As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c
Cas:591-50-4
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/2036.html Product Name Iodobenzene CAS No.
Items Standard Result Appearance Colorless or pale yellow liquid Pale yellow liquid Assay 99%
Cas:591-50-4
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Iodobenzene Basic information Product Name: Iodobenzene Synonyms: IODOBENZENE;AKOS BBS-00004395;Benzene iodide;Benzene,iodo-;benzeneiodide;iodinebenzol;iodo-benzen;Phenyl iodide
Cas:591-50-4
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:591-50-4
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:591-50-4
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Iodobenzene CAS No.: 591-50-4 Molecular Formula:C6H5I Molecular Weight:204.01 Appearance: Colorless or light yellow transparent liquid Specification: GC>99.5%,Impurity max<0.2% Melting point: -29℃ Packaging:25kg/drum Capacity
We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:591-50-4
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Iodobenzene CAS:591-50-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
Cas:591-50-4
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Cas:591-50-4
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:591-50-4
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Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:591-50-4
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:591-50-4
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inquirySuperior quality Appearance:CLEAR YELLOW LIQUID Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:suzuki reaction Transportation:as per your request
Conditions | Yield |
---|---|
With cobalt(III) acetate; trifluoroacetic acid; potassium iodide In water at 25℃; for 0.00333333h; Mn(OAc)3 or (NH4)2Ce(SO4)3 instead Co(OAc)3; object of study: oxidative iodination promoted by Co(III), Ni(III) or Ce(IV); | 100% |
With cobalt(III) acetate; trifluoroacetic acid In water at 25℃; for 0.00333333h; | 100% |
With iodine; silver trifluoromethanesulfonate In dichloromethane at 20℃; | 100% |
Conditions | Yield |
---|---|
With copper(l) iodide; potassium iodide at 200℃; for 5h; Finkelstein reaction; Inert atmosphere; | 100% |
With aluminum oxide; copper(l) iodide In neat (no solvent) at 150℃; for 27h; Product distribution; different substrates, reagents, solvents and reaction times and temperature; | 94% |
With aluminum oxide; copper(l) iodide In neat (no solvent) at 150℃; for 27h; | 94% |
Conditions | Yield |
---|---|
In water Product distribution; Mechanism; Irradiation; laser flash photolyses, λ: 355 nm; | 100% |
Conditions | Yield |
---|---|
In dichloromethane 1) 0 deg C, 2 h, 2) 20 deg C, 1 h; | A n/a B 100% C 87% |
(Z)-4-methyl-2-pentene
iodosylbenzene
A
iodobenzene
B
(2S,3S)-2-Isopropyl-3-methyl-oxirane
Conditions | Yield |
---|---|
iron 5(pentafluorophenyl)-10,15,20-tris(2,6-dichloropheny.. In dichloromethane Oxidation; iron 5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphyrin was used as catalyst; | A n/a B 100% |
5,10,15,20-tetrakis(2,3,4,5,6-pentafluorophenyl)porphyrin iron(II) In dichloromethane Oxidation; | A n/a B 100% |
iron 5,10,15,20-tetrakis-(2',6'-dichlorophenyl)porphyrinate In dichloromethane Oxidation; | A n/a B 54% |
