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Lonwin Chemical Group Limited

Dimethylamine CAS:124-40-3 Specification low price and high purity Welcome to contact us to get complete COA. Shanghai Lonwin Chemical Co.,Ltd is a leading manufacturer and supplier of chemicals in China.We develop,produce and distribute high

Factory supply Dimethylamine

Cas:124-40-3

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

low price and high purityAppearance:solid or liquid Storage:in sealed air resistant place Package:As customer require Application:Pharma;Industry;Agricultural Transportation:by sea or by airplane Port:any port in China

Dimethylamine solution, 40 wt. % in water 124-40-3

Cas:124-40-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

N-Nitrosodimethylamine
62-75-9

N-Nitrosodimethylamine

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With iron; nickel In water pH=6.3 - 9.2; Kinetics; Further Variations:; Reagents; Hydrogenation;100%
With isocyanate de chlorosulfonyle In diethyl ether for 10h; Ambient temperature;65%
With titanium(III) chloride; water
3-ethynyl-cyclohepta-1.3.5-triene
85809-41-2

3-ethynyl-cyclohepta-1.3.5-triene

(dimethylamino)trimethyltin
993-50-0

(dimethylamino)trimethyltin

A

3-(trimethylstannylethynyl)-1,3,5-cycloheptatriene
286387-63-1

3-(trimethylstannylethynyl)-1,3,5-cycloheptatriene

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
In neat (no solvent) Me3SnNMe2 added to 3-ethynyl-1,3,5-cycloheptatriene, react. mixture stirred without a solvent for 5 min at ambient temp., Me2NH evapd.; Me2NH evapd., product isolated in quant. yield;A 100%
B n/a
N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

benzylamine
100-46-9

benzylamine

A

N-benzylformamide
6343-54-0

N-benzylformamide

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With 2,3-dihydrophthalazine-1,4-dione at 80 - 95℃; for 40h;A 99%
B n/a
With cerium(IV) oxide at 100℃; for 12h; Reagent/catalyst;
C13H23N3O3S

C13H23N3O3S

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

A

C15H23N3O5S

C15H23N3O5S

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With 2,3-dihydrophthalazine-1,4-dione at 80 - 95℃; for 40h;A 98%
B n/a
1-dimethylamino-2,4-dinitronaphthalene
39139-79-2

1-dimethylamino-2,4-dinitronaphthalene

ethylamine
75-04-7

ethylamine

A

N-ethyl-2,4-dinitro-1-naphthylamine
27210-67-9

N-ethyl-2,4-dinitro-1-naphthylamine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
In water at 30℃; for 2h;A 98%
B n/a
propylamine
107-10-8

propylamine

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester
71240-22-7

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester

A

dimethyl amine
124-40-3

dimethyl amine

B

(E)-2-(1H-Benzoimidazol-2-yl)-3-propylamino-acrylic acid ethyl ester

(E)-2-(1H-Benzoimidazol-2-yl)-3-propylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 40℃; for 0.5h; Irradiation;A n/a
B 98%
SEC-BUTYLAMINE
33966-50-6

SEC-BUTYLAMINE

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester
71240-22-7

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester

A

dimethyl amine
124-40-3

dimethyl amine

B

(E)-2-(1H-Benzoimidazol-2-yl)-3-sec-butylamino-acrylic acid ethyl ester

(E)-2-(1H-Benzoimidazol-2-yl)-3-sec-butylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 60℃; for 0.5h; Irradiation;A n/a
B 98%
N,N-dimethylammonium chloride
506-59-2

N,N-dimethylammonium chloride

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With potassium hydroxide In water Inert atmosphere;98%
With potassium hydroxide In dichloromethane at -15 - -5℃; for 1h;90%
With potassium hydroxide Alkaline conditions;
N',N''-dicyclohexyl-N,N-dimethylguanidine
29882-02-8

N',N''-dicyclohexyl-N,N-dimethylguanidine

cyclohexylamine
108-91-8

cyclohexylamine

A

N,N',N''-tricyclohexylguanidine
4833-41-4

N,N',N''-tricyclohexylguanidine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A 98%
B n/a
2-benzooxazol-2-yl-3-dimethylamino-acrylic acid ethyl ester
71240-24-9

