As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryItems Standard Result Assay 98%min ----------------------------------------------------------------------------------------------
Cas:501-52-0
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inquiryThe company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dry, m
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:501-52-0
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquirychengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
Cas:501-52-0
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inquiryOur company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble metal catalysts, synthesis of electronic chemical materials and general chemicals Imp&Exp trading business. The company
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inquiryOur advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be sent
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:501-52-0
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:501-52-0
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inquiryProduct 3-Phenylpropionic acid Appearance White crystal powder Purity (min) 99%min Boiling P
Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryProduct Name: 3-Phenylpropionic acid CAS: 501-52-0 MF: C9H10O2 MW: 150.17 EINECS: 207-924-5 Mol File: 501-52-0.mol 3-Phenylpropionic acid Structure 3-Phenylpropionic acid Chemical Properties Melting point 45-48 °C (lit.) B
Cas:501-52-0
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
3-Phenylpropionic acid CAS:501-52-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inte
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:501-52-0
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inquiry3-Phenylpropionic acid CAS: 501-52-0 Specification Item Standard Identification A.H-NMR:Comply with the structure B.LC-MS:Comply with the structure C.The IR spect
Cas:501-52-0
Min.Order:1 Kilogram
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inquiryPRODUCT DETAILS
Cas:501-52-0
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Product Detail Minimum Order Qty. 10 Gram
Cas:501-52-0
Min.Order:10 Gram
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Type:Trading Company
inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Specification : benzenepropionicacid;hydrocinnami
Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcin
Cas:501-52-0
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:501-52-0
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inquiryAdvantage 1: The product passed the professional production process and quality inspection, the purity is 99% +. 2: Highly qualified engineers to provide technical documents and service. 3: We could provide sample for your test. 4: High qualit
Cas:501-52-0
Min.Order:1 Kilogram
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Conditions | Yield |
---|---|
With formic acid; palladium In methanol; water Ambient temperature; | 100% |
With hydrogen; palladium In ethyl acetate at 25℃; under 760.051 Torr; for 1h; | 100% |
With hydrogen; palladium in polystyrene In tetrahydrofuran at 25℃; under 760.051 Torr; for 1.5h; | 100% |
Conditions | Yield |
---|---|
With 2,2,6,6-tetramethyl-piperidine-N-oxyl; trichloroisocyanuric acid; sodium hydrogencarbonate; sodium bromide In water; acetone at 20℃; for 6h; | 100% |
With oxygen; potassium hydroxide In methanol; water at 50℃; under 760.051 Torr; for 12h; | 100% |
With sodium hypochlorite; 4-hydroxy-TEMPO benzoate; silica gel In acetone at 0℃; for 0.5h; | 99% |
allyl 3-phenylpropionate
