Dayang Chem (Hangzhou) Co.,Ltd.
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
Cas:100-46-9
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryHangzhou Dingyan Chem Co., Ltd
Items Standard Result Appearance Colorless Transparent Liquid Complies Assay 99%min
Cas:100-46-9
Min.Order:1 Kilogram
FOB Price: $1.9 / 2.5
Type:Trading Company
inquirySimagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:100-46-9
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryAlity Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Hebei yanxi chemical co.,LTD.
hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:100-46-9
Min.Order:1 Kilogram
FOB Price: $1.0 / 3.0
Type:Trading Company
inquiryChemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Henan Tianfu Chemical Co., Ltd.
TIANFUCHEM--100-46-9--Benzylamine in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relationships wi
Cas:100-46-9
Min.Order:1 Metric Ton
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryLIDE PHARMACEUTICALS LIMITED
Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:100-46-9
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHenan Sinotech Import&Export Corporation
Chemical Name: Benzylamine CAS No.: 100-46-9 Molecular Fomula:C7H9N Chemical Structure: Molecular weight: 107.15 Appearance: Colorless Transparent Liquid Assay:99%min Appearance: Colorless Liquid Storage:Store in cool and dry place, away
Shijiazhuang Sdyano Fine Chemical Co., Ltd
1. Best prices with satisfied quality; 2. It's clients' right to choose the package's Courier (EMS, DHL, FedEx, UPS); 3.It's clients' right to choose the packing way for his produccts from many recent effective packing ways;
Baoji Guokang Healthchem co.,ltd
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:100-46-9
Min.Order:1 Kilogram
FOB Price: $35.0 / 50.0
Type:Trading Company
inquiryHebei Mojin Biotechnology Co.,Ltd
Hebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have sever
Cas:100-46-9
Min.Order:25 Liter
FOB Price: $90.0 / 900.0
Type:Trading Company
inquiryLonwin Chemical Group Limited
Store in cool and dry place, away from...Benzyl amine CAS：100-46-9 Specification Items Standard Result Appearance Colorless Transparent Liquid Complies
Triumph International Development Limilted
Appearance:white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Aripiprazole Intermediate Transportation:Common products:Sea/Air/Courier Dangerous Chem:Se
Hangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:100-46-9
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryZibo Dorne chemical technology co. LTD
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Henan Wentao Chemical Product Co., Ltd.
We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:100-46-9
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryHangzhou Zhongqi chem Co.,Ltd.
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and
Cas:100-46-9
Min.Order:1 Gram
Negotiable
Type:Other
inquirySiwei Development Group Ltd.
Product name: Benzylamine CAS No.：100-46-9 Molecule Formula：C7H9N Molecule Weight：107.1551 Purity: 99.0% Package: 200kg/drum Description：Colorless transparent liquid Manufacture Standards：Enterprise Standard TESTIN
Hangzhou Huarong Pharm Co., Ltd.
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Hangzhou Keyingchem Co.,Ltd
Hangzhou Keying Chem Co., Ltd. Is a comprehensive enterprise, dedicated to the development, production and marketing of chemicals. As a technology innovative and service professional enterprise, Our company mainly engages in global pharmaceutical,
Cas:100-46-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHunan chemfish Pharmaceutical co.,Ltd
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
HANGZHOU YUNUO CHEMICAL CO.,LTD
Superior quality, moderate price & quick delivery. Appearance:colorless transparent liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmaceuti
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
JINHUA HUAYI CHEMICAL CO., LTD.
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Hangzhou ZeErRui Chemical Co., Ltd.
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home
Cas:100-46-9
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHenan Allgreen Chemical Co.,Ltd
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Aecochem Corp.
