H33NO6*C6H10O5S
Conditions | Yield |
---|---|
In water at 20℃; for 10h; Inert atmosphere; Schlenk technique; | 99% |
Tris(3,6-dioxaheptyl)amine
(2-hydroxyphenyl)acetic acid disodium salt
potassium 2-iodo-5-methylbenzoate
2-<2-(carboxymethyl)phenoxy>-5-methylbenzoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; copper(l) chloride In 1,4-dioxane; sodium hydroxide | 91% |
para-iodoanisole
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
With CuI; potassium carbonate | 90% |
Tris(3,6-dioxaheptyl)amine
N,N-dimethylethylenediamine
ortho-nitrofluorobenzene
N1,N1-dimethyl-N2-(2-nitrophenyl)ethane-1,2-diamine
Conditions | Yield |
---|---|
With potassium carbonate | 90% |
Tris(3,6-dioxaheptyl)amine
toluene-4-sulfonic acid
Conditions | Yield |
---|---|
With iodosylbenzene; ammonium carbamate In acetonitrile at 25℃; for 2h; | 89% |
3-formyl-10-methylphenothiazine
Tris(3,6-dioxaheptyl)amine
(E)-3-(10-methyl-10H-phenothiazin-3-yl)acrylaldehyde
Conditions | Yield |
---|---|
With (1,3-dioxolan-2-yl-methyl)triphenylphosphonium bromide; potassium carbonate In dichloromethane for 20h; Reflux; | 88.6% |
Tris(3,6-dioxaheptyl)amine
ethyl iodide
Conditions | Yield |
---|---|
In acetonitrile at 50℃; Inert atmosphere; | 88% |
butyldimethylsilyl chloride
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
With sodium iodide | 85% |
3,4-Dinitrotoluene
Tris(3,6-dioxaheptyl)amine
N,N-dimethylethylenediamine
A
N,N-Dimethyl-2-(5-methyl-2-nitroanilino)ethanamine
B
N,N,N-Trimethyl-2-(5-methyl-2-nitroanilino)ethanaminium Iodide
Conditions | Yield |
---|---|
In dimethyl sulfoxide | A 80% B n/a |
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
With pyridine; copper(l) chloride In acetonitrile at 100℃; under 7500.75 - 22502.3 Torr; for 24h; Autoclave; regioselective reaction; | 75% |
Tris(3,6-dioxaheptyl)amine
aniline
N-(2-(2-methoxyethoxy)ethyl)aniline
Conditions | Yield |
---|---|
With 1-hydroxytetraphenylcyclopentadienyl(tetraphenyl-2,4-cyclopentadien-1-one)-μ-hydrotetracarbonyldiruthenium(II) In tert-Amyl alcohol at 150℃; for 24h; Inert atmosphere; | 74% |
Conditions | Yield |
---|---|
In diethyl ether; cyclohexane for 1h; | 72% |
2,4-imidazolidinedione
Benzyloxymethyl chloride
Tris(3,6-dioxaheptyl)amine
3-benzyloxymethyl-imidazolidine-2,4-dione
Conditions | Yield |
---|---|
With potassium hydroxide In water; 4-methyl-2-pentanone | 70% |
2,4-Difluoronitrobenzene
Tris(3,6-dioxaheptyl)amine
N,N-dimethylethylenediamine
N,N,N-Trimethyl-2-(5-β-hydroxyethoxy-2-nitroanilino)ethanaminium Iodide
Conditions | Yield |
---|---|
With potassium carbonate In N-methyl-acetamide; ethylene glycol; dimethyl sulfoxide | 70% |
Conditions | Yield |
---|---|
In hexane Inert atmosphere; Schlenk technique; | 69% |
1-(6-bromohexyl)-2,3-dimethoxybenzene
1-hexyl-4-methyl-benzene
Tris(3,6-dioxaheptyl)amine
benzyl bromide
1,2-bis-(phenylmethoxy)-3-(6-bromohexyl)benzene
Conditions | Yield |
---|---|
With hydrogenchloride; boron tribromide; potassium carbonate In dichloromethane; water; toluene | 67% |
