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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Hydrocinnamoyl chloride Manufacturer/High quality/Best price/In stock

Cas:645-45-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 3-Phenyl Propanoyl Chlovide supplier in China

Cas:645-45-4

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Henan Allgreen Chemical Co.,Ltd

The company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dry, m

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 3-phenylpropionyl chloride

Cas:645-45-4

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% 645-45-4 Hydrocinnamoyl chloride Manufacturer

Cas:645-45-4

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

3-Phenylpropionyl chloride

Cas:645-45-4

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Our advantage:Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scient

TIANFU-CHEM Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturing

Hydrocinnamoyl chloride cas:645-45-4

Cas:645-45-4

Min.Order:1 Kilogram

FOB Price: $25.0 / 55.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

New production CAS 645-45-4 with best quality

Cas:645-45-4

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product name: 3-Phenylpropanoyl chlovide CAS No.: 645-45-4 Molecular formula C9H9CLO Appearance: Colorless transparent liquid Assay: 98.0%

3-Phenylpropanoyl chlovide

Cas:645-45-4

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:645-45-4

Cas:645-45-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:1 Kilogram

FOB Price: $10.0 / 100.0

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Hydrocinnamoyl Chloride

Cas:645-45-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:clear colorless to light yellow liquid Storage:Well-sealed and put in dry and cool conditions. Protected from direct sunlight or high temperature. Package:as per your request A

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:100 Gram

Negotiable

Type:Trading Company

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

Hydrocinnamoylchloride

Cas:645-45-4

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

Hydrocinnamoyl chloride Chemical Properties Melting point −7-−5 °C(lit.) Boiling point 107 °C11 mm Hg(lit.) density 1.135 g/mL at 25 °C(lit.) refractive index n20/D 1.5265(lit.) Fp 227 °F storage temp.

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:1 Gram

FOB Price: $66.0

Type:Lab/Research institutions

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:0

Negotiable

Type:Other

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

3-Phenylpropionyl chloride

Cas:645-45-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hefei Zhaobo Technology Co., Ltd.

Our Advantage Q1:How is the quality We can provide free samples for you to test its quality. Q2:Safest and fastest delivery We have adequate stock so that we can deliver the products with 24 hours as soon as receiving the payment. Fast and discre

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:1 Kilogram

FOB Price: $10.0

Type:Trading Company

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Hydrocinnamoyl chloride

Cas:645-45-4

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

3-Phenylpropanoyl chlovide cas no. 645-45-4 98%

Cas:645-45-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Newgreat Chemical Co., Ltd

ProName:Hydrocinnamoyl chloride 99% CasNo:645-45-4 Molecular Formula:C9H9ClO Appearance: Light yellow transparent liquid Application:3-Phenylpropionyl Chloride is a deriva... DeliveryTime:Within 3 worjdays after paymengt PackAge:0.5kgs/bottle

High quality 3-Phenyl propionyl chloride 645-45-4

Cas:645-45-4

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Synthetic route

3-Phenylpropionic acid
501-52-0

3-Phenylpropionic acid

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
With thionyl chloride; N,N-dimethyl-formamide In dichloromethane at 23℃;100%
With oxalyl dichloride In dichloromethane at 20℃;100%
With oxalyl dichloride In dichloromethane for 24h; Inert atmosphere;100%
tert-butyl 3-phenylpropanoate
16537-10-3

tert-butyl 3-phenylpropanoate

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
With phosphorus trichloride In acetonitrile at 80℃; for 3h; Schlenk technique;57%
With thionyl chloride; water at 20℃; for 0.5h; Reagent/catalyst; Sealed tube;
4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl-amine
383865-57-4

4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl-amine

A

N-(4-Methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-3-phenyl-propionamide

N-(4-Methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-3-phenyl-propionamide

B

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
A 3%
B n/a
oxalyl dichloride
79-37-8

oxalyl dichloride

3-Phenylpropionic acid
501-52-0

3-Phenylpropionic acid

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Dichloromethyl methyl ether
4885-02-3