iron 5(pentafluorophenyl)-10,15,20-tris(2,6-dichloropheny.. In dichloromethane Oxidation; iron 5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphyrin fixed on silica was used as catalyst; | A n/a B 33% |
(E)-4-methylpent-2-ene
iodosylbenzene
A
2.3-Epoxy-4-methylpentan
B
iodobenzene
Conditions | Yield |
---|---|
5,10,15,20-tetrakis(2,3,4,5,6-pentafluorophenyl)porphyrin iron(II) In dichloromethane Oxidation; | A 100% B n/a |
iron 5,10,15,20-tetrakis-(2',6'-dichlorophenyl)porphyrinate In dichloromethane Oxidation; | A 96% B n/a |
iron 5(pentafluorophenyl)-10,15,20-tris(2,6-dichloropheny.. In dichloromethane Oxidation; iron 5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphyrin fixed on silica was used as catalyst; | A 60% B n/a |
iron 5(pentafluorophenyl)-10,15,20-tris(2,6-dichloropheny.. In dichloromethane Oxidation; iron 5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphyrin was used as catalyst; | A 60% B n/a |
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In dichloromethane at 20℃; for 10h; Elimination; | A 94% B 100% |
2,2-dimethyl-5-(phenyl-λ3-iodaneylidene)-1,3-dioxane-4,6-dione
A
cycl-isopropylidene malonate
B
iodobenzene
C
acetone
Conditions | Yield |
---|---|
With dirhodium tetraacetate In dichloromethane at 20℃; Product distribution; | A 33% B 100% C 5% |
tetrabutylammonium trifluoromethylsulfonate
A
iodobenzene
B
(R)-4-methylcycloheptanone
Conditions | Yield |
---|---|
Stage #1: tetrabutylammonium trifluoromethylsulfonate; (R)-4-methylcyclohexylidenemethyl(phenyl)iodonium tetrafluoroborate In chloroform at 60℃; Stage #2: With sulfuric acid In methanol; water at 60℃; for 9h; | A 100% B n/a C n/a |
A
iodobenzene
Conditions | Yield |
---|---|
With tetrabutylammonium trifluoromethylsulfonate In chloroform at 60℃; | A 100% B 34% C 63% |
diphenyliodonium bromide
A
iodobenzene
B
biphenyl
D
bromo(phenyl)mercury
E
benzene
Conditions | Yield |
---|---|
In acetonitrile Kinetics; byproducts: C6H5Br; at different temp. between 20-70°C; UV; yields for 45°C; | A 100% B 6-7 C n/a D n/a E 1.4% |
diphenyliodonium chloride
A
iodobenzene
C
biphenyl
D
phenylmercury(II) chloride
E
benzene
Conditions | Yield |
---|---|
In acetonitrile Kinetics; at different temp. between 20-70°C; UV; yields for 45°C; | A 100% B 10-11 C 4-5 D 89-92 E 1.4% |
copper
A
fluorobenzene
B
iodobenzene
C
biphenyl
D
copper(I) tetrafluoroborate
E
benzene
Conditions | Yield |
---|---|
In acetonitrile Kinetics; stirred at 20-70°C; GLC; | A <1 B 100% C 95% D 99% E 5% |
m-carboran-9-yl(phenyl)iodonium tetrafluoroborate
sodium chloride
A
iodobenzene
B
9-chloro-m-carborane
Conditions | Yield |
---|---|
In chloroform; water mixt. of aryl(m-carboran-9-yl)iodonium tetrafluoroborate, NaF, water and chloroform was vigorously stirred under reflux at 56°C, 1 h; internal standard (chlorobenzene) added and org. layer was analysed by GLC; | A 100% B 100% |
triphenylphosphinediiodogermylene
phenyllithium
A
iodobenzene
B
biphenyl
C
triphenylgermane
D
tetraphenylgermane
E
triphenylphosphine
Conditions | Yield |
---|---|
In diethyl ether under N2, to suspn. of Ph3PGeI2 in ether PhLi added dropwise (1:4 molarratio), stirred for 5 d under reflux, hydrolyzed; dried, analyzed by gas chromy.; | A 10% B 13% C 39% D 36% E 100% |
In diethyl ether under N2, to suspn. of Ph3PGeI2 in ether PhLi added dropwise (1:1 molarratio), stirred for 5 d under reflux, hydrolyzed; dried, analyzed by gas chromy.; | A 2.9% B 2.9% C 1.9% D 14% E 82% |