2-benzooxazol-2-yl-3-dimethylamino-acrylic acid ethyl ester

tert-butylamine
75-64-9

tert-butylamine

A

dimethyl amine
124-40-3

dimethyl amine

B

(E)-2-Benzooxazol-2-yl-3-tert-butylamino-acrylic acid ethyl ester

(E)-2-Benzooxazol-2-yl-3-tert-butylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 40℃; for 0.5h; Irradiation;A n/a
B 97%
tert-butylamine
75-64-9

tert-butylamine

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester
71240-22-7

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester

A

dimethyl amine
124-40-3

dimethyl amine

B

(E)-2-(1H-Benzoimidazol-2-yl)-3-tert-butylamino-acrylic acid ethyl ester

(E)-2-(1H-Benzoimidazol-2-yl)-3-tert-butylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 40℃; for 0.5h; Irradiation;A n/a
B 97%
o-chloranil
1198-55-6

o-chloranil

Hexamethylphosphorous triamide
1608-26-0

Hexamethylphosphorous triamide

A

dimethyl amine
124-40-3

dimethyl amine

B

tetrachlorobenzo<1,3,2>dioxaphosphol-2-yl-dimethylamine
320747-63-5

tetrachlorobenzo<1,3,2>dioxaphosphol-2-yl-dimethylamine

Conditions
ConditionsYield
With ammonium chloride In toluene for 1.5h; Heating;A n/a
B 97%
pyrrolidine
123-75-1

pyrrolidine

N',N''-dicyclohexyl-N,N-dimethylguanidine
29882-02-8

N',N''-dicyclohexyl-N,N-dimethylguanidine

A

N,N'-dicyclohexylpyrrolidine-1-carboximidamide
60006-28-2

N,N'-dicyclohexylpyrrolidine-1-carboximidamide

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A 97%
B n/a
N',N''-dicyclohexyl-N,N-dimethylguanidine
29882-02-8

N',N''-dicyclohexyl-N,N-dimethylguanidine

isopropylamine
75-31-0

isopropylamine

A

N,N'-Dicyclohexyl-N''-isopropyl-guanidin

N,N'-Dicyclohexyl-N''-isopropyl-guanidin

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A 97%
B n/a
tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

3-Dimethylamino-2-(formylaminomethyl)acrylsaeure-ethylester
74119-34-9

3-Dimethylamino-2-(formylaminomethyl)acrylsaeure-ethylester

A

ethyl 3-(dimethylamino)acrylate
924-99-2, 1117-37-9, 114894-59-6

ethyl 3-(dimethylamino)acrylate

B

dimethyl amine
124-40-3

dimethyl amine

C

tert-butyl alcohol
75-65-0

tert-butyl alcohol

Conditions
ConditionsYield
at 160℃; for 3h;A 96%
B n/a
C n/a
piperidine
110-89-4

piperidine

N',N''-dicyclohexyl-N,N-dimethylguanidine
29882-02-8

N',N''-dicyclohexyl-N,N-dimethylguanidine

A

N,N'-dicyclohexylpiperidine-1-carboximidamide
60006-25-9

N,N'-dicyclohexylpiperidine-1-carboximidamide

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A 96%
B n/a
N,N-dimethylhexa-1,5-dien-3-amine
75712-80-0

N,N-dimethylhexa-1,5-dien-3-amine

A

hex-5-en-1-al
764-59-0

hex-5-en-1-al

B

(E)-N,N-Dimethyl-1,5-hexadien-1-amin
82574-98-9

(E)-N,N-Dimethyl-1,5-hexadien-1-amin

C

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
at 223.5℃; for 12h;A n/a
B 95.8%
C n/a
at 160.2 - 200.1℃; Yield given. Yields of byproduct given;
With N,N-dimethyl-cyclohexanamine at 160.2 - 200.1℃; under 3 Torr; Kinetics; Thermodynamic data; Cope rearrengament, ΔH*, ΔG*, ΔS*, Ea;
((CH3)2N)2PH(Fe(CO)4)
116018-88-3

