CAS No.7647-01-0,Hydrogen chloride Suppliers,MSDS download

: 940-71-6
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine

: 7664-39-3
hydrogen fluoride

A: 7647-01-0
hydrogenchloride

B: ammonium hexafluorophosphate

Conditions

Conditions	Yield
In not given react. with HF;;	A n/a B 100%

...Expand

: 107-06-2
1,2-dichloro-ethane

A: 7647-01-0
hydrogenchloride

B: 75-01-4
chloroethylene

Conditions

Conditions	Yield
at 450 - 550℃; under 10501.1 - 26252.6 Torr; for 0.00416667 - 0.00833333h;	A n/a B 99.52%
at 362 - 485℃; eine nahezu homogene Reaktion erster Ordnung, die wahrscheinlich von Chloratomen und 1.2-Dichlor-aethyl-Radikalen unterhalten wird.Thermolysis;
at 600℃; Conversion of starting material;
at 615℃; Rate constant;
at 650℃; Rate constant;

: magnesium chloride hydrate

: 7732-18-5
water

: 7647-01-0
hydrogenchloride

Conditions

Conditions	Yield
In neat (no solvent) dehydration at 120 - 165°C; hydrolysis at 450°C;;	99%

: 67-56-1
methanol

: 1648-30-2
2-fluorosulfonyl-2,2-difluoroacetyl chloride

A: 7647-01-0
hydrogenchloride

B: 680-15-9
2,2-difluoro-2-(fluorosulfonyl)acetate

Conditions

Conditions	Yield
In neat (no solvent)	A n/a B 99%

...Expand

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 1,3-bis(diisopropylphosphinomethylene)mesitylene

A: 7647-01-0
hydrogenchloride

: 182918-33-8
Pt(Cl)(((C3H7)2PCH2)2C6HCH2(CH3)2)

Conditions

Conditions	Yield
In tetrahydrofuran byproducts: cycloocta-1,5-diene; stirring (room temp., 12 h); filtering, concg., pptn. on pentane addn. (-30°C), drying (vac.);elem. anal.;	A n/a B 99%

...Expand

: 325744-49-8
1,1'-dicarboxylic cobalticinium chloride monohydrate

A: 7647-01-0
hydrogenchloride

B: 232598-14-0
Co(III)(η5-C5H4COOH)(η5-C5H4COO)

C: 7732-18-5
water

Conditions

Conditions	Yield
In neat (no solvent) heated at 440 K for 1 h at low pressure; XRD;	A n/a B 99% C n/a

...Expand

: 7664-93-9
sulfuric acid

: 7647-14-5
sodium chloride

A: 7647-01-0
hydrogenchloride

B: 7681-38-1
sodium hydrogen sulfate

Conditions

Conditions	Yield
In not given reaction mixture containing 28 % NaCl and 21 % SO3; reaction at 400 °C;;	A n/a B 98%
In not given reaction mixture containing 28 % NaCl and 21 % SO3; reaction at 400 °C;;	A n/a B 98%
In sulfuric acid

...Expand

: 64-17-5
ethanol

: 1648-30-2
2-fluorosulfonyl-2,2-difluoroacetyl chloride

A: 7647-01-0
hydrogenchloride

B: 756-21-8
ethyl 2,2-difluoro-2-(fluorosulfonyl)acetate

Conditions

Conditions	Yield
In neat (no solvent)	A n/a B 98%

...Expand

: 187544-74-7
(CO)2ReNH(CH3)C2H4(η(5)-C5H4)

: 931-59-9
benzenesulfenyl chloride

A: 7647-01-0
hydrogenchloride

B: 201035-45-2
[(CO)2PhSReNH(CH3)CH2CH2(η(5)-C5H4)]Cl

Conditions

Conditions	Yield
In dichloromethane Ar-atmosphere; stirring (0°C, 5 min); concg. (reduced pressure), pptn. on ether addn., washing (ether); elem. anal.;	A n/a B 98%

...Expand

: 7732-18-5
water

: 7647-14-5
sodium chloride

: 7647-01-0
hydrogenchloride

Conditions

Conditions	Yield
With clay In neat (no solvent) mixt. is treated with steam at dark-red heat;;	97%
With aluminum oxide In neat (no solvent) byproducts: Na-aluminate; passing over steam at red heat;;
byproducts: Na2O; equil. react. with steam;