In diethyl ether under N2, to suspn. of Ph3PGeI2 in ether PhLi added dropwise (1:2 molarratio), stirred for 5 d under reflux, hydrolyzed; dried, analyzed by gas chromy.; | A 7.7% B 9.6% C 1.3% D 19% E 79% |
Conditions | Yield |
---|---|
In acetonitrile soln. of iodine addn. to soln. of Tl-compd., mixing, standing (dark, 220h, room temperature), evacuation (under Ar, room temperature, then wate r bath, distillation of I-compd.), product remaining in solid residue; | A 99% B 100% |
phenyl(p-carboran-2-yl)iodonium tetrafluoroborate
A
iodobenzene
B
2-iodo-closo-1,12-dodecaborane
C
2-fluoro-p-caborane
D
benzene
Conditions | Yield |
---|---|
In dichloromethane; water 25°C, 0.6 h; | A 99% B 0% C 99.5% D <0.5 |
phenyl(p-carboran-2-yl)iodonium tetrafluoroborate
A
iodobenzene
B
2-fluoro-p-caborane
C
(Dichloroiodo)benzene
Conditions | Yield |
---|---|
With sodium fluoride In dichloromethane; water mixt. of iodonium salt, NaF, H2O and CH2Cl2 stirred at 25°C for 35 min; org. phase sepd. off, filtered through a short alumina plug and evapd., the residue is a mixt. of C6H5I and 2-fluoro-p-carborane; solid dissolved in dry CCl4; soln. satd. with Cl2 at 5°C, and then evapd., to give the mixt. of C6H3Cl2I and the fluorocarborane; the latter extd. with pentane, filtered through an alumina plug, evapd. to dryness, vac. sublimation; elem. anal.; | A n/a B 99.5% C 70% |
phenylthalium(III) di(trifluoroacetate)
iodobenzene
Conditions | Yield |
---|---|
With iodine In acetonitrile for 220h; Ambient temperature; | 99.4% |
dimethylsulfide
benzene
A
iodobenzene
B
methoxydimethylsulfonium tosylate
Conditions | Yield |
---|---|
In dichloromethane for 0.25h; | A n/a B 99% |
3,3-diethyl-1-phenyltriaz-1-ene
iodobenzene
Conditions | Yield |
---|---|
With cation exchange resin BioRad AG 50W-X12 (H+); sodium iodide In acetonitrile at 75℃; Product distribution; further solvent: THF, DMSO; | 99% |
With chloro-trimethyl-silane; sodium iodide In acetonitrile at 60℃; for 0.0833333h; | 65% |
With diiodomethane; isopentyl nitrite 1.) room temperature, 30 min, 2.) 80 deg C, 4 h; |
(4-bromophenyl)thioanisole
benzene
A
iodobenzene
B
C8H10BrOS(1+)*C7H7O3S(1-)
Conditions | Yield |
---|---|
In dichloromethane for 0.25h; | A n/a B 99% |
dibenzyl sulfide
benzene
A
iodobenzene
B
C15H17OS(1+)*C7H7O3S(1-)
Conditions | Yield |
---|---|
In dichloromethane for 0.25h; | A n/a B 99% |
Conditions | Yield |
---|---|
In chloroform; water at 20℃; for 64h; | A n/a B 99% |
In chloroform; water at 56℃; for 2.5h; Product distribution; other temperatures, other reaction time; | A 99 % Chromat. B 97% |
phenyl(p-carboran-2-yl)iodonium tetrafluoroborate
A
iodobenzene
B
2-iodo-closo-1,12-dodecaborane
C
2-fluoro-p-caborane
D
benzene
Conditions | Yield |
---|---|
In dichloromethane; water at 25°C, 0.5 h; | A 95% B <1 C 99% D <0.5 |
{3-(p-tolylthio)propyl}triphenyltin
A
iodobenzene
B
(C6H5)2SnI(CH2)3SC6H4CH3
Conditions | Yield |
---|---|
With iodine In tetrachloromethane Kinetics; to soln. of Sn compd. I2 added dropwise, soln. left until become colourless; | A 99% B n/a |
Conditions | Yield |
---|---|
With iodine In tetrachloromethane Kinetics; to soln. of Sn compd. I2 added dropwise, soln. left until become colourless; | A 99% B n/a |
iodine
A
iodobenzene
B
1,16-diiodo-1,16-diphenyl-3,3,14,14,18,18,29,29-octamethyl-3,14,18,29-tetrasila-1,16-distanna-[5,5]-ferrocenophane