((CH3)2N)2PH(Fe(CO)4)

(PPh4)(hydridoiron(carbonyl)4)
103616-27-9

(PPh4)(hydridoiron(carbonyl)4)

A

((CH3)2N)PH(Fe(CO)4)2(1-)*(C6H5)4P(1+)={(C6H5)4P}{(CH3)2NPH(Fe(CO)4)2}

((CH3)2N)PH(Fe(CO)4)2(1-)*(C6H5)4P(1+)={(C6H5)4P}{(CH3)2NPH(Fe(CO)4)2}

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
A 95%
B n/a
3-(Dimethylaminomethyl)indole
87-52-5

3-(Dimethylaminomethyl)indole

ethylamine
75-04-7

ethylamine

A

3-(N-ethylamino)methylindole
57506-90-8

3-(N-ethylamino)methylindole

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
Heating;A 94%
B n/a
isopropylamine
75-31-0

isopropylamine

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester
71240-22-7

2-(1H-benzoimidazol-2-yl)-3-dimethylamino-acrylic acid ethyl ester

A

dimethyl amine
124-40-3

dimethyl amine

B

(E)-2-(1H-Benzoimidazol-2-yl)-3-isopropylamino-acrylic acid ethyl ester

(E)-2-(1H-Benzoimidazol-2-yl)-3-isopropylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 30℃; for 0.5h; Irradiation;A n/a
B 94%
isopropylamine
75-31-0

isopropylamine

N′,N″-diisopropyl-N,N-dimethyl guanidine
68897-42-7

N′,N″-diisopropyl-N,N-dimethyl guanidine

A

N,N', N''-tri(isopropyl)guanidine
121948-77-4

N,N', N''-tri(isopropyl)guanidine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A 94%
B n/a
N-(N3-p-toluenesulfonyl)-3-aminopropylphthalimide
38353-77-4

N-(N3-p-toluenesulfonyl)-3-aminopropylphthalimide

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

A

2,3-dihydrophthalazine-1,4-dione
1445-69-8

2,3-dihydrophthalazine-1,4-dione

B

N1-formyl-N3-tosyl-1,3-propanediamine
107976-50-1

N1-formyl-N3-tosyl-1,3-propanediamine

C

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With hydrazine hydrate at 80℃; for 3h;A n/a
B 93%
C n/a
ethyl (2E/Z)-2-(1,3-benzothiazol-2-yl)-3-(dimethylamino)acrylate
71240-23-8

ethyl (2E/Z)-2-(1,3-benzothiazol-2-yl)-3-(dimethylamino)acrylate

propylamine
107-10-8

propylamine

A

dimethyl amine
124-40-3

dimethyl amine

B

(Z)-2-Benzothiazol-2-yl-3-propylamino-acrylic acid ethyl ester

(Z)-2-Benzothiazol-2-yl-3-propylamino-acrylic acid ethyl ester

Conditions
ConditionsYield
at 40℃; for 0.5h; Irradiation;A n/a
B 93%
tetrakis(dimethylamido)diborane
1630-79-1

tetrakis(dimethylamido)diborane

N-butylamine
109-73-9

N-butylamine

A

tetrakis(n-butylamino)diborane(4)
7360-73-8

tetrakis(n-butylamino)diborane(4)

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
In hexane heating from 76 to 174°C during 21.6 h;A 93%
B n/a
4 equiv. n-C4H9NH2, slow react. at room temp.;
4 equiv. n-C4H9NH2, slow react. at room temp.;
(2-bromoethyl)dimethyl-(3,3-dimethylallyl)ammonium bromide
58369-78-1

