Dayang Chem (Hangzhou) Co.,Ltd.
Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Puyang Huicheng Electronic Material Co., Ltd
Puyang Huicheng Electronic Material Co., Ltd was founded in 2002, which is focus on high complex new type intermediates and fine chemical custom synthesis, LED&OLED materials and related intermediates, catalyst design and synthesis.
Cas:98-80-6
Min.Order:100 Gram
Negotiable
Type:Manufacturers
inquiryBeijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)
Capability on chemical synthesis 1. Beijing High-Tech Enterprises 2. Strong R&D Team 3. 8 years of experiences in R & D of high-tech Catalyst; 4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales; 5.
Jinan Finer Chemical Co., Ltd
Product Description Product website: http://www.finerchem.com/pro01en/id/53.html Product Name Phenylboronic acid CAS No. 98-80-6 Appearance White powder Assay ≥99% Capacity
Cas:98-80-6
Min.Order:1 Gram
FOB Price: $23.0
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:98-80-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquirySuzhou Sinosun Imp.&Exp. Corporation
We supply good quality phenylboronic acid 98-80-6 at competitive price. Our phenylboronic acid 98-80-6 has been exported to many countries and regions. If you are looking for phenylboronic acid 98-80-6 suppliers in China, Sinosun is your best
LEAP CHEM Co., Ltd.
Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP
Simagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Hangzhou Dingyan Chem Co., Ltd
Items Standard Result Appearance White crystalline powder Conforms Assay (HPLC) 99.0% min
Cas:98-80-6
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Manufacturers
inquiryHebei yanxi chemical co.,LTD.
Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
Cas:98-80-6
Min.Order:1 Metric Ton
FOB Price: $1.0 / 2.0
Type:Manufacturers
inquiryHenan Allgreen Chemical Co.,Ltd
T he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality service Appearance:White or
Hangzhou Think Chemical Co. Ltd
Phenylboronic acid CAS No.:98-80-6 Name: Phenylboronic acid Synonyms: Benzeneboronic acid; Phenylboron dihydroxide Molecular Structure Molecular Form
Cas:98-80-6
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Other
inquiryAlity Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Xi'an Xszo Chem Co., Ltd.
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:98-80-6
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryShanghai SE Pharm Co., Ltd
1. made in GMP plant, commerially 2. Normal Stock: 500kgs 3. Audit accepted. Related documents are available to offer and audited by many clients, such as Lupin, MSN, Dr reddy etc 4. Chromatographic Purity (HPLC): not less than 99.0% Appearan
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:98-80-6
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryHenan Tianfu Chemical Co., Ltd.
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:98-80-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHebei Nengqian Chemical Import and Export Co., LTD
Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:98-80-6
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryZhuozhou Wenxi import and Export Co., Ltd
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:98-80-6
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryWuhan Han Sheng New Material Technology Co.，Ltd
Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:98-80-6
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryHenan Sinotech Import&Export Corporation
Product Name Phenylboronic acid Synonyms Phenylboronic acid;Phenylboron dihydroxide CAS: 98-80-6 MF: C6H7BO2 MW: - EINECS:
Cas:98-80-6
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiryHubei Langyou International Trading Co., Ltd
1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White or Yellowish Crystals Storage:Store in sealed containe
Cas:98-80-6
Min.Order:100 Gram
Negotiable
Type:Other
inquiryShanghai Upbio Tech Co.,Ltd
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:98-80-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryShanghai Minstar Chemical Co., Ltd
Melting point 216-219 °C(lit.) Boiling point 265.9±23.0 °C(Predicted) density 1.13±0.1 g/cm3(Predicted) storage temp. 0-6°C pka 8.83(at 25℃) form Crystalline Powder color White to off-white Water S
Cas:98-80-6
Min.Order:100 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryBaoji Guokang Healthchem co.,ltd
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:98-80-6
Min.Order:1 Kilogram
FOB Price: $85.0 / 100.0
Type:Trading Company
inquiryQingdao Beluga Import and Export Co., LTD
Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates, steroids, pharmaceutical
Cas:98-80-6
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryShandong Hanjiang Chemical Co., Ltd.
Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:98-80-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryLIDE PHARMACEUTICALS LIMITED
Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:98-80-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Changchun Artel lmport and Export trade company
Product Detail Minimum Order Qty. 10 Gram
Cas:98-80-6
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquirySynthetic route
-
-
24388-23-6
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole
-
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| Stage #1: 2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole With potassium hydrogen difluoride In methanol at 20℃; for 0.25h; Stage #2: With lithium hydroxide In acetonitrile at 20℃; for 20h; | 100% |
| With hydrogenchloride In water at 20℃; for 15h; | 100% |
| With polystyrene boronic acid; trifluoroacetic acid In acetonitrile for 18h; Heating; | 98% |
| Multi-step reaction with 2 steps 1: diethyl ether / 0.5 h / 20 °C 2: hydrogenchloride / water / 0.33 h View Scheme | |
| With dimyristoylphosphatidylcholine; water In dimethyl sulfoxide at 20℃; for 168h; |
-
-
556-97-8
1-chloro-3,5-dimethylbenzene
-
A
-
17057-88-4
3,5-dimethylbiphenyl
-
B
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| With cesium fluoride; Pd(dba)2 In toluene | A n/a B 99% |
| Conditions | Yield |
|---|---|
| In methanol at 15℃; for 3h; Microwave irradiation; | 98% |
| Conditions | Yield |
|---|---|
| With montmorillonite K10 at 25℃; for 0.5h; Catalytic behavior; Reagent/catalyst; Temperature; | 97% |
| With 1H-imidazole; iron(III) chloride at 20℃; for 0.25h; Catalytic behavior; Solvent; Reagent/catalyst; Time; Inert atmosphere; | 87% |
| With glass or Cs2CO3 In tetrahydrofuran; water Kinetics; hydrolysis at 55°C in THF/H2O in the presence of glass powder or Cs2CO3; not isolated; |
-
-
13061-96-6
dihydroxy-methyl-borane
-
-
24388-23-6
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole
-
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| With trifluoroacetic acid In dichloromethane at 20℃; Reagent/catalyst; Solvent; | 97% |
| Conditions | Yield |
|---|---|
| With borane; water In tetrahydrofuran for 1h; Heating; | 96% |
| Conditions | Yield |
|---|---|
| at -78 - -45℃; | 95% |
-
-
22092-92-8
diisopropopylaminoborane
-
-
7732-18-5
water
-
-
100-58-3
phenylmagnesium bromide
-
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| Stage #1: diisopropopylaminoborane; phenylmagnesium bromide In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; Stage #2: water With hydrogenchloride In tetrahydrofuran at 0℃; for 0.583333h; Inert atmosphere; | 95% |
-
-
55124-35-1
diisopropylamine borane
-
-
7732-18-5
water
-
-
100-58-3
phenylmagnesium bromide
-
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| Stage #1: diisopropylamine borane; phenylmagnesium bromide In tetrahydrofuran at 20℃; Stage #2: water In tetrahydrofuran; methanol | 95% |
| Conditions | Yield |
|---|---|
| excess acid addn. to soln. of Sb-compd., refluxing (3 h), volatile products collecting in cooled trap; products sepn. by ether; | A 94% B 92% |
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 20℃; Temperature; Concentration; Flow reactor; | 93.9% |
| Conditions | Yield |
|---|---|
| In methanol at 15℃; for 3h; Microwave irradiation; | 92% |
| With [{Pd(μ-Cl){κ2-P,C-P(iPr)2(OC6H3-2-Ph)}}2]; sodium acetate In dichloromethane; water at 40℃; for 6h; Inert atmosphere; | |
