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inquirySulfur Dioxide SO2 CAS No.: 7446-09-5 EINECS No.: 231-195-2 UN No.: UN1079 Purity: 99.9% Dot Class: 2.3 Appearance: Colorless Liquid Grade Standard: Industrial Grade Precursor to sulfuric acid: Sulfur dioxide is an
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Application:Valuable reagent offered as a solution in tetrahydrofuran for more convenient handling.
sulfur dichloride
sulfur trioxide
A
thionyl chloride
B
sulfur dioxide
Conditions | Yield |
---|---|
In neat (no solvent) below -10°C or under pressure;; | A 100% B n/a |
Conditions | Yield |
---|---|
With oxygen 1000°C; | A 100% B 0% |
With O2 1000°C; | A 100% B 0% |
N-benzyl-2,4-dinitro-N-(prop-2-yn-1-yl)benzenesulfonamide
B
S-(2,4-Dinitrophenyl)-cystein
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
A
S-(2,4-Dinitrophenyl)-cystein
B
2-methoxy-N-propylaniline
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
A
S-(2,4-Dinitrophenyl)-cystein
B
butyl-(2-methoxy-phenyl)amine
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
A
N-methylpropargylamine
B
S-(2,4-Dinitrophenyl)-cystein
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
N-benzyl-N-(3-(N-(2-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide
A
S-(2,4-Dinitrophenyl)-cystein
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
N-benzyl-N-(3-(N-(3-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide
A
S-(2,4-Dinitrophenyl)-cystein
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
N-benzyl-N-(3-(N-(4-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide
A
S-(2,4-Dinitrophenyl)-cystein
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B 100% C n/a |
(N-benzyl, N-methyl) 2,4-dinitrophenylsulfonamide
A
S-(2,4-Dinitrophenyl)-cystein
B
sulfur dioxide
C
benzyl-methyl-amine
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B 100% C n/a |
Conditions | Yield |
---|---|
995 °C in N2; part of a Mg-S-I water splitting cycle; | A 99% B 99% |
copper(II) oxide In gas equil. react.; | |
platinum In gas equil. react.; |
A
S-(2,4-Dinitrophenyl)-cystein
B
sulfur dioxide
C
N-allyl-3-methoxyaniline
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B 99% C n/a |
sulfur dichloride
sulfur trioxide
A
thionyl chloride
B
sulfur dioxide
Conditions | Yield |
---|---|
In neat (no solvent) below -10°C or under pressure;; | A 100% B n/a |
Conditions | Yield |
---|---|
With oxygen 1000°C; | A 100% B 0% |
With O2 1000°C; | A 100% B 0% |
N-benzyl-2,4-dinitro-N-(prop-2-yn-1-yl)benzenesulfonamide
A
N-propargylbenzylamine
B
S-(2,4-Dinitrophenyl)-cystein
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
A
S-(2,4-Dinitrophenyl)-cystein
B
2-methoxy-N-propylaniline
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
A
S-(2,4-Dinitrophenyl)-cystein
B
butyl-(2-methoxy-phenyl)amine
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
A
N-methylpropargylamine
B
S-(2,4-Dinitrophenyl)-cystein
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 100% |
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 99% |
sulfur dioxide
Conditions | Yield |
---|---|
With oxygen In neat (no solvent) heating Ag2S in a quartz tube (4 cm*cm cross section) under O2/N2 (15 vol % O2) at 1200°C;; | 98% |
With O2 In neat (no solvent) heating Ag2S in a quartz tube (4 cm*cm cross section) under O2/N2 (15 vol % O2) at 1200°C;; | 98% |
With sulfuric acid by concd. H2SO4, formation of SO2 promoted by SeO2 or HgSO4; |
A
S-(2,4-Dinitrophenyl)-cystein
B
N-ethyl-m-anisidine
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 98% |
N-benzyl-N-(3-(N-(2-fluorophenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide
A
S-(2,4-Dinitrophenyl)-cystein
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 98% |
Conditions | Yield |
---|---|
With sulfuryl dichloride In benzene equimolar amt. of SO2Cl2 in boiling benzene; mechanism discussed;; a small amt. of polymeric products forms in addition;; | A 97% B >99 |