(2-bromoethyl)dimethyl-(3,3-dimethylallyl)ammonium bromide

1-amino-2-propene
107-11-9

1-amino-2-propene

A

Allyl-[3,3-dimethyl-pent-4-en-(E)-ylidene]-amine
88019-80-1

Allyl-[3,3-dimethyl-pent-4-en-(E)-ylidene]-amine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With potassium hydroxide In water at 90 - 95℃; for 1h;A 92.7%
B 79.5%
With potassium hydroxide In water at 90 - 95℃; for 1h; Product distribution; ratio of reactants;A 92.7%
B 79.5%
cyclohexylamine
108-91-8

cyclohexylamine

N′,N″-diisopropyl-N,N-dimethyl guanidine
68897-42-7

N′,N″-diisopropyl-N,N-dimethyl guanidine

A

dimethyl amine
124-40-3

dimethyl amine

B

2-Cyclohexyl-1,3-diisopropylguanidine

2-Cyclohexyl-1,3-diisopropylguanidine

Conditions
ConditionsYield
With [ς:η1:η5-(OCH2)(Me2CH2)C2B9H9]Ti(NMe2) at 110 - 115℃;A n/a
B 92%
3-(Dimethylaminomethyl)indole
87-52-5

3-(Dimethylaminomethyl)indole

cyclohexylamine
108-91-8

cyclohexylamine

A

N-indol-3-ylmethylcyclohexylamine
53924-03-1

N-indol-3-ylmethylcyclohexylamine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
Heating;A 91%
B n/a
Conditions
ConditionsYield
With water at 25℃; Product distribution; Mechanism; anodic oxidation, carbonate buffer, pH 10; effect of substituents investigated with different types of β-alkanolamines;A 6.4%
B 0.5%
C 91%
D 90%
E 91%
1,1-dimethylhydrazine
57-14-7

1,1-dimethylhydrazine

β-naphthol
135-19-3

β-naphthol

A

1-amino-2-naphthol
2834-92-6

1-amino-2-naphthol

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
at 80℃; for 4h;A 91%
B n/a
(2-bromoethyl)dimethyl-(3,3-dimethylallyl)ammonium bromide
58369-78-1

(2-bromoethyl)dimethyl-(3,3-dimethylallyl)ammonium bromide

aniline
62-53-3

aniline

A

[3,3-Dimethyl-pent-4-en-(E)-ylidene]-phenyl-amine
88019-86-7

[3,3-Dimethyl-pent-4-en-(E)-ylidene]-phenyl-amine

B

dimethyl amine
124-40-3

dimethyl amine

Conditions
ConditionsYield
With potassium hydroxide In water at 90 - 95℃; for 1h;A 90.9%
B 84.9%
2-methyl-1,2-epoxypropane
558-30-5

2-methyl-1,2-epoxypropane

dimethyl amine
124-40-3

dimethyl amine

1-dimethylamino-2-methyl-propan-2-ol
14123-48-9

1-dimethylamino-2-methyl-propan-2-ol

Conditions
ConditionsYield
In water at -5 - 20℃; Schlenk technique; Inert atmosphere; Sealed tube;100%
With water In water at 20 - 50℃; for 120h; Sealed tube;91%
In water at 20℃; for 12h; Cooling with ice; Inert atmosphere;89%
2-chloropyridine-5-sulfonyl chloride
6684-39-5

2-chloropyridine-5-sulfonyl chloride

dimethyl amine
124-40-3

dimethyl amine

6-chloro-N,N-dimethylpyridine-3-sulfonamide
52480-31-6

6-chloro-N,N-dimethylpyridine-3-sulfonamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 2h;100%
With triethylamine In tetrahydrofuran at 20℃; for 0.5h;95%
With triethylamine In tetrahydrofuran at 20℃; for 0.5h;95%
1,10-dibromodecane
4101-68-2

1,10-dibromodecane

dimethyl amine
124-40-3

dimethyl amine

N,N,N',N'-tetramethyl-1,10-diaminodecane
1938-62-1

N,N,N',N'-tetramethyl-1,10-diaminodecane

Conditions
ConditionsYield
In chloroform at 20℃; for 24h;100%
With sodium carbonate In ethanol; water for 24h; Heating;92%
With ethanol
In benzene at 4 - 5℃;
at 4 - 5℃;
succinoyl dichloride
543-20-4

succinoyl dichloride

dimethyl amine
124-40-3

dimethyl amine

N,N,N',N'-tetramethylsuccinamide
7334-51-2

N,N,N',N'-tetramethylsuccinamide

Conditions
ConditionsYield
In water at 0℃; for 0.5h;100%
In diethyl ether at -78 - 20℃;91%
In dichloromethane; water at 0 - 20℃; for 20h; Inert atmosphere;81%
With diethyl ether
In water at 0℃; for 0.5h;
1 ,6-dibromohexane
629-03-8