Dichloromethyl methyl ether

3-Phenylpropionic acid
501-52-0

3-Phenylpropionic acid

A

Methyl formate
107-31-3

Methyl formate

B

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
With zinc(II) chloride at 100℃;
benzyl alcohol
100-51-6

benzyl alcohol

azide of <3,4-dimethoxy-phenyl>-succinic acid dihydrazide

azide of <3,4-dimethoxy-phenyl>-succinic acid dihydrazide

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: potassium / toluene / 4 h / Heating
1.2: 51 percent / toluene; benzene / 16 h / Heating
2.1: thionyl chloride / toluene / 2 h / 70 - 75 °C
View Scheme
(E)-3-phenylacrylic acid
140-10-3

(E)-3-phenylacrylic acid

isotope ene

isotope ene

A

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

B

1.2.2.3-tetramethyl-cyclopentylcarbinol

1.2.2.3-tetramethyl-cyclopentylcarbinol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 80 percent / H2 / 5percent Pd-C / ethyl acetate / 10 h
2: thionyl chloride / CHCl3 / Ambient temperature
View Scheme
(E)-3-phenylacrylic acid
140-10-3

(E)-3-phenylacrylic acid

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 83 percent / H2 / platinum / ethanol
2: thionyl chloride / benzene
View Scheme
Multi-step reaction with 2 steps
1: 5% Pd(OH)2/C; hydrogen / ethyl acetate / 22 h / 20 °C / 5171.62 Torr
2: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 0 - 20 °C
View Scheme
2-methylpropyl 3-phenypropionate
28048-94-4

2-methylpropyl 3-phenypropionate

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 3 N aq. NaOH / ethanol / 12 h / Ambient temperature
2: dicyclohexylcarbodiimide / CH2Cl2
3: 1.) hexamethyldisilazane, 1.6 M n-BuLi, 2.) CS2, 3.) PhSeO2H / 1.) THF, hexane, -20 deg C, 30 min, 2.) THF, rt, 3.) THF, rt, 5 h
4: oxalyl chloride, DMF / benzene / Ambient temperature
View Scheme
Multi-step reaction with 2 steps
1: 3 N aq. NaOH / ethanol / 12 h / Ambient temperature
2: oxalyl chloride, DMF / benzene / Ambient temperature
View Scheme
3-phenyl-N-(pyridin-3-yl)propanamide
119520-49-9

3-phenyl-N-(pyridin-3-yl)propanamide

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) hexamethyldisilazane, 1.6 M n-BuLi, 2.) CS2, 3.) PhSeO2H / 1.) THF, hexane, -20 deg C, 30 min, 2.) THF, rt, 3.) THF, rt, 5 h
2: oxalyl chloride, DMF / benzene / Ambient temperature
View Scheme
N-(4-nitrophenyl)-3-phenylpropionamide
119520-57-9

N-(4-nitrophenyl)-3-phenylpropionamide

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) phosgene, 2.) pyridine / 1.) CH2Cl2, 0 deg C, 2.) CH2Cl2, rt, 30 min, 3.) CH2Cl2, 3 h
2: 3 N aq. NaOH / ethanol / 12 h / Ambient temperature
3: oxalyl chloride, DMF / benzene / Ambient temperature
View Scheme
3-Phenyl-N-pyridin-3-yl-thiopropionimidic acid pyridin-2-yl ester
119541-41-2

3-Phenyl-N-pyridin-3-yl-thiopropionimidic acid pyridin-2-yl ester

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 90 percent / water / dioxane / 12 h / Ambient temperature
2: 1.) hexamethyldisilazane, 1.6 M n-BuLi, 2.) CS2, 3.) PhSeO2H / 1.) THF, hexane, -20 deg C, 30 min, 2.) THF, rt, 3.) THF, rt, 5 h
3: oxalyl chloride, DMF / benzene / Ambient temperature
View Scheme
Cinnamic acid
621-82-9

Cinnamic acid

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrogen; palladium 10% on activated carbon / ethanol / 5 h / 20 °C / Inert atmosphere
2: oxalyl dichloride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: hydrogen; palladium on activated charcoal
2: oxalyl dichloride / Inert atmosphere
View Scheme
3-phenyl-propionaldehyde
104-53-0