Conditions | Yield |
---|---|
In tetrahydrofuran; cyclohexane for 1h; | 64% |
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
With potassium carbonate | 64% |
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
In acetonitrile for 96h; Reflux; | 62% |
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
With potassium carbonate | 55% |
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
In hexane for 0.166667h; Schlenk technique; Inert atmosphere; | 49% |
Tris(3,6-dioxaheptyl)amine
potassium 2-chlorobenzoate
sodium 2-allyl-4-methylphenolate
2-(2-allyl-4-methylphenoxy)benzoic acid
Conditions | Yield |
---|---|
copper(l) chloride In methoxybenzene | 47% |
6-(bromomethyl)-1,3,8-trimethoxyanthracene-9,10-dione
Tris(3,6-dioxaheptyl)amine
Conditions | Yield |
---|---|
for 24h; Reflux; | 31.4% |
Conditions | Yield |
---|---|
In acetonitrile for 72h; Reflux; | 25% |
The Ethanamine,2-(2-methoxyethoxy)-N,N-bis[2-(2-methoxyethoxy)ethyl]-, with CAS registry number 70384-51-9, has the systematic name of 2-(2-methoxyethoxy)-N,N-bis[2-(2-methoxyethoxy)ethyl]ethanamine. This chemical is a kind of clear pale yellow to brown liquid. And its classification code is TSCA Flag P [A commenced PMN (Premanufacture Notice) substance]. What's more, its EINECS is 274-590-5.
Physical properties of Ethanamine,2-(2-methoxyethoxy)-N,N-bis[2-(2-methoxyethoxy)ethyl]-: (1)ACD/LogP: -3.49; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): -4.91; (4)ACD/LogD (pH 7.4): -3.61; (5)ACD/BCF (pH 5.5): 1; (6)ACD/BCF (pH 7.4): 1; (7)ACD/KOC (pH 5.5): 1; (8)ACD/KOC (pH 7.4): 1; (9)#H bond acceptors: 7; (10)#H bond donors: 0; (11)#Freely Rotating Bonds: 18; (12)Polar Surface Area: 58.62 Å2; (13)Index of Refraction: 1.445; (14)Molar Refractivity: 85.73 cm3; (15)Molar Volume: 321.5 cm3; (16)Polarizability: 33.98×10-24cm3; (17)Surface Tension: 33.3 dyne/cm; (18)Enthalpy of Vaporization: 62.1 kJ/mol; (19)Vapour Pressure: 8.78E-06 mmHg at 25°C.
Uses of Ethanamine,2-(2-methoxyethoxy)-N,N-bis[2-(2-methoxyethoxy)ethyl]-: it can be used to produce C15H33NO6.2C2H5BrMg. This reaction will need solvents cyclohexane, diethyl ether. The reaction time is 1 hour(s). The yield is about 72 %.
When you are using this chemical, please be cautious about it as the following:
The Ethanamine,2-(2-methoxyethoxy)-N,N-bis[2-(2-methoxyethoxy)ethyl]- may cause burns. When use it, wear suitable protective clothing, gloves and eye/face protection. If contact with eyes, rinse immediately with plenty of water and seek medical advice. In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
You can still convert the following datas into molecular structure:
(1)SMILES: O(C)CCOCCN(CCOCCOC)CCOCCOC
(2)InChI: InChI=1/C15H33NO6/c1-17-10-13-20-7-4-16(5-8-21-14-11-18-2)6-9-22-15-12-19-3/h4-15H2,1-3H3
(3)InChIKey: XGLVDUUYFKXKPL-UHFFFAOYAF
(4)Std. InChI: InChI=1S/C15H33NO6/c1-17-10-13-20-7-4-16(5-8-21-14-11-18-2)6-9-22-15-12-19-3/h4-15H2,1-3H3
(5)Std. InChIKey: XGLVDUUYFKXKPL-UHFFFAOYSA-N
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