: 7732-18-5
water

: 7782-50-5
chlorine

: 7647-01-0
hydrogenchloride

Conditions

Conditions	Yield
With catalyst: 20percent MgO, 25percent MgCl2, 25percent CaO; In neat (no solvent) at 900°C;; 38.65% HCl with 0.05% Cl2;;	97%
With iron(III) oxide; pyrographite In neat (no solvent)
With pyrographite In neat (no solvent) byproducts: CO2; apparatus described;;

: 1333-74-0
hydrogen

: 7782-50-5
chlorine

: 7647-01-0
hydrogenchloride

Conditions

Conditions	Yield
With catalyst:glass In neat (no solvent) combustion of Cl2 and H2 in presence of glass at 390 - 540°C;;	97%
With water In neat (no solvent) combustion of Cl2 and H2 in presence of glass at 390 - 540°C;;	97%
water In neat (no solvent) passing over a slow stream of Cl2 and H2 over quartz;;

: 14989-30-1
hypochloric acid

: 13898-47-0
hypochloric acid

A: 7647-01-0
hydrogenchloride

B: 10049-04-4, 25052-55-5
chlorine dioxide

C: 7732-18-5
water

D: 7790-93-4
chloric acid

Conditions

Conditions	Yield
In water reaction of HClO2 and HClO in weakly acidic or neutral soln. at ambient temp.;; removing of ClO2 with air;;	A n/a B 97% C n/a D n/a
In water reaction of HClO2 and HClO in aq. soln. at ambient temp.; influence of pH;;
In water reaction of HClO2 and HClO in weakly acidic or neutral soln. at ambient temp.; acceleration on low concn. of ClO2(1-); no influence of ClO3(1-);;
In water reaction of HClO2 and HClO in weakly acidic or neutral soln. at ambient temp.;;
In water Kinetics; reaction of HClO2 and HClO in aq. soln. at ambient temp.;;

...Expand

: 98773-05-8, 115958-66-2
trichlorogallium * ethanethiol

A: 7647-01-0
hydrogenchloride

B: dichloro(ethylthio)gallane

Conditions

Conditions	Yield
In neat (no solvent) decompn. at 96°C, 0.1 Torr; elem. anal.;	A n/a B 97%

: 5035-74-5
(2-chlorovinyl)dichloroborane

: 1333-74-0
hydrogen

A: 7647-01-0
hydrogenchloride

B: 1739-53-3
ethyl-dichloro-borane

Conditions

Conditions	Yield
With catalyst : Pd	A n/a B 97%
With catalyst : Pd	A n/a B 97%

...Expand

: 97-99-4
Tetrahydrofurfuryl alcohol

: 7550-45-0
titanium tetrachloride

A: 7647-01-0
hydrogenchloride

B: titanium(IV) trichloride(tetrahydrofuran-2-methanolate)

Conditions

Conditions	Yield
In hexane N2-atmosphere; alcohol dropvise addn. with stirring (pptn.); washing (n-hexane), drying (vac.); elem. anal.;	A n/a B 97%

...Expand

: Ferulic acid

: 10026-11-6
zirconium(IV) chloride

A: 7647-01-0
hydrogenchloride

B: (C7H7)2ZrCl2

Conditions

Conditions	Yield
In benzene reflux of benzene soln. of ZrCl4/C7H8 (molar ratio: 1:2) until evolution of HCl ceases; cooling to room temp.;;	A n/a B 95%

...Expand

: 1648-30-2
2-fluorosulfonyl-2,2-difluoroacetyl chloride

: 67-63-0
isopropyl alcohol

A: 7647-01-0
hydrogenchloride

B: 2927-22-2
difluoro-fluorosulfonyl-acetic acid isopropyl ester

Conditions

Conditions	Yield
In neat (no solvent)	A n/a B 95%

...Expand

: 14700-96-0, 14835-24-6, 15723-23-6, 16547-50-5, 16885-04-4, 16887-00-6, 16904-11-3, 16904-12-4, 16999-02-3, 20337-89-7, 20499-73-4, 22537-15-1, 22537-27-5, 22541-73-7, 22541-74-8, 24203-47-2, 33944-49-9, 34937-26-3, 37352-90-2
chlorine

