hangzhou verychem science and technology co.ltd
Product name: Phenyl cyanide Cas No: 100-47-0 Assay: 99.5%min Commercial lots Hangzhou Verychem Science And Technology Co. Ltd. was set up in year 2004, it’s a young but fast growing
Cas:100-47-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryDayang Chem (Hangzhou) Co.,Ltd.
img heightAppearance:colourless oily liquid Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:100-47-0 Transportation:by air or by sea Port:Shanghai
Cas:100-47-0
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquirySimagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:100-47-0
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryJinan Finer Chemical Co., Ltd
Product description: Product name Benzonitrile CAS number 100-47-0 Assay ≥99% Appearance Colorless oily liquid Capacity 1000mt/year Application Pharmaceuticals/pesticideses i
Cas:100-47-0
Min.Order:1 Kilogram
FOB Price: $12.0
Type:Lab/Research institutions
inquiryHefei TNJ chemical industry co.,ltd
1,ISO Certificate 2,Factory price 3,Free sample and Fast delivery Appearance:Colorless transparent liquid Storage:All products should be stored at a dry and ventilated location away from fire and other dangerous goods, and should avoid direct sunl
Cas:100-47-0
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryHenan Allgreen Chemical Co.,Ltd
he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality se T rvice Appearance:White or
Ality Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Henan Tianfu Chemical Co., Ltd.
Our company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble metal catalysts, synthesis of electronic chemical materials and general chemicals Imp&Exp trading business. The company
Cas:100-47-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryAntimex Chemical Limied
ProName: Benzonitrile CasNo: 100-47-0 Molecular Formula: C7H5N Appearance: COLORLESS TRANSPARENT LIQUID Application: Used as pesticides, dye intermediates ... DeliveryTime: as the client like PackAge: 200kg drums or iso t
Cas:100-47-0
Min.Order:1 Metric Ton
FOB Price: $2.0
Type:Lab/Research institutions
inquiryHenan Sinotech Import&Export Corporation
Product Name: Benzonitrile Synonyms: Benzonitrile ReagentPlus(R), 99%;Benzonitrile, 99+%;Benzonitrile, 99%, J&KSeal;Benzonitrile, 99%, SuperDry, water≤30 ppm, J&KSeal;phenylcyanide,benzonitrile,c
Changchun Artel lmport and Export trade company
Superiority We can customize and synthesize products that other suppliers may not be able to provide. Advantage cof, mof ligand manufacturer Product Detail Quick Details Quick
Cas:100-47-0
Min.Order:100 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Hangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:100-47-0
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHANGZHOU YUNUO CHEMICAL CO.,LTD
Superior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum;200kg/drum as per your request Application:Mainly used for benzene gene
Henan Wentao Chemical Product Co., Ltd.
we are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
Cas:100-47-0
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryHunan chemfish Pharmaceutical co.,Ltd
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
JINHUA HUAYI CHEMICAL CO., LTD.
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Hangzhou Dingyan Chem Co., Ltd
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Wuhan Fortuna Chemical Co.,Ltd
Best service,high quality and cheap price. Storage:Keep away from heat,sparks and flames. Package:25kg/50kg/200kg drum or Customer demand Application:Used as pharmaceutical intermediates Transportation:BY sea/air or by courier
Aecochem Corp.
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Zhuozhou Wenxi import and Export Co., Ltd
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:100-47-0
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryHunan Russell Chemicals Technology Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
Xiamen AmoyChem Co.,Ltd
Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
Hubei Langyou International Trading Co., Ltd
Cyanobenzene CAS NO. 100-47-0 CAS NO.100-47-0 Application:Cyanobenzene CAS NO. 100-47-0 CAS NO.100-47-0
Cas:100-47-0
Min.Order:0
Negotiable
Type:Other
inquiryHangzhou Fandachem Co.,Ltd
Benzonitrile cas 100-47-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Hangzhou ZeErRui Chemical Co., Ltd.