1,2,2-trifluorodichloroethanesulfonyl chloride
A
1,1,2-Trichloro-1,2,2-trifluoroethane
B
sulfur dioxide
Conditions | Yield |
---|---|
200°C, 7 days; | A 97% B 97% |
100°C, 7 days; | A 19% B 18% |
A
S-(2,4-Dinitrophenyl)-cystein
B
3-methoxy-N-methylaniline
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 97% |
A
N-(ethyl)propargylamine
B
S-(2,4-Dinitrophenyl)-cystein
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 97% |
A
S-(2,4-Dinitrophenyl)-cystein
B
N-benzyl-2-methoxyaniline
C
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 96% |
sulfuryl dichloride
A
sulfur dioxide
B
sulfur
C
cadmium(II) chloride
Conditions | Yield |
---|---|
3-4 h at 350°C in a sealed bombe tube; | A n/a B n/a C 95% |
3-4 h at 350°C in a sealed bombe tube; | A n/a B n/a C 95% |
16 h at 250°C in a sealed bombe tube; | A n/a B n/a C 94% |
Conditions | Yield |
---|---|
With oxygen In neat (no solvent) heating in a stream of O2 at 550 - 600°C (formation of SO2 from 82 % of S and of Ag2SO4), later at 980 - 1070°C (decomposition of Ag2SO4);; | A 95% B 5% |
With O2 In neat (no solvent) heating in a stream of O2 at 550 - 600°C (formation of SO2 from 82 % of S and of Ag2SO4), later at 980 - 1070°C (decomposition of Ag2SO4);; | A 95% B 5% |
carbon disulfide
dihydrogen peroxide
oxygen
A
sulfur dioxide
B
hydroperoxyl radical
Conditions | Yield |
---|---|
In gas Kinetics; byproducts: HS; other Radiation; H2O2 is photolysed at 266 nm (Nd:YAG laser) in a flow reactor, addn. of CS2 (NO) and O2 (N2); HO2 yield measurement by LMR (laser magnetic resonance), SO2 yield measurement by CIMS (chemical ionization mass spectometry); | A 90% B 95% |
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B n/a C 95% |
A
S-(2,4-Dinitrophenyl)-cystein
B
sulfur dioxide
C
2-methoxy-N-(prop-2-yn-1-yl)aniline
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B 91% C n/a |
1-phenyl-1,4-dihydro-2,3-benzoxathiin-3-oxide
A
sulfur dioxide
Conditions | Yield |
---|---|
In aq. phosphate buffer; acetonitrile at 37℃; for 0.65h; pH=7.4; Kinetics; Inert atmosphere; | A 89% B n/a |
sulfur dioxide
water
iodine
A
sulfuric acid
B
hydrogen iodide
Conditions | Yield |
---|---|
0 - 25 °C; part of a Mg-S-I water splitting cycle; | A 100% B 100% |
Conditions | Yield |
---|---|
at 170-180°C; in very dilute soln. complete decompn. in 2 h, incomplete decompn. in concd. solns.; | A n/a B 100% |
byproducts: H2S4O6; | |
sodium thiosulfate In water 100°C; |
sulfur dioxide
Conditions | Yield |
---|---|
other Radiation; by electron impact (70 eV); | 100% |
other Radiation; by electron impact (70 eV); | 100% |
Irradiation (UV/VIS); |
Conditions | Yield |
---|---|
exothermic; | 100% |
In Petroleum ether 50 min; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; redn. of SO2 by H2 (1:2), SO2-conversion at 114°C practically 100%;; | A 100% B n/a |
In neat (no solvent) byproducts: H2O; redn. of SO2 by H2 (1:2), SO2-conversion at 114°C practically 100%;; | A 100% B n/a |
In neat (no solvent) byproducts: H2O; redn. of SO2 by H2, investigation of equilibrium constants;; |
Conditions | Yield |
---|---|
With catalyst: CeO2.Co3O4 284-465°C, metal oxide mixture catalysts activity: CuCo2O4; | 100% |
With catalyst: CuCo2O4 284-465°C, metal oxide mixture catalysts activity: CuCo2O4; | 100% |
With catalyst: LaCoO3 284-465°C, metal oxide mixture catalysts activity: CuCo2O4; | 100% |
Conditions | Yield |
---|---|
With catalyst: cobalt molybdate/SiO2 great excess of CH4; Co molybdate supported on SiO2; at 593-704°C and 1 atm; | 100% |
With catalyst: V/Al2O3 20 vol% SO2 : 80 vol% CH4; 5 % V on γ-Al2O3; at 545°C and atm. pressure; | 95-100 |
calcium(II) sulfide |
selenium
arsenic pentafluoride
fluorosulfonylchloride
sulfur dioxide
iodine
Conditions | Yield |
---|---|
byproducts: AsF3; SO2 and AsF5 were condensed into Se and I2; after 16 h no insoluble material was observed; condensed SO2ClF into the soln.; react. time 3 h; slowly (ca.20 h) condension; cooling; crystn.; washing; removed volatile materials by evacuation; subjected to vac. for <0.2 h; elem. anal.; | 100% |
