Dayang Chem (Hangzhou) Co.,Ltd.
Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:11113-50-1
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquirySimagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:11113-50-1
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryJinan Finer Chemical Co., Ltd
Product Description
Cas:11113-50-1
Min.Order:1 Kilogram
FOB Price: $5.0 / 30.0
Type:Lab/Research institutions
inquiryHenan Allgreen Chemical Co.,Ltd
T he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality service Appearance:White
Ality Chemical Corporation
We are the manufacturer of this product. If you are looking for the material's manufacturer or supplier in China, AlityGroup is your best choice. Our advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise
Henan Tianfu Chemical Co., Ltd.
11113-50-1 Boric acid Basic information Product Name: Boric acid Synonyms: Boric acid;Borsrenatliche CAS: 11113-50-1 MF: BH3O3
Zhuozhou Wenxi import and Export Co., Ltd
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:11113-50-1
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Lonwin Chemical Group Limited
Boric acid CAS: 11113-50-1 Specification Product name Boric acid flakes CAS No 11113-50-1 Purity 99%min MW 61.83 Brand Crovell Address China Welcome to contact us to get
Changchun Artel lmport and Export trade company
Product Detail Minimum Order Qty. 10 Gram
Cas:11113-50-1
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryAfine Chemicals Limited
Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:11113-50-1
Min.Order:1 Kilogram
FOB Price: $1.0 / 100000.0
Type:Lab/Research institutions
inquiryHangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Hangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:11113-50-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHunan chemfish Pharmaceutical co.,Ltd
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Hangzhou Lingrui Chemical Co.,Ltd.
High purity Boric acid 11113-50-1 in stock immediately delivery good supplierAppearance:Powder Storage:Dry and ventilated Package:according to customers' requirements Application:APIs Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea
Cas:11113-50-1
Min.Order:1 Gram
Negotiable
Type:Other
inquiryHANGZHOU YUNUO CHEMICAL CO.,LTD
Superior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediates Tr
Siwei Development Group Ltd.
Product name: Boric Acid CAS No.：11113-50-1 Molecule Formula：H3BO3 Molecule Weight：61.83 Purity: 99.0% Package: 25kg/drum Description：White crystalline powder Manufacture Standards：CP/USP/EP TESTING ITEMS SPECIFIC
Cas:11113-50-1
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryZibo Dorne chemical technology co. LTD
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
GIHI CHEMICALS CO.,LIMITED
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
Aecochem Corp.
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Wuxi TAA Chemical Industry Co.,LTD.
1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re
Cas:11113-50-1
Min.Order:0
Negotiable
Type:Other
inquiryHubei Taiho Chemical Co.,LTD
TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
Xiamen AmoyChem Co.,Ltd
Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
Hangzhou Fandachem Co.,Ltd
Boric acidAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Wuhan ZeShanCheng Biomedical Technology Co., Ltd.
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl
Hangzhou ZeErRui Chemical Co., Ltd.
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
Koning Pharmchem Co., Ltd.
