DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryProduct name: 3-Phenylpropanoyl chlovide CAS No.: 645-45-4 Molecular formula C9H9CLO Appearance: Colorless transparent liquid Assay: 98.0%
1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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Superior quality, moderate price & quick delivery. Appearance:clear colorless to light yellow liquid Storage:Well-sealed and put in dry and cool conditions. Protected from direct sunlight or high temperature. Package:as per your request A
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Hydrocinnamoyl chloride Chemical Properties Melting point −7-−5 °C(lit.) Boiling point 107 °C11 mm Hg(lit.) density 1.135 g/mL at 25 °C(lit.) refractive index n20/D 1.5265(lit.) Fp 227 °F storage temp.
Cas:645-45-4
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryProName:Hydrocinnamoyl chloride 99% CasNo:645-45-4 Molecular Formula:C9H9ClO Appearance: Light yellow transparent liquid Application:3-Phenylpropionyl Chloride is a deriva... DeliveryTime:Within 3 worjdays after paymengt PackAge:0.5kgs/bottle
Cas:645-45-4
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inquiryConditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide In dichloromethane at 23℃; | 100% |
With oxalyl dichloride In dichloromethane at 20℃; | 100% |
With oxalyl dichloride In dichloromethane for 24h; Inert atmosphere; | 100% |
tert-butyl 3-phenylpropanoate
hydrocinnamic acid chloride
Conditions | Yield |
---|---|
With phosphorus trichloride In acetonitrile at 80℃; for 3h; Schlenk technique; | 57% |
With thionyl chloride; water at 20℃; for 0.5h; Reagent/catalyst; Sealed tube; |
4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl-amine
B
hydrocinnamic acid chloride
Conditions | Yield |
---|---|
A 3% B n/a |
Dichloromethyl methyl ether
3-Phenylpropionic acid
A
Methyl formate
B
hydrocinnamic acid chloride
Conditions | Yield |
---|---|
With zinc(II) chloride at 100℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: potassium / toluene / 4 h / Heating 1.2: 51 percent / toluene; benzene / 16 h / Heating 2.1: thionyl chloride / toluene / 2 h / 70 - 75 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 80 percent / H2 / 5percent Pd-C / ethyl acetate / 10 h 2: thionyl chloride / CHCl3 / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 83 percent / H2 / platinum / ethanol 2: thionyl chloride / benzene View Scheme | |
Multi-step reaction with 2 steps 1: 5% Pd(OH)2/C; hydrogen / ethyl acetate / 22 h / 20 °C / 5171.62 Torr 2: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 0 - 20 °C View Scheme |
2-methylpropyl 3-phenypropionate
hydrocinnamic acid chloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 3 N aq. NaOH / ethanol / 12 h / Ambient temperature 2: dicyclohexylcarbodiimide / CH2Cl2 3: 1.) hexamethyldisilazane, 1.6 M n-BuLi, 2.) CS2, 3.) PhSeO2H / 1.) THF, hexane, -20 deg C, 30 min, 2.) THF, rt, 3.) THF, rt, 5 h 4: oxalyl chloride, DMF / benzene / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: 3 N aq. NaOH / ethanol / 12 h / Ambient temperature 2: oxalyl chloride, DMF / benzene / Ambient temperature View Scheme |
3-phenyl-N-(pyridin-3-yl)propanamide
hydrocinnamic acid chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) hexamethyldisilazane, 1.6 M n-BuLi, 2.) CS2, 3.) PhSeO2H / 1.) THF, hexane, -20 deg C, 30 min, 2.) THF, rt, 3.) THF, rt, 5 h 2: oxalyl chloride, DMF / benzene / Ambient temperature View Scheme |
N-(4-nitrophenyl)-3-phenylpropionamide
hydrocinnamic acid chloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) phosgene, 2.) pyridine / 1.) CH2Cl2, 0 deg C, 2.) CH2Cl2, rt, 30 min, 3.) CH2Cl2, 3 h 2: 3 N aq. NaOH / ethanol / 12 h / Ambient temperature 3: oxalyl chloride, DMF / benzene / Ambient temperature View Scheme |
3-Phenyl-N-pyridin-3-yl-thiopropionimidic acid pyridin-2-yl ester
