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inquiryCadmium chloride CAS 10108-64-2 Product Description Product Name Cadmium chloride CAS N
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Product name: Cadmium Chloride CAS No.:10108-64-2 Molecule Formula: CdCl2 Molecule Weight:183.31 Purity: 98.0% Package: 25kg/bag Description:White or colorless monoclinic crystals Manufacture Standards:Enterprise Standard
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inquiryCadmium chloride CAS NO.10108-64-2 Application:Cadmium chloride CAS NO.10108-64-2
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Conditions | Yield |
---|---|
In neat (no solvent) 250°C (4 h/CO2 stream);; | 96% |
In neat (no solvent) 250°C (4 h/CO2 stream);; | 96% |
In neat (no solvent) 250°C (16 h/sealed tube);; | 94% |
sulfuryl dichloride
A
sulfur dioxide
B
sulfur
C
cadmium(II) chloride
Conditions | Yield |
---|---|
3-4 h at 350°C in a sealed bombe tube; | A n/a B n/a C 95% |
3-4 h at 350°C in a sealed bombe tube; | A n/a B n/a C 95% |
16 h at 250°C in a sealed bombe tube; | A n/a B n/a C 94% |
Conditions | Yield |
---|---|
In sulfolane N2 atm.; stirring (4-5 d, 60°C); distn. (vac., 50°C); elem. anal.; | A 94% B n/a |
Conditions | Yield |
---|---|
In sulfolane N2 atm.; stirring (4-5 d, 60°C); distn. (vac., 80°C); elem. anal.; | A 76% B n/a |
sulfuryl dichloride
A
selenium tetrachloride
B
diselenium dichloride
C
cadmium(II) chloride
Conditions | Yield |
---|---|
SO2Cl2 vapor diluted with CO2, 2.5h at 280-290°C; | A n/a B n/a C 71% |
SO2Cl2 vapor diluted with CO2, 2.5h at 280-290°C; | A n/a B n/a C 71% |
SO2Cl2 vapor diluted with CO2, 5h in room temp., then short heating at 180-190°C; | A n/a B n/a C 60% |
SO2Cl2 vapor diluted with CO2, 5h in room temp., then short heating at 180-190°C; | A n/a B n/a C 60% |
Conditions | Yield |
---|---|
In water The formed CdCl2 behaves as catalyst in the reaction.; | A 66% B 7% C 19% D 8% |
In water The formed CdCl2 behaves as catalyst in the reaction.; | A 66% B 7% C 19% D 8% |
dicarbonyl(cyclopentadienyl)iron(II) chloride
cadmium
A
cyclopentadienyl iron(II) dicarbonyl dimer
C
cadmium(II) chloride
Conditions | Yield |
---|---|
In tetrahydrofuran (Ar); at 20°C; sepd., evapd., treated with Et2O, sepd., concd. (vac.), pentane added at-5°C, washed (cold pentane), dried (vac.); elem. anal.; | A 14% B 53.6% C 20.6% |
Conditions | Yield |
---|---|
In acetonitrile N2 atm.; stirring (4-5 d, 60°C), pptn.; filtn., washing (CH3CN), extraction (pentane), distn.; elem. anal.; | A 52% B n/a |
bis(pentafluorophenyl)cadmium
indium(III) chloride
B
cadmium(II) chloride
Conditions | Yield |
---|---|
In acetonitrile byproducts: C6F5H; N2 atm.; heating (-30 to 0°C), stirring (24 h, room temp.), refluxing; evapn., extraction (n-pentane), evapn.; elem. anal.; | A 42.7% B n/a |
bis(pentafluorophenyl)cadmium
indium(III) chloride
B
cadmium(II) chloride
Conditions | Yield |
---|---|
In further solvent(s) byproducts: C6F5H; N2 atm.; glyme, heating (-30 to 0°C), stirring (24 h, room temp.), refluxing; evapn., extraction (n-pentane), evapn.; | A 34.7% B n/a |
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) dehydrn. between 60-180 °C, pyrolysis in the range of 220-800 °C; | A 18.53% B n/a |
cadmium(II) chloride
Conditions | Yield |
---|---|
In neat (no solvent) thermal decomposition; |
cadmium(II) chloride
Conditions | Yield |
---|---|
With triethyl orthoformate refluxing for several hours in triethyl orthoformate; | |
In neat (no solvent) dehydratation (433K, vac.); | |
In neat (no solvent) at 200°C for 12 h; |
Conditions | Yield |