High quality Hot sale boric acid 10043-35-3 ; 11113-50-1 with reasonable price and fast delivery !!Appearance:WhitePowder Storage:regualr storage Package:25kg/ drum, or as your requirements Application:pharmaceutical intermediates Transportation:By a
Cas:11113-50-1
Min.Order:0
Negotiable
Type:Trading Company
inquiryHunan Longxianng Runhui Trading Co.,Ltd
Factory supply PD 173074 CAS NO.219580-11-7 with best priceAppearance:white powder Storage:keep in dry place Package:according to your request Application:Pharmaceutical Intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS f
Cas:11113-50-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquirySynthetic route
-
-
916730-63-7
1-boranyl-1,3,5-triaza-7-phosphaadamantane
-
-
7732-18-5
water
-
A
-
11113-50-1
boric acid
-
B
-
53597-69-6
(1,3,5-triaza-7-phosphaadamantane)
| Conditions | Yield |
|---|---|
| In water; acetone B-complex reacted with water in acetone/water (1:1) at 80°C for ca. 48 h; detn. by IR, 11B-NMR; | A 100% B n/a |
| In acetone slow reaction of B-complex with water; acceleration at higher temp.; | A 100% B n/a |
-
-
4262-38-8
1,3,5,7-Tetra-tert-butyl-2,4,6,8-tetrachloro-[1,3,5,7,2,4,6,8]tetrazatetraborocane
-
A
-
11113-50-1
boric acid
-
B
-
75-64-9
tert-butylamine
| Conditions | Yield |
|---|---|
| With water In further solvent(s) byproducts: HCl; solvent cyclohexanol, in tube 20.5 h at 160°C; | A n/a B 97% |
| With H2O In further solvent(s) byproducts: HCl; solvent cyclohexanol, in tube 20.5 h at 160°C; | A n/a B 97% |
| With water In xylene byproducts: HCl; in tube 20.5 h boiling; | A n/a B 62% |
| With H2O In xylene byproducts: HCl; in tube 20.5 h boiling; | A n/a B 62% |
-
-
27120-66-7
closo-1-sulfinic acid-1,12-dicarbadodecaborane(12)
-
-
7722-84-1
dihydrogen peroxide
-
A
-
226255-50-1
closo-1,12-(H)2-1,12-C2B10(OH)10
-
B
-
396695-66-2
closo-2,3,4,5,6,7,8,9,10,11-decahydroxy-1-sulfonic acid-1,12-dicarbadodecaborane(12)
-
C
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| In water aq. 30% H2O2 added to B compd.; refluxed for 3.5 h; monitored by (11)B NMR spectra; cond. HBr added; stirred (room temp., 2 h); kept. (80°C, 8 h); Br2 removed by N2 steam; volatiles removed in vac.; triturated in MeOH; centrifuged; supernatant sepd.; repeated 5 times; residue dissolved in water; filtered; dried; | A 5% B 88% C 3% |
-
-
5720-07-0
4-methoxyphenylboronic acid
-
B
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| In tetrahydrofuran byproducts: (c-C5H9)7Si7O9(OH)3; (Ar); std. Schlenk technique; B compd. was added to soln. of Pt complex in THF; heated at 60°C for 30 min; concd. (vac.); hexane added; cooled at -20°C; filtered; washed (H2O); dried (vac.); elem. anal.; | A 88% B n/a |
| In benzene-d6 byproducts: (c-C5H9)7Si7O9(OH)3; (Ar); std. Schlenk technique; mixt. of B compd. and Pt complex in C6D6 was heated at 60°C for 30 min; NMR monitoring; | |
| In tetrahydrofuran-d8 byproducts: (c-C5H9)7Si7O9(OH)3; (Ar); std. Schlenk technique; mixt. of B compd. and Pt complex in THF-d8was heated at 60°C for 15 min; NMR monitoring; |
-
-
1666-13-3
diphenyl diselenide
-
-
4844-17-1
2,4,5-triphenyl-1,3-dioxoborole
-
A
-
11113-50-1
boric acid
-
B
-
84-11-7
9,10-phenanthrenequinone
| Conditions | Yield |
|---|---|
| In benzene Irradiation (UV/VIS); irrdn. for 2 h 40 min with a 450 W medium pressure mercury lamp (290 to 330 nm), under Ar; extn. (aq. NaOH), dried (Na2SO4), evapd., crystn. from hexane, yields 9,10-phenanthraquinone; | A n/a B 84% |
-
-
182482-25-3
2,4,6-trifluorophenylboronic acid
-
-
899439-56-6
Pt(C6H2F3-2,4,6)(Ph)(1,5-cyclooctadiene)