| With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N-ethyl-N,N-diisopropylamine; triphenylphosphine In ethanol at 80℃; for 4h; Miyaura Borylation Reaction; Schlenk technique; Inert atmosphere; Sealed tube; |
-
-
131765-96-3
dicyclohexylamine borane complex
-
-
7732-18-5
water
-
-
100-58-3
phenylmagnesium bromide
-
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| Stage #1: dicyclohexylamine borane complex; phenylmagnesium bromide In tetrahydrofuran at 20℃; Stage #2: With methanol In tetrahydrofuran Stage #3: water In tetrahydrofuran | 92% |
| Conditions | Yield |
|---|---|
| With bis(pinacol)diborane; Ir(o-O-C6H4-CH=N=CH2Ph)(cod) at 80℃; for 21h; Product distribution; Further Variations:; Solvents; | 91% |
| Stage #1: benzene With Pinacolborane; bis(pinacol)diborane; 4,4'-di-tert-butyl-2,2'-bipyridine; (1,5-cyclooctadiene)(methoxy)iridium(l) dimer at 80℃; for 24h; Stage #2: With sodium periodate In tetrahydrofuran; water for 0.5h; Stage #3: With hydrogenchloride In tetrahydrofuran; water at 20℃; for 17h; | |
| Multi-step reaction with 2 steps 1: Pd 2: H2O View Scheme |
| Conditions | Yield |
|---|---|
| With tetra-2-pyridinylpyrazine; [Ir(I)(salicylidenebenzyliminato)(1,5-cyclooctadiene)] In dichloromethane; benzene under Ar; mixt. was heated at 80°C for 21 h in mixt. of 3 ml benzene and 2 ml each CH2Cl2 and ionic liquid TBPD (tributyltetradecylphosphonium dodecylbenzenesulfonate) as solvent; solvent was removed under reduced pressure, Et2O was added, after 10% aq. HCl was added, mixt. stirred for 4 h, organic layer dried with MgSO4, solvent was removed under reduced pressure, residue was chromd. (flash chromy, SiO2); NMR; | 91% |
| With tetra-2-pyridinylpyrazine; [Ir(I)(salicylidenebenzyliminato)(1,5-cyclooctadiene)] In benzene under Ar; soln. of Ir complex and pyridinylpyrazine was prepared, pinacolato soln. was added, mixt. was then heated at 80°C for 21 h; solvent was removed under reduced pressure, Et2O was added, after 10% aq. HCl was added, mixt. stirred for 4 h, organic layer dried with MgSO4, solvent was removed under reduced pressure, residue was chromd. (flash chromy, SiO2); NMR; | 70% |
| With tetra-2-pyridinylpyrazine; [Ir(I)(salicylidenebenzyliminato)(1,5-cyclooctadiene)] In benzene High Pressure; under Ar; soln. of Ir complex and pyridinylpyrazine was prepared in glove box, pinacolato soln. and prepared catalyst and ligand soln. were placed in autoclave, mixt. was then heated at 100°C for 40 h; solvent was removed under reduced pressure, Et2O was added, after 10% aq. HCl was added, mixt. stirred for 4 h, organic layer dried with MgSO4, solvent was removed under reduced pressure, residue was chromd. (flash chromy, SiO2); NMR; | 67% |
| Conditions | Yield |
|---|---|
| With hydrogenchloride In dichloromethane; benzene other Radiation; under Ar atm. mixt. HBpin, nano-Ir(0) cat. prepd by reduction (Ph3P)2Ir(H)(7,8-nido-C2B9H11), tetra-2-pyridinylpyrazine, benzene, CH2Cl2 and trihexyltetradecylphosphonium methylsulfonate was heated at 130°C for 1 h in microwave, hydrolysis aq.HCl; flash chromy.; | 91% |
| With hydrogenchloride In dichloromethane; benzene Sonication; under Ar atm. mixt. HBpin, nano-Ir(0) cat. prepd by reduction (Ph3P)2Ir(H)(7,8-nido-C2B9H11), tetra-2-pyridinylpyrazine, benzene, CH2Cl2 and trihexyltetradecylphosphonium methylsulfonate was heated at 80°C for4 h in ultrasonic, hydrolysis aq.HCl; flash chromy.; | 61% |