hydrocinnamic acid chloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 90 percent / water / dioxane / 12 h / Ambient temperature 2: 1.) hexamethyldisilazane, 1.6 M n-BuLi, 2.) CS2, 3.) PhSeO2H / 1.) THF, hexane, -20 deg C, 30 min, 2.) THF, rt, 3.) THF, rt, 5 h 3: oxalyl chloride, DMF / benzene / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogen; palladium 10% on activated carbon / ethanol / 5 h / 20 °C / Inert atmosphere 2: oxalyl dichloride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; palladium on activated charcoal 2: oxalyl dichloride / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With trichloroisocyanuric acid In dichloromethane at 20℃; for 120h; Inert atmosphere; | |
With trichloroisocyanuric acid In dichloromethane at 20℃; Inert atmosphere; | |
With trichloroisocyanuric acid In dichloromethane at 20℃; Inert atmosphere; | |
With trichloroisocyanuric acid In dichloromethane at 20℃; for 4h; Inert atmosphere; Irradiation; |
diazomethane
hydrocinnamic acid chloride
1-diazo-4-phenyl-2-butanone
Conditions | Yield |
---|---|
In diethyl ether 1.) ice-salt bath, 1 h, 2.) ice-salt bath -> room temperature, 1 h; | 100% |
With potassium hydroxide; ethoxyethoxyethanol; N-methyl-N-nitrosotoluene-p-sulfonamide In tetrahydrofuran; diethyl ether; water at 55℃; | 100% |
for 4h; Ambient temperature; | 93% |
diethylamine
hydrocinnamic acid chloride
N,N-diethyl-3-phenylpropanamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 14h; Inert atmosphere; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere; | 96% |
dimethyl amine
hydrocinnamic acid chloride
N,N-dimethyl-3-phenylpropanamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere; | 100% |
With triethylamine In diethyl ether | 93% |
With triethylamine In diethyl ether Inert atmosphere; | 93% |
1-amino-2-propene
hydrocinnamic acid chloride
N-(prop-2-enyl)-3-phenylpropanamide
Conditions | Yield |
---|---|
In tetrahydrofuran at 25℃; for 24h; Inert atmosphere; | 100% |
hydrocinnamic acid chloride
(S)-5,5-Di(4'-tolyl)-4-isopropyl-1,3-oxazolidin-2-one
(S)-5,5-Di(4'-tolyl)-4-isopropyl-3-(1'-oxo-3'-phenylpropyl)-1,3-oxazolidin-2-one
Conditions | Yield |
---|---|
With dmap; triethylamine | 100% |
With dmap; triethylamine In dichloromethane at 20℃; for 5h; | 100% |
hydrocinnamic acid chloride
dibenzylamine
(N,N)-dibenzyl-3-phenylpropanamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere; | 100% |
With triethylamine In dichloromethane at 20℃; Inert atmosphere; | 90% |
With triethylamine In dichloromethane at 0 - 23℃; for 16h; Inert atmosphere; | 80% |
With triethylamine In dichloromethane at 20℃; for 0.333333h; | 62% |
With triethylamine In dichloromethane at 23℃; for 1h; |
β-naphthol
hydrocinnamic acid chloride
naphthalen-2-yl 3-phenylpropanoate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
2-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline
hydrocinnamic acid chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 23h; | 100% |
With triethylamine In dichloromethane for 23h; | 100% |
pyrrolidine
hydrocinnamic acid chloride
3-phenyl-1-pyrrolidin-1-yl-propane-1-one
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere; | 99% |
In dichloromethane at 0 - 20℃; Inert atmosphere; | 78% |
With triethylamine In dichloromethane at 20℃; for 12h; | |
at 0 - 20℃; for 20h; Alkaline conditions; |
methyl pyrrolidine-2-carboxylate hydrochloride
hydrocinnamic acid chloride
methyl 1-(3-phenylpropanoyl)pyrrolidine-2-carboxylate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction; | 99% |
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h; | 85% |
2,2-dimethoxyethylamine
hydrocinnamic acid chloride
N-(2,2-dimethoxyethyl)-3-phenylpropanamide
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide; ethyl acetate at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction; | 99% |
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h; | 86% |
In dichloromethane at 5 - 20℃; |
N-methylhydroxyamine hydrochloride
hydrocinnamic acid chloride