-
B
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| In water; toluene room temp., 1 h, toluene/H2O = 100/1; | A 83% B n/a |
| In toluene under inert atm. to suspn. Pt complex in toluene water and (C6H2F3-2,4,6)B(OH)2 were added and stirred at room temp. for 1 h; solvent was evapd., residue was extd. by CDCl3; product was identified by NMR; | A 83% B n/a |
| Conditions | Yield |
|---|---|
| With hydrogenchloride; formaldehyd In dichloromethane; water byproducts: H2, CH3OH; addn. of CH2Cl2, aq. soln. of CH2O and aq. HCl to suspn. of B-compd. in H2O, stirring (ambient temp., 20 min); sepn. of CH2Cl2 layer, drying (CaCl2), evapn. to dryness, sublimation (25°C, 1.3 Pa, cold surface at -70°C); | A 81% B n/a |
-
-
31139-16-9
cyanoborane
-
-
7732-18-5
water
-
A
-
74-90-8
hydrogen cyanide
-
B
-
1333-74-0
hydrogen
-
C
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| hydrolysis at 90-95°C; | A 60% B 80% C 60% |
-
-
1111-47-3
tris(triphenylsiloxy)borane
-
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| With acetic acid In benzene byproducts: triphenylacetoxysilane; reflux for 3h, molar ratio B-compd.:AcOH=1:3; H3BO3 pptd., elem. anal.; | 78% |
-
-
1259401-57-4
[Pt((c-C5H9)7Si7O10(OH)2)(C6H5)(2,2'-bipyridine)]
-
-
5720-07-0
4-methoxyphenylboronic acid
-
B
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| In tetrahydrofuran byproducts: (c-C5H9)7Si7O9(OH)3; (Ar); std. Schlenk technique; B compd. was added to soln. of Pt complex in THF; heated at 60°C for 4 h; concd. (vac.); hexane added; cooled at -20°C; filtered; washed (H2O); dried (vac.); elem. anal.; | A 75% B n/a |
-
-
20644-59-1
o-carboranylacetic acid
-
-
443770-01-2
2-aminoethyl β-D-galactopyranosyl-(1->4)-O-β-D-glucopyranoside
-
C
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| With 4-(4,6-dimethoxy[1.3.5]triazin-2-yl)-4-methylmorph In methanol; water under Ar atm. to soln. carbohydrate amine and o-carboranylacetic acid inaq. MeOH 4-(4,6-dimethoxy(1.3.5)triazin-2-yl)4-methylmorpholinium chlor ide was added and stirred at room temp. for 22 h; volatiles were removed in vacuo, residue was dissolved in H2O, reverse-phase chromy. (SepPak C18, H2O -> MeOH); | A 7.6% B 74.2% C n/a |
-
-
121-43-7
Trimethyl borate
-
-
102-24-9
cyclotriboric acid trimethyl ester
-
A
-
67-56-1
methanol
-
B
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| With water | A 72.5% B n/a |
| Conditions | Yield |
|---|---|
| In ethanol; water stirred in air for 12 h; EtOH removed in vac., extd. (hexane), filtered on SiO2, evapd., productyield dependence on H2O concn. in EtOH (40-60%); | A 48% B 68% |
-
-
98-80-6
phenylboronic acid
-
B
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| In water; toluene room temp., 1 h, toluene/H2O = 100/1; | A 66% B n/a |
| In toluene under inert atm. to suspn. Pt complex in toluene water and PhB(OH)2 wereadded and stirred at room temp. for 1 h; solvent was evapd., residue was extd. by CDCl3; product was identified by NMR; | A 66% B n/a |
| In toluene room temp., 1 h; | A 38% B n/a |
-
-
5720-07-0
4-methoxyphenylboronic acid
-
-
791838-95-4
(1,5-cyclooctadiene)Pt(C6H4-4-OMe)(C6H5)
-
C
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| In toluene room temp., 1 h; | A 64% B 14% C n/a |
-
-
99506-47-5
phenyl(m-carboran-9-yl)chloronium tetrafluoroborate
-
A
-
17819-85-1
9-chloro-m-carborane
-
B
-
54360-42-8
9-hydroxy-1,7-dicarba-closo-dodecaborane
-
C
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| With water In water stirred for 200 h, 20-40°C; extracted with benzene, evaporated to dryness, chromatographed on silica (1. benzene-hexane (1:1), 2. ether), IR; | A 8% B 56% C 33% |