: 7782-44-7
hydroperoxyl radical

A: 7647-01-0
hydrogenchloride

B: 80937-33-3
oxygen

Conditions

Conditions	Yield
In gaseous matrix Kinetics; Cl concn. 3E11 - 3E12 molecule/cm3, HO2 concn. 1E10 - 5E11 molecule/cm3,236 K, 1 Torr of He;	A 94.5% B n/a
In gaseous matrix Kinetics; Cl concn. 3E11 - 3E12 molecule/cm3, HO2 concn. 1E10 - 5E11 molecule/cm3,256 K, 1 Torr of He;	A 79.4% B n/a
In gaseous matrix Kinetics; Cl concn. 3E11 - 3E12 molecule/cm3, HO2 concn. 1E10 - 5E11 molecule/cm3,276 K, 1 Torr of He;	A 74.8% B n/a
In gaseous matrix Kinetics; Cl concn. 3E11 - 3E12 molecule/cm3, HO2 concn. 1E10 - 5E11 molecule/cm3,296 K, 1 Torr of He;	A 70.4% B n/a

...Expand

: 354-24-5
chlordifluoroacetyl chloride

A: 7647-01-0
hydrogenchloride

B: 354-27-8
chlorodifluoroacetyl fluoride

Conditions

Conditions	Yield
With tri-n-butylamine * 2.6 (hydrofluoride) at -30 - 50℃;	A 1.4% B 91.7%

: 7732-18-5
water

: calcium chloride

: 7647-01-0
hydrogenchloride

Conditions

Conditions	Yield
With silica gel In neat (no solvent) at 670 - 700°C;;	90%
With feldspar In neat (no solvent) heating with some more than 2 equiv. of feld spar;;	66%
With silica gel In neat (no solvent) heating with 1 equiv. SiO2;;	63.9%

: 7681-38-1
sodium hydrogen sulfate

: 7647-14-5
sodium chloride

A: 7647-01-0
hydrogenchloride

B: 7757-82-6
sodium sulfate

Conditions

Conditions	Yield
In neat (no solvent) at 200 - 450°C;;	A 90% B n/a
In sulfuric acid

...Expand

: 75-44-5
phosgene

: 108-95-2
phenol

A: 102-09-0
bis(phenyl) carbonate

B: 7647-01-0
hydrogenchloride

Conditions

Conditions	Yield
Stage #1: phenol; pyridine at 50 - 150℃; Heating / reflux; Stage #2: phosgene at 150℃;	A 89.9% B n/a

...Expand

: 1486-19-7
Bis(trifluormethyl)-monothiophosphinigsaeure

A: 7647-01-0
hydrogenchloride

B: 650-52-2
bis(trifluoromethyl)chlorophosphine

C: mercury sulfide

Conditions

Conditions	Yield
With HgCl2	A n/a B 88% C n/a

...Expand

: 10026-13-8, 874483-75-7
phosphorus pentachloride

: 14700-20-0, 2817-45-0
phosphoramidic acid

A: 7647-01-0
hydrogenchloride

B: 13966-08-0
dichlorophosphinylphosphorimidic trichloride

C: 10025-87-3, 12599-09-6, 63736-95-8
trichlorophosphate

Conditions

Conditions	Yield
In further solvent(s) heating a suspension of PO(OH)2NH2 in tetrachlorethane with PCl4 on refluxing under exclusion of H2O for 4 h;; filtration of insol. products; continous removal of HCl with stream of dry air; expelling POCl3 and solvent at 90 °C and 14 Torr; solidification in high vac. at 55-58 °C;;	A n/a B 88% C n/a
In further solvent(s) heating a suspension of PO(OH)2NH2 in tetrachlorethane with PCl4 on refluxing under exclusion of H2O for 4 h;; filtration of insol. products; continous removal of HCl with stream of dry air; expelling POCl3 and solvent at 90 °C and 14 Torr; solidification in high vac. at 55-58 °C;;	A n/a B 88% C n/a
In further solvent(s) react. with PCl5 in tetrachlorethane;;
In further solvent(s) react. with PCl5 in tetrachlorethane;;

...Expand

: 140-89-6
potassium ethyl xanthogenate

: 3172-43-8
bis(salicylidene)-4,4'-biphenylenediamine

: 68-12-2, 33513-42-7
N,N-dimethyl-formamide

: nickel dichloride

A: 7647-01-0
hydrogenchloride

B: 2Ni(2+)*OC6H4CHNC6H4C6H4NCHC6H4O(2-)*2C2H5OCS2(1-)*4HC(O)N(CH3)2=[Ni2(OC6H4CHNC12H8NCHC6H4O)(C2H5OCS2)2(HC(O)N(CH3)2)4]