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
Hunan Longxianng Runhui Trading Co.,Ltd
Cyanobenzene CAS NO. 100-47-0 CAS NO.100-47-0Appearance:powder Storage:Store at RT. Package:in foil bag or customized Application:Industrial Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport)
Cas:100-47-0
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquirySynthetic route
| Conditions | Yield |
|---|---|
| With phosphorus pentoxide In methanol at 20℃; for 1h; | 100% |
| With oxalyl dichloride; triethylamine; Triphenylphosphine oxide In acetonitrile at 20℃; for 0.166667h; Solvent; | 98% |
| With trimethylsilylphosphate for 0.666667h; Heating; | 97% |
| Conditions | Yield |
|---|---|
| With iron(III) chloride; hydroxylamine hydrochloride In dimethyl sulfoxide Molecular sieve; | 100% |
| With [bis(acetoxy)iodo]benzene; ammonium bicarbonate In methanol; water at 36℃; for 12h; Sealed tube; | 100% |
| With N-(4-sulphonic acid)butylpyridinium hydrogen sulphate; 1-sulfobutylpyridine hydrogensulfate hydroxylamine In toluene at 100℃; under 760.051 Torr; for 2h; Temperature; Solvent; Reagent/catalyst; | 100% |
| Conditions | Yield |
|---|---|
| With nickel(II) chloride dihydrate In acetonitrile at 80℃; Molecular sieve; Inert atmosphere; | 100% |
| With oxalyl dichloride; triethylamine In dimethyl sulfoxide; acetonitrile at 20℃; for 0.333333h; Reagent/catalyst; Swern Oxidation; | 100% |
| With zinc trifluoromethanesulfonate In toluene at 100℃; for 24h; | 99% |
| Conditions | Yield |
|---|---|
| With tetrakis(triphenylphosphine) palladium(0) In benzene at 120℃; for 12h; Product distribution; other acyl cyanides, var. solvents, temp. and time; | 100% |
| With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 180℃; for 24h; Temperature; Glovebox; Inert atmosphere; Sealed tube; | 95 %Chromat. |
| Conditions | Yield |
|---|---|
| With potassium tert-butylate; N,N-dimethyl-formamide at 35℃; for 24h; Schlenk technique; Inert atmosphere; Irradiation; | 100% |
| With C60H48BP3Pd; potassium formate; [2.2.2]cryptande In tetrahydrofuran at 60℃; for 72h; Schlenk technique; Inert atmosphere; | 99% |
| With formic acid; Cyclohexanethiol; 10-phenyl-10H-phenothiazine; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; under 2625.26 Torr; for 0.05h; Catalytic behavior; Reagent/catalyst; Time; Wavelength; Irradiation; Flow reactor; | 96% |
-
-
932-90-1, 622-31-1, 140461-24-1, 140461-25-2, 622-32-2
syn-benzaldehyde oxime
-
-
100-47-0
benzonitrile
| Conditions | Yield |
|---|---|
| With triethylamine; 2,4-Dichloro-5-nitropyrimidine In acetonitrile for 5h; Ambient temperature; | 100% |
| With 1,3,5-trichloro-2,4,6-triazine In N,N-dimethyl-formamide at 20℃; Beckmann rearrangement; | 100% |
| With oxalyl dichloride; Triphenylphosphine oxide In chloroform at 20℃; for 1h; | 99% |
-
-
55-21-0
benzamide
-
-
78303-22-7
chloro(tert-butyl)diethylamino(methylene)phosphorane
-
A
-
100-47-0
benzonitrile
| Conditions | Yield |
|---|---|
| In diethyl ether -10 dec C, then +20 deg C.; | A 70% B 100% C 85% |
-
-
149540-88-5
(E)-benzaldehyde O-pivaloyloxime
-
-
