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Cas:60-35-5
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Good quality Competitive price First-class service Acetamide Basic information Product Name: Acetamide Synonyms: ACETAMIDE;ACETIC ACID AMIDE;AMIDE C2;LABOTEST-BB LT00795814;ETHANAMIDE;Acetamid;A
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inquiryProduct Name:Acetamide CAS:60-35-5 Molecular Formula:C2H5NO Molecular Weight:59.07 EINECS:200-473-5 Purity:99% Appearance: White Powder Storage:Store in cool and dry place, away from sun light. Package: 25 KG/Woven Bag Or Fiber Dr
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inquiry1.Prompt Goods; 2.Flexible payment terms; 3.Documents & Certificate support. Name: Acetamide Structure: Formula: C2H5NO Molecular Weight : 59.07 Synonyms: ACETAMIDE;ACETIC ACID AMIDE;Acetamidum;AMIDE C2;Acetamid;Acetamid(trigonaleForm);ac
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Cas:60-35-5
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inquirymoderate price & quick delivery Appearance:colourless deliquescent crystals Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Acetamide is ofte
Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Product name: Acetamide CAS No.:60-35-5 Molecule Formula:C2H5NO Molecule Weight:59.07 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS SPECIFICATION
Cas:60-35-5
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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Acetamide Chemical Properties Melting point 78-80 °C(lit.) Boiling point 221 °C(lit.) density 1.159 vapor pressure 1 mm Hg ( 65 °C) refractive index 1.4274 Fp 220-222°C storage temp. Store at RT solubility
Conditions | Yield |
---|---|
With manganese(IV) oxide; water In isopropyl alcohol at 70℃; under 5171.62 Torr; for 0.25h; | 99% |
With C43H42Cl2NRu; water at 20℃; for 4h; Catalytic behavior; | 99% |
With (PN3P)Ni(OH); water In tetrahydrofuran at 100℃; for 24h; Mechanism; Inert atmosphere; Schlenk technique; Sealed tube; | 99% |
Conditions | Yield |
---|---|
With ethyl hydrazine hydrochloride In methanol at 10 - 20℃; for 2h; Temperature; | A 98.9% B 98.29% |
acetamide
Conditions | Yield |
---|---|
With sodium at 90℃; under 15001.5 Torr; for 6h; Reagent/catalyst; Temperature; Pressure; Time; Autoclave; | 98.5% |
Conditions | Yield |
---|---|
With ammonium hydroxide at 36℃; under 525.053 Torr; for 8h; Temperature; Pressure; | 98% |
With ammonia; water |
Conditions | Yield |
---|---|
With Candida antarctica lipase B; ammonium carbamate In various solvent(s) at 35℃; for 72h; Substitution; | 98% |
With ammonia; zirconium(IV) oxide In benzene at 150℃; | 97% |
With ammonium hydroxide; tin(IV) oxide at 200℃; | 3% |
Conditions | Yield |
---|---|
With bismuth(III) nitrate In acetonitrile for 0.166667h; Heating; | 97% |
With tetrabutylammonium periodite In dichloromethane at 20℃; for 0.0333333h; | 96% |
With Oxone for 0.0833333h; | 95% |
Conditions | Yield |
---|---|
With borohydride exchange resin; nickel diacetate In methanol for 1h; Ambient temperature; | 97% |
acetamide
Conditions | Yield |
---|---|
With sodium at 140℃; for 5h; Autoclave; | 96.2% |
acetamide
Conditions | Yield |
---|---|
With sodium at 140℃; for 4h; Autoclave; | 95.6% |
N-(tert-butoxycarbonyl)acetamide
acetamide
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane for 1h; Ambient temperature; | 95% |
tris(2-acetoxyethyl)methane
A
acetamide
B
3-(2-hydroxyethyl)pentane-1,5-diol
Conditions | Yield |
---|---|
Stage #1: tris(2-acetoxyethyl)methane With ammonia In methanol at 80℃; for 96h; Stage #2: With ammonia at 80℃; for 24h; | A n/a B 92.1% |
Conditions | Yield |
---|---|
With [RuCl2(η2-C6H6){P(NMe2)3}]; water at 100℃; for 7h; Inert atmosphere; Sealed tube; | 92% |
With nickel at 100℃; | |
bei der Belichtung; | |
With (ethylenediamine)palladium(II) dinitrate; water at 80℃; Inert atmosphere; |
2,4,6-trimethyl-2-(2,4-dimethoxyphenyl)-1,2-dihydro-1,3,5-triazine