Conditions | Yield |
---|---|
In dichloromethane under N2atm. i2 was added to soln. fc(SiMe2CH2SnPh2CH2SiMe2)2fc in CH2Cl2, react. mixt. was stirred overnight; solvent and iodobenzene were removed in vacuo, residue was recrystd. from hexane; elem. anal.; | A n/a B 99% |
Conditions | Yield |
---|---|
With iodine In chloroform Ambient temperature; | 98% |
With iodine In chloroform Product distribution; Ambient temperature; further regents, further products; | 98% |
With hydrogen bromide at 0℃; for 0.333333h; Yield given; |
1-cyclohexyl-2-phenylcyclopropane
A
iodobenzene
B
2-cyclohexyl-1-(4-iodophenyl)-cyclopropane
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; iodine In chloroform; trifluoroacetic acid at -30℃; for 8h; | A n/a B 98% |
Conditions | Yield |
---|---|
With [Pd{C6H4(CH2N(CH2Ph)2)}(μ-Br)]2; potassium carbonate In 1-methyl-pyrrolidin-2-one at 130℃; for 2h; Microwave irradiation; | 100% |
With sodium tetraphenyl borate; sodium carbonate In 1-methyl-pyrrolidin-2-one at 130℃; for 4h; Suzuki coupling; Inert atmosphere; | 99% |
With potassium carbonate In ethanol; water at 80℃; for 4h; Reagent/catalyst; Solvent; Ullmann Condensation; Green chemistry; | 99.2% |
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hypochlorite In water at 20℃; for 0.0833333h; | 100% |
With hydrogenchloride; sodium hypochlorite at 15℃; for 0.0833333h; | 99% |
With chlorine In dichloromethane at 20℃; | 98% |
Conditions | Yield |
---|---|
With tetrabutoxytitanium; diisobutylaluminium hydride In diethyl ether for 6h; Heating; | 100% |
With sodium hydroxide; ethanol; PdCl2-poly(N-vinyl-2-pyrrolidone); palladium dichloride at 65℃; under 760 Torr; for 1h; | 100% |
With potassium tert-butylate; benzaldehyde In N,N-dimethyl-formamide at 90℃; for 1h; Schlenk technique; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 5h; Sonogashira coupling; Inert atmosphere; | 100% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 12h; Inert atmosphere; | 100% |
Stage #1: iodobenzene With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 0.166667h; Inert atmosphere; Stage #2: propargyl alcohol Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With acetamide; potassium phosphate; CuI In dodecane; ethyl acetate; toluene | 100% |
With potassium phosphate; copper(l) iodide; L-arginine In 1,4-dioxane at 100℃; for 24h; Goldberg reaction; | 99% |
With aluminum oxide; potassium fluoride; copper(l) iodide; 1,10-Phenanthroline In toluene at 110℃; for 5h; | 97% |
Conditions | Yield |
---|---|
With triethylamine In 1-butyl-3-methylimidazolium methyl phosphonate at 110℃; for 5h; Heck Reaction; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 5h; Heck reaction; | 100% |
With triethylamine In dimethyl sulfoxide at 120℃; for 12h; Heck reaction; | 100% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; triethylamine; Pd-PVP at 90℃; for 3h; | 100% |
With tetrabutyl-ammonium chloride; triethylamine; [Pd[P(O)(OPh)2]2]n at 90℃; under 3800 Torr; for 3h; | 100% |
With 1-n-butyl-4-methylpyridinium chloride; triethylamine; PdCl2{P(OC6H5)3}2 at 90℃; under 3800 Torr; for 3h; Product distribution; Further Variations:; Catalysts; Reagents; | 100% |
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In tetrahydrofuran at 20℃; for 12h; Inert atmosphere; | 100% |