byproducts: AsF3; SO2 and AsF5 were condensed onto Se and I2; after 16 h no insoluble material was observed; condensation of SO2ClF onto the soln.; react. time 7 h; slowly (ca.20 h) condensation of solvent; cooling; crystn.; washing; removal of volatile material by evacuation; elem. anal.; | 104 % |
Conditions | Yield |
---|---|
AsF5 was condensed onto a mixture of Se and I2 in liq. SO2; react. time 4 h; slowly (ca.20 h) condensation of solvent; crystn.; after 16 h removal of volatile material by evacuation; elem. anal.; X-ray diffraction; | 100% |
AsF5 was condensed onto a mixture of Se and I2 in liq. SO2; react. time 6 h; slowly (ca.20 h) condensation; crystn.; after 16 h removal of volatile materials by evacuation; elem. anal.; X-ray diffraction; | 106 % |
sulfur dioxide
dicarbonylbis{μ-bis(diphenylphosphino)methane-P,P'}-μ-sulfur-μ-(sulfurdioxide)-dirhodium(I)
Conditions | Yield |
---|---|
In dichloromethane (Ar), SO2 bubbled for 5 min through soln.; n-hexane added, dried for a short time in vacuum, elem. anal., MS; | 100% |
(RhCO)(Mn(CO)3)(((C6H5)2P)2CH2)2
sulfur dioxide
bis{μ-bis(diphenylphosphino)methane-P,P'}-tricarbonyl{carbonylrhodium(0)}-μ-(sulfurdioxide)-mangan(0)
Conditions | Yield |
---|---|
In dichloromethane (Ar), SO2 bubbled for 5 min through soln.; solvent removed in vacuum, dried in vacuum, elem. anal., MS; | 100% |
(RhClCO)(Mo(CO)3)(((C6H5)2P)2CH2)2
sulfur dioxide
bis{μ-bis(diphenylphosphino)methane-P,P'}-μ-carbonyl-dicarbonyl{chlororhodium(I)}-μ-(sulfurdioxide)-molybdenum(0)
Conditions | Yield |
---|---|
In dichloromethane (Ar), SO2 bubbled for 10 min through soln., stirred for 1 h under SO2-atmosphere; n-hexane added, dried in vacuum, elem. anal., MS; | 100% |
[RhCl(O2)(2,6-(C(Me)=NiPr)2C5H3N)]
sulfur dioxide
[RhCl(O2SO2)(2,6-(C(Me)=NiPr)2C5H3N)]
Conditions | Yield |
---|---|
In dichloromethane-d2 SO2-bubbling (room temp., 1 min); detd. by (1)H NMR spectroscopy; | 100% |
Conditions | Yield |
---|---|
In ethanol; dichloromethane a soln. of complex in CH2Cl2 was mixed with ethanol and satd. with SO2 for 15 min at room temp., stirred for 1 h (N2); the solvent was removed under reduced pressure; elem. anal.; | 100% |
[dicyclohexyl(2-methoxyethyl)phosphine-O,P](pentamethylcyclopentadienyl)(triethyl phosphite)ruthenium(II) tetraphenylborate
sulfur dioxide
[dicyclohexyl(2-methoxyethyl)phosphine-P](pentamethylcyclopentadienyl)(η(1)-sulphur dioxide)(triethyl phosphite)ruthenium(II)tetraphenylborate
Conditions | Yield |
---|---|
In dichloromethane absence of air and moisture; bubbling SO2 for 5 min, stirring for 5 min; solvent removal (reduced pressure), washing (pentane), collection (filtration), drying (vac.); elem. anal.; | 100% |
(RhClCO)(W(CO)3)(((C6H5)2P)2CH2)2
sulfur dioxide
bis{μ-bis(diphenylphosphino)methane-P,P'}-μ-carbonyl-dicarbonyl{chlororhodium(I)}-μ-(sulfurdioxide)-tungsten(0)
Conditions | Yield |
---|---|
In dichloromethane (Ar), SO2 bubbled for 10 min through soln., stirred for 6 h under SO2-atmosphere; n-hexane added, dried in vacuum, elem. anal., MS; | 100% |
(IrClCO)(Mo(CO)3)(((C6H5)2P)2CH2)2
sulfur dioxide
bis{μ-bis(diphenylphosphino)methane-P,P'}-μ-carbonyl-dicarbonyl{chloroiridium(I)}-μ-(sulfurdioxide)-molybdenum(0)
Conditions | Yield |
---|---|
In dichloromethane (Ar), SO2 bubbled for 10 min through soln., stirred for 1 h under SO2-atmosphere; n-hexane added, dried in vacuum, elem. anal., MS; | 100% |
selenium
silver tetrakis([2,2,2-trifluoro-1,1-bis(trifluoromethyl)ethyl]oxy)aluminate
sulfur dioxide
Conditions | Yield |
---|---|
In sulfur dioxide liq. SO2 was condensed into mixt. Se and Ag(Al(OC(CF3)3)4) (6:1), stirred for several days; react. mixt. was filtered and cooled to 2°C for 2 days, solvent was removed in vacuo; elem. anal.; | 100% |
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