A
acetamide
B
N-acetylacetamide
C
2',4'-dimethoxyacetophenone
Conditions | Yield |
---|---|
With sodium carbonate In water for 1.5h; Heating; | A 2.5% B 5% C 91% |
Conditions | Yield |
---|---|
With sodium hydroxide; sodium tetrahydroborate In water for 4h; Product distribution; pH=10.8-11.0; | A n/a B 90% |
2-methyl-1H-indole
(2-nitroethenyl)benzene
A
acetamide
B
3-phenyl-1H-quinolin-2-one
Conditions | Yield |
---|---|
With polyphosphoric acid at 80 - 100℃; for 1.5h; | A n/a B 90% |
Conditions | Yield |
---|---|
In acetone at 20℃; for 2h; Inert atmosphere; Schlenk technique; | A 87% B 90% |
Conditions | Yield |
---|---|
With indium(III) nitrate at 100℃; for 18h; | A n/a B 89% |
2-methyl-1H-indole
1-isopropyl-4-(2-nitrovinyl)benzene
A
acetamide
B
3-(4-isopropylphenyl)quinolin-2(1H)-one
Conditions | Yield |
---|---|
With polyphosphoric acid at 80 - 100℃; for 1.5h; | A n/a B 89% |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; methanesulfonyl chloride In neat (no solvent) at 70℃; for 4h; | 88% |
With hydroxylamine hydrochloride; C27H27ClIrNO; sodium hydrogencarbonate In dimethyl sulfoxide at 50℃; for 6h; | 88% |
With [Ru(L1)Cl(CO)(PPh3)2]; hydroxylamine hydrochloride; sodium hydrogencarbonate In toluene for 12h; Catalytic behavior; Inert atmosphere; Reflux; | 78% |
2-methyl-1H-indole
1,2-dimethyl-4-(2-nitrovinyl)benzene
A
acetamide
B
3-(3,4-dimethylphenyl)quinolin-2(1H)-one
Conditions | Yield |
---|---|
With polyphosphoric acid at 80 - 100℃; for 1.5h; | A n/a B 88% |
2-methyl-1H-indole
1,2-dichloro-4-(2-nitrovinyl)benzene
A
acetamide
B
3-(3,4-dichloro-phenyl)quinolin-2(1H)-one
Conditions | Yield |
---|---|
With polyphosphoric acid at 80 - 100℃; for 1.5h; | A n/a B 88% |
N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(3,4-dimethoxybenzylidene)rhodanine
A
acetamide
B
N-β-D-glucopyranosylthiourea
Conditions | Yield |
---|---|
With ammonia In methanol Ambient temperature; | A n/a B 87% C n/a |
A
acetamide
B
5-ethoxycarbonyl-6-methyl-3-acetyl-4-phenyl-3,4-dihydropyrimidin-2(1H)-one
Conditions | Yield |
---|---|
With ammonia In tetrahydrofuran at 20℃; | A 78% B 86% |
Conditions | Yield |
---|---|
With ammonium bromide In water for 15h; Electrochemical reaction; | 86% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; ammonium hydroxide In water at 100℃; for 16h; | 85% |
1,2-dimethylindole
(2-nitroethenyl)benzene
A
acetamide
B
1-methyl-3-phenyl-1H-quinolin-2-one
Conditions | Yield |
---|---|
With polyphosphoric acid at 130℃; | A n/a B 84% |
Conditions | Yield |
---|---|
With ammonium formate; acetic acid; palladium hydroxide on carbon for 1.4h; Product distribution / selectivity; Heating / reflux; | A n/a B 83.2% |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol; acetic acid under 2585.7 Torr; Product distribution; various phenylhydrazides, hydrogenolytic cleavage; | A 82% B n/a |
With hydrogen; palladium In ethanol; acetic acid under 2585.7 Torr; | A 82% B n/a |
With titanium tetrachloride; magnesium In diethyl ether; dichloromethane at 20℃; Inert atmosphere; | A 63% B 74% |
Conditions | Yield |
---|---|
In water; acetone for 18h; Heating / reflux; | 100% |
In water | |
In acetone for 18h; Reflux; |
Conditions | Yield |
---|---|
With acetamide; potassium phosphate; CuI In dodecane; ethyl acetate; toluene | 100% |
With potassium phosphate; copper(l) iodide; L-arginine In 1,4-dioxane at 100℃; for 24h; Goldberg reaction; | 99% |
With aluminum oxide; potassium fluoride; copper(l) iodide; 1,10-Phenanthroline In toluene at 110℃; for 5h; | 97% |
acetamide
1-bromo-3,5,7-trimethyladamantane
N-acetyl-3,5,7-trimethyl-1-aminoadamantane
Conditions | Yield |
---|---|
Heating; | 100% |
Conditions | Yield |
---|---|
In acetone for 20h; Heating; | 100% |
In acetone |
acetamide
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 2h; | 100% |
acetamide
3-Hydroxy-2-thiophen-3-ylmethyl-2,3-dihydro-isoindol-1-one
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 48h; Heating; | 100% |