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With aminomethyl resin-supported N-propylbarbituric acid; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 20℃; for 1h; | 100% |
With 2,2'-azobis(isobutyronitrile) In benzene at 65 - 70℃; for 3h; | 100% |
With formic acid; triethylamine In acetonitrile at 80℃; for 0.5h; Inert atmosphere; | 100% |
(S)-(2,3,4,5,6-pentafluorophenyl) 3-phenylpropanethioate
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With potassium hydroxide In acetone at 50℃; for 1h; | 100% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen at 20℃; for 24h; Neat (no solvent); | 100% |
With palladium 10% on activated carbon; hydrogen In methanol at 100℃; under 750.075 Torr; Reagent/catalyst; Temperature; Flow reactor; | 100% |
With hydrogen In methanol at 20℃; under 760.051 Torr; for 24h; chemoselective reaction; | 100% |
Conditions | Yield |
---|---|
With hydrogen; potassium hydroxide In water at 20℃; under 760.051 Torr; for 1h; Sealed tube; | 100% |
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With potassium phosphate; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; ascorbic acid In water; acetonitrile at 20℃; for 1h; Irradiation; | 100% |
With 2-H-1,3-di-tert-butyl-1,3,2-diazaphosphorinane; 2,2'-azobis(isobutyronitrile); 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In toluene at 90℃; for 12h; chemoselective reaction; | 99% |
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With ammonium cerium (IV) nitrate In water at 25℃; | 100% |
Conditions | Yield |
---|---|
With NaSiO(CH3)3 In tetrahydrofuran at 20℃; for 6h; | 99% |
With pyrographite; sodium hydroxide In water at 20℃; for 24h; Reagent/catalyst; Temperature; | 95% |
With potassium hydroxide | |
With samarium diiodide; water; triethylamine In tetrahydrofuran at 20℃; Inert atmosphere; | |
Multi-step reaction with 2 steps 1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 20 °C / Inert atmosphere 1.2: 12 h / -78 °C / Inert atmosphere 2.1: 24 h / 120 °C / Autoclave; Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With samarium diiodide; water In tetrahydrofuran for 1.33333h; Ambient temperature; | 99% |
With Pd(SIPr)(PCy3); hydrogen In methanol at 20℃; under 750.075 Torr; for 24h; | 99% |
With isopropyl alcohol; potassium hydroxide In water at 70℃; for 20h; | 99% |
Conditions | Yield |
---|---|
With LaNi5 hydride In tetrahydrofuran; methanol 1) 0 deg C, 2 h, 2) r.t., 15 h; | 99% |
With ferrous ammonium sulphate hexahydrate; isopropyl β-D-thiogalactopyranoside In aq. phosphate buffer at 37℃; for 48h; | 92% |
With water; palladium diacetate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In dichloromethane at 25℃; for 12h; Schlenk technique; Inert atmosphere; | 71% |
Conditions | Yield |
---|---|
With iodine; aluminium In acetonitrile at 80℃; for 18h; | 99% |
With NaSiO(CH3)3 In tetrahydrofuran at 20℃; for 2h; | 95% |
With water; triethylamine; lithium bromide In acetonitrile at 20℃; for 48h; | 89% |
1-methylethyl 3-phenylpropionoate
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With NaSiO(CH3)3 In tetrahydrofuran at 20℃; for 48h; | 99% |
With samarium diiodide; water; triethylamine In tetrahydrofuran at 20℃; Inert atmosphere; |
phenyl-3 propanedithioate de methyle
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With sodium hydroxide; dihydrogen peroxide In methanol; water at 20℃; for 0.0833333h; | 99% |
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With (R)-10-camphorsulfonic acid; acetic acid In water at 60℃; for 19h; Mitsunobu Displacement; Sealed tube; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With potassium phosphate buffer at 30℃; for 17h; Rhodococcus sp. AJ270 cells; | 98.3% |