| With hydrogenchloride In dichloromethane; benzene High Pressure; under Ar atm. mixt. HBpin, nano-Ir(0) cat. prepd by reduction (Ph3P)2Ir(H)(7,8-nido-C2B9H11), tetra-2-pyridinylpyrazine, benzene, CH2Cl2 and trihexyltetradecylphosphonium methylsulfonate was heated at 180°C for 12 h, hydrolysis with aq.HCl; flash chromy.; | 50% |
| Conditions | Yield |
|---|---|
| With acetic acid In water | 90% |
-
-
67-56-1
methanol
-
-
108-86-1
bromobenzene
-
-
55124-35-1
diisopropylamine borane
-
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| Stage #1: diisopropylamine borane With magnesium; phenylmagnesium bromide In tetrahydrofuran at 20℃; for 0.166667h; Stage #2: bromobenzene In tetrahydrofuran at 70℃; Stage #3: methanol Further stages; | 88% |
-
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| With iron(III) chloride; water In tetrahydrofuran at 20℃; for 0.5h; | 86% |
| With water; silica gel at 20℃; for 4h; Inert atmosphere; | 65% |
| In phosphate buffer pH=6.9 - 7.0; Kinetics; | |
| With water In tetrahydrofuran at 55℃; Kinetics; Reagent/catalyst; |
| Conditions | Yield |
|---|---|
| With n-butyllithium In tetrahydrofuran at -78℃; Inert atmosphere; | 82.7% |
| With n-butyllithium In tetrahydrofuran |
| Conditions | Yield |
|---|---|
| Stage #1: bromobenzene With triethylamine; bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran at 65℃; Stage #2: With sodium hydroxide In tetrahydrofuran Further stages.; | 82% |
| Stage #1: bromobenzene With Trimethyl borate In tetrahydrofuran at -20 - 0℃; Inert atmosphere; Stage #2: With sulfuric acid In tetrahydrofuran at 0 - 10℃; for 10h; Inert atmosphere; | 82.4% |
| Stage #1: bromobenzene With magnesium In tetrahydrofuran Stage #2: With Trimethyl borate In tetrahydrofuran at -70℃; | 82.4% |
| Conditions | Yield |
|---|---|
| With 1H-imidazole; thionyl chloride In acetonitrile the B complex was obtained by a treatment of the boronic ester with SOCl2 and imidazole in the presence of borosilicate glass (the catalyst); this complex was hydrolized in aq. CH3CN; | 82% |
-
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane; water at 20℃; for 8h; | 81% |
-
-
121-43-7
Trimethyl borate
-
-
100-58-3
phenylmagnesium bromide
-
A
-
108-95-2
phenol
-
B
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at -12℃; Temperature; Concentration; Flow reactor; | A 7.9% B 80.7% |
| Conditions | Yield |
|---|---|
| Stage #1: iodobenzene With diisopropopylaminoborane; triethylamine; triphenylphosphine; palladium dichloride In tetrahydrofuran at 65℃; for 12h; Alcaraz-Vaultier borylation; Inert atmosphere; Stage #2: With methanol In tetrahydrofuran at 0℃; Inert atmosphere; Further stages; | 80% |
| Multi-step reaction with 2 steps 2: H2O View Scheme |
-
-
121-43-7
Trimethyl borate
-
-
100-58-3
phenylmagnesium bromide
-
A
-
108-90-7
chlorobenzene
-
B
-
108-95-2
phenol
-
C
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 22℃; Temperature; Concentration; Flow reactor; | A 8.9% B 5.7% C 79.6% |
| Conditions | Yield |
|---|---|
| With lithium In tetrahydrofuran at -10℃; Inert atmosphere; | 76% |
-
-
13283-31-3
borane
-
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| With water; phenylmagnesium bromide In tetrahydrofuran slow addn. of 10 mmol of the Grignard reagent to a stirred soln. of borane in THF (40 mmol); the mixt. was poured into ice-water and acidified with 10% HCl;; extn. into ether three-times; the combined extracts were dried over NaSO4; removal of solvent under reduced pressure; trituration with petroleum ether; recrystn. from H2O;; | 75% |