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Synthetic route
| Conditions | Yield |
|---|---|
| With Zn(BH4)2(Ph3P)2 In tetrahydrofuran for 0.25h; Reduction; Heating; | 100% |
| With sodium tetrahydroborate; tin bis(1,2-benzenedithiolate) In tetrahydrofuran; phosphate buffer at 10℃; for 0.5h; pH=10; Product distribution; Further Variations:; pH-values; Solvents; Reduction; | 100% |
| With (Sn(SPh)3)(Et3N) In benzene at 15℃; for 0.0833333h; | 99% |
| Conditions | Yield |
|---|---|
| With lithium borohydride; 9-methoxy-9-BBN In diethyl ether at 25℃; for 5h; Product distribution; rate of reduction; | 100% |
| With borane N-ethyl-N-isopropylaniline complex In tetrahydrofuran for 0.1h; Heating; | 100% |
| With hydrogen; palladium In methanol at 20℃; for 432h; | 100% |
-
-
104669-74-1
benzyl carbamic acid allyl ester
-
-
100-46-9
benzylamine
| Conditions | Yield |
|---|---|
| With diethylamine; palladium diacetate; trisodium tris(3-sulfophenyl)phosphine In water; acetonitrile for 0.166667h; Ambient temperature; | 100% |
| Conditions | Yield |
|---|---|
| With Thiosalicylic acid; 1,4-di(diphenylphosphino)-butane; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran at 60℃; for 0.5h; effect of temperature on deprotection of various primary and secondary allylamines; | 100% |
| With Thiosalicylic acid; 1,4-di(diphenylphosphino)-butane; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran at 60℃; for 0.5h; | 100% |
| With polymethylhydrosiloxane; zinc(II) chloride; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 20℃; | 92% |
| With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); diisobutylaluminium hydride In toluene for 1h; Ambient temperature; | 66% |
| Conditions | Yield |
|---|---|
| With Thiosalicylic acid; 1,4-di(diphenylphosphino)-butane; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran at 60℃; for 0.5h; | 100% |
| With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); diisobutylaluminium hydride In toluene for 1h; Ambient temperature; | 79% |
-
-
42116-44-9
N-tert-butoxycarbonylbenzylamine
-
-
100-46-9
benzylamine
| Conditions | Yield |
|---|---|
| With methanol; Acetyl bromide In dichloromethane at 25℃; for 0.333333h; | 100% |
| With 3-butyl-l-methyl-1H-imidazol-3-iumtrifloroacetate In 1,4-dioxane; water at 80 - 82℃; for 4h; | 98% |
| With nitric acid In dichloromethane at 0℃; for 1h; | 95% |
| Conditions | Yield |
|---|---|
| In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B 100% C n/a |
-
-
52826-45-6
(benzylimino)triphenylphosphorane
-
-
100-46-9
benzylamine
| Conditions | Yield |
|---|---|
| With phenylsilane In toluene at 111℃; for 12h; | 100% |
| Conditions | Yield |
|---|---|
| With ammonia; hydrogen In methanol at 90℃; under 15001.5 Torr; for 4h; Solvent; Temperature; Pressure; Autoclave; | 99.7% |
| With Candida boidinii formate dehydrogenase; Geobacillus stearothermophilus ε‐deaminating L‐lysine dehydrogenase variant 1; nicotinamide adenine dinucleotide In aq. buffer at 30℃; for 24h; pH=8.5; Reagent/catalyst; Enzymatic reaction; | 99% |
| With ammonium hydroxide; hydrogen In ethanol at 130℃; under 7500.75 Torr; for 12h; Autoclave; | 96.9% |
| Conditions | Yield |
|---|---|
| Stage #1: N-benzyl-p-toluenesulfonamide With n-butyllithium In tetrahydrofuran at 0℃; Stage #2: With naphthalene; lithium In tetrahydrofuran at -78 - 20℃; | 99% |