C: potassium chloride

Conditions

Conditions	Yield
In N,N-dimethyl-formamide addn. of soln. of MCl2 in DMF to hot soln. of Schiff base in DMF (stirring), addn. of soln. of xanthate in water (stirring), pptn. on addn. of vater; filtration, washing (DMF), drying (over P4O10); elem. anal.;	A n/a B 87% C n/a

...Expand

: manganese(II) chloride dihydrate

: 7664-93-9
sulfuric acid

A: 7647-01-0
hydrogenchloride

: manganese hydrogen sulfate

Conditions

Conditions	Yield
at 20℃; for 1h;	A n/a B 86%

...Expand

: 871-58-9
potassium butylxanthate

: 3172-43-8
bis(salicylidene)-4,4'-biphenylenediamine

: 68-12-2, 33513-42-7
N,N-dimethyl-formamide

: 7646-79-9
cobalt(II) chloride

A: 7647-01-0
hydrogenchloride

B: 2Co(2+)*OC6H4CHNC6H4C6H4NCHC6H4O(2-)*2C4H9OCS2(1-)*4HC(O)N(CH3)2=[Co2(OC6H4CHNC12H8NCHC6H4O)(C4H9OCS2)2(HC(O)N(CH3)2)4]

C: potassium chloride

Conditions

Conditions	Yield
In N,N-dimethyl-formamide addn. of soln. of MCl2 in DMF to hot soln. of Schiff base in DMF (stirring), addn. of soln. of xanthate in water (stirring), pptn. on addn. of vater; filtration, washing (DMF), drying (over P4O10); elem. anal.;	A n/a B 85% C n/a

...Expand

: 140-89-6
potassium ethyl xanthogenate

: 3172-43-8
bis(salicylidene)-4,4'-biphenylenediamine

: 68-12-2, 33513-42-7
N,N-dimethyl-formamide

: 7646-79-9
cobalt(II) chloride

A: 7647-01-0
hydrogenchloride

B: 2Co(2+)*OC6H4CHNC6H4C6H4NCHC6H4O(2-)*2C2H5OCS2(1-)*4HC(O)N(CH3)2=[Co2(OC6H4CHNC12H8NCHC6H4O)(C2H5OCS2)2(HC(O)N(CH3)2)4]

C: potassium chloride

Conditions

Conditions	Yield
In N,N-dimethyl-formamide addn. of soln. of MCl2 in DMF to hot soln. of Schiff base in DMF (stirring), addn. of soln. of xanthate in water (stirring), pptn. on addn. of vater; filtration, washing (DMF), drying (over P4O10); elem. anal.;	A n/a B 83% C n/a

...Expand

: 7647-01-0
hydrogenchloride

: 2-(2-(4-fluoro-2-methoxyphenyl)piperazin-4-yl)-3-methyl-6-(4-pyridyl)-pyrimidin-4-one

: 2-(2-(4-fluoro-2-methoxyphenyl)piperazin-4-yl)-3-methyl-6-(4-pyridyl)-3H-pyrimidin-4-one dihydrochloride

Conditions

Conditions	Yield
In 1,4-dioxane; dichloromethane for 0.25h;	100%

: 7647-01-0
hydrogenchloride

: 478623-93-7
1,1-dimethylethyl 4,7-dihydro-1-methyl-4-[(2-propenyloxy)amino]-1H-pyrazolo[3,4-c]pyridine-6(5H)-carboxylate

: 478623-94-8
1-methyl-N-(2-propenyloxy)-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridin-4-amine hydrochloride

Conditions

Conditions	Yield
In AcOEt at 0℃; for 0.5h;	100%

: 7647-01-0
hydrogenchloride

: 849351-11-7
N-{3-amino-4-[(tetrahydro-2H-pyran-4-ylmethyl)amino]phenyl}-N-methylacetamide

: 849426-73-9
N-{3-amino-4-[(tetrahydro-2H-pyran-4-ylmethyl)amino]phenyl}-N-methylacetamide hydrochloric acid salt

Conditions

Conditions	Yield
	100%

: 7647-01-0
hydrogenchloride

: 1304-76-3
bismuth(III) oxide

: 7787-60-2
bismuth(III) chloride

Conditions

Conditions	Yield
In acetic acid byproducts: H2O;	100%
In acetic acid byproducts: H2O;	100%
In neat (no solvent) volatilization of Bi2O3 in HCl-stream at 130 °C;;	> 99
In neat (no solvent) volatilization of Bi2O3 in HCl-stream at 130 °C;;	> 99
In perchloric acid aq. HClO4; prepn. by dissolving Bi2O3 in 6 M HCl;