acetamide
3-Hydroxy-2-thiophen-2-ylmethyl-2,3-dihydro-isoindol-1-one
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 48h; Heating; | 100% |
Conditions | Yield |
---|---|
With aluminum oxide In water for 0.2h; Condensation; microwave irradiation; | 100% |
acetamide
1,3-dibromo-5-fluorobenzene
N-(3-bromo-5-fluorophenyl)acetamide
Conditions | Yield |
---|---|
With caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium(0) In 1,4-dioxane at 80℃; Inert atmosphere; | 100% |
With copper(l) iodide; (S,S)-1,2-diaminocyclohexane; potassium carbonate In toluene at 130℃; for 18h; | 76% |
With caesium carbonate; palladium diacetate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 105℃; | 44% |
acetamide
4,5-diethyl-2,5-dihydro-1,2,2,3-tetramethyl-1H-1,2,5-azasilaborole
A
ethylbis(dimethyl(2-penten-2-yl)silyloxy)borane
B
methylamine
Conditions | Yield |
---|---|
In 1,2,5-trimethyl-benzene dropwise addn. of acetamide to boron compd. soln., 160°C, 3.5h; heating (reflux), 10h; evapn.; all under Ar; distn.; elem. anal.; | A 100% B 98% |
acetamide
2,3-pyrazinedicarboxylic anhydride
N-acetylpyrazine-2-carboxamide
Conditions | Yield |
---|---|
for 4h; Reflux; | 100% |
Conditions | Yield |
---|---|
at 90℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With Iron(III) nitrate nonahydrate In toluene for 24h; Reflux; | 100% |
acetamide
Conditions | Yield |
---|---|
Stage #1: acetamide; (R)-5-chloro-3-(4-(methoxymethyl)-6-(3-methoxytetrahydrofuran-3-yl)pyridin-2-yl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazolo[3,4-c]pyridine With caesium carbonate In dimethyl amine for 0.5h; Stage #2: With [(2-di-cyclohexylphosphino-3,6-dimethoxy-2’,4’,6’-triisopropyl-1,1‘-biphenyl)-2-(2‘-amino-1,1’-biphenyl)]palladium(II) methanesulfonate at 120℃; for 0.666667h; | 100% |
Conditions | Yield |
---|---|
With C33H37N4P; potassium carbonate; bis(dibenzylideneacetone)-palladium(0) In tert-butyl alcohol at 95℃; for 5h; Inert atmosphere; Sonication; | 99.3% |
With 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; potassium carbonate In 1,4-dioxane at 90℃; for 18h; Buchwald-Hartwig Coupling; Inert atmosphere; Glovebox; | 83% |
With potassium phosphate; 2-Phenyl-1,3,2-dioxaborinane In 1,4-dioxane at 115℃; for 30h; Inert atmosphere; | 28% |
With C33H37N4P; potassium carbonate; bis(dibenzylideneacetone)-palladium(0) In tert-butyl alcohol at 95℃; for 5h; Inert atmosphere; Sonication; |
Conditions | Yield |
---|---|
With C33H37N4P; potassium carbonate; bis(dibenzylideneacetone)-palladium(0) In tert-butyl alcohol at 95℃; for 18h; Catalytic behavior; Solvent; Temperature; Reagent/catalyst; Time; Inert atmosphere; Sonication; | 99.1% |
With 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; potassium carbonate In 1,4-dioxane at 90℃; for 18h; Buchwald-Hartwig Coupling; Inert atmosphere; Glovebox; | 80% |
With potassium phosphate; copper(l) iodide In N,N-dimethyl-formamide at 120℃; for 48h; Ullmann condensation; | 33% |
With copper(l) iodide; potassium carbonate; pipecolic Acid In N,N-dimethyl-formamide at 110℃; for 30h; Goldberg coupling reaction; | 24% |
With C33H37N4P; potassium carbonate; bis(dibenzylideneacetone)-palladium(0) In tert-butyl alcohol at 95℃; for 18h; Catalytic behavior; Reagent/catalyst; Solvent; Inert atmosphere; Sonication; |
acetamide
3-phenyl-propionaldehyde
N-(1-acetylamino-3-phenylpropyl)acetamide
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane for 2h; Heating; | 99% |
With toluene-4-sulfonic acid at 100℃; for 1h; Neat (no solvent); | 99% |
With toluene-4-sulfonic acid at 100℃; for 0.0166667h; Microwave irradiation; neat (no solvent); | 98% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane for 4h; Heating; | 99% |
With acetic acid | |
With benzene Entfernen des entstehenden Wassers; | |
at 80 - 100℃; | |
With carbon monoxide; hydrogen; dicobalt octacarbonyl In ethyl acetate at 90 - 100℃; |
Conditions | Yield |
---|---|
With nanosized zeolite beta In neat (no solvent) at 100℃; for 24h; | 99% |