3-phenyl-propionaldehyde

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

Conditions
ConditionsYield
With trichloroisocyanuric acid In dichloromethane at 20℃; for 120h; Inert atmosphere;
With trichloroisocyanuric acid In dichloromethane at 20℃; Inert atmosphere;
With trichloroisocyanuric acid In dichloromethane at 20℃; Inert atmosphere;
With trichloroisocyanuric acid In dichloromethane at 20℃; for 4h; Inert atmosphere; Irradiation;
hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

1-diazo-4-phenyl-2-butanone
10290-42-3

1-diazo-4-phenyl-2-butanone

Conditions
ConditionsYield
In diethyl ether 1.) ice-salt bath, 1 h, 2.) ice-salt bath -> room temperature, 1 h;100%
With potassium hydroxide; ethoxyethoxyethanol; N-methyl-N-nitrosotoluene-p-sulfonamide In tetrahydrofuran; diethyl ether; water at 55℃;100%
for 4h; Ambient temperature;93%
diethylamine
109-89-7

diethylamine

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N,N-diethyl-3-phenylpropanamide
18859-19-3

N,N-diethyl-3-phenylpropanamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 14h; Inert atmosphere;100%
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere;96%
dimethyl amine
124-40-3

dimethyl amine

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N,N-dimethyl-3-phenylpropanamide
5830-31-9

N,N-dimethyl-3-phenylpropanamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere;100%
With triethylamine In diethyl ether93%
With triethylamine In diethyl ether Inert atmosphere;93%
1-amino-2-propene
107-11-9

1-amino-2-propene

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N-(prop-2-enyl)-3-phenylpropanamide
133055-17-1

N-(prop-2-enyl)-3-phenylpropanamide

Conditions
ConditionsYield
In tetrahydrofuran at 25℃; for 24h; Inert atmosphere;100%
hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

(S)-5,5-Di(4'-tolyl)-4-isopropyl-1,3-oxazolidin-2-one
213887-79-7

(S)-5,5-Di(4'-tolyl)-4-isopropyl-1,3-oxazolidin-2-one

(S)-5,5-Di(4'-tolyl)-4-isopropyl-3-(1'-oxo-3'-phenylpropyl)-1,3-oxazolidin-2-one
213887-83-3

(S)-5,5-Di(4'-tolyl)-4-isopropyl-3-(1'-oxo-3'-phenylpropyl)-1,3-oxazolidin-2-one

Conditions
ConditionsYield
With dmap; triethylamine100%
With dmap; triethylamine In dichloromethane at 20℃; for 5h;100%
hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

dibenzylamine
103-49-1

dibenzylamine

(N,N)-dibenzyl-3-phenylpropanamide
180747-56-2

(N,N)-dibenzyl-3-phenylpropanamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere;100%
With triethylamine In dichloromethane at 20℃; Inert atmosphere;90%
With triethylamine In dichloromethane at 0 - 23℃; for 16h; Inert atmosphere;80%
With triethylamine In dichloromethane at 20℃; for 0.333333h;62%
With triethylamine In dichloromethane at 23℃; for 1h;
β-naphthol
135-19-3

β-naphthol

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

naphthalen-2-yl 3-phenylpropanoate
94305-35-8

naphthalen-2-yl 3-phenylpropanoate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃;100%
2-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline
461699-81-0

2-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N-[2-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-3-phenylpropanamide

N-[2-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-3-phenylpropanamide

Conditions
ConditionsYield
With triethylamine In dichloromethane for 23h;100%
With triethylamine In dichloromethane for 23h;100%
pyrrolidine
123-75-1

pyrrolidine

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

3-phenyl-1-pyrrolidin-1-yl-propane-1-one
151647-54-0

3-phenyl-1-pyrrolidin-1-yl-propane-1-one

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃;100%
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere;99%
In dichloromethane at 0 - 20℃; Inert atmosphere;78%
With triethylamine In dichloromethane at 20℃; for 12h;
at 0 - 20℃; for 20h; Alkaline conditions;
methyl pyrrolidine-2-carboxylate hydrochloride
2133-40-6, 65365-28-8, 79397-50-5

methyl pyrrolidine-2-carboxylate hydrochloride

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

methyl 1-(3-phenylpropanoyl)pyrrolidine-2-carboxylate
946438-16-0

methyl 1-(3-phenylpropanoyl)pyrrolidine-2-carboxylate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1h; Inert atmosphere;100%
hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

phenol
108-95-2

phenol

phenyl 3-phenylpropanoate
726-26-1

phenyl 3-phenylpropanoate

Conditions
ConditionsYield
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction;99%
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h;85%
2,2-dimethoxyethylamine
22483-09-6