100-47-0
benzonitrile
| Conditions | Yield |
|---|---|
| With triethylamine In acetonitrile at 25℃; Rate constant; Mechanism; variation of base/solvent system; | 100% |
| With diisobutylamine In acetonitrile at 20℃; for 10h; | 94 %Chromat. |
| With diisopropylamine In acetonitrile at 25℃; Kinetics; |
-
-
149540-89-6
C12H14(2)HNO2
-
-
100-47-0
benzonitrile
| Conditions | Yield |
|---|---|
| With triethylamine In acetonitrile at 25℃; Rate constant; variation of base/solvent system; | 100% |
| Conditions | Yield |
|---|---|
| With sodium carbonate; palladium diacetate In 1-methyl-pyrrolidin-2-one; Hexadecane at 140℃; for 16h; Product distribution / selectivity; | 100% |
| With [Pd{C6H3(CH2CH2NH2)-4-OMe-5-κ2-C,N}(μ-Br)]2; potassium carbonate In N,N-dimethyl-formamide at 130℃; for 0.166667h; Microwave irradiation; | 94% |
| With sodium carbonate; palladium diacetate; tri-tert-butyl phosphine In 1-methyl-pyrrolidin-2-one; Hexadecane at 140℃; for 16h; Product distribution / selectivity; | 88% |
-
-
2042-37-7
o-cyanobromobenzene
-
-
7440-66-6
zinc
-
A
-
4341-02-0
biphenyl-2,2'-dicarbonitrile
-
B
-
100-47-0
benzonitrile
-
C
-
131379-17-4
2-cyanophenylzinc bromide
| Conditions | Yield |
|---|---|
| With trifluoroacetic acid; cobalt(II) bromide; zinc dibromide In acetonitrile the mixt. in CH3CN was stirred at room temp., then arylbromide was added, stirred at room temp.; GC analysis; | A 0% B 0% C 100% |
-
-
10102-43-9
nitrogen(II) oxide
-
B
-
100-47-0
benzonitrile
| Conditions | Yield |
|---|---|
| With NaClO4; CH2Cl2 In dichloromethane room temp., 15 min; | A 80% B 100% |
| With CH2Cl2 In dichloromethane room temp., 15 min; | A n/a B 73% |
| Conditions | Yield |
|---|---|
| With sodium carbonate; palladium diacetate In 1-methyl-pyrrolidin-2-one; Hexadecane at 140℃; for 16h; Product distribution / selectivity; | 100% |
| With [Pd{C6H3(CH2CH2NH2)-4-OMe-5-κ2-C,N}(μ-Br)]2; potassium carbonate In N,N-dimethyl-formamide at 130℃; for 0.116667h; Microwave irradiation; | 95% |
| With 1-methyl-pyrrolidin-2-one; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium carbonate at 120℃; for 12h; Schlenk technique; Inert atmosphere; | 95% |
| Conditions | Yield |
|---|---|
| With oxygen; sodium hydroxide In tetrahydrofuran; water at 20℃; for 3h; | 99% |
| With p-methoxybenzenetellurinic acid anhydride In dichloromethane for 0.5h; Ambient temperature; | 95% |
| With bis(4-methoxyphenyl)telluride; tetrabutylammonium acetate In water; acetonitrile electrolysis; | 95% |
| Conditions | Yield |
|---|---|
| With oxygen In acetone at 20℃; for 5.3h; Electrochemical reaction; | 99% |
| With aluminum oxide In N,N-dimethyl-formamide at 120℃; for 6h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; | 99% |
| With water; potassium hydroxide at 25℃; pH=13.6; Electrochemical reaction; | 98% |
| Conditions | Yield |
|---|---|
| With ammonium hydroxide; oxygen In tert-Amyl alcohol at 130℃; under 3750.38 Torr; for 24h; Reagent/catalyst; Solvent; | 99% |
| With ammonia; oxygen In tert-Amyl alcohol; water at 100℃; under 3750.38 Torr; for 5h; Autoclave; High pressure; | 99% |