---|---|
decomposition in presence of water;; | |
decomposition in presence of water;; |
Conditions | Yield |
---|---|
In not given heating for several days;; |
Conditions | Yield |
---|---|
dissolving CdS in hot concd. HCl; filtration; precipitation with (NH4)2CO3; glowing the precipitate; dissolving the residue in HCl;; | |
dissolving CdS in hot concd. HCl; filtration; precipitation with (NH4)2CO3; glowing the precipitate; dissolving the residue in HCl;; |
Conditions | Yield |
---|---|
slow heating of CdS containing Cl; 1/2 h at 800°C or 1000°C; | |
slow heating of CdS containing Cl; 1/2 h at 800°C or 1000°C; |
thionyl chloride
A
disulfur dichloride
B
sulfur dioxide
C
cadmium(II) chloride
Conditions | Yield |
---|---|
In neat (no solvent) reaction of CdS with SOCl2 in a sealed tube at 200 °C;; | |
In neat (no solvent) reaction of CdS with SOCl2 in a sealed tube at 200 °C;; |
diselenium dichloride
A
selenium
B
sulfur
C
cadmium(II) chloride
Conditions | Yield |
---|---|
reaction of CdS with COCl2 at 400 °C;; | |
400°C; | |
reaction of CdS with COCl2 at 400 °C;; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: COS; passing stream of COCl2 over CdS at 400 °C;; |
Conditions | Yield |
---|---|
In benzene addition of dry CdS to a solution of S2Cl2 in benzene; decantation from green-black lumps; heating solution at 70 °C;; heterogenous product mixture obtained;; | |
In toluene addition of dry CdS to a solution of S2Cl2 in toluene; decantation from green-black lumps; heating solution at 70 °C;; heterogenous product mixture obtained;; | |
In carbon disulfide addition of dry CdS to a solution of S2Cl2 in CS2; decantation from green-black lumps; heating solution at 70 °C;; heterogenous product mixture obtained;; |
Conditions | Yield |
---|---|
In toluene shaking;; | |
In toluene shaking;; |
Conditions | Yield |
---|---|
In neat (no solvent) Kinetics; reaction at 200-500°C;; enthalpy of reaction;; |
hydrogenchloride
A
sulfuric acid
B
Iodine monochloride
C
cadmium(II) chloride
Conditions | Yield |
---|---|
With potassium iodate In not given byproducts: S, KCl, H2O; oxidation with KIO3 in presence of HCl;; | |
With KIO3 In not given byproducts: S, KCl, H2O; oxidation with KIO3 in presence of HCl;; |
Conditions | Yield |
---|---|
In neat (no solvent) passing gaseous HCl over CdS;; | |
In neat (no solvent) passing gaseous HCl over CdS;; |
Conditions | Yield |
---|---|
In water equil. reaction at 20 and 80°C; amt. of H2S depends on the temp. and the presence of NaCl; | |
In neat (no solvent) 232-352°C; heterogenous equil.; | |
In neat (no solvent) 232-352°C; heterogenous equil.; |
Conditions | Yield |
---|---|
at room temp.; SO2Cl2 vapor dild. with CO2; |
sulfuryl dichloride
A
tellurium dichloride
B
tellurium tetrachloride
C
cadmium(II) chloride
Conditions | Yield |
---|---|
420-450°C; SO2Cl2 vapor dild. with CO2; |
Conditions | Yield |
---|---|
In water ratio Cd/picoline 1:5; elem. anal.; | 100% |
In neat (no solvent) excess of picoline; elem. anal.; | 92.5% |
In ethanol; water treatment of aq. soln. CdCl2 with picoline in EtOH (ratio Cd/picoline 1:5); elem. anal.; | 67% |
In water; acetone treatment of aq. soln. CdCl2 with picoline in acetone (ratio Cd/picoline 1:5); elem. anal.; | 58.9% |
cadmium(II) chloride
Conditions | Yield |
---|---|
In not given 2 d; | 100% |
diclofenac sodium
cadmium(II) chloride
{Cd(C6H3Cl2NHC6H4CH2COO)2(H2O)}
Conditions | Yield |
---|---|
With H2O; KOH In water byproducts: NaCl; mixing aq. soln. of the components, adjusting to pH 5.5-7.5 with KOH and stirring at room temp. for 4-6 h; filtn., washing with water, drying over silica gel (vac.) and over P4O10 at 90°C (vac.); | 100% |