1 ,6-dibromohexane

dimethyl amine
124-40-3

dimethyl amine

N,N,N',N'-tetramethylhexamethylenediamine
111-18-2

N,N,N',N'-tetramethylhexamethylenediamine

Conditions
ConditionsYield
In tetrahydrofuran at 0 - 20℃; for 24h;100%
In chloroform at 20℃; for 24h;100%
With sodium carbonate In ethanol; water for 24h; Heating;98%
cholic acid
81-25-4

cholic acid

dimethyl amine
124-40-3

dimethyl amine

(R)-N,N-dimethyl-4-((3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-3,7,12-trihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthrene-17-yl)valeramide
86678-85-5

(R)-N,N-dimethyl-4-((3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-3,7,12-trihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthrene-17-yl)valeramide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 16h; Inert atmosphere;100%
With tributyl-amine; chloroformic acid ethyl ester In 1,4-dioxane 10 deg C, 30 min then rt., 2 h;78%
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; for 10h;74.2%
With water at 250℃;
With tributyl-amine; chloroformic acid ethyl ester Multistep reaction;
dimethyl amine
124-40-3

dimethyl amine

ethylene dibromide
106-93-4

ethylene dibromide

N,N,N,N,-tetramethylethylenediamine
110-18-9

N,N,N,N,-tetramethylethylenediamine

Conditions
ConditionsYield
In tetrahydrofuran at 0 - 20℃; for 24h;100%
In chloroform at 20℃; for 24h;100%
dimethyl amine
124-40-3

dimethyl amine

propynoic acid methyl ester
922-67-8

propynoic acid methyl ester

methyl 3-(N,N-dimethylamino)-2-propenoate
999-59-7

methyl 3-(N,N-dimethylamino)-2-propenoate

Conditions
ConditionsYield
In diethyl ether at 20℃; for 1h;100%
With benzene
dimethyl amine
124-40-3

dimethyl amine

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

N,N,4-trimethylbenzenesulfonamide
599-69-9

N,N,4-trimethylbenzenesulfonamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 25℃; for 1h;100%
99%
With cesium fluoride supported on Celite at 50℃; for 0.75h; chemoselective reaction;91%
dimethyl amine
124-40-3

dimethyl amine

N-Nitrosodimethylamine
62-75-9

N-Nitrosodimethylamine

Conditions
ConditionsYield
With sulfuric acid; silica gel; sodium nitrite In dichloromethane at 20℃; for 0.5h; Nitrosation;100%
With Nafion-H(R); silica gel; sodium nitrite In dichloromethane at 20℃; for 0.166667h;100%
With trichloromelamine; silica gel; sodium nitrite In dichloromethane; water at 20℃; for 0.0333333h;100%
2-chloro-1,3-benzoxazole
615-18-9

2-chloro-1,3-benzoxazole

dimethyl amine
124-40-3

dimethyl amine

2-dimethylaminobenzoxazole
13858-89-4

2-dimethylaminobenzoxazole

Conditions
ConditionsYield
In tetrahydrofuran; water for 0.166667h; Inert atmosphere; Reflux;100%
In water at 20℃; for 1h;90%
In water at 20℃; for 5h; Green chemistry;71%
benzonitrile
100-47-0

benzonitrile

dimethyl amine
124-40-3

dimethyl amine

N,N-Dimethyl-benzamidine
20548-18-9, 39116-58-0

N,N-Dimethyl-benzamidine

Conditions
ConditionsYield
Stage #1: dimethyl amine With n-butyllithium In diethyl ether; hexane at -20℃; for 0.166667h;
Stage #2: benzonitrile at -20℃; for 1h;
100%
phenylborondichloride
873-51-8

phenylborondichloride

dimethyl amine
124-40-3

dimethyl amine

Bis-(dimethylamino)-phenylboran
1201-45-2

Bis-(dimethylamino)-phenylboran

Conditions
ConditionsYield
In pentane at -78 - 20℃; Inert atmosphere;100%
In hexane87%
In hexane87%
1 ,4-phenylenediisothiocyanate
4044-65-9