| Stage #1: N-benzyl-p-toluenesulfonamide With n-butyllithium In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: With naphthalene; lithium In tetrahydrofuran at -78 - 25℃; Stage #3: With water In tetrahydrofuran | 99% |
| With naphthalene; water; lithium 1.) THF, -78 deg C, 2 h; Yield given. Multistep reaction; |
-
-
383865-57-4
4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl-amine
-
B
-
100-46-9
benzylamine
| Conditions | Yield |
|---|---|
| A 99% B n/a |
| Conditions | Yield |
|---|---|
| With sodium ethanolate In methanol at 80℃; for 2h; | 99% |
| With sodiumsulfide nonahydrate In water at 100℃; for 12h; | 86% |
| Multi-step reaction with 2 steps 1: 3 h / Reflux 2: triphenylphosphine; triethylamine / dichloromethane; tetrachloromethane / 4 h / Reflux; Inert atmosphere View Scheme |
| Conditions | Yield |
|---|---|
| With 5%-palladium/activated carbon; hydrogen; ammonium formate In methanol under 2068.65 Torr; Flow reactor; | 98% |
| With palladium on activated charcoal; tetrabutylammomium bromide; water; sodium hydroxide; silicon at 100℃; for 6h; Reagent/catalyst; | 94% |
| With hydrazine hydrate In dichloromethane at 20℃; for 1h; | 71% |
-
-
122954-29-4
benzylammonium O-ethylstyrylphosphonate
-
A
-
5849-49-0
styrylphosphonic acid ethylester
-
B
-
100-46-9
benzylamine
| Conditions | Yield |
|---|---|
| With sodium hydroxide at 20℃; for 0.5h; | A 98% B 83% |
| Conditions | Yield |
|---|---|
| With ammonium cerium (IV) nitrate; water; acetic acid In dichloromethane at 20℃; for 7.5h; Inert atmosphere; | 98% |
| With water; ytterbium(III) triflate In tetrahydrofuran at 20℃; Product distribution; Further Variations:; Catalysts; Reagents; Hydrolysis; | 93% |
-
-
54535-21-6
2-(benzylamino-methylene)-malonic acid diethyl ester
-
-
100-46-9
benzylamine
| Conditions | Yield |
|---|---|
| With ethylenediamine In ethanol at 20℃; for 0.75h; | 98% |
-
-
100-46-9
benzylamine
| Conditions | Yield |
|---|---|
| Stage #1: N-benzyl-3,3-dimethoxypropylsulfonamide With p-toluenesulfonic acid monohydrate In water; acetone at 0 - 20℃; for 6h; Stage #2: With sodium hydroxide In methanol; water; acetone at 0 - 20℃; for 1.08333h; | 98% |
| Conditions | Yield |
|---|---|
| With sodium hydrogensulfate monohydrate; molybdenum(V) chloride; sodium cyanoborohydride In N,N-dimethyl-formamide for 1.5h; Reflux; | 96% |
| With sodium tetrahydroborate at 20℃; for 0.0333333h; neat (no solvent, solid phase); | 94% |
| With iron oxide; zirconium(IV) chloride; sodium cyanoborohydride In neat (no solvent) at 75 - 80℃; for 0.25h; Reagent/catalyst; Temperature; | 93% |
| Conditions | Yield |
|---|---|
| With sodium azide; triphenylphosphine In dichloromethane; N,N-dimethyl-formamide at 90℃; for 4h; Substitution; Mitsunobu reaction; Staudinger reaction; | 96% |
| With ammonia In toluene at 110℃; under 5250.53 Torr; for 20h; | 91% |
| With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); ammonia; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In tert-Amyl alcohol at 140℃; for 20h; Inert atmosphere; Cooling; | 87% |
| Conditions | Yield |
|---|---|
| With hydrogen; palladium on activated charcoal; ethylenediamine In tetrahydrofuran at 20℃; for 24h; atmospheric pressure; | A 96% B n/a |
| Conditions | Yield |
|---|---|
| With 5-methyl-1,3,4-thiadiazol-2-amine; triethylamine In ethanol; water at 25℃; for 1h; | 96% |