: 7647-01-0
hydrogenchloride

: 7732-18-5
water

: 7439-89-6
iron

: iron(II) chloride tetrahydrate

Conditions

Conditions	Yield
In water soln. of Fe in concd. HCl was refluxed; ppt. filtered off, washed with Et2O, dried in vac.;	100%
In hydrogenchloride evapn. a soln. of iron filings in dild. aq. HCl over iron filings until the hot soln. starts foaming; crystn. on cooling;; filtn.; crystn.; drying in a stream of dry air at 30-40°C;;
In hydrogenchloride evapn. a soln. of iron filings in dild. aq. HCl over iron filings until the hot soln. starts foaming; crystn. on cooling;; filtn.; crystn.; drying in a stream of dry air at 30-40°C;;
In water slight excess of 0.1 M hydrochloric acid added to iron powder, heated to dissolution; evapd.;
In hydrogenchloride iron powder and aq. HCl;

...Expand

: 7647-01-0
hydrogenchloride

: rubidium magnesium monophosphate

: rubidium chloride

Conditions

Conditions	Yield
With calcium hydroxide In water byproducts: CaCl2, alkaline earth carbonates; stirring of a soln. of RbMgPO4 in HCl (D=1.055) with Ca(OH)2 suspended in H2O;; introduction of CO2 into the filtrated soln.; separation of Mg- and Ca-carbonates; evapn. of the filtrate; impurities: small amounts of CaCl2;;	100%
With Ca(OH)2 In water

: 7647-01-0
hydrogenchloride

: 24670-32-4
Pd(PPh3)(CO)

: 28966-81-6
trans-bis(triphenylphosphine)palladium dichloride

Conditions

Conditions	Yield
In acetonitrile (CO); Pd compd. addn. to solvent with HCl, heating in autoclave (70°C, 2 h); cooling, depressurizing, ppt. filtration, washing, drying; identified byIR;	100%

: 7647-01-0
hydrogenchloride

: 219611-35-5
N(CH3)4(1+)*AuCl2(1-) = [N(CH3)4][AuCl2]

: 53514-38-8
tetramethylammonium tetrachloroaurate(III)

Conditions

Conditions	Yield
With O2; O3 In hydrogenchloride bubbling O2/O3 through a soln. of (Me4N)AuCl2 in aq. HCl (pH 2) for 30 min; filtration, washing (cold H2O); elem. anal.;	100%

: 7647-01-0
hydrogenchloride

: tungstic acid

: 7440-66-6
zinc

: 13470-13-8
tungsten(IV) chloride

Conditions

Conditions	Yield
strong HCl;	100%
strong HCl;	100%

...Expand

: 7647-01-0
hydrogenchloride

: methyl(carbonyl)bis(trimethylphosphine)iridium(I)

: 20790-91-4
cis,trans-{IrHCl2(CO)(PMe3)2}

Conditions

Conditions	Yield
In benzene-d6 bubbling HCl through soln. of Ir complex; NMR;	100%

: 7647-01-0
hydrogenchloride

: 101997-82-4
(tris(diisopropylamino)triphosphine)diiron hexacarbonyl

: 101997-84-6
(((CH3)2CH)2NP)2P(Cl)Fe2(CO)6

Conditions

Conditions	Yield
In hexane inert-atmosphere; reaction of Fe-compound with anhydrous HCl for 5 min;; filtration; solvent removed; elem. anal.;;	100%
With catalyst: acetic acid In hexane boiling in presence of catalytic amounts of acetic acid for several hours;;	>99

: 7647-01-0
hydrogenchloride

: sodium tetrasulfitodioxygenosmate

: sodium hexachloroosmate(IV)

Conditions

Conditions	Yield
Na6{OsO2(SO3)4}*5H2O is heated to red heat in a stream of dry HCl;;	100%
Na6{OsO2(SO3)4}*5H2O is heated to red heat in a stream of dry HCl;;	100%