| With bromobenzene; water; magnesium In tetrahydrofuran a 2.0 M soln. of borane (40 mmol) in THF was added to flame dried Mg turnings (12 mmol) at 0°C; slow addn. of the aryl bromide (10 mmol)in THF; stirring at room temp. for 12-16 h; the mixt. was poured into ice-water and acidified with 10% HCl;; extn. into ether three-times; the combined extracts were dried over NaSO4; removal of solvent under reduced pressure; trituration with petroleum ether; recrystn. from H2O;; |
-
-
17763-67-6
Phenyl triflate
-
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| Stage #1: Phenyl triflate With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; diisopropopylaminoborane; triethylamine; triphenylphosphine In tetrahydrofuran at 65℃; for 12h; Alcaraz-Vaultier borylation; Inert atmosphere; Stage #2: With methanol In tetrahydrofuran at 0℃; Inert atmosphere; Further stages; | 74% |
| Conditions | Yield |
|---|---|
| at 80℃; for 1h; | 100% |
| for 0.166667h; Schlenk technique; | 96% |
| In dichloromethane; ethyl acetate at 20℃; | 81% |
-
-
95-54-5
1,2-diamino-benzene
-
-
98-80-6
phenylboronic acid
-
-
2479-64-3
2-phenyl-2,3-dihydro-1H-benzo[1,3,2]diazaborole
| Conditions | Yield |
|---|---|
| at 40℃; for 1h; | 100% |
| In toluene for 2h; Reflux; | 92% |
| In toluene stirring mixt. of diamine deriv. and phenylboric acid in toluene for 2 hat reflux; filtration, washing with petroleum ether, NMR; | 92% |
-
-
87-66-1
2-hydroxyresorcinol
-
-
98-80-6
phenylboronic acid
-
-
108880-02-0
2-phenyl-1,3,2-benzodioxaborole-4-ol
| Conditions | Yield |
|---|---|
| at 40℃; for 2h; | 100% |
-
-
69-65-8
mannitol
-
-
98-80-6
phenylboronic acid
-
-
6638-75-1, 62560-54-7
(2R,3R,4R,5R)-1:2,3:4,5:6-O1:O2,O3:O4,O5:O6-tris(phenylboranato)-D-mannitol
| Conditions | Yield |
|---|---|
| at 20℃; for 1h; | 100% |
| Conditions | Yield |
|---|---|
| at 110℃; for 6h; | 100% |
| at 110℃; for 6h; Inert atmosphere; Neat (no solvent); | 100% |
| Stage #1: phenylboronic acid With barium(II) hydroxide In water at 80℃; for 0.0833333h; Stage #2: With Au38(SCH2CH2Ph)24 In toluene at 80℃; for 12h; Reagent/catalyst; | 100% |
-
-
118-92-3
anthranilic acid
-
-
98-80-6
phenylboronic acid
-
-
42409-65-4
2-phenyl-1,2-dihydro-benzo[a][1,3,2]-oxazaborinin-4-one
| Conditions | Yield |
|---|---|
| at 20℃; for 1h; | 100% |
| In toluene for 16h; Inert atmosphere; Dean-Stark; Reflux; | 93% |
| In toluene | |
| In tetrahydrofuran for 24h; Reflux; | 72 %Spectr. |
-
-
126-30-7
2,2-Dimethyl-1,3-propanediol
-
-
98-80-6
phenylboronic acid
-
-
5123-13-7
5,5-dimethyl-2-phenyl-1,3,2-dioxaborinane
| Conditions | Yield |
|---|---|
| With magnesium sulfate In diethyl ether at 25℃; for 20h; Inert atmosphere; | 100% |
| In tetrahydrofuran for 0.666667h; Inert atmosphere; Dean-Stark; Reflux; | 100% |
| With magnesium sulfate In diethyl ether at 20℃; for 20h; | 100% |
| Conditions | Yield |
|---|---|
| 100% | |
| In di-isopropyl ether |
-
-
479-27-6
naphthalene-1,8-diamine
-
-
98-80-6
phenylboronic acid
-
-
24341-81-9
2-phenyl-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine
| Conditions | Yield |
|---|---|
| at 0℃; for 1h; | 100% |
| With 1H-imidazole; iron(III) chloride In water; acetonitrile at 20℃; for 2h; Catalytic behavior; Temperature; Time; Inert atmosphere; | 93% |