| Conditions | Yield |
|---|---|
| In water under N2 or Ar; by a react. of B-contg. compd. with H2O; evapn. of water at 80°C under vac.; | 52% |
| Conditions | Yield |
|---|---|
| With H2; N2 In neat (no solvent) Electric Arc; pulse heating (plasma, puls repitition rate 5-12,5 Hz, N2 flow 0.2 - 1.65 l/min, H2 flow 1.13 - 3.5 l/min9; further products; X-ray diffraction; | A n/a B n/a C 50% D n/a E n/a |
-
-
23704-81-6
1,6-dicarba-closo-decaborane(10)
-
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| With HCl In tetrahydrofuran 25°C, 10 h, acidic hydrolysis; | 50% |
-
-
16940-66-2
sodium tetrahydroborate
-
-
109-63-7
trifluoroborane diethyl ether
-
A
-
13755-29-8
sodium tetrafluoroborate
-
B
-
17702-41-9
nido-decaborane
-
C
-
60-29-7
diethyl ether
-
D
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| With potassium permanganate; sulfuric acid In water; diethylene glycol; benzene byproducts: H2; NaBH4 in diglyme heated to 105°C and BF3*OEt2 added for 6 h and stirred for 1 h, mixt. cooled under N2 atm., water added, diglyme removed, H2SO4, benzene and KMnO4 added and react. mixt. stirred at 10°C; mixt. filtered, layers separated, benzene layer washed with water and dried over anhyd. MgSO4, evapd. and sublimed; | A n/a B 47% C n/a D n/a |
| With sulfuric acid; dihydrogen peroxide; iron(II) sulfate In hexane; water; diethylene glycol byproducts: H2; NaBH4 in diglyme heated to 105°C and BF3*OEt2 added for 6 h and stirred for 1 h, mixt. cooled under N2 atm., water added, diglyme removed, H2SO4, hexane and FeSO4, then H2O2 added and react. mixt. stirred at 35°C; mixt. filtered, layers separated, hexane layer washed with water and dried over anhyd. MgSO4; | A n/a B 44% C n/a D n/a |
| With sulfuric acid; dihydrogen peroxide In water; diethylene glycol; benzene byproducts: H2; NaBH4 in diglyme heated to 105°C and BF3*OEt2 added for 6 h and stirred for 1 h, mixt. cooled under N2 atm., water added, diglyme removed, H2SO4, benzene and then H2O2 added and react. mixt. stirred for 68 h; mixt. filtered, layers separated, benzene layer washed with water and dried over anhyd. MgSO4; | A n/a B 41.1% C n/a D n/a |
-
-
396695-62-8
closo-1,12-bis(sulfonic acid)-1,12-dicarbadodecaborane(12)
-
-
7722-84-1
dihydrogen peroxide
-
A
-
396695-66-2
closo-2,3,4,5,6,7,8,9,10,11-decahydroxy-1-sulfonic acid-1,12-dicarbadodecaborane(12)
-
C
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| In water excess of aq. 30% H2O2 added to B compd.; refluxed for 5 h; monitored by(11)B NMR spectra; concd. HBr added; stirred for 2 h at room temp.; kep t at 80°C for 8 h; Br2 removed by N2 steam; volatiles removed in vac.; triturated in MeOH; centrifuged; supernatant sepd.; repeated 5 times; residue dissolved in water; filtered; dried (mono-sulfonic acid compd.); MeOH washings evapd. slowly (bis-sulfonic acid compd.); | A 15% B 45% C n/a |
-
-
173788-87-9
2-phenoxy-4-methyl-1,3,2-dioxaborinane
-
-
98-88-4
benzoyl chloride
-
A
-
7647-01-0
hydrogenchloride
-
B
-
93-99-2
benzoic acid phenyl ester
-
C
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| In benzene byproducts: 1,3-butanediol; acylchlorid dropwise addn. to soln. of B-compd., boiling (40 min), 1 d at room temperature, aq. HCl addn.; | A n/a B 43% C n/a |
-
-
75-18-3
dimethylsulfide
-
-
1179328-70-1
[closo-1-CB9H9-1-N2]
-
A
-
201339-68-6
(CH3)2SCB9H9
-
B
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| A 40% B n/a |
-
-
182482-25-3
2,4,6-trifluorophenylboronic acid
-
-
899439-56-6
Pt(C6H2F3-2,4,6)(Ph)(1,5-cyclooctadiene)