enzyme from Synechocystis sp. PCC 6803 In phosphate buffer at 30℃; for 12h; pH=7.2; | 94% |
With potassium hydroxide; diethylene glycol |
Conditions | Yield |
---|---|
Stage #1: 3-phenyl-propionaldehyde With potassium permanganate; disodium hydrogenphosphate In methanol; water at 25℃; Continuous flow conditions; Sonication; Stage #2: With hydrogenchloride; sodium thiosulfate; sodium chloride In methanol; water; ethyl acetate | 98% |
With Iron(III) nitrate nonahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium chloride In 1,2-dichloro-ethane at 25℃; for 16h; | 98% |
With tris[2-(4,6-difluorophenyl)pyridinato-C2,N]-iridium(III); oxygen In acetonitrile at 20℃; Irradiation; Sealed tube; Green chemistry; chemoselective reaction; | 97% |
Conditions | Yield |
---|---|
In water for 0.25h; Decarboxylation; microwave irradiation; | 98% |
copper(I) oxide In acetonitrile for 6h; Heating; | 97% |
With poly-4-vinylpyridine In N,N-dimethyl-formamide for 0.05h; microwave irradiation; | 94% |
1,1,1,3,3,3-hexafluoropropan-2-yl 3-phenylpropanoate
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran; water at 20℃; for 12h; | 98% |
Benzyl 3-phenylpropionate
toluene
A
1-methyl-3-(phenylmethyl)-benzene
B
1-methyl-4-(phenylmethyl)benzene
C
2-benzyltoluene
D
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate; water at 80℃; for 2h; regioselective reaction; | A n/a B n/a C n/a D 98% |
(4R,5S)-3-(3-phenylpropionyl)-4-methyl-5-phenyl-oxazolidin-2-one
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With water; ytterbium(III) triflate In acetonitrile at 110℃; for 48h; Sealed tube; Inert atmosphere; | 98% |
2-tosylethyl 3-phenylpropanoate
A
tolyl vinyl sulfone
B
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 0℃; for 1h; | A 97% B 95% |
tert-butyl 3-phenylpropanoate
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With 1,1,3,3-Tetramethyldisiloxane; pyrographite; palladium dichloride In 1,2-dimethoxyethane at 25 - 40℃; for 4h; Catalytic behavior; Reagent/catalyst; Solvent; | 97% |
With (μ3,η2,η3,η5-acenaphthylene)Ru3(CO)7; Dimethylphenylsilane In 1,2-dimethoxyethane at 40℃; for 7h; Inert atmosphere; | 95% |
With zinc dibromide In dichloromethane for 12h; dealkylation; | 91% |
With samarium diiodide; water; triethylamine In tetrahydrofuran at 20℃; Inert atmosphere; |
Conditions | Yield |
---|---|
With formic acid; potassium hydroxide In ethanol at 70℃; for 1h; | 97% |
With ammonium formate; silica gel; palladium dichloride In formic acid; water for 0.133333h; microwave irradiation; | 84% |
3-Oxo-5-phenyl-2-(triphenyl-λ5-phosphanylidene)-pentanoic acid ethyl ester
A
Triphenylphosphine oxide
B
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With sodium hydroxide; sodium hypochlorite In acetonitrile at 25℃; for 4.5h; | A n/a B 96% |
(E)-3-phenylpropenal
trimethylsilyl cyanide
A
2-hydroxy-4-phenyl-3-butenenitrile
B
3-Phenylpropionic acid
Conditions | Yield |
---|---|
Stage #1: (E)-3-phenylpropenal; trimethylsilyl cyanide With tris(2,4,6-trimethoxyphenyl)phosphine In diethyl ether at 32℃; for 2h; Stage #2: With hydrogenchloride In diethyl ether; water at 20℃; for 3h; | A 96% B 1% |
Conditions | Yield |
---|---|
Stage #1: 4-Phenylbut-1-ene With ozone In water; acetonitrile at 0℃; Inert atmosphere; Stage #2: With sodium chlorite In water; acetonitrile at 15 - 20℃; under 760.051 Torr; Inert atmosphere; Stage #3: With sodium hydrogen sulfate In water; acetonitrile at 35℃; for 0.166667h; Inert atmosphere; | 96% |
With potassium peroxymonosulfate; iodobenzene In water; acetonitrile at 60℃; for 8h; | 90% |