: 7647-01-0
hydrogenchloride

: 123591-18-4
CF3NGeHON(CF3)2

A: 123591-20-8
F3CNGeHCl

B: 359-63-7
N,N-bis(trifluoromethyl)hydroxylamine

Conditions

Conditions	Yield
Elem. anal.;	A 53% B 100%

...Expand

: 7647-01-0
hydrogenchloride

: 123591-19-5
CF3NGe(ON(CF3)2)2

A: 123591-21-9
F3CNGeCl2

B: 359-63-7
N,N-bis(trifluoromethyl)hydroxylamine

Conditions

Conditions	Yield
Elem. anal.;	A 57% B 100%

...Expand

: 7647-01-0
hydrogenchloride

: 56848-21-6
{PtF5Cl}(2-)

: 137636-15-8, 56848-18-1
trans-{PtF4Cl2}(2-)

Conditions

Conditions	Yield
In dichloromethane HCl-gas is bubbled through a soln. of educt in dichlormethane at -30°C;	100%

: 7647-01-0
hydrogenchloride

: bis(indenyl)zirconium dimethyl

: 12148-49-1
bis(indenyl)zirconium(IV) dichloride

Conditions

Conditions	Yield
In diethyl ether; di-isopropyl ether; toluene (N2); a soln. of HCl in Et2O added to a soln. of Zr complex in toluene and iPr2O, stirred at room temp. for 2 h, evapd. (vac.), treated with ether, toluene and a soln. of HCl in Et2O, stirred for 2 h; evapd. (vac.);	100%
In diethyl ether byproducts: CH4; (N2); Zr complex dissolved in Et2O, a soln. of HCl/Et2O added at room temp., stirred for 2 h, stirred for 5 h, addnl. HCl in Et2O added; evapd. (vac.);	96%

: 7647-01-0
hydrogenchloride

: (biphenyl-2,2'-diyl)zirconocene

: 1291-32-3
zirconocene dichloride

Conditions

Conditions	Yield
In diethyl ether Zr-complex dissolved in HCl in Et2O; evapd., residue triturated with hexane, recrystd. from THF;	100%

: 7647-01-0
hydrogenchloride

: 233257-02-8
[(trifluoroacetyl)imino]tris-(2-methylphenyl)-λ(5)-bismuthane

: 6729-60-8
tris(2-methylphenyl)bismuth dichloride

Conditions

Conditions	Yield
In dichloromethane aq. HCl, 1 h;	100%
In dichloromethane; water under Ar; to a CH2Cl2 soln. of the bismuthane was added aq. HCl, the mixt. was vigorously stirred at 25°C for 1 h; the org. layer was sepd. and the aq. phase was extd. with CH2Cl2, the org. layers were dried over MdSO4, concd. under vac., the oily residue wasrecrystd. from hexane/CH2Cl2;	100%

: 7647-01-0
hydrogenchloride

: 2,3-bis(acetonitrile)-1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-μ-hydrido-triangulo-triosmium tricarbonyltrichloro-osmate(1-)

: [Os3(CO)10(μ-H)(μ-Cl)]

Conditions

Conditions	Yield
In hexane HCl bubbled through claster soln., refluxed for 4 h; solvent removed under N2, recrystd. (CH2Cl2/hexane);	100%

: 7647-01-0
hydrogenchloride

: 98499-51-5
nitridophthalocyaninato(2-)rhenium(V)

: 67-64-1
acetone

: Re(phthalocyaninato)(OH)(NC6H11O)

Conditions

Conditions	Yield
In acetone stirring (room temp., several days);	100%

...Expand

: 7647-01-0
hydrogenchloride

: bis[tris(trimethylsilyl)germyl]zinc

: 104164-54-7
tris(trimethylsilyl)germane

Conditions

Conditions	Yield
In diethyl ether; water Et2O soln. of ((Me3Si)3Ge)2Zn, excess amt. of concd. HCl, and nonadecaneas internal std. stirred in Schlenk tube under Ar at room temp. for 2 h; products identified by GC, GC-MS, and NMR;	100%

: 7647-01-0
hydrogenchloride

: (207)Pb(2+)*CO3(2-)=(207)PbCO3

: (207)lead dichloride

Conditions

Conditions	Yield
In water byproducts: CO2; N2 atmosphere, addn. of aq. HCl to (207)PbCO3, stirring (20°C, 10min); removement of solvent (reduced pressure), drying (100°C, 4 h); 92.8% (207)Pb-enrichment;	100%