-
-
94352-68-8
Pt(C6H2F3-2,4,6)2(cod)
-
C
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| In toluene room temp., 1 h; | A 36% B 1% C n/a |
-
-
396695-64-0
closo-1,12-bis(sulfinic acid)-1,12-dicarbadodecaborane(12)
-
-
7722-84-1
dihydrogen peroxide
-
A
-
396695-66-2
closo-2,3,4,5,6,7,8,9,10,11-decahydroxy-1-sulfonic acid-1,12-dicarbadodecaborane(12)
-
C
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| In water excess of aq. 30% H2O2 added to B compd.; refluxed for 5 h; monitored by(11)B NMR spectra; concd. HBr added; stirred for 2 h at room temp.; kep t at 80°C for 8 h; Br2 removed by N2 steam; volatiles removed in vac.; triturated in MeOH; centrifuged; supernatant sepd.; repeated 5 times; residue dissolved in water; filtered; dried (mono-sulfonic acid compd.); MeOH washings evapd. slowly (bis-sulfonic acid compd.); | A 25% B 35% C n/a |
-
-
79193-50-3
2-(1-adamantyl)-1,3,2-dioxaborinane
-
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| With water In neat (no solvent) (N2), boiled with reflux condenser for 30 min; extd. (ether); | 29% |
| With hydrogenchloride; water In diethyl ether Kinetics; byproducts: adamantane, adamantanol; (N2), C10H15B02C3H6 hydrolysed by 5% HCl (stirred at 20°C for several days); GLC; | |
| With water In diethyl ether Kinetics; byproducts: adamantane, adamantanol; (N2), soln. of C10H15B02C3H6 added to water and stirred at 20°C for several days; aq. layer removed, washed (ether); GLC; |
-
-
84633-96-5
bis-9-M-carboranylbromonium borofluoride
-
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| With water soln. of bis(9-m-carboranyl)bromonium borofluoride in water boiled for 4h; diluted with acetone, extn. with CH2Cl2, distn. in vac., addn. of etherpptn. of unreacted carborane, evapn. of aq. ext. left boric acid; | 25% |
| Conditions | Yield |
|---|---|
| With steam In neat (no solvent) heating of a mixt. of RbCl and boric acid in a stream of water-vapour at 100-150°C;; | 100% |
| With steam In neat (no solvent) heating of a mixt. of RbCl and boric acid in a stream of water-vapour at 100-150°C;; | 100% |
| With water byproducts: HCl; 100-150°C with steam; | |
| With H2O byproducts: HCl; 100-150°C with steam; |
| Conditions | Yield |
|---|---|
| In toluene boiling a mixt. of D-mannitol, H3BO3, and n-propanol in toluene on a Dean-Stark apparatus (azeotropic removal of H2O);; removal of toluene and propanol; elem. anal.;; | 100% |
-
-
90-01-7
salicylic alcohol
-
-
11113-50-1
boric acid
-
-
791-31-1
triphenylhydroxysilane
-
-
82172-56-3
2-triphenylsiloxy-4H-1,3,2-benzodioxaborin
| Conditions | Yield |
|---|---|
| In benzene byproducts: H2O; azeotropic removal of water; elem. anal.; | 100% |
-
-
11113-50-1
boric acid
-
-
120-80-9
benzene-1,2-diol
-
-
791-31-1
triphenylhydroxysilane
-
-
82172-55-2
2-triphenylsiloxy-1,3,2-benzodioxaborole
| Conditions | Yield |
|---|---|
| In benzene byproducts: H2O; azeotropic removal of water; elem. anal.; | 100% |
-
-
11113-50-1
boric acid
-
-
107-21-1
ethylene glycol
-
-
791-31-1
triphenylhydroxysilane
-
-
82172-50-7
2-triphenylsiloxy-1,3,2-dioxaborolane
| Conditions | Yield |
|---|---|
| In benzene byproducts: H2O; azeotropic removal of water; distd. in vac., elem. anal.; | 100% |
| Conditions | Yield |
|---|---|
| With lead(II) fluoride In neat (no solvent, solid phase) at 450 - 800℃; for 48h; | 100% |
| Conditions | Yield |
|---|---|
| In toluene Dean-Stark; Reflux; | 100% |
| Conditions | Yield |
|---|---|
| at 750℃; for 72h; | 100% |
| Conditions | Yield |
|---|---|
| at 750℃; for 72h; | 100% |
| Conditions | Yield |