1 ,4-phenylenediisothiocyanate

dimethyl amine
124-40-3

dimethyl amine

3-[4-(3,3-dimethyl-thioureido)-phenyl]-1,1-dimethyl-thiourea
16349-56-7

3-[4-(3,3-dimethyl-thioureido)-phenyl]-1,1-dimethyl-thiourea

Conditions
ConditionsYield
at 20℃; under 750.06 Torr; Addition; solid-gas reaction;100%
dimethyl amine
124-40-3

dimethyl amine

Cinnamoyl chloride
102-92-1

Cinnamoyl chloride

(E)-N,N-dimethylcinnamamide
17431-39-9

(E)-N,N-dimethylcinnamamide

Conditions
ConditionsYield
In water at 0℃; for 0.75h;100%
In methanol for 15h; Ambient temperature;81%
In diethyl ether for 0.5h;46.9%
dimethyl amine
124-40-3

dimethyl amine

NBD chloride
10199-89-0

NBD chloride

N,N-dimethyl-7-nitrobenzo[c][1,2,5]oxadiazol-4-amine
1455-87-4

N,N-dimethyl-7-nitrobenzo[c][1,2,5]oxadiazol-4-amine

Conditions
ConditionsYield
In methanol100%
In dichloromethane at 20℃; for 2h;98%
With triethylamine In dichloromethane; water at 20℃; for 1.5h;52.7%
In ethanol
In water; ethyl acetate 1.) 0 deg C, 30 min, 2.) r.t., 2 h;
dimethyl amine
124-40-3

dimethyl amine

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N,N-dimethyl-3-phenylpropanamide
5830-31-9

N,N-dimethyl-3-phenylpropanamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere;100%
With triethylamine In diethyl ether93%
With triethylamine In diethyl ether Inert atmosphere;93%
Benzyloxymethyl-oxiran
2930-05-4

Benzyloxymethyl-oxiran

dimethyl amine
124-40-3

dimethyl amine

(+/-)-dimethyl<2-hydroxy-3-(benzyloxy)propyl>amine
97807-83-5

(+/-)-dimethyl<2-hydroxy-3-(benzyloxy)propyl>amine

Conditions
ConditionsYield
In tetrahydrofuran; water for 2h; Heating;100%
1,8-naphtholactone
5247-85-8

1,8-naphtholactone

dimethyl amine
124-40-3

dimethyl amine

N,N-Dimethyl-8-hydroxy-naphthalin-1-carboxamid
69674-57-3

N,N-Dimethyl-8-hydroxy-naphthalin-1-carboxamid

Conditions
ConditionsYield
In toluene Heating;100%
6-chloro-N,N'-diphenyl-1,3,5-triazine-2,4-diamine
1973-09-7

6-chloro-N,N'-diphenyl-1,3,5-triazine-2,4-diamine

dimethyl amine
124-40-3

dimethyl amine

N,N’-diphenyl-6-(isopropylamino)-[1,3,5]triazine-2,4-diamine
7710-42-1

N,N’-diphenyl-6-(isopropylamino)-[1,3,5]triazine-2,4-diamine

Conditions
ConditionsYield
With water; sodium carbonate for 1.5h; Heating;100%
ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle
52813-87-3

ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle

dimethyl amine
124-40-3

dimethyl amine

ethylthio-8 trimethyl-N,N,5 5H-dibenzazepine-10-acetamide
52813-88-4

ethylthio-8 trimethyl-N,N,5 5H-dibenzazepine-10-acetamide

Conditions
ConditionsYield
In chloroform for 1h; Ambient temperature;100%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

dimethyl amine
124-40-3

dimethyl amine

N,N,2-trimethylbenzamide
6639-19-6

N,N,2-trimethylbenzamide

Conditions
ConditionsYield
100%
In water; toluene
In diethyl ether at 20℃; for 16h;
5-methyl-3-(methylsulfanyl)-1,2,4-triazine
28735-24-2