| With ammonia at 320℃; for 2h; Catalytic behavior; Reagent/catalyst; Temperature; Flow reactor; | 98% |
| Conditions | Yield |
|---|---|
| With ammonium formate In water at 20℃; for 6h; | 99% |
| With Triethoxysilane; C20H24N4Ni; sodium t-butanolate In toluene at 80℃; for 8h; Kumada Cross-Coupling; Inert atmosphere; Schlenk technique; | 83% |
| With cyclohexa-1,4-diene; 9-ethyl-N3,N3,N6,N6,-tetramethyl-9H-carbazole-3,6-diamine; N-ethyl-N,N-diisopropylamine In N,N-dimethyl acetamide at 23℃; for 0.8h; Inert atmosphere; UV-irradiation; Schlenk technique; | 83% |
| Conditions | Yield |
|---|---|
| With Palladium Nanoparticles with two shape-persistent covalent cages CC1' In N,N-dimethyl-formamide at 140℃; for 15h; Reagent/catalyst; Inert atmosphere; | 99% |
| With tetrabutylammomium bromide; copper(II) acetate monohydrate; potassium iodide; N,N`-dimethylethylenediamine In water at 20 - 140℃; Microwave irradiation; | 89% |
| With sodium carbonate In N,N-dimethyl-formamide at 110℃; for 20h; Catalytic behavior; Sealed tube; | 99 %Chromat. |
| Conditions | Yield |
|---|---|
| With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 12h; Catalytic behavior; Reagent/catalyst; Solvent; Time; Temperature; Inert atmosphere; | 99% |
| With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 3h; | 95% |
| With [Pd{C6H4(CH2N(CH2Ph)2)}(μ-Br)]2; tetrabutylammomium bromide; potassium carbonate In N,N-dimethyl-formamide at 130℃; for 0.0833333h; Microwave irradiation; | 92% |
| Conditions | Yield |
|---|---|
| With triethylamine In water at 25℃; for 1h; UV-irradiation; | 99% |
| With triethylamine In tetrahydrofuran at 20℃; for 12h; Irradiation; Inert atmosphere; Sealed tube; | 80.7% |
| With triethylamine; Lumogen F Orange 240 In N,N-dimethyl-formamide at 40℃; for 4h; Irradiation; | 98 %Chromat. |
| Conditions | Yield |
|---|---|
| With sodium hydroxide at 24.84℃; under 760.051 Torr; for 96h; Inert atmosphere; UV-irradiation; Sealed tube; | 99% |
-
-
100-47-0
benzonitrile
| Conditions | Yield |
|---|---|
| With copper(l) iodide In dimethyl sulfoxide at 90℃; for 12h; | 99% |
| Conditions | Yield |
|---|---|
| With iron(III) chloride; 2,6-di-tert-butyl-4-methyl-phenol In dichloromethane; toluene at 20℃; for 0.0333333h; Reagent/catalyst; | 99% |
| With iron(III) chloride; 2,6-di-tert-butyl-4-methyl-phenol In toluene at 20℃; for 0.0333333h; Catalytic behavior; Reagent/catalyst; Solvent; Schlenk technique; | 64% |
-
-
18322-87-7, 63561-63-7
syn-O-(4-Chlorbenzoyl)-benzaldoxim
-
-
100-47-0
benzonitrile
| Conditions | Yield |
|---|---|
| With iron(III) chloride; 2,6-di-tert-butyl-4-methyl-phenol In dichloromethane; toluene at 20℃; for 0.05h; | 99% |
-
-
100-47-0
benzonitrile
| Conditions | Yield |
|---|---|
| With iron(III) chloride; 2,6-di-tert-butyl-4-methyl-phenol In dichloromethane; toluene at 20℃; for 0.05h; | 99% |
| Conditions | Yield |
|---|---|
| With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene In various solvent(s) at 60℃; for 1h; | 98% |
| With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene In various solvent(s) at 60℃; for 1h; other catalyst, other solvent, other temperature; | 98% |