Multi-step reaction with 3 steps 1.1: bis(pinacol)diborane; caesium carbonate; methanol / tetrahydrofuran / 6 h / 70 °C 1.2: 1 h / 0 °C 2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / toluene; aq. phosphate buffer / 25 °C / pH 6.8 2.2: 4 h / 25 °C 3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium chlorite; sodium hypochlorite / toluene; aq. phosphate buffer / 12 h / 25 °C / pH 6.8 View Scheme | |
Multi-step reaction with 3 steps 1.1: bis(pinacol)diborane; caesium carbonate; methanol / tetrahydrofuran / 6 h / 70 °C 1.2: 1 h / 0 °C 2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / 1,4-dioxane; aq. phosphate buffer / 25 °C / pH 6.8 2.2: 22 h / 25 °C 3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium chlorite; sodium hypochlorite / toluene; aq. phosphate buffer / 12 h / 25 °C / pH 6.8 View Scheme | |
Multi-step reaction with 2 steps 1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; tert-butyl alcohol; water / 12 h / 20 °C / Sealed tube 2: silver trifluoromethanesulfonate; oxygen; sodium methylate / tetrahydrofuran; methanol / 37 °C / 760.05 Torr / Sealed tube View Scheme |
Conditions | Yield |
---|---|
With [Rh(OH)(cod)]2; water at 75℃; for 16h; Miyaura-Hayashi reaction; Inert atmosphere; | 96% |
4-phenylbutane-1,2-diol
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With 1‐methyl‐2‐azaadamantane‐N‐oxyl; sodium hypochlorite; sodium chlorite In aq. phosphate buffer; acetonitrile at 20℃; for 2.5h; pH=6.8; Inert atmosphere; | 96% |
With oxygen; sodium methylate; silver trifluoromethanesulfonate In tetrahydrofuran; methanol at 37℃; under 760.051 Torr; Sealed tube; | 85% |
Multi-step reaction with 2 steps 1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / toluene; aq. phosphate buffer / 25 °C / pH 6.8 1.2: 4 h / 25 °C 2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium chlorite; sodium hypochlorite / toluene; aq. phosphate buffer / 12 h / 25 °C / pH 6.8 View Scheme | |
Multi-step reaction with 2 steps 1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / 1,4-dioxane; aq. phosphate buffer / 25 °C / pH 6.8 1.2: 22 h / 25 °C 2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium chlorite; sodium hypochlorite / toluene; aq. phosphate buffer / 12 h / 25 °C / pH 6.8 View Scheme |
Conditions | Yield |
---|---|
With dmap; benzenesulfonic anhydride In dichloromethane at 20℃; for 1h; | 100% |
With tetrakis(pyridin-2-yloxy)silane In tetrahydrofuran at 20℃; for 24h; | 97% |
With BuSi(Im)3 In tetrahydrofuran at 20℃; | 96% |
Conditions | Yield |
---|---|
With 4-methyl-morpholine; N-[4-methoxy-6-(N'-phenylbenzamido)-1,3,5-triazin-2-yl]-N-methylmorpholinium chloride at 20℃; for 3h; Reagent/catalyst; | 100% |
With 4-(1H,1H-perfluorotetradecyl)-C6F4-CH(SO2CF3)2 at 70℃; for 7h; | 99% |
With sulfuric acid for 5h; Reflux; | 99% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane at 80℃; for 3h; Friedel-Crafts Acylation; High pressure; Inert atmosphere; Green chemistry; | 100% |
With trifluorormethanesulfonic acid at 5 - 20℃; for 2h; Cyclization; | 99% |
With polyphosphoric acid at 90℃; for 0.5h; | 98.2% |
Conditions | Yield |
---|---|
Stage #1: 3-Phenylpropionic acid With resin-bound amine; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate In N,N-dimethyl-formamide at 20℃; Stage #2: With pyridine; trifluoroacetic anhydride In dichloromethane at 20℃; for 16h; | 100% |
With ammonium carbonate; diphosphorus tetraiodide In carbon disulfide at 20℃; for 6h; | 90% |
With hydroxyammonium sulfate; zinc for 0.333333h; Microwave irradiation; | 90% |
Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide In dichloromethane at 23℃; | 100% |