| at 150℃; for 0.25h; Microwave irradiation; Sealed tube; | 90% |
-
-
29180-72-1
oxalodihydrazonic acid dianilide
-
-
98-80-6
phenylboronic acid
| Conditions | Yield |
|---|---|
| 100% | |
| In di-isopropyl ether |
| Conditions | Yield |
|---|---|
| With potassium phosphate; bis(tricyclohexylphosphine)nickel(II) dichloride In tert-Amyl alcohol for 12h; Solvent; Suzuki-Miyaura Coupling; Heating; | 100% |
| With cesiumhydroxide monohydrate; 2-dicyclohexylphosphino-2′,6′-diisopropoxybiphenyl; palladium diacetate In water; butan-1-ol at 25℃; for 0.25h; Solvent; Reagent/catalyst; Suzuki-Miyaura Coupling; Inert atmosphere; | 100% |
| With potassium phosphate; catacxium A; palladium diacetate In toluene at 100℃; for 20h; Suzuki reaction; | 99% |
| Conditions | Yield |
|---|---|
| With [Pd(N-(naphthyl)-salicylaldimine(-2H))(triphenylphosphine)]; sodium hydroxide at 120℃; for 24h; Reagent/catalyst; Suzuki Coupling; | 100% |
| With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; water; toluene for 18h; Inert atmosphere; Reflux; | 100% |
| With potassium phosphate; (PdCl2)(2-pyridyl)-6-isopropyl cis piperidine complex In water; N,N-dimethyl-formamide at 110℃; for 2h; | 99% |
| Conditions | Yield |
|---|---|
| With tetrabutyl ammonium fluoride; tricyclohexylphosphine; dichloro bis(acetonitrile) palladium(II) at 85 - 90℃; for 5h; Suzuki-Miyaura reaction; | 100% |
| With potassium phosphate; C46H52Cl3N3O2Pd In tetrahydrofuran; water at 60℃; for 4h; Suzuki-Miyaura Coupling; | 99% |
| With 2-((3-sulfonatomesityl)-5-sulfonatoindenyl)dicyclohexylphosphinehydrate sodium salt; palladium diacetate; potassium carbonate In water at 100℃; for 24h; Suzuki-Miyaura Coupling; | 95% |
| Conditions | Yield |
|---|---|
| With caesium carbonate; palladium diacetate In N,N-dimethyl-formamide at 80℃; for 6h; Suzuki-Miyaura cross-coupling reaction; | 100% |
| With potassium carbonate In ethanol; water at 30℃; for 1h; Suzuki-Miyaura Coupling; | 100% |
| With N,N,N′,N′-tetra(diphenylphosphinomethyl)-1,2-ethylenediamine; potassium carbonate; palladium dichloride In 1,4-dioxane; N,N-dimethyl-formamide at 90℃; for 6h; Suzuki coupling; Inert atmosphere; | 99% |
| Conditions | Yield |
|---|---|
| With Cs2O3; PCy3 adduct of cyclopalladated ferrocenylimine In 1,4-dioxane at 100℃; for 15h; Suzuki cross-coupling reaction; | 100% |
| With dichloro(cycloocta-1,5-diene)palladium (II); 2,2-[μ-(N,N'-piperazindiyl)dimethyl]-bis(4,6-di-tert-butyl-phenol); potassium carbonate In methanol for 0.166667h; Suzuki cross-coupling reaction; Microwave irradiation; Inert atmosphere; | 100% |
| With potassium carbonate In methanol at 100℃; for 0.0833333h; Suzuki-Miyaura Coupling; Microwave irradiation; | 100% |
| Conditions | Yield |
|---|---|
| With potassium phosphate monohydrate; 4,4'-di-tBu-2,2'-dipyridylpalladium(II) dichloride In methanol; water at 80℃; for 2h; Suzuki-Miyaura Coupling; | 100% |
| With potassium carbonate; palladium dichloride In water at 20 - 90℃; Suzuki coupling; Inert atmosphere; | 99% |
| With potassium carbonate In water at 90℃; for 0.25h; Suzuki reaction; Inert atmosphere; | 99% |
| Conditions | Yield |
|---|---|
| With trans-dibromobis(1-butyl-3-methylimidazol-2-ylidene)palladium(II); sodium hydrogencarbonate In ethylene glycol at 110℃; for 1h; Catalytic behavior; Suzuki-Miyaura Coupling; Schlenk technique; | 100% |