With [Ru-NHC] In toluene at 110℃; for 8h; Inert atmosphere; Schlenk technique; Sealed tube; | 98% |
With H-β-zeolite In neat (no solvent) at 130℃; for 24h; Reagent/catalyst; Green chemistry; | 97% |
Conditions | Yield |
---|---|
With sulfuric acid; lithium bromide; bis(triphenylphosphine)palladium dibromide In various solvent(s) at 120℃; under 45003.6 Torr; for 12h; | 99% |
With 1-methyl-pyrrolidin-2-one; sulfuric acid; lithium bromide; palladium on activated charcoal at 100℃; under 45003.6 Torr; for 12h; | 75% |
With sulfuric acid; triphenylphosphine; lithium bromide; palladium on activated charcoal In 1-methyl-pyrrolidin-2-one; toluene at 90℃; under 45003.6 Torr; for 16h; | 64.4% |
With 3-ethyl-1-methyl-1H-imidazol-3-ium bromide; triphenylphosphine; palladium(II) bromide at 100℃; under 45004.5 Torr; for 15h; | 63% |
With hydrogenchloride; potassium tetrachloroplatinate; triphenylphosphine In 1,4-dioxane at 120℃; under 45600 Torr; for 15h; | 44% |
Conditions | Yield |
---|---|
In tetrahydrofuran; toluene at 80℃; Inert atmosphere; | 99% |
In toluene at 60 - 80℃; for 62h; Solvent; Temperature; | 87% |
With acetic acid In n-heptane; Isopropyl acetate; toluene at 55 - 60℃; for 1h; | 85% |
acetamide
bis(trimethylsilyl)sulphate
A
Hexamethyldisiloxane
C
acetonitrile
Conditions | Yield |
---|---|
Dehydration; sulfation; silylation; Heating; | A 69% B 5% C 94% D 99% |
Conditions | Yield |
---|---|
With aluminum oxide; potassium fluoride; copper(l) iodide; 1,10-Phenanthroline In toluene at 110℃; for 8h; | 99% |
With potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine In N,N-dimethyl-formamide at 80℃; for 23h; | 95% |
With aluminum oxide; potassium fluoride; copper(l) iodide; N,N'-Dibenzylethylenediamine In toluene at 110℃; for 3h; Ullmann reaction; Inert atmosphere; | 90% |
acetamide
Conditions | Yield |
---|---|
Stage #1: acetamide; (5-bromo-1-methyl-1H-indol-2-yl)-(4-fluoro-phenyl)-methanone With copper(l) iodide; phosphate potassium salt In 1,4-dioxane for 0.333333h; Argon atmosphere; Stage #2: With N,N`-dimethylethylenediamine In 1,4-dioxane at 110℃; | 99% |
Conditions | Yield |
---|---|
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) In tert-butyl alcohol at 110℃; for 4h; | 99% |
With 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; potassium carbonate In 1,4-dioxane at 90℃; for 18h; Buchwald-Hartwig Coupling; Inert atmosphere; Glovebox; | 82% |
Conditions | Yield |
---|---|
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) In tert-butyl alcohol at 110℃; for 24h; | 99% |
With 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; potassium carbonate In 1,4-dioxane at 90℃; for 18h; Buchwald-Hartwig Coupling; Inert atmosphere; Glovebox; | 92% |
With 2-di-tertbutylphosphino-3,4,5,6-tetramethyl-2',4',6'-triisopropyl-1,1'-biphenyl; potassium phosphate; water; palladium diacetate In tert-butyl alcohol at 110℃; for 3h; Inert atmosphere; | 84% |
With copper(I) oxide; potassium phosphate; N1,N2-bis(thiophen-2-ylmethyl)oxalamide In dimethyl sulfoxide at 120℃; for 24h; Inert atmosphere; Schlenk technique; | 50% |
Conditions | Yield |
---|---|
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) In tert-butyl alcohol at 110℃; for 12h; | 99% |
With copper(I) oxide; potassium phosphate; N1,N2-bis(thiophen-2-ylmethyl)oxalamide In tert-butyl alcohol at 130℃; for 24h; Schlenk technique; | 81% |
Stage #1: acetamide; para-chlorotoluene With copper(l) iodide; potassium carbonate; trans-N,N'-dimethylcyclohexane-1,2-diamine In acetonitrile for 0.00277778h; Inert atmosphere; Glovebox; Stage #2: In acetonitrile at 200℃; for 1h; Microwave irradiation; | 74% |
Conditions | Yield |
---|---|
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) In tert-butyl alcohol at 110℃; for 7h; | 99% |
With potassium phosphate; t-BuBrettPhos; water; palladium diacetate In tert-butyl alcohol at 110℃; for 3h; Inert atmosphere; | 91% |
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