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In tetrahydrofuran at 20℃; for 12h; | 100% |
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In tetrahydrofuran at 20℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With tributyl-amine; [bmim]PF6; palladium diacetate; silica gel at 100℃; for 4h; Mizoroki-Heck reaction; | 100% |
With triethylamine; Pd(OAc)2 in [bmim]PF6 layer in silica pores In dodecane at 150℃; for 15.5h; Mizoroki-Heck reaction; | 99% |
With tributyl-amine; montmorilloniteethylsilyldiphenylphosphine palladium(II) chloride at 100℃; for 6h; | 94% |
Conditions | Yield |
---|---|
tetrakis(triphenylphosphine) palladium(0) In toluene Heating; | 100% |
Conditions | Yield |
---|---|
tetrakis(triphenylphosphine) palladium(0) at 80℃; for 4h; | 100% |
Conditions | Yield |
---|---|
With sulfur; potassium fluoride; copper(II) ferrite; caesium carbonate at 120℃; for 20.5h; Catalytic behavior; Reagent/catalyst; Temperature; | 100% |
With potassium carbonate; thiourea In ethanol for 0.25h; Catalytic behavior; Solvent; Reagent/catalyst; Temperature; Reflux; | 100% |
With potassium phosphate; copper(l) iodide; potassium thioacyanate In PEG-400 at 150℃; for 20h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 100℃; for 18h; Heck reaction; | 100% |
With tetrabutyl-ammonium chloride; sodium hydrogencarbonate; palladium diacetate In N,N-dimethyl-formamide at 25℃; for 48h; | 98% |
With triphenylphosphine on reverse phase silica; triethylamine; Pd(OAc)2 on reverse phase silica In methanol; water Addition; Heck reaction; | 97% |
Conditions | Yield |
---|---|
With C33H33N2(1+)*Cl(1-); palladium diacetate; potassium carbonate In water; N,N-dimethyl-formamide for 2h; Heck Reaction; Inert atmosphere; Sealed tube; Heating; | 100% |
With sodium acetate; aluminum oxide; ruthenium In N,N-dimethyl-formamide at 115℃; for 12h; Heck-type olefination; | 99% |
With triethylamine In d7-N,N-dimethylformamide at 120℃; for 1h; Heck Reaction; | 99% |
Conditions | Yield |
---|---|
ς4,λ5-phosphinine palladium In 1-methyl-pyrrolidin-2-one at 100℃; for 120h; Heck reaction; | 100% |
With palladium diacetate; 15-crown-15 tagged triarylphoshine; triethylamine In tetrahydrofuran for 8h; Heck reaction; Heating; | 100% |
With triethylamine; polymer(fiber)-supported palladium In 1,4-dioxane at 100℃; for 1h; Heck reaction; | 100% |
Conditions | Yield |
---|---|
palladium/alumina for 0.166667h; Product distribution / selectivity; | 100% |
With hollow carbonnanonets supported palladium nanoparticles; potassium carbonate In N,N-dimethyl-formamide at 120℃; for 0.5h; Heck Reaction; | 100% |
With triethylamine at 145℃; for 3h; Catalytic behavior; Heck Reaction; | 100% |
Conditions | Yield |
---|---|
With triethylamine; bis(tert-butylaminophosphine)palladium(II) at 80℃; for 0.25h; Sonogashira cross-coupling reaction; | 100% |
With copper(l) iodide; diisopropylamine; triphenylphosphine; silica gel; palladium at 85℃; for 18h; Sonogashira coupling; | 100% |
With triethylamine; [Pd{t-Bu2PCH2N(CH2Ph)CH2Pt-Bu2}(OAc)2] at 80℃; for 0.25h; Sonogashira coupling; | 100% |
Conditions | Yield |
---|---|
With C11H14Cl2N6O2Pd; triethylamine In 1,4-dioxane at 100℃; under 2280.15 Torr; for 6h; Reagent/catalyst; | 100% |
With triethylamine In N,N-dimethyl-formamide at 100℃; under 750.075 Torr; for 4h; Catalytic behavior; Pressure; Reagent/catalyst; Schlenk technique; Inert atmosphere; | 99% |