| With tetrabutylammomium bromide; sodium carbonate In water at 100℃; for 2h; Suzuki coupling; | 99% |
| With sodium carbonate In 1,2-dimethoxyethane; water for 16h; Heating / reflux; | 86% |
| Conditions | Yield |
|---|---|
| With potassium carbonate; copper-palladium In N,N-dimethyl-formamide at 110℃; for 4h; Suzuki cross-coupling; | 100% |
| With tetra-butylammonium acetate; Pd EnCat-30TM In ethanol at 120℃; for 0.166667h; Suzuki cross-coupling; microwave irradiation; | 97% |
| With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water at 100 - 102℃; Suzuki Coupling; Inert atmosphere; | 93% |
| Conditions | Yield |
|---|---|
| With sodium hydroxide; palladium dichloride In water for 0.166667h; Product distribution; Ambient temperature; other reagents, reaction times; | 100% |
| With sodium hydroxide; palladium diacetate In water at 20℃; for 2h; Suzuki reaction; | 100% |
| With disodium hydrogenphosphate; Pd(OAc)2(2-amino-4,6-dihydroxypyrimidine disodium salt)2 In water at 120℃; for 0.166667h; Suzuki-Miyaura coupling; Microwave irradiation; | 98% |
| Conditions | Yield |
|---|---|
| With potassium carbonate In ethanol at 80℃; for 36h; Suzuki-Miyaura Coupling; Inert atmosphere; | 100% |
| With C28H38Cl2N2O6PdS2(2-)*2Na(1+); tetrabutylammomium bromide; potassium carbonate In water at 75℃; Suzuki coupling; Inert atmosphere; | 99% |
| With Br(1-)*C28H29BrN5O2Pd(1+); potassium carbonate In methanol; water at 100℃; for 3h; Suzuki-Miyaura coupling; | 99% |
| Conditions | Yield |
|---|---|
| With potassium carbonate; {1,3-di[(R)-1-PhEt]imidazolin-2-ylidene}(PPh3)PdI2 In xylene at 130℃; for 13h; Suzuki-Miyaura cross-coupling reaction; | 100% |
| With potassium phosphate; triphenylphosphine; Ni(II) complexes of bidentate carbene; phosphine ligand In toluene at 80℃; Suzuki cross-coupling; | 100% |
| With [PdCl2(2-ethyl-2-oxazoline)2]; potassium carbonate In toluene at 110℃; for 3h; Suzuki reaction; | 100% |
| Conditions | Yield |
|---|---|
| With potassium carbonate; {1,3-di[(R)-1-PhEt]imidazolin-2-ylidene}(PPh3)PdI2 In xylene at 130℃; for 14h; Suzuki-Miyaura cross-coupling reaction; | 100% |
| With 1,2-bis(diphenylphosphino)-1'-(diisopropylphosphino)-3',4-di-tert-butyl ferrocene; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) In xylene at 130℃; for 20h; Suzuki cross-coupling; | 100% |
| With 1,4-diaza-bicyclo[2.2.2]octane; PEG-400; potassium carbonate; palladium diacetate at 110℃; for 2h; Suzuki-Miyaura cross-coupling reaction; | 100% |
| Conditions | Yield |
|---|---|
| With potassium carbonate; copper-palladium In N,N-dimethyl-formamide at 110℃; Kinetics; Product distribution; Further Variations:; Catalysts; Reaction partners; Suzuki cross-coupling; | 100% |
| With sodium hydroxide; Pd-dodecanethiolate nanoparticles In tetrahydrofuran at 20℃; for 24h; Suzuki-Miyaura cross-coupling; | 100% |
| With sodium carbonate; 1-butyl-3-methylimidazolium Tetrafluoroborate; 2C10H15N2(1+)*Cl4Pd(2-) In water at 110℃; for 12h; Conversion of starting material; Suzuki Coupling; | 100% |
| Conditions | Yield |
|---|---|
| With di-tert-butyl(4-sulfonatobenzyl)phosphonium; palladium diacetate; sodium carbonate In water at 50℃; for 24h; Solvent; Temperature; Reagent/catalyst; Suzuki Coupling; Inert atmosphere; Glovebox; | 100% |
| With di-tert-butyl(4-sulfonatobenzyl)phosphonium; palladium diacetate; sodium carbonate In water at 50℃; Reagent/catalyst; Solvent; Temperature; Suzuki Coupling; Inert atmosphere; Glovebox; | 100% |
