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Min.Order:1 Gram
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Min.Order:1 Kilogram
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Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por
hexaethynylbenzeneAppearance:white to off-white powder Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Po
Benzene, hexaethynyl-Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Protect them
1,2,3,4,5,6-hexa(2-trimethylsilylethynyl)benzene
1,2,3,4,5,6-hexaethynylbenzene
Conditions | Yield |
---|---|
With potassium fluoride In 1,2-dimethoxyethane at 0℃; for 2.5h; | 99% |
With potassium fluoride; 18-crown-6 ether In 1,2-dimethoxyethane at 23℃; | |
With potassium fluoride; 18-crown-6 ether In 1,2-dimethoxyethane at 23℃; for 0.5h; Hydrolysis; |
2-Methyl-4-[pentakis-(3-hydroxy-3-methyl-but-1-ynyl)-phenyl]-but-3-yn-2-ol
1,2,3,4,5,6-hexaethynylbenzene
Conditions | Yield |
---|---|
With potassium tert-butylate In tert-butyl alcohol |
hexabromobenzene
trimethylsilylacetylene
1,2,3,4,5,6-hexaethynylbenzene
Conditions | Yield |
---|---|
With potassium fluoride; copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; 18-crown-6 ether 1.) 100 deg C, 72 h; 2.) glyme, 10 min; Yield given. Multistep reaction; |
1,2,3,4,5,6-hexaethynylbenzene
Conditions | Yield |
---|---|
With N-chloro-succinimide; tetrabutyl-ammonium chloride; silver carbonate In acetonitrile at 20℃; for 12h; | 63% |
iodobenzene
1,2,3,4,5,6-hexaethynylbenzene
Hexakis(phenylethynyl)benzene
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine; bis(triphenylphosphane)palladium(II) In 1,2-dimethoxyethane at 60℃; for 68h; Sonogashira cross coupling; | 41% |
1,2,3,4,5,6-hexaethynylbenzene
Bis(trimethylsilyl)ethyne
2,3,6,7,10,11-hexakis(trimethylsilyl)starphenylene
Conditions | Yield |
---|---|
dicarbonylcyclopentadienylcobalt for 19.5h; Heating; | 39% |
1,6-Bis(triisopropylsilyl)-1,3,5-hexatriyne
1,2,3,4,5,6-hexaethynylbenzene
Conditions | Yield |
---|---|
cyclopentadienyl-biscarbonyl-cobalt(I) In toluene for 16h; Heating; Irradiation; Yield given; |
Conditions | Yield |
---|---|
With dicarbonylcyclopentadienylcobalt In xylene for 8h; Cycloaddition; Heating; Irradiation; |
1,2,3,4,5,6-hexaethynylbenzene
dihexyl 6-bromoazulene-1,3-dicarboxylate
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In tetrahydrofuran for 18h; Sonogashira-Hagihara coupling; Heating; | 214 mg |
1,2,3,4,5,6-hexaethynylbenzene
4',5'-bis(butylthio)-4-iodotetrathiafulvalene
Conditions | Yield |
---|---|
With triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 20℃; for 5h; Sonogashira coupling; | 143 mg |
4'-(4-iodo-2,6-dimethylphenyl)-2,2':6',2''-terpyridine
1,2,3,4,5,6-hexaethynylbenzene
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran; toluene at 20 - 80℃; for 48h; Sonogashira coupling; | 262 mg |
3,4,3',4'-tetrabutyl-5''-iodo-5-phenyl-[2,2';5',2'']terthiophene
1,2,3,4,5,6-hexaethynylbenzene
hexakis[2-(3',4',3'',4''-tetrabutyl-5''-phenyl-[5,2';5',2'']terthienyl)ethynyl]benzene
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In tetrahydrofuran at 20℃; Sonogashira coupling; | 175 mg |
2-iodo-3-[(trimethylsilyl)ethynyl]naphthalene
1,2,3,4,5,6-hexaethynylbenzene
hexakis(2-{3-[(trimethylsilyl)ethynyl]naphthyl}ethynyl)benzene
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In tetrahydrofuran at 45 - 80℃; for 65h; Sonogashira Cross-Coupling; Inert atmosphere; | 36.2 mg |
1-iodo-2-[(trimethylsilyl)ethynyl]naphthalene
1,2,3,4,5,6-hexaethynylbenzene
hexakis(1-{2-[(trimethylsilyl)ethynyl]naphthyl}ethynyl)benzene
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In tetrahydrofuran at 45 - 85℃; for 120h; Sonogashira Cross-Coupling; Inert atmosphere; | 92.3 mg |
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