|---|---|
| at 750℃; for 72h; | 100% |
-
-
739319-89-2
cadmium(II) carbonate
-
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| at 950℃; for 120h; | 100% |
| Conditions | Yield |
|---|---|
| for 0.166667h; Heating; | 100% |
-
-
107641-99-6
2,5-Bis(2-hydroxypropylthio)-1,3,4-thiadiazole
-
-
10213-78-2
N,N-diethanolstearylamine
-
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| for 8h; | 100% |
| Conditions | Yield |
|---|---|
| In chloroform for 66h; Reflux; | 100% |
| Conditions | Yield |
|---|---|
| at 119.84℃; for 24h; Sealed tube; | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: butanoic acid anhydride; boric acid at 90 - 120℃; for 3h; Inert atmosphere; Stage #2: C14H11F2NO4 at 115℃; for 2h; | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: rubidium carbonate; neodymium(III) oxide; boric acid; germanium dioxide at 1050℃; for 48h; Stage #2: at 950℃; | 100% |
| Conditions | Yield |
|---|---|
| at 300℃; for 3h; | 100% |
-
-
1633-05-2
strontium(II) carbonate
-
-
7664-93-9
sulfuric acid
-
-
7446-11-9
sulfur trioxide
-
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| at 180℃; for 24h; | 100% |
| Conditions | Yield |
|---|---|
| In N,N-dimethyl-formamide at 10℃; under 750.075 Torr; for 12h; Flow reactor; | 99.1% |
| Conditions | Yield |
|---|---|
| In water at 20℃; under 0 Torr; for 8h; Flow reactor; | 99.1% |
| Conditions | Yield |
|---|---|
| byproducts: H2O; B(OH)3 excess; 160°C; | 99% |
| byproducts: H2O; B(OH)3 excess; 160°C; | 99% |
-
-
11113-50-1
boric acid
-
-
107-15-3
ethylenediamine
| Conditions | Yield |
|---|---|
| In melt heating at 180°C for 3 days; | 99% |
| Conditions | Yield |
|---|---|
| With multi-walled carbon nanotubes In solid byproducts: CO, H2, H2O; mixt. of multi-walled carbon nanotubes and H3BO3 taken in quartz tube, NH3 gas passed through with 10 sccm flow rate at 200 °C 2 h, temp.slowly raised to 1000 °C for 3 h; | 99% |
| With pyrographite; iron In neat (no solvent) byproducts: CO, H2, H2O; mixt. of activated carbon, H3BO3 and ferric nitrate (mole ratio of 3:1:0.1) taken in quartz tube, dried in oven at 60 °C 6 h, NH3 gas passed through with 10 sccm flow rate, heating at 1300 °C for 4 h; | |
| byproducts: H2O; synthesis of BN coating on the surfaces of carbon nanotubes and nanofibers around 1150°C using infiltration of nanotubes with boric acid and nitridation in ammonia; |
| Conditions | Yield |
|---|---|
| In acetone mixt. of alkaloid, boric acid and 2,3-dihydroxynaphthalene (molar ratio 1:1:2) dissolved in hot acetone, warmed; evapd., noncryst. solid product; | 99% |
-
-
86119-84-8, 7664-38-2
phosphoric acid
-
-
11113-50-1
boric acid
| Conditions | Yield |
|---|---|
| In water hydrothermal synthesis (180°C, 5 d); elem. anal.; | 99% |
| Conditions | Yield |
|---|---|
| In water malic acid dissolved in H2O, treated with boric acid, aq. NaOH added, stirred in open flask at 100 °C for ca. 4 h; mixt. evapd.; detd. by NMR, XRD; | 99% |
| Conditions | Yield |
|---|---|
| In toluene byproducts: H2O; (N2); stirring of mixt. of boric acid and 6-methyl-5-hepten-3-yn-1-ol intoluene under reflux for 12 h with removal of water by a Dean-Stark tra p; evapn. of solvent by distn. (180-230°C/0.5 mmHg); | 99% |
| Conditions | Yield |
|---|---|
| In toluene phenol (excess) and acid heated for 2 h (Dean-Stark trape), volatiles removed (vac.), dissolved (THF), added dropwise to a soln. of Na compd. (THF), stirred for 1-12 h; ppt. filtered, washed (diethyl ether, pentane), dried (high vac.); elem.anal.; | 99% |
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