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Cas:10025-67-9
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Min.Order:10 Gram
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Disulfide dichloride Melting point −80 °C (lit.) Boiling point 138 °C (lit.) Density 1.688 g/mL at 25 °C (lit.) Vapor density 4.7 (vs air) Vapor pressure 6.8 mm Hg ( 20 °C) Refractive index n20/D 1.658(lit.) Flas
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Disulfur dichlorideAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl
Disulfur Dichloride Application:Low temperature vulcanizing agent and adhesive for rubber Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/FCL for large amount.
Disulfur dichloride Basic information Product Name: Disulfur dichloride Synonyms: DISULFUR DICHLORIDE;U.N. 1828;SULFUR (I) CHLORIDE;SULFUR MONOCHLORIDE;SULPHURE CHLORIDE;SULPHUR MONO
Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Our advantages:1, High quality with competitive price:1) Standard:BP/USP/EP/Enterprise standard2) All Purity≥99%3) We are manufacturer
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Min.Order:1 Gram
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inquiryAppearance:Pale yellow liquid Storage:in low temperature, dry and ventilated environment Package:200KG Application:The rubber vulcanizing agent in low temperature Transportation:UN 3390 6.1/PG 1
Hangzhou KieRaychem Co.,Ltd.is located in Yuhang District of Hangzhou City and specialized in the chemical product customization, development, sales, import and export. Current business is focused on fine chemicals, pharmaceutical materials and int
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Min.Order:1 Gram
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Joyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom
Molecular Formula Cl2S2 Molecular Weight 135.03 CAS Registry Number 10025-67-9 EINECS 233-036-2 NameDisulfur dichlorid…
please contact us to confirm the required quantity and quote, we will provide you with COA,NMR,HPLC and other relevant informationAppearance:Red oily liquid Storage:Store in a cool place. Keep container tightly closed in a dry and well-ventilated pla
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Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por
sulfur
A
disulfur dichloride
Conditions | Yield |
---|---|
In further solvent(s) (under exclusion of moisture); refluxing in S2Cl2 at 160°C for 5 h; ppt. filtered, washed (CHCl2); | A n/a B 96% |
tetrachloromethane
sulfur
A
disulfur dichloride
B
carbon disulfide
Conditions | Yield |
---|---|
byproducts: S(x)Cl2; (N2), bomb reed, heated at 250°C for 24 h; cooled in liquid air in vac., distd.; | A 95% B n/a |
byproducts: S(x)Cl2; (N2), bomb reed, heated at 250°C for 15 h; cooled in liquid air in vac., distd.; | A 86% B n/a |
byproducts: S(x)Cl2; (N2), bomb reed, heated at 210°C for 8 d; cooled in liquid air in vac., distd.; | A 70% B n/a |
Conditions | Yield |
---|---|
With chaircoal with activated chaircoal at 500 °C; | A n/a B 90% |
With chaircoal with activated chaircoal at 500 °C; | A n/a B 90% |
In melt reduction to BaS in molten BaCl2; blowing chlorine into the melt; | |
With coal or coke or hydrocarbons at higher temp.; | |
In melt reduction to BaS in molten BaCl2; blowing chlorine into the melt; |
sulfur
chloroform
A
hydrogenchloride
B
disulfur dichloride
C
carbon disulfide
Conditions | Yield |
---|---|
(N2), bomb reed, heated at 205°C for 60 h; cooled in liquid air in vac. for a week, distd.; Raman spectr.; | A n/a B 80% C n/a |
sulfur
diselenium dichloride
A
disulfur dichloride
B
sulfur selenium dichloride
C
sulfur dichloride
D
selenium tetrachloride
Conditions | Yield |
---|---|
In neat (no solvent) heating of equimolar amount in closed tube to 200°C for 6 h;; fractional distillation;; | A n/a B 30% C n/a D n/a |
In neat (no solvent) heating of equimolar amount in closed tube to 200°C for 6 h;; fractional distillation;; | A n/a B 30% C n/a D n/a |
In neat (no solvent) heating of equimolar amount in closed tube to 100, 150, 200 or 250°C for 6 h;; fractional distillation;; | |