2,2-dimethoxyethylamine

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N-(2,2-dimethoxyethyl)-3-phenylpropanamide
133950-89-7

N-(2,2-dimethoxyethyl)-3-phenylpropanamide

Conditions
ConditionsYield
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide; ethyl acetate at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction;99%
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h;86%
In dichloromethane at 5 - 20℃;
N-methylhydroxyamine hydrochloride
4229-44-1

N-methylhydroxyamine hydrochloride

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N-hydroxy-N-methyl-3-phenylpropanamide
111750-23-3

N-hydroxy-N-methyl-3-phenylpropanamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere;99%
With triethylamine In dichloromethane for 1h; Ambient temperature;88%
With sodium hydrogencarbonate In dichloromethane at 0 - 20℃; Inert atmosphere;75%
(3aS,7aS)-hexahydrobenzo[d]oxazol-2(3H)-one
189942-51-6

(3aS,7aS)-hexahydrobenzo[d]oxazol-2(3H)-one

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

(3aS,7aS)-3-(3-phenylpropanoyl)hexahydrobenzo[d]oxazol-2(3H)-one

(3aS,7aS)-3-(3-phenylpropanoyl)hexahydrobenzo[d]oxazol-2(3H)-one

Conditions
ConditionsYield
Stage #1: (4S,5S)-trans-hexahydrobenzoxazolidin-2-one With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h;
Stage #2: hydrocinnamic acid chloride In tetrahydrofuran; hexane at -78 - 20℃; for 1h;
99%
(3aR,7aS)-hexahydrobenzo[d]oxazol-2(3H)-one
189942-50-5

(3aR,7aS)-hexahydrobenzo[d]oxazol-2(3H)-one

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

(4R,5S)-(N-hydrocinnamoyl)hexahydrobenzoxazolidin-2-one

(4R,5S)-(N-hydrocinnamoyl)hexahydrobenzoxazolidin-2-one

Conditions
ConditionsYield
Stage #1: (3aR,7aS)-hexahydrobenzo[d]oxazol-2(3H)-one With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h;
Stage #2: hydrocinnamic acid chloride In tetrahydrofuran; hexane at -78 - 20℃; for 1h;
99%
(3aS,7aR)-3a,4,5,6,7,7a-hexahydrobenzoxazolin-2-one
21651-79-6

(3aS,7aR)-3a,4,5,6,7,7a-hexahydrobenzoxazolin-2-one

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

(4S,5R)-(N-hydrocinnamoyl)hexahydrobenzoxazolidin-2-one

(4S,5R)-(N-hydrocinnamoyl)hexahydrobenzoxazolidin-2-one

Conditions
ConditionsYield
Stage #1: (3aS,7aR)-3a,4,5,6,7,7a-hexahydrobenzoxazolin-2-one With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h;
Stage #2: hydrocinnamic acid chloride In tetrahydrofuran; hexane at -78 - 20℃; for 1h;
99%
N,O-dimethylhydroxylamine*hydrochloride
6638-79-5

N,O-dimethylhydroxylamine*hydrochloride

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N-methoxy-N-methyl-3-phenylpropionamide
170646-96-5

N-methoxy-N-methyl-3-phenylpropionamide

Conditions
ConditionsYield
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h;99%
With pyridine In dichloromethane at 0 - 20℃;93%
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide; ethyl acetate at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction;91%
(2-furyl)methyl alcohol
98-00-0