cadmium(II) chloride
B
cadmium
Conditions | Yield |
---|---|
In tetrahydrofuran N2-atmosphere; stirring Yb-complex with 0.5 equiv. of halide (room temp., 16 h); filtration, washing (THF), evapn. (vac.), drying (vac.); | A 80% B 100% |
methyl methylphenylphosphinate
cadmium(II) chloride
Conditions | Yield |
---|---|
In further solvent(s) byproducts: MeCl; slow heating in neat Ph(Me)P(O)OMe until complete pptn.; particle size and polymerization degree depending on heating rate; | 100% |
cadmium(II) chloride
Conditions | Yield |
---|---|
With triethylamine In chloroform; acetonitrile CdCl2 in MeCN was refluxed for 15 min, soln. vacataporphyrin in CHCl3 and Et3N were added and refluxed for 20 min; solvent was evapd., residue was mixed with CH2Cl2 and filtered, solvent was evapd.; | 100% |
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) at 720°C for 6 d; | 99% |
With Er2O3 In neat (no solvent, solid phase) ground, pressed, sealed, heated at 720°C for 6 d; cooled to 300°C at 4°C/h; |
tellurium(IV) oxide
cadmium(II) chloride
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) at 670°C for 6 d; | 99% |
cadmium(II) chloride
cadmium(II) tetraisopropyldiselenoimidodiphosphinate
Conditions | Yield |
---|---|
With sodium methoxide In methanol byproducts: NaCl; sodium methoxide added to a soln. of P compd., stirred for 10 min at room temp., metal salt added, stirred for 2-3 h; ppt. filtered, dried (vac.), recrystd. (CH2Cl2/methanol); elem. anal.; | 99% |
With sodium methylate In methanol for 3h; Inert atmosphere; Schlenk technique; Heating; | 77% |
N,N'-ethylenebis(pyrrolidine-2-thione)
cadmium(II) chloride
Conditions | Yield |
---|---|
In ethanol pptn. on mixing equimolar amts.; elem. anal.; | 99% |
cadmium(II) chloride
Conditions | Yield |
---|---|
In chloroform; acetonitrile a mixt. of the ligand and anhyd. CdCl2 was refluxed in 1:1 CH2Cl2-MeCN for ca. 2 h, the reaction was monitored by UV-vis spectroscopy; filtd. and evapd. to dryness; | 99% |
cadmium(II) chloride
Conditions | Yield |
---|---|
With triethylamine In chloroform dissolving ligand in CHCl3 with NEt3, addn. of metal salt, reflux for 30min; evapn., dissolving in CH2Cl2, washing with water, drying org. layer withNa2SO4, filtration, evapn., recrystn. (CHCl3/hexane); | 99% |
Conditions | Yield |
---|---|
In water stirring (pH=4-6), pptn., digestion (water bath, 30 min), cooling; filtration, washing (water, ether), drying (vac.); elem. anal.; | 99% |
cadmium(II) chloride
Conditions | Yield |
---|---|
In chloroform; acetonitrile a mixt. in CHCl3 and CH3CN was refluxed under N2 for 30 min; evapd. to dryness, dissolved in min CH2Cl2, filtered, the solvent was removed; | 99% |
cadmium(II) chloride
chlorocadmium(II) 11,16-bis(4-nitrophenyl)-6,6,21,21-tetraphenyl-meta-benziporphodimethene
Conditions | Yield |
---|---|
In chloroform; acetonitrile a mixt. of the ligand and anhyd. CdCl2 was refluxed in 1:1 CH2Cl2-MeCN for ca. 2 h, the reaction was monitored by UV-vis spectroscopy; filtd. and evapd. to dryness; | 99% |
cadmium(II) chloride
Conditions | Yield |
---|---|
In chloroform; acetonitrile under N2 atm. soln. CdCl2 and ligand in CHCl3-MeCN was refluxed for 1 h; solvents were removed in vacuo, residue was dissolved in dry CH2Cl2, filtered and evapd.; | 99% |
2-[bis(2-phenylethyl)thiophosphorylhydroxymethyl]-1-ethylimidazole
cadmium(II) chloride
Conditions | Yield |
---|---|
In acetone org. ligand and CdCl2 mixed in anhyd. acetone (20-25°C); kept (8 h); pptd. with ether; filtered; washed with acetone-ether mixt. (1:1); dried (vac.); elem. anal.; | 99% |