In neat (no solvent) heating of equimolar amount in closed tube to 100, 150, 200 or 250°C for 6 h;; fractional distillation;; |
Conditions | Yield |
---|---|
In not given room temp.;; |
Conditions | Yield |
---|---|
In not given | |
In not given |
Conditions | Yield |
---|---|
In further solvent(s) introduction of NOCl into soln. of S in S2Cl2;; |
sulfur
nitrosylchloride
A
disulfur dichloride
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In neat (no solvent) introduction of NOCl, 100°C;; |
chlorine dioxide
sulfur
A
disulfur dichloride
B
sulfur dioxide
Conditions | Yield |
---|---|
In neat (no solvent) decompn. under explosion;; |
carbon disulfide
iodine trichloride
A
disulfur dichloride
B
tetrachloromethane
Conditions | Yield |
---|---|
In neat (no solvent) room temp.;; |
carbon disulfide
chlorine
A
disulfur dichloride
B
tetrachloromethane
C
thiophosgene
Conditions | Yield |
---|---|
In gas passing through glowing tube of porcelaine;; |
Conditions | Yield |
---|---|
In neat (no solvent) room temp.;; | |
In not given | 0% |
carbon disulfide
chlorine
A
disulfur dichloride
B
tetrachloromethane
Conditions | Yield |
---|---|
In neat (no solvent) room temp.; presence of iodine, SbCl5, MoCl5;; |
Conditions | Yield |
---|---|
In neat (no solvent) fast reaction of FeS and Cl2 with evolution of heat;; |
thionyl chloride
A
disulfur dichloride
B
sulfur dioxide
C
cadmium(II) chloride
Conditions | Yield |
---|---|
In neat (no solvent) reaction of CdS with SOCl2 in a sealed tube at 200 °C;; | |
In neat (no solvent) reaction of CdS with SOCl2 in a sealed tube at 200 °C;; |
disulfur dichloride
Conditions | Yield |
---|---|
With sulfur | |
With S | |
With sulfur |
Conditions | Yield |
---|---|
With S In melt reaction during melting;; | |
With sulfur In melt reaction during melting;; |
copper(I) sulfide
sodium chloride
A
disulfur dichloride
C
copper(II) sulfate
Conditions | Yield |
---|---|
With oxygen byproducts: Na2SO4, SO2; information about the react. eqs. in detail and about dependence on temp.; | |
With oxygen byproducts: Na2SO4, SO2; information about the react. eqs. in detail and about dependence on temp.; |
Conditions | Yield |
---|---|
below 200°C;; almost pure;; | A n/a B n/a C >99 |
Conditions | Yield |
---|---|
In neat (no solvent) excess of SOCl2;; | |
In neat (no solvent) excess of SOCl2;; |
Conditions | Yield |
---|---|
Electrolysis; |
magnesium chloride
A
disulfur dichloride
B
sulfur
C
magnesium
Conditions | Yield |
---|---|
Electrolysis; |
Conditions | Yield |
---|---|
In neat (no solvent) slow reaction of PbS and Cl2 without evolution of heat;; |
thionyl chloride
A
disulfur dichloride
B
sulfur dioxide
C
zinc(II) chloride
Conditions | Yield |
---|---|
In neat (no solvent) reaction last several days at 150 - 200 °C;; |
Conditions | Yield |
---|---|
below 150°C; | |
below 150°C; |
thionyl chloride
A
disulfur dichloride
B
sulfur dioxide
C
phosphorus trichloride
Conditions | Yield |
---|---|
In neat (no solvent) excess SOCl2; 125°C;; | |
In neat (no solvent) excess SOCl2; 125°C;; |
Conditions | Yield |
---|---|
heating Bi with S2Cl2 at 138.6°C, 10 hours;; | 100% |
addition of S2Cl2 to Bi;; | |
addition of S2Cl2 to Bi;; |
disulfur dichloride
[(C5H5)2Ti(S4C6H10)]
bis(cyclopentadienyl)titanium dichloride
Conditions | Yield |
---|---|
In carbon disulfide byproducts: C6H10S6; air atm.; equimolar ratio, stirring, pptn.; filtn. (SiO2); | 100% |
Conditions | Yield |
---|---|
With chlorine heating in a stream of S2Cl2 and chlorine; | 100% |
With chlorine heating in a stream of S2Cl2 and chlorine; | 100% |
Conditions | Yield |
---|---|
In diethyl ether at -78 - 20℃; for 1.23333h; | 99% |
With triethylamine In dichloromethane at -20 - 20℃; for 1h; | 73% |
Conditions | Yield |
---|---|
In neat (no solvent) sealed quartz ampoule (vac.), heating (150°C, 2 h; then 420°C, 40 h); drying (vac., 150°C); elem. anal.; | 98% |
Conditions | Yield |
---|---|
In neat (no solvent) sealed quartz ampoule (vac.), heating (150°C, 2 h; then 420°C, 40 h); drying (vac., 150°C); | 98% |
Conditions | Yield |
---|---|
In neat (no solvent) sealed quartz ampoule (vac.), heating (150°C, 2 h; then 420°C, 40 h); drying (vac., 150°C); | 98% |