| Multi-step reaction with 2 steps 1.1: n-butyllithium / tetrahydrofuran / Inert atmosphere 1.2: 8 h / Inert atmosphere 1.3: 2 h / 60 °C / Inert atmosphere 2.1: titanium(III) chloride; water / tetrahydrofuran / pH 10 / Reflux; Alkaline aq. solution; Inert atmosphere View Scheme | |
| Multi-step reaction with 2 steps 1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C 2: hydrogenchloride / water / 3 h / 100 °C View Scheme | |
| Multi-step reaction with 2 steps 1.1: potassium carbonate / 1 h / Milling 1.2: 1 h / Milling 2.1: ethylenediamine / neat (no solvent) / Milling View Scheme |
| Conditions | Yield |
|---|---|
| With C25H19BrMnN2O2P; potassium tert-butylate; hydrogen In toluene at 130℃; under 15001.5 Torr; for 48h; | A 98 %Spectr. B 96% |
| Conditions | Yield |
|---|---|
| With potassium hydroxide at 20℃; for 0.25h; | 95% |
| Conditions | Yield |
|---|---|
| at 220℃; under 10 Torr; for 0.0833333h; Product distribution; pyrolysis without solvent, isolated as sulfate; | A n/a B 95% |
-
-
100-46-9
benzylamine
| Conditions | Yield |
|---|---|
| With ammonium formate; 1,2-bis-(diphenylphosphino)ethane; bis(dibenzylideneacetone)-palladium(0) In dimethyl sulfoxide at 80℃; for 12h; deprotection; | 95% |
| Conditions | Yield |
|---|---|
| With ammonium bromide; 3-azapentane-1,5-diamine at 110℃; for 5h; Temperature; Microwave irradiation; | 95% |
| Conditions | Yield |
|---|---|
| With [RuCl2(2-(diphenylphosphino)-N-((6-((diphenylphosphino)methyl)pyridin-2-yl)methyl)ethan-1-amine)]; potassium tert-butylate; hydrogen In tetrahydrofuran at 100℃; under 37503.8 Torr; for 20h; Catalytic behavior; Autoclave; chemoselective reaction; | A 95% B 87% |
| With C25H19BrMnN2O2P; potassium tert-butylate; hydrogen In tetrahydrofuran at 130℃; under 22502.3 Torr; for 48h; Mechanism; Inert atmosphere; Glovebox; Autoclave; Green chemistry; | A 94% B 92% |
| With [Ru(PtBuNNHtBu)H(CO)Cl]; potassium tert-butylate; hydrogen In tetrahydrofuran at 110℃; under 15001.5 Torr; for 24h; Autoclave; | |
| With C25H19BrMnN2O2P; potassium tert-butylate; hydrogen In 1,4-dioxane at 130℃; under 22502.3 Torr; for 48h; Catalytic behavior; Solvent; Reagent/catalyst; Pressure; Inert atmosphere; Glovebox; Autoclave; Green chemistry; | A 92 %Spectr. B 97 %Spectr. |
| Conditions | Yield |
|---|---|
| With copper(ll) sulfate pentahydrate; ammonium hydroxide In PEG1000-DIL; methyl cyclohexane at 60℃; for 3h; | 94% |
| With 5-methyl-1,3,4-thiadiazol-2-amine; triethylamine In ethanol; water at 25℃; for 1h; Reagent/catalyst; | 94% |
| With hydrogenchloride; potassium hydride; 1,1,3,3-tetramethyldisilazane In tetrahydrofuran at 0 - 25℃; multistep selective monoamination reaction of various alkyl halides; | 88% |
-
-
119592-74-4
N-benzyl-2,2,6,6-tetramethyl-2,6-disilapiperidine
-
-
100-46-9
benzylamine
| Conditions | Yield |
|---|---|
| In hydrogenchloride for 8h; Heating; | 94% |
| Conditions | Yield |
|---|---|
| In dichloromethane at 0 - 20℃; | 100% |
| In dichloromethane at 0 - 20℃; | 100% |
| In dichloromethane at 0 - 20℃; | 100% |
| Conditions | Yield |
|---|---|
| With bis(trifluoromethane)sulfonimide lithium In chloroform at 85℃; for 40h; | 100% |
| Stage #1: benzylamine With diisobutylaluminium hydride In tetrahydrofuran; toluene Stage #2: 4-butanolide In tetrahydrofuran at 20℃; for 0.5h; | 98% |
| In benzene for 12h; Reflux; | 98% |
| Conditions | Yield |
|---|---|