| Stage #1: potassium cyanide; (E)-N1,N1-dimethyl-N2-(pyridin-2-ylmethylene)ethane-1,2-diamine; copper(I) oxide at 100℃; Stage #2: iodobenzene In N,N-dimethyl-formamide at 110℃; for 24h; Product distribution / selectivity; | 83% |
| Stage #1: potassium cyanide; copper(I) oxide; trans-N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine at 100℃; Stage #2: iodobenzene In N,N-dimethyl-formamide at 110℃; for 24 - 48h; Product distribution / selectivity; | 73.7% |
| With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran for 1h; Substitution; Heating; |
-
-
79-46-9
2-nitropropane
-
-
80670-36-6
3-diazo-5-phenyl-3H-1,2,4-triazole
-
A
-
100-47-0
benzonitrile
-
B
-
127-06-0
acetone oxime
| Conditions | Yield |
|---|---|
| at 80℃; Yields of byproduct given; | A n/a B 98% |
-
-
21272-78-6
α-nitrobenzyl phenyl sulfone
-
A
-
77853-07-7
Benzenethiosulfonic acid; compound with ammonia
-
B
-
100-47-0
benzonitrile
| Conditions | Yield |
|---|---|
| With sulfur; ammonia at 100℃; for 4h; | A 98% B 70% |
-
-
55986-20-4
N-(p-tolylsulfonyl)dibenzylselenimide
-
-
2227-79-4
benzenecarbothioamide
-
A
-
1842-38-2
dibenzyl selenide
-
B
-
70-55-3
toluene-4-sulfonamide
-
C
-
100-47-0
benzonitrile
| Conditions | Yield |
|---|---|
| In methanol for 0.5h; Mechanism; Ambient temperature; | A 98% B 98% C 81% |
-
-
80503-58-8
4-hydroxy-4-octyl-3-phenylisoxazoline-5-one
-
A
-
333-60-8
2-oxodecanoic acid
-
B
-
100-47-0
benzonitrile
| Conditions | Yield |
|---|---|
| With 2,6-dichloro-benzonitrile In benzene for 3h; Heating; | A 98% B n/a |
-
-
100-47-0
benzonitrile
-
-
18039-42-4
5-Phenyl-1H-tetrazole
| Conditions | Yield |
|---|---|
| With sodium azide In dimethyl sulfoxide at 140℃; for 1h; Solvent; Time; Temperature; | 100% |
| With sodium azide In dimethyl sulfoxide at 120℃; for 0.166667h; Catalytic behavior; Solvent; Reagent/catalyst; Temperature; Green chemistry; | 100% |
| With sodium azide In N,N-dimethyl-formamide at 120℃; for 8h; Catalytic behavior; Reagent/catalyst; Solvent; Green chemistry; | 100% |
| Conditions | Yield |
|---|---|
| With ammonia; lanthanum(lll) triflate at 200℃; for 24h; in a stainless steel pressure vessel; | 100% |
| With samarium diiodide; hexan-1-amine at 80℃; for 3h; cyclotrimerization; | 96% |
| With samarium diiodide; hexan-1-amine at 80℃; for 3h; Product distribution; Further Variations:; Reagents; Temperatures; nitrile:amine mole ratio; cyclotrimerization; | 96% |
| Conditions | Yield |
|---|---|
| With water; nitrile hydratase from Rhodococcus rhodochrous J1 at 25℃; for 24h; K2HPO4-KH2PO4 puffer pH=8.0; | 100% |
| With manganese(IV) oxide; silica gel In 2,2,4-trimethylpentane for 2h; Heating; | 100% |
| With sodium hydroxide; trisodium tris(3-sulfophenyl)phosphine; water; chloro(1,5-cyclooctadiene)rhodium(I) dimer In ethyl acetate at 90℃; for 24h; pH=11.7; hydration; | 100% |
| Conditions | Yield |
|---|---|
| With pyridine; diammonium sulfide; triethylamine In water at 50℃; | 100% |