With oxalyl dichloride In dichloromethane at 20℃; | 100% |
With oxalyl dichloride In dichloromethane for 24h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With [Cl(C6F13C2H4)2SnOSn(C2H4C6F13)2Cl]2 In various solvent(s) at 150℃; for 10h; | 100% |
With N,N'-dimethylaminopyridine; di-tert-butyl dicarbonate In nitromethane at 50℃; for 16h; | 99% |
With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 1h; | 99% |
3-Phenyl-1-propanol
3-Phenylpropionic acid
3-phenylpropionic acid 3-phenylpropyl ester
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 15.5h; Esterification; | 100% |
With octamethylcyclotetrasiloxane; titanium(IV) chloride tris(trifluoromethanesulfonate) In toluene at 50℃; for 18h; | 99% |
With dmap In dichloromethane at 20℃; for 1h; | 97% |
Conditions | Yield |
---|---|
With 1-chloro-3-hydroxy-1,1,3,3-tetrabutyldistannoxane at 120℃; for 24h; Esterification; | 100% |
Zn4O (OCOCF3)6(CF3COOH)n In di-isopropyl ether for 18h; Product distribution / selectivity; Inert atmosphere; Reflux; | 100% |
With di-tert-butyl dicarbonate; magnesium chloride at 20℃; | 97% |
Conditions | Yield |
---|---|
With dmap; trimethylsilylethoxyacetylene; mercury(II) oxide In 1,2-dichloro-ethane at 40℃; for 0.5h; | 100% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; | 100% |
With dmap; di-2-thienyl carbonate In dichloromethane at 20℃; for 2h; | 95% |
1-Hydroxy-2-pyridon
3-Phenylpropionic acid
2(1H)-oxo-1-pyridyl 3-phenylpropanoate
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In dichloromethane | 100% |
3-hydroxy-3,4-dihydrobenzotriazine-4-one
3-Phenylpropionic acid
3-Phenyl-propionic acid 4-oxo-4H-benzo[d][1,2,3]triazin-3-yl ester
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In tetrahydrofuran | 100% |
3-Phenylpropionic acid
1,1-d2-3-phenylpropan-1-ol
Conditions | Yield |
---|---|
With lithium aluminium deuteride In diethyl ether at 0 - 20℃; for 2h; | 100% |
With lithium aluminium deuteride In diethyl ether 1.) RT, 1 h, 2.) reflux, 8 h; | 94% |
With lithium aluminium deuteride In diethyl ether for 16h; Heating; | 94% |
Conditions | Yield |
---|---|
With 4-methyl-morpholine; 2-chloro-4-(2,6-dimethylphenyl)-6-methoxy-1,3,5-triazine In methanol at 20℃; for 0.0833333h; Catalytic behavior; Solvent; Reagent/catalyst; | 100% |
With 4-methyl-morpholine In dichloromethane at 20℃; for 24h; | 99% |
Stage #1: 3-Phenylpropionic acid With 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; trimethylamine In dichloromethane at 20℃; for 1h; Stage #2: phenethylamine In dichloromethane at 20℃; for 3h; | 98% |
Conditions | Yield |
---|---|
With tetrakis(2-methylimidazol-1-yl)silane In tetrahydrofuran at 20℃; for 3h; | 100% |
With aluminum oxide; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride In dichloromethane at 20℃; for 0.5h; | 99% |
With borane-ammonia complex In 5,5-dimethyl-1,3-cyclohexadiene for 12h; Reflux; | 99% |
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
3-Phenylpropionic acid
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
With 4-methyl-morpholine In 1,4-dioxane; water at 20℃; for 0.25h; |
Conditions | Yield |
---|---|
With [Cl(C6F13C2H4)2SnOSn(C2H4C6F13)2Cl]2 In various solvent(s) at 150℃; for 10h; | 100% |
With sulfonated polypyrene In n-heptane at 110℃; for 2h; | 98% |
With trifluorormethanesulfonic acid at 80℃; for 18h; Reagent/catalyst; Temperature; Sealed tube; | 98% |
benzyl-methyl-amine
3-Phenylpropionic acid
N-benzyl-N-methyl-3-phenylpropionamide
Conditions | Yield |
---|---|
With 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride In methanol at 20℃; for 3h; | 100% |
With tetrakis(2-methylimidazol-1-yl)silane In tetrahydrofuran at 20℃; for 12h; | 99% |