| With copper(II) bis(trifluoromethanesulfonate) In water at 20℃; for 0.0166667h; | 100% |
| In water at 20℃; for 2h; | 93% |
| In dichloromethane Inert atmosphere; Molecular sieve; | 81% |
-
-
286-20-4
cyclohexane-1,2-epoxide
-
-
100-46-9
benzylamine
-
-
40571-86-6, 40571-87-7, 51925-39-4, 131164-07-3, 141553-09-5
rac-(1R,2R)-2-(benzylamino)cyclohexanol
| Conditions | Yield |
|---|---|
| bismuth(lll) trifluoromethanesulfonate at 160℃; for 0.25h; microwave irradiation; | 100% |
| at 150℃; Neat (no solvent); | 99% |
| With zinc(II) perchlorate hexahydrate at 80℃; for 1h; | 97% |
| Conditions | Yield |
|---|---|
| With N-ethyl-N,N-diisopropylamine In acetonitrile at 25℃; for 1h; | 100% |
| With triethylamine In dichloromethane at 0 - 20℃; for 4h; Inert atmosphere; | 100% |
| With 1-methyl-1H-imidazole In dichloromethane at 0℃; Inert atmosphere; | 99% |
| Conditions | Yield |
|---|---|
| With formic acid; Cp*IrCl(N-(phenyl(pyridin-2-yl)methyl)methanesulfonamide)complex In ethyl acetate at 40℃; for 18h; Reagent/catalyst; Inert atmosphere; | 100% |
| Stage #1: cyclohexanone; benzylamine With formic acid; chlorido(8-quinolinolato-k2N,O)(η5-pentamethylcyclopentadienyl)iridium(III) In ethyl acetate at 0 - 40℃; Inert atmosphere; Schlenk tube; Cooling with ice; Stage #2: With sodium hydrogencarbonate In water; ethyl acetate Product distribution / selectivity; | 98% |
| With 4 A molecular sieve; borane pyridine complex In methanol for 16h; | 96% |
| Conditions | Yield |
|---|---|
| In chloroform at 20℃; for 1h; | 100% |
| for 6h; Kinetics; Molecular sieve; Reflux; | 100% |
| With magnesium sulfate In dichloromethane at 20℃; Inert atmosphere; | 65% |
-
-
104-88-1
4-chlorobenzaldehyde
-
-
100-46-9
benzylamine
-
-
130517-96-3, 13540-93-7
N-(4-chlorobenzylidene)benzylamine
| Conditions | Yield |
|---|---|
| for 6h; Molecular sieve; Reflux; | 100% |
| In ethanol at 20℃; | 94% |
| In dichloromethane at 20℃; for 16h; Molecular sieve; | 92% |
| Conditions | Yield |
|---|---|
| In methanol at 20℃; | 100% |
| In methanol at 20℃; | 80% |
| Conditions | Yield |
|---|---|
| In hexane at 20℃; for 2h; | 100% |
| In dichloromethane at 20℃; | 98% |
| In chloroform for 0.5h; Heating; | 88% |
| Conditions | Yield |
|---|---|
| In toluene at 120℃; for 24h; | 100% |
| With magnesium sulfate In dichloromethane for 3h; Reflux; | 100% |
| With aluminum oxide at 20℃; for 2.5h; | 99% |
| Conditions | Yield |
|---|---|
| In chloroform at 20℃; for 1h; | 100% |
| With sodium sulfate In dichloromethane at 20℃; | 99% |
| In chloroform at 20℃; for 1h; | 96.8% |
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 20℃; | 100% |
| With sodium hydroxide In 1,2-dimethoxyethane; water at 25℃; for 0.5h; pH 10.45; | 99% |
| Stage #1: benzoyl chloride; benzylamine With triethylamine In dichloromethane at 20℃; for 0.333333h; Stage #2: With poly{trans-bicyclo[2.2.1]hept-5-ene-2,3-di(chlorocarbonyl)} In dichloromethane at 20℃; for 0.5h; | 99% |
| Conditions | Yield |
|---|---|
| In acetonitrile at 20℃; for 3h; | 100% |
| In acetonitrile at 25℃; for 0.166667h; Milling; | 99% |
| With C64H52CaN6 In neat (no solvent) at 60℃; for 12h; Schlenk technique; Glovebox; Inert atmosphere; | 98% |
| Conditions | Yield |
|---|---|
| With Iron(III) nitrate nonahydrate In toluene for 2h; Concentration; Reflux; | 100% |
| With H-β-zeolite In neat (no solvent) at 80℃; for 24h; Green chemistry; | 99% |