5-methyl-3-(methylsulfanyl)-1,2,4-triazine

dimethyl amine
124-40-3

dimethyl amine

N,N,5-trimethyl-1,2,4-triazin-3-amine
115125-15-0

N,N,5-trimethyl-1,2,4-triazin-3-amine

Conditions
ConditionsYield
In water a.) RT, 12 h b.) 70 deg C, 30 min;100%
formaldehyd
50-00-0

formaldehyd

6,7,8,9-tetrahydrobenzoindole
67720-26-7

6,7,8,9-tetrahydrobenzoindole

dimethyl amine
124-40-3

dimethyl amine

3-dimethylaminomethyl-6,7,8,9-tetrahydrobenzoindole
110595-87-4

3-dimethylaminomethyl-6,7,8,9-tetrahydrobenzoindole

Conditions
ConditionsYield
In acetic acid at 80℃; for 0.166667h;100%
formaldehyd
50-00-0

formaldehyd

dimethyl amine
124-40-3

dimethyl amine

1,3-Bis(3-thienyloxy)propane
155330-95-3

1,3-Bis(3-thienyloxy)propane

{3-[3-(2-Dimethylaminomethyl-thiophen-3-yloxy)-propoxy]-thiophen-2-ylmethyl}-dimethyl-amine

{3-[3-(2-Dimethylaminomethyl-thiophen-3-yloxy)-propoxy]-thiophen-2-ylmethyl}-dimethyl-amine

Conditions
ConditionsYield
With acetic acid Mannich reaction; Heating;100%
With acetic acid
formaldehyd
50-00-0

formaldehyd

dimethyl amine
124-40-3

dimethyl amine

C14H18O4S2
155330-77-1

C14H18O4S2

[3-(2-{2-[2-(2-Dimethylaminomethyl-thiophen-3-yloxy)-ethoxy]-ethoxy}-ethoxy)-thiophen-2-ylmethyl]-dimethyl-amine

[3-(2-{2-[2-(2-Dimethylaminomethyl-thiophen-3-yloxy)-ethoxy]-ethoxy}-ethoxy)-thiophen-2-ylmethyl]-dimethyl-amine

Conditions
ConditionsYield
With acetic acid at 20℃; for 48h; Mannich reaction;100%
With acetic acid
formaldehyd
50-00-0

formaldehyd

dimethyl amine
124-40-3

dimethyl amine

(+/-)-3-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-4,4-dimethyl-3,4-dihydro-2H,10H-<1,4>dioxepino<2,3-g>indole
172226-45-8

(+/-)-3-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-4,4-dimethyl-3,4-dihydro-2H,10H-<1,4>dioxepino<2,3-g>indole

(+/-)-3-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-4,4-dimethyl-8-<(N,N-dimethylamino)methyl>-3,4-dihydro-2H,10H-<1,4>dioxepino<2,3-g>indole
172226-24-3

(+/-)-3-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-4,4-dimethyl-8-<(N,N-dimethylamino)methyl>-3,4-dihydro-2H,10H-<1,4>dioxepino<2,3-g>indole

Conditions
ConditionsYield
In water; acetic acid for 24h;100%
With acetic acid99%
With acetic acid99%
(Z)-9-octadecenoyl chloride
112-77-6

(Z)-9-octadecenoyl chloride

dimethyl amine
124-40-3

dimethyl amine

N,N-dimethyl oleamide
2664-42-8

N,N-dimethyl oleamide

Conditions
ConditionsYield
In benzene for 1h; Ambient temperature;100%
In water for 1h; cooling;
Nonanoyl chloride
764-85-2

Nonanoyl chloride

dimethyl amine
124-40-3

dimethyl amine

octanecarboxylic acid dimethylamide
6225-08-7

octanecarboxylic acid dimethylamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 14h; Inert atmosphere;100%
In benzene 1.) 0 deg C, 1 h, 2.) r.t., 1h;90%
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