Stage #1: 3-Phenylpropionic acid With 1,1'-carbonyldioxydi[2(1H)-pyridone] In dichloromethane at 20℃; for 1h; Stage #2: benzyl-methyl-amine In dichloromethane at 20℃; | 97% |
Conditions | Yield |
---|---|
Stage #1: 3-Phenylpropionic acid With (chloro-phenylthio-methylene)dimethylammonium chloride In dichloromethane at 0℃; for 0.5h; Stage #2: N-butylamine In dichloromethane at 20℃; for 12h; | 100% |
With dmap; triethylamine; trichlorophosphate In dichloromethane at 20℃; for 2h; | 95% |
Stage #1: 3-Phenylpropionic acid With 1,1'-carbonyldiimidazole In water; acetonitrile at 30℃; for 0.25h; Stage #2: N-butylamine In water; acetonitrile Reagent/catalyst; |
Conditions | Yield |
---|---|
With [Cl(C6F13C2H4)2SnOSn(C2H4C6F13)2Cl]2 In various solvent(s) at 150℃; for 10h; | 100% |
Stage #1: 3-Phenylpropionic acid With iodine; triphenylphosphine In dichloromethane at 20℃; for 0.166667h; Stage #2: With gadolinium(III) trifluoromethanesulfonate In dichloromethane at 50℃; for 0.5h; Stage #3: Geraniol In dichloromethane | 71% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 16h; | |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; |
Conditions | Yield |
---|---|
Stage #1: 3-Phenylpropionic acid With 1,1'-carbonyldioxydi[2(1H)-pyridone] In dichloromethane at 20℃; for 1h; Stage #2: Benzhydrylamine In dichloromethane at 20℃; | 100% |
With dmap In dichloromethane at 0℃; for 1h; | 97% |
Stage #1: 3-Phenylpropionic acid With dmap; nicotinic anhydride In dichloromethane at 0℃; for 0.166667h; Stage #2: Benzhydrylamine In dichloromethane at 0℃; for 1h; | 97% |
Conditions | Yield |
---|---|
Stage #1: 3-Phenylpropionic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate at 20℃; for 0.166667h; Stage #2: 1-Adamantanamine at 20℃; for 1h; | 100% |
With dmap; 2-methyl-6-nitrobenzoic anhydride In dichloromethane at 20℃; | 96% |
Stage #1: 3-Phenylpropionic acid With 1,1'-carbonyldioxydi[2(1H)-pyridone] In dichloromethane at 20℃; for 1h; Stage #2: 1-Adamantanamine In dichloromethane at 20℃; | 90% |
Conditions | Yield |
---|---|
Stage #1: 3-Phenylpropionic acid With 1,1'-carbonyldioxydi[2(1H)-pyridone] In dichloromethane at 20℃; for 1h; Stage #2: 3-Phenylpropan-1-amine In dichloromethane at 20℃; | 100% |
With dmap; benzenesulfonic anhydride In dichloromethane at 20℃; for 1h; | 100% |
With tetrakis(2-methylimidazol-1-yl)silane In tetrahydrofuran at 20℃; for 3h; Product distribution; Further Variations:; Solvents; molar ratios, reaction times; | 99% |
Conditions | Yield |
---|---|
Stage #1: 3-Phenylpropionic acid With trifluoroacetic anhydride; indium(III) chloride at 20℃; Stage #2: β-naphthol at 20℃; for 0.166667h; | 100% |
3-Phenylpropionic acid
1-[(R)-1-(tert-butyldimethylsilyloxy)-4-(6-aminoindol-1-yl)-2-butyl]imidazole-4-carboxamide
1-[(R)-1-(tert-butyldimethylsilyloxy)-4-(6-(3-phenylpropionylamino)indol-1-yl)-2-butyl]imidazole-4-carboxamide
Conditions | Yield |
---|---|
Stage #1: 3-Phenylpropionic acid With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In dichloromethane at 20℃; for 0.666667h; Stage #2: 1-[(R)-1-(tert-butyldimethylsilyloxy)-4-(6-aminoindol-1-yl)-2-butyl]imidazole-4-carboxamide In dichloromethane at 20℃; for 4h; | 100% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 11h; Esterification; | 100% |
With 4-nitro-diphenylammonium triflate In toluene at 80℃; for 8h; | 94% |
With toluene-4-sulfonic acid at 20℃; for 0.5h; |
(S)-1-Phenyl-3-buten-1-ol
3-Phenylpropionic acid
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide; dmap In dichloromethane at 20℃; for 12h; | 100% |
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