| With sodium hydrogensulfide; diethyl amine hydrochloride In 1,4-dioxane; water at 55℃; for 6h; | 98% |
| With diisopropyldithiophosphoric acid In methanol at 60℃; for 4h; | 97% |
| Conditions | Yield |
|---|---|
| With sodium hydroxide; hydroxylamine hydrochloride In methanol Heating; | 100% |
| With hydroxylamine In ethanol; water for 48h; Heating / reflux; | 100% |
| With hydroxylamine In ethanol; water Reflux; | 100% |
| Conditions | Yield |
|---|---|
| With water at 45℃; pH=7.2; Microbiological reaction; aq. buffer; | 100% |
| With potassium tert-butylate; water In isopropyl alcohol at 25℃; Inert atmosphere; | 100% |
| With benzene-1,2-dicarboxylic acid at 250℃; under 7600 Torr; for 0.25h; microwave irradiation; | 99% |
| Conditions | Yield |
|---|---|
| With lithium borohydride; 9-methoxy-9-BBN In diethyl ether at 25℃; for 5h; Product distribution; rate of reduction; | 100% |
| With borane N-ethyl-N-isopropylaniline complex In tetrahydrofuran for 0.1h; Heating; | 100% |
| With hydrogen; palladium In methanol at 20℃; for 432h; | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: benzonitrile With woollins’ reagent In toluene for 4h; Heating; Stage #2: With water In toluene for 1h; | 100% |
| With selenium; sodium tetrahydroborate In pyridine; ethanol Heating; | 98% |
| Stage #1: benzonitrile With woollins’ reagent In toluene under 760.051 Torr; for 8h; Inert atmosphere; Schlenk technique; Reflux; Stage #2: With water In toluene at 90℃; under 760.051 Torr; for 1h; Inert atmosphere; Schlenk technique; Reflux; | 98% |
| Conditions | Yield |
|---|---|
| Stage #1: dimethyl amine With n-butyllithium In diethyl ether; hexane at -20℃; for 0.166667h; Stage #2: benzonitrile at -20℃; for 1h; | 100% |
| Conditions | Yield |
|---|---|
| With phenyllithium In diethyl ether for 2.5h; Heating; | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: 1-indoline; benzonitrile With aluminum (III) chloride; water; boron trichloride In dichloromethane; toluene at 110℃; Stage #2: With hydrogenchloride; water In dichloromethane; toluene at 80℃; for 1h; | 100% |
| Stage #1: 1-indoline; benzonitrile With aluminum (III) chloride; boron trichloride In dichloromethane; toluene at 0 - 110℃; Stage #2: With hydrogenchloride; water at 80℃; for 1h; | 100% |
| With aluminum (III) chloride; boron trichloride In toluene Friedel-Crafts Acylation; Inert atmosphere; Reflux; | 84% |
| Conditions | Yield |
|---|---|
| (η3-allyl)(η5-pentamethylcyclopentadienyl)cobalt In hexane at 20℃; for 72h; | 100% |
| With aluminium trichloride 1.) CH2Cl2, -85 deg C, 2.) -50 deg C; Yield given. Multistep reaction; |
-
-
100-47-0
benzonitrile
-
-
20046-60-0, 38774-32-2
3β-acetoxy-16β,17β-epoxymethyleneandrost-5-ene
| Conditions | Yield |
|---|---|
| With tetrafluoroboric acid diethyl ether In diethyl ether; dichloromethane for 30h; Ambient temperature; | 100% |
-
-
100-47-0
benzonitrile
-
-
3287-99-8, 39110-74-2
benzylamine hydrochloride
| Conditions | Yield |
|---|---|
| With hydrogenchloride; hydrogen In propan-1-ol; water at 60℃; under 375.038 Torr; for 18h; Flow reactor; | 100% |