With triethylamine In toluene at 100℃; under 3750.38 Torr; for 8h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
at 230 - 270℃; for 8h; Mechanism; other aryl iodides; | 100% |
at 230 - 270℃; for 8h; | 100% |
With caesium carbonate In dimethyl sulfoxide at 100℃; for 24h; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With tributyl-amine; tetra-(n-butyl)ammonium iodide; trifluoroacetic acid; bis(triphenylphosphine) palladium (Il) acetate In N,N-dimethyl-formamide at 70℃; | 100% |
With triethylamine; palladium diacetate In carbon dioxide at 80℃; under 75006 Torr; for 60h; Arylation; Hydroarylation; | 88% |
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine for 16h; Sonogashira Cross-Coupling; Reflux; Inert atmosphere; Schlenk technique; | 100% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 10h; Inert atmosphere; | 99% |
With copper(l) iodide; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp In N,N-dimethyl-formamide at 100℃; Sonogashira reaction; | 97% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; potassium acetate; Pd(0)-ferrocenyl In N,N-dimethyl-formamide at 60℃; for 2.5h; | 100% |
With palladium nanoparticles on graphene; triethylamine In N,N-dimethyl-formamide at 120 - 125℃; for 2h; Heck Reaction; | 100% |
With triethylamine; silica aerogel nanocomposite; palladium In acetonitrile for 8h; Mizoroki-Heck reaction; Heating; | 99% |
Conditions | Yield |
---|---|
With copper(I) oxide; caesium carbonate; hydroxybenzaldoxime; 3 A molecular sieve In acetonitrile at 82℃; for 24h; Ullmann-type coupling; | 100% |
With caesium carbonate; copper(I) oxide; trans-N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine In acetonitrile at 82℃; for 24h; Conversion of starting material; activated 3 A molecular sieve (KnNa12-n[(AlO2)12(SiO2)12]); | 100% |
Stage #1: phenol With caesium carbonate; copper(I) oxide; trans-N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine at 100℃; Molecular sieve 3 Å; Stage #2: iodobenzene In acetonitrile at 82℃; for 24h; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate; copper-palladium In N,N-dimethyl-formamide at 110℃; Kinetics; Product distribution; Further Variations:; Catalysts; Reaction partners; Suzuki cross-coupling; | 100% |
With sodium hydroxide; Pd-dodecanethiolate nanoparticles In tetrahydrofuran at 20℃; for 24h; Suzuki-Miyaura cross-coupling; | 100% |
With sodium carbonate; 1-butyl-3-methylimidazolium Tetrafluoroborate; 2C10H15N2(1+)*Cl4Pd(2-) In water at 110℃; for 12h; Conversion of starting material; Suzuki Coupling; | 100% |
Conditions | Yield |
---|---|
With triethylamine; PdCl2(4,4'-bis(n-C10F21CH2OCH2)-2,2'-bpy) In N,N-dimethyl-formamide at 140℃; for 3h; Heck reaction; | 100% |
With potassium carbonate; palladium dichloride In water at 20 - 100℃; Heck reaction; Inert atmosphere; | 99% |
With potassium hydroxide In water at 90℃; for 5h; Mizoroki-Heck reaction; | 99% |
Conditions | Yield |
---|---|
With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide In tetrahydrofuran Phenylation; Sonogashira coupling; Heating; | 100% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 2h; | 96% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine In tetrahydrofuran at 20℃; for 24h; | 94% |
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