1,4-bis((1H-pyrrol-2-yl)methylene)thiosemicarbazide
cadmium(II) chloride
Cd(1,4-bis((1H-pyrrol-2-yl)methylene)thiosemicarbazide)Cl2
Conditions | Yield |
---|---|
In methanol Reflux; | 98.29% |
1,4-bis((1H-pyrrol-2-yl)methylene)thiosemicarbazide
cadmium(II) chloride
Conditions | Yield |
---|---|
In methanol Reflux; | 98.27% |
3-(vinylthio)-1,2,4-triazole
cadmium(II) chloride
Conditions | Yield |
---|---|
In not given mixing calcd. amts. of ligand and metal salt dissolved in solvent (alc.or alc. and ether); ppt. formed was filtered off, washed, dried (room temp., vac.); elem. anal.; | 98% |
N,N-dimethylthiourea
cadmium(II) chloride
cadmium(II) Cl2 bis(N,N'-dimetylthiourea)
Conditions | Yield |
---|---|
In ethanol mixed in hot ethanol, stirred and refluxed for 2 h; filtered hot, crystd. at room temp. for 24 h, filtered, washed twice (ethanol), dried (vac.), dried (vac.), elem. anal.; | 98% |
2-[bis(2-phenylethyl)thiophosphorylhydroxymethyl]-1-vinylimidazole
cadmium(II) chloride
Conditions | Yield |
---|---|
In acetone org. ligand and CdCl2 mixed in anhyd. acetone (20-25°C); kept (8 h); pptd. with ether; filtered; washed with acetone-ether mixt. (1:1); dried (vac.); elem. anal.; | 98% |
1-(1-silatranylmethyl)-3,5-dimethyl-1H-pyrazole
cadmium(II) chloride
(1-(1-silatranylmethyl)-3,5-dimethyl-1H-pyrazole)*CdCl2
Conditions | Yield |
---|---|
In not given to soln. of CdCl2 in C6H6, CHCl3 or MeCN was added soln. of silatrane inC6H6, CHCl3 or MeCN, stirred at 70-80°C for 6-10 h; filtered, washed with MeCN, elem. anal.; | 98% |
ammonium phenyldithiocarbamate
ammonium N-ethyl-N-phenyldithiocarbamate
cadmium(II) chloride
Conditions | Yield |
---|---|
In water at 20℃; for 1h; | 98% |
pyridine-2-carboxamide thiosemicarbazide
water
cadmium(II) chloride
Conditions | Yield |
---|---|
In ethanol soln. of Cd salt mixed with soln. of ligand, stirred under reflux for 2 h; filtered, washed with anhydrous ether to apparent dryness, placed on warm plate at 35°C, elem. anal.; | 97.4% |
Conditions | Yield |
---|---|
In not given org. solvent (alcohol, acetone, ether or dioxane), stirring (room temp., 0.25 - 24 h); washing, drying (vacuum); elem. anal.; | 97% |
Conditions | Yield |
---|---|
In tetrahydrofuran under N2, mixt. of the phosphorane and CdCl2 in THF stirred for 12 h; filtration, washed (THF), pumped dry; elem. anal.; | 97% |
sodium N,N-diethyldithiocarbamate
cadmium(II) chloride
cadmium(II) diethyldithiocarbamate
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) byproducts: NaCl; placing of CdCl2 and NaS2CNEt2 in 1:2 ratio to the reactor; sealing, vibrating for 60 min; sublimating in vac. at 180-230°C; crystn.; elem. anal.; | 96.6% |
In water byproducts: NaCl; pptn. of complex from soln. at room temp., filtration while hot, drying (80°C, vac.); recrystn. (benzene); (1)H- and (13)C-NMR; | |
In water byproducts: NaCl; ZnCl2, the thiocarbamate in water, immediately pptn.; filtered hot to remove NaCl and any excess of unreacted thiocarbamate, dried (vac. at 80°C), recrystn. (boiling benzene); | |
In water solution of CdCl2 added to stirred solution of the ligand; filtered, dried, recrystd. from chloroform; |
cadmium(II) chloride
Conditions | Yield |
---|---|
In tetrahydrofuran; water byproducts: KCl; React. of 2 equiv of K-compd. in THF with CdCl2 in H2O; the 2 solns. are combined, along with addnl. H2O, and the mixt. is shaken.; Extn. with CH2Cl2, sepn. of CH2Cl2 layer from mixt., removal of solvent, mass spectroscopy, elem. anal.; | 96% |
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