| With sodium carbonate In water at 100℃; Suzuki-Miyaura reaction; | 99.1% |
| Conditions | Yield |
|---|---|
| With potassium phosphate; (η5-C5H5)Re(NO)(P(C6H5)3)(C(CH3)3)2; palladium diacetate In toluene at 100℃; for 1h; Suzuki cross-couplings reaction; | 100% |
| With N,N-dicyclohexyl-2-(dicyclohexylphosphanyl)benzenesulfonamide; tris(dibenzylideneacetone)dipalladium (0); caesium carbonate In 1,4-dioxane at 80℃; for 3h; Suzuki-Miyaura cross coupling; | 100% |
| With potassium phosphate; 3-(2,6-diisopropylphenyl)-1-(2-diphenylphosphanylbenzyl)-3H-imidazol-1-ium chloride; bis(η3-allyl-μ-chloropalladium(II)) In 1,4-dioxane at 80℃; for 12h; Product distribution; Further Variations:; Catalysts; Reagents; Solvents; Suzuki cross-coupling; | 100% |
| Conditions | Yield |
|---|---|
| With [Pd(1-butylimidazole)2Cl2]; potassium hydroxide In water; isopropyl alcohol at 40℃; for 1h; Suzuki-Miyaura reaction; Under air; | 100% |
| With caesium carbonate In water; isopropyl alcohol at 80℃; for 3h; Suzuki-Miyaura reaction; Inert atmosphere; | 100% |
| With potassium hydroxide In propan-1-ol; water at 60℃; for 1h; Reagent/catalyst; Suzuki-Miyaura Coupling; Schlenk technique; | 100% |
| Conditions | Yield |
|---|---|
| With C31H26N6O4Pd; potassium carbonate In water at 100℃; for 3h; Suzuki-Miyaura coupling; | 100% |
| With potassium phosphate; 1,1'-bis(4-methoxyphenyl)-3,3'-methylene-diimidazoline-2,2'-diylidene-palladium(II)-dibromide In toluene at 40℃; for 2h; Reagent/catalyst; Temperature; Time; Suzuki-Miyaura Coupling; Inert atmosphere; | 100% |
| With C16H21ClN2Pd; sodium carbonate In methanol at 85℃; for 1h; Reagent/catalyst; Suzuki-Miyaura Coupling; | 100% |
-
-
5111-65-9
2-Bromo-6-methoxynaphthalene
-
-
98-80-6
phenylboronic acid
-
-
59115-43-4
2-methoxy-6-phenylnaphthalene
| Conditions | Yield |
|---|---|
| With potassium phosphate; (η5-C5H5)Re(NO)(P(C6H5)3)P(C6H5)2; palladium diacetate In toluene at 100℃; for 0.25h; Suzuki cross-couplings reaction; | 100% |
| With palladium diacetate; tetrabutylammomium bromide; potassium carbonate In water at 70℃; for 1h; | 99% |
| With potassium fluoride; o-(dicyclohexylphosphino)diisopropylbenzamide; tris(dibenzylideneacetone)dipalladium (0) In N,N-dimethyl-formamide at 80℃; for 40h; Suzuki cross-coupling; | 98% |
-
-
619-42-1
4-methoxycarbonylphenyl bromide
-
-
98-80-6
phenylboronic acid
-
-
720-75-2
methyl 4-phenylbenzoate
| Conditions | Yield |
|---|---|
| With potassium phosphate; second generation phosphine dendrimer-stabilized palladium In 1,4-dioxane for 20h; Suzuki coupling; Heating; | 100% |
| With potassium phosphate; silica gel; palladium In toluene at 110℃; for 5h; Suzuki-Miyaura reaction; | 100% |
| With potassium phosphate tribasic heptahydrate In 1,4-dioxane for 20h; Suzuki coupling; Reflux; | 100% |
| Conditions | Yield |
|---|---|
| With 1,4-diaza-bicyclo[2.2.2]octane; potassium carbonate; palladium diacetate In acetone at 110℃; for 2h; Suzuki-Miyaura cross-coupling reaction; | 100% |
| With sodium hydroxide; Pd-dodecanethiolate nanoparticles In tetrahydrofuran at 20℃; for 17h; Suzuki-Miyaura cross-coupling; | 100% |
| With caesium carbonate; (1-adamantylisonitrile)2PdCl2 In 1,4-dioxane for 18h; Product distribution; Further Variations:; Catalysts; Suzuki-Miyaura reaction; Heating; | 100% |
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