(2-furyl)methyl alcohol

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

furan-2-ylmethyl 3-phenylpropanoate

furan-2-ylmethyl 3-phenylpropanoate

Conditions
ConditionsYield
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h;99%
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide; ethyl acetate at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction;97%
(S)-1-phenyl-ethylamine
2627-86-3

(S)-1-phenyl-ethylamine

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N-(3-phenylpropanoyl)-(S)-1-phenylethylamine
200803-30-1

N-(3-phenylpropanoyl)-(S)-1-phenylethylamine

Conditions
ConditionsYield
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h;99%
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction;75%
tert-butylamine
75-64-9

tert-butylamine

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N-tert-butyl-3-phenylpropionamide
58680-45-8

N-tert-butyl-3-phenylpropionamide

Conditions
ConditionsYield
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 25℃; for 2h;99%
With triethylamine In diethyl ether86%
With triethylamine In diethyl ether Inert atmosphere;86%
2,4-dichlorophenol
120-83-2

2,4-dichlorophenol

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

2,4-dichlorophenyl 3-phenylpropanoate
40123-46-4

2,4-dichlorophenyl 3-phenylpropanoate

Conditions
ConditionsYield
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h;99%
2,4-Dichloroaniline
554-00-7

2,4-Dichloroaniline

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N-(2,4-dichlorophenyl)-3-phenylpropanamide

N-(2,4-dichlorophenyl)-3-phenylpropanamide

Conditions
ConditionsYield
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h;99%
1-hydroxy-pyrrolidine-2,5-dione
6066-82-6

1-hydroxy-pyrrolidine-2,5-dione

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

2,5-dioxopyrrolidin-1-yl 3-phenylpropanoate
109318-10-7

2,5-dioxopyrrolidin-1-yl 3-phenylpropanoate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 1h;99%
C15H16N4O2

C15H16N4O2

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

C24H24N4O3

C24H24N4O3

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 3h;99%
2-(Methylthio)aniline
2987-53-3

2-(Methylthio)aniline

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N-(hydrocinnamoyl)-2-methylthioaniline
708222-26-8

N-(hydrocinnamoyl)-2-methylthioaniline

Conditions
ConditionsYield
With triethylamine In dichloromethane99%
1-(3-phenylpropanoyl)-(3R,4R)-3-[1(R)-hydroxyethyl]-4-(acetoxy)-azetidin-2-one
1197421-92-3

1-(3-phenylpropanoyl)-(3R,4R)-3-[1(R)-hydroxyethyl]-4-(acetoxy)-azetidin-2-one

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

1-(3-phenylpropanoyl)-(3R,4R)-3-[1(R)-(3-phenylpropanoyloxy)-ethyl]-4-(acetoxy)-azetidin-2-one
1197421-94-5

1-(3-phenylpropanoyl)-(3R,4R)-3-[1(R)-(3-phenylpropanoyloxy)-ethyl]-4-(acetoxy)-azetidin-2-one

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 15h; Inert atmosphere;99%
C22H22O4

C22H22O4

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

C31H30O5

C31H30O5

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 0 - 20℃; Molecular sieve;99%
2-(3,4-dimethoxyphenyl)-ethylamine
120-20-7

2-(3,4-dimethoxyphenyl)-ethylamine

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N-(3,4-dimethoxyphenethyl)-3-phenylpropanamide
2878-60-6

N-(3,4-dimethoxyphenethyl)-3-phenylpropanamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 2h;99%
With triethylamine In tetrahydrofuran at 0 - 20℃;93%
With sodium hydroxide In dichloromethane; water at 0℃; for 0.166667h;1920 mg
5-(benzyloxy)-3,4,6-trimethylpyridine-2-amine
1444335-07-2

5-(benzyloxy)-3,4,6-trimethylpyridine-2-amine

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

N-[5-(benzyloxy)-3,4,6-trimethylpyridin-2-yl]-3-phenylpropanamide
1616249-57-0

N-[5-(benzyloxy)-3,4,6-trimethylpyridin-2-yl]-3-phenylpropanamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃;99%
With triethylamine In dichloromethane at 20℃; for 8h;99%
With triethylamine In dichloromethane at 20℃; for 8h;99%
With triethylamine In dichloromethane at 20℃;99%

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