| at 20 - 120℃; for 15h; | 99% |
| Conditions | Yield |
|---|---|
| With magnesium sulfate In dichloromethane at 20℃; Inert atmosphere; | 100% |
| With aluminum oxide at 20℃; for 7h; | 90% |
| In water Condensation; | 65.12% |
-
-
292638-85-8
acrylic acid methyl ester
-
-
100-46-9
benzylamine
-
-
23574-01-8
3-benzylamino-propionic acid methyl ester
| Conditions | Yield |
|---|---|
| at -40℃; for 12h; | 100% |
| With [HP(HNCH2CH2)3N]NO3 In acetonitrile at 20℃; for 48h; Michael addition; | 98% |
| copper In methanol at 20℃; for 0.3h; Aza-Michael Addition; | 98% |
-
-
292638-85-8
acrylic acid methyl ester
-
-
100-46-9
benzylamine
-
-
793-19-1
bis(2-methoxycarbonylethyl)benzylamine
| Conditions | Yield |
|---|---|
| In methanol at 20℃; for 8h; Reflux; | 100% |
| In methanol Reflux; | 99% |
| In methanol at 34℃; for 72h; Inert atmosphere; | 99% |
| Conditions | Yield |
|---|---|
| In dichloromethane | 100% |
| With triethylamine In dichloromethane at 0 - 20℃; for 4h; Inert atmosphere; | 98% |
| With potassium carbonate In dichloromethane Heating; | 97% |
| Conditions | Yield |
|---|---|
| With triethylamine In tetrahydrofuran at 20℃; for 2h; | 100% |
| With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 16h; | 99% |
| In dichloromethane at 0 - 20℃; for 0.5h; Inert atmosphere; | 98% |
| Conditions | Yield |
|---|---|
| With triethylamine In dichloromethane 1) 0 deg C, 1 h, 2) room temperature; | 100% |
| With sodium hydroxide In water at 25℃; for 2h; pH 9.6; | 99.9% |
| With Fe3O4-supported (diisopropylamino)acetamide In dichloromethane at 25℃; | 98% |
| Conditions | Yield |
|---|---|
| With triethylamine In dichloromethane at 4℃; | 100% |
| With pyridine; dmap In dichloromethane at 0 - 20℃; for 16h; | 99% |
| With triethylamine at 20℃; for 1h; Inert atmosphere; | 99% |
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 10 - 35℃; for 16h; | 100% |
| In dichloromethane at 5℃; for 0.5h; | 99% |
| Multistep reaction; | 96% |
| Conditions | Yield |
|---|---|
| at 100℃; for 12h; Ionic liquid; Green chemistry; | 100% |
| aluminum oxide; zinc(II) oxide at 100℃; for 2h; Condensation; | 98% |
| In water at 20℃; for 1.33333h; Solvent; Time; Green chemistry; | 97% |
| Conditions | Yield |
|---|---|
| In chloroform at 20℃; for 288h; | 100% |
| In dichloromethane for 13h; Inert atmosphere; Reflux; | 98.3% |
| In dichloromethane for 13h; Reflux; Inert atmosphere; | 95.3% |
| Conditions | Yield |
|---|---|
| With sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ethyl cyanoglyoxylate-2-oxime In water; N,N-dimethyl-formamide at 20℃; for 3h; Reagent/catalyst; Solvent; | 100% |
| With 4-methyl-morpholine; dmap; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine In dichloromethane at 35℃; for 0.1h; microwave irradiation; | 99% |
| With sulfated tungstate at 70℃; for 0.166667h; Neat (no solvent); | 99% |
-
-
54221-37-3
diethyl meso-2,5-dibromoadipate
-
-
100-46-9
benzylamine
-
-
17740-40-8
diethyl meso-1-benzyl-2,5-pyrrolidinedicarboxylate
| Conditions | Yield |
|---|---|
| In toluene for 4h; Reflux; | 100% |
-
-
97-65-4
2-methylenesuccinic acid
-
-
100-46-9
benzylamine
-
-
5733-86-8
1-benzyl-5-oxopyrrolidine-3-carboxylic acid
| Conditions | Yield |
|---|---|
| at 130℃; Inert atmosphere; | 100% |
| 86% | |
| at 130℃; for 2.5h; Inert atmosphere; | 82.9% |
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