disulfur dichloride
molybdenum hexacarbonyl
Conditions | Yield |
---|---|
With CH2Cl2 In dichloromethane byproducts: CO; Irradiation (UV/VIS); standard Schlenk or glove-box techniques, addn. of S2Cl2 to a suspension of Mo(CO)6 in CH2Cl2, heating to reflux, irradiation (150 W W filament bulb), CO evolution, cooling to room temp. after 3.5 h; pptn., filtration, washing (CH2Cl2, Et2O), drying in vac., elem. anal.; | 98% |
disulfur dichloride
molybdenum hexacarbonyl
Conditions | Yield |
---|---|
In chloroform byproducts: CO, S; 65°C, 0.5 h; | 97% |
In tetrachloromethane byproducts: CO, S; 80°C, 0.5 h; | 85% |
disulfur dichloride
N-2-pyridylimidoyl-2-pyridylamidine
Conditions | Yield |
---|---|
In acetonitrile for 16h; Inert atmosphere; Reflux; | 96% |
Conditions | Yield |
---|---|
With antimony pentafluoride 60°C, 1 h; | 94% |
With SbF5 60°C, 1 h; | 94% |
disulfur dichloride
Conditions | Yield |
---|---|
In dichloromethane addn. of S2Cl2 to a soln. of the Tc-complex; stirring (room temp., 2 h).;; filtn., washing (ether), elem. anal.;; | 94% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: SO2; heating of dry As2O3 to 95 to 100°C under reflux; addition of S2Cl2 in portions that temp. arise to 120 to 125°C;; distillation; 99% AsCl3;; | 93% |
In neat (no solvent) room temp.;; | |
In neat (no solvent) byproducts: SO2, S; at 120°C;; |
Conditions | Yield |
---|---|
In neat (no solvent) | 93% |
disulfur dichloride
TcN(et2dtc)2
Conditions | Yield |
---|---|
In dichloromethane S2Cl2 was added to soln. of Tc-complex in CH2Cl2, vol. was reduced, silica-gel column was used, eluted with CH2Cl2 and ethyl acetate/CH2Cl2; collected, recrystd. from ethyl acetate/CH2Cl2; elem. anal.; | 92% |
disulfur dichloride
tetrasulfur tetranitride
thiotrithiazyl chloride
Conditions | Yield |
---|---|
In tetrachloromethane addn. of 6 fold excess S2Cl2 to S4Cl4 (in CCl4); heating with exclusion of moisture and air; pptn. on boiling; detailed description of apparatus and handling given;; washing (CCl4/N2 atm.); drying (vac.);; | 90% |
In tetrachloromethane boiling for two hours;; | |
In tetrachloromethane according H. G. Heal, Adv. Inorg. Chem. Radiochim. 15 (1972) 375; boiling CCl4; crystn. on slowly cooling; XRD; DSC; TGA; DTA; |
disulfur dichloride
Conditions | Yield |
---|---|
With sodium carbonate In dichloromethane under Ar; to a mixt. of the Cr complex and Na2CO3 in CH2Cl2 was added S2Cl2 in CH2Cl2, stirred for 2 d at 0°C; filtered, solvent was removed under reduced pressure, fractionated withEt2O; elem. anal.; | 90% |
disulfur dichloride
Conditions | Yield |
---|---|
In chloroform refluxed (2 h); cooled; filtered; washed (CHCl3, Et2O); dissolved in water, filtered, NH4PF6 added to induce pptn.; elem. anal.; | 90% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at -20 - 20℃; for 1h; | 90% |
Conditions | Yield |
---|---|
In further solvent(s) byproducts: SO2; Oso4 added to 22% soln. of Se in S2Cl2, heated at 60-80°C until SO2 ceased to evolve, sealed, heated at 100°C for 40 h; ppt. septd., filtered under inert atm., washed (S2Cl2, CS2, CCl4), elem.anal.; | 90% |
disulfur dichloride
sulfur
tungsten
tungsten(VI) sulfide tetrachloride
Conditions | Yield |
---|---|
In neat (no solvent) heating (2E-4 Torr, 425°C, 48 h), slow cooling; | 89% |
disulfur dichloride
lithium perfluoro isopropylideneamide
bis(hexafluoroisopropylidene amino) disulfane
Conditions | Yield |
---|---|
25°C 8 h,; | 89% |
25°C 8 h,; | 89% |
disulfur dichloride
ReCl2N(n-propyldiphenylphosphine)2
trichlorobis(n-propyldiphenylphosphine)(thionitrosyl)rhenium
Conditions | Yield |
---|---|
In dichloromethane N2-atmosphere; addn. of 0.5 equiv. S2Cl2 to Re-complex, stirring (1.5 h); evapn. (1E-2 Torr), crystn. (acetone); elem. anal.; | 89% |
disulfur dichloride
bromochlorotris(diethylphenylphosphine)(thionitrosyl)rhenium
Conditions | Yield |
---|---|
In dichloromethane N2-atmosphere; addn. of 0.5 equiv. S2Cl2 to Re-complex, stirring (room temp., 0.5 h); evapn. (1E-2 Torr), recrystn. (1,2-dichloroethane/pentane); elem. anal.; | 87% |
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