N-hydroxy-N-methyl-3-phenylpropanamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; | 99% |
With triethylamine In dichloromethane for 1h; Ambient temperature; | 88% |
With sodium hydrogencarbonate In dichloromethane at 0 - 20℃; Inert atmosphere; | 75% |
(3aS,7aS)-hexahydrobenzo[d]oxazol-2(3H)-one
hydrocinnamic acid chloride
Conditions | Yield |
---|---|
Stage #1: (4S,5S)-trans-hexahydrobenzoxazolidin-2-one With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: hydrocinnamic acid chloride In tetrahydrofuran; hexane at -78 - 20℃; for 1h; | 99% |
(3aR,7aS)-hexahydrobenzo[d]oxazol-2(3H)-one
hydrocinnamic acid chloride
Conditions | Yield |
---|---|
Stage #1: (3aR,7aS)-hexahydrobenzo[d]oxazol-2(3H)-one With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: hydrocinnamic acid chloride In tetrahydrofuran; hexane at -78 - 20℃; for 1h; | 99% |
(3aS,7aR)-3a,4,5,6,7,7a-hexahydrobenzoxazolin-2-one
hydrocinnamic acid chloride
Conditions | Yield |
---|---|
Stage #1: (3aS,7aR)-3a,4,5,6,7,7a-hexahydrobenzoxazolin-2-one With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: hydrocinnamic acid chloride In tetrahydrofuran; hexane at -78 - 20℃; for 1h; | 99% |
N,O-dimethylhydroxylamine*hydrochloride
hydrocinnamic acid chloride
N-methoxy-N-methyl-3-phenylpropionamide
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h; | 99% |
With pyridine In dichloromethane at 0 - 20℃; | 93% |
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide; ethyl acetate at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction; | 91% |
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h; | 99% |
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide; ethyl acetate at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction; | 97% |
(S)-1-phenyl-ethylamine
hydrocinnamic acid chloride
N-(3-phenylpropanoyl)-(S)-1-phenylethylamine
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h; | 99% |
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction; | 75% |
tert-butylamine
hydrocinnamic acid chloride
N-tert-butyl-3-phenylpropionamide
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 25℃; for 2h; | 99% |
With triethylamine In diethyl ether | 86% |
With triethylamine In diethyl ether Inert atmosphere; | 86% |
2,4-dichlorophenol
hydrocinnamic acid chloride
2,4-dichlorophenyl 3-phenylpropanoate
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h; | 99% |
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h; | 99% |
1-hydroxy-pyrrolidine-2,5-dione
hydrocinnamic acid chloride
2,5-dioxopyrrolidin-1-yl 3-phenylpropanoate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 1h; | 99% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 3h; | 99% |
2-(Methylthio)aniline
hydrocinnamic acid chloride
N-(hydrocinnamoyl)-2-methylthioaniline
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 99% |
1-(3-phenylpropanoyl)-(3R,4R)-3-[1(R)-hydroxyethyl]-4-(acetoxy)-azetidin-2-one
hydrocinnamic acid chloride
1-(3-phenylpropanoyl)-(3R,4R)-3-[1(R)-(3-phenylpropanoyloxy)-ethyl]-4-(acetoxy)-azetidin-2-one
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 15h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 20℃; Molecular sieve; | 99% |
2-(3,4-dimethoxyphenyl)-ethylamine
hydrocinnamic acid chloride
N-(3,4-dimethoxyphenethyl)-3-phenylpropanamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 2h; | 99% |
With triethylamine In tetrahydrofuran at 0 - 20℃; | 93% |
With sodium hydroxide In dichloromethane; water at 0℃; for 0.166667h; | 1920 mg |
5-(benzyloxy)-3,4,6-trimethylpyridine-2-amine
hydrocinnamic acid chloride
N-[5-(benzyloxy)-3,4,6-trimethylpyridin-2-yl]-3-phenylpropanamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 99% |
With triethylamine In dichloromethane at 20℃; for 8h; | 99% |
With triethylamine In dichloromethane at 20℃; for 8h; | 99% |
With triethylamine In dichloromethane at 20℃; | 99% |
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