| Stage #1: benzonitrile With [2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]triethylphosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; diethylphenylsilane at 20℃; for 18h; Glovebox; Inert atmosphere; Stage #2: With hydrogenchloride In diethyl ether at 20℃; for 1h; Glovebox; Inert atmosphere; | 99% |
| Stage #1: benzonitrile With hydrogen at 130℃; under 750.075 Torr; for 6h; Stage #2: Acidic conditions; chemoselective reaction; | 99% |
| Conditions | Yield |
|---|---|
| Stage #1: benzonitrile With Li(2,2,6,6-tetramethylpiperidide)*Al(iBu)3 In tetrahydrofuran; hexane at -78℃; for 2h; Stage #2: With iodine In tetrahydrofuran; hexane at 0℃; for 1h; | 100% |
| Stage #1: benzonitrile With Li(2,2,6,6-tetramethylpiperidide)*Al(iBu)3 In tetrahydrofuran; hexane at -78℃; for 2h; Stage #2: With iodine In tetrahydrofuran; hexane at -78 - 0℃; for 1h; | 100% |
| Stage #1: benzonitrile With 2,2,6,6-tetramethylpiperidin-4-yl heptanoate; n-butyllithium; dichloro(N,N,N’,N‘-tetramethylethylenediamine)zinc In tetrahydrofuran; hexane at 0 - 20℃; Inert atmosphere; Stage #2: With iodine In tetrahydrofuran; hexane Inert atmosphere; | 100% |
| Conditions | Yield |
|---|---|
| With hydroxylamine In ethanol for 1h; Heating / reflux; | 100% |
| With hydroxylamine In ethanol for 1h; Reflux; | 100% |
| With hydroxylamine hydrochloride; sodium carbonate In ethanol for 17h; Reflux; | 100% |
-
-
635-46-1
1,2,3,4-tetrahydroisoquinoline
-
-
100-47-0
benzonitrile
-
-
28748-92-7
phenyl(1,2,3,4-tetrahydroquinolin-8-yl)methanone
| Conditions | Yield |
|---|---|
| Stage #1: 1,2,3,4-tetrahydroisoquinoline; benzonitrile With aluminum (III) chloride; water; boron trichloride In dichloromethane; toluene at 110℃; Stage #2: With hydrogenchloride; water In dichloromethane; toluene at 80℃; for 1h; | 100% |
| Stage #1: 1,2,3,4-tetrahydroisoquinoline; benzonitrile With aluminum (III) chloride; boron trichloride In dichloromethane; toluene at 0 - 110℃; Stage #2: With hydrogenchloride; water at 80℃; for 1h; | 100% |
| With aluminium trichloride; boron trichloride In 1,2-dichloro-ethane Acylation; |
| Conditions | Yield |
|---|---|
| Stage #1: (2-picolyl)trimethylsilane With lithium diisopropyl amide In tetrahydrofuran at -80℃; for 1h; Stage #2: benzonitrile In tetrahydrofuran at -80 - 20℃; for 3h; | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: N,N-dimethyl(trimethylsilyl)acetamide With n-butyllithium In tetrahydrofuran; hexane at -80℃; for 1h; Stage #2: benzonitrile In tetrahydrofuran at -80 - 20℃; for 3h; | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: benzonitrile; ethyl(diphenyl)phosphine borane With N,N,N,N,N,N-hexamethylphosphoric triamide; sec.-butyllithium In tetrahydrofuran at -90℃; for 0.5h; Stage #2: allyl bromide In tetrahydrofuran at -90℃; for 2h; | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: benzonitrile; ethyl(diphenyl)phosphine borane With N,N,N,N,N,N-hexamethylphosphoric triamide; sec.-butyllithium In tetrahydrofuran at -90℃; for 0.5h; Stage #2: methyl iodide In tetrahydrofuran at -90℃; for 2h; | 100% |
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