: 7647-01-0
hydrogenchloride

: 2816-39-9
hexaphenyldigermane

: 32284-98-3
1,1,2,2-tetrachlorodiphenyldigermane

Conditions

Conditions	Yield
In neat (no solvent) High Pressure; pressure react. of dry HCl and Ph6Ge2 in autoclave (molar ratio HCl/Ph6Ge2 = 44.0), room temp., initial pressure 47 atm, 8h; rinsing react. mixt. with pentane into retort; evapn.; addn. of pentane; cooling to -15°C; crystn. overnight; filtration; recrystn. (petroleum ether); elem. anal.;	100%

: 7647-01-0
hydrogenchloride

: 10466-65-6
potassium perrhenate

: cesium chloride

A: dipotassium oxopentachlororhenate(5+)

B: 2Cs(1+)*{ReOCl5}(2-)=Cs2{ReOCl5}

Conditions

Conditions	Yield
With hydroquinone In acetic anhydride; acetic acid under N2 at room temp.; passing HCl gas through soln. of KReO4 in acetic acid and (Ac)2O till clear soln. (rhenate), mixed with hydroquinone inacetic acid, pptn. of KReOCl5, to mother liquor addn. of CsCl in AcOH contg. (Ac)2O, pptn.; filtered, washed (acetic acid), kept in vacuo for 5 h;	A 100% B 99%

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: 91-22-5
quinoline

: 7647-01-0
hydrogenchloride

: 10466-65-6
potassium perrhenate

A: dipotassium oxopentachlororhenate(5+)

B: 2C9H7NH(1+)*ReOCl5(2-)=(C9H7NH)2(ReOCl5)

Conditions

Conditions	Yield
With hydroquinone In acetic anhydride; acetic acid under N2 at room temp.; passing HCl gas through soln. of KReO4 in acetic acid and acetic anhydride till clear soln. (rhenate), mixed with hydroquinone in acetic acid, pptn. of KReOCl5, to mother liquor addn. of quinoline in AcOH contg. (Ac)2O, pptn.; filtered, washed (acetic acid), kept in vacuo for 5 h; elem. anal.;	A 100% B 94%

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: 7647-01-0
hydrogenchloride

: 207984-93-8
per-rhenic acid

: 2001-45-8
tetraphenyl phosphonium chloride

: 57437-75-9
(C6H5)4P(1+)*ReOCl5(1-)=(C6H5)4P[ReOCl5]

Conditions

Conditions	Yield
In hydrogenchloride; sulfuric acid aq. H2SO4; molar ratio Re:Ph4PCl=1:1; addn. of concd. HCl to mixt. of HReO4, Ph4PCl, concd. H2SO4 and concd. HCl (pptn.); extn. (CHCl3), crystn. (1-2 h), washing (CHCl3), drying (vac., over NaOH); elem. anal.;	100%

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: 7647-01-0
hydrogenchloride

: 10466-65-6
potassium perrhenate

: rubidium chloride

A: dipotassium oxopentachlororhenate(5+)

B: rubidium oxopentachlororhenate(V)

Conditions

Conditions	Yield
With hydroquinone In acetic anhydride; acetic acid under N2 at room temp.; passing HCl gas through soln. of KReO4 in acetic acid and (Ac)2O till clear soln. (rhenate), mixed with hydroquinone inacetic acid, pptn. of KReOCl5, to mother liquor addn. of RbCl in AcOH contg. (Ac)2O, pptn.; filtered, washed (acetic acid), kept in vacuo for 5 h;	A 100% B 98%

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: 7647-01-0
hydrogenchloride

: 79-37-8
oxalyl dichloride

: (5,7,12,14-tetramethyldibenzo[b,i][1,4,8,11]tetraazacyclotetradecinate(2-))V=O

: 79820-76-1
[(5,7,12,14-tetramethyldibenzo[b,i][1,4,8,11]tetraazacyclotetradecinate(1-))VCl2]Cl

Conditions

Conditions	Yield
In 1,2-dichloro-ethane (Ar); react. (5-10 min, pptn.);	100%

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: 7647-01-0
hydrogenchloride

: 66-71-7
1,10-Phenanthroline

: 10466-65-6
potassium perrhenate

A: dipotassium oxopentachlororhenate(5+)

B: 17428-51-2
o-phenanthrolinium oxopentachlororhenate(V)

Conditions

Conditions	Yield
With hydroquinone In acetic anhydride; acetic acid under N2 at room temp.; passing HCl gas through soln. of KReO4 in acetic acid and (Ac)2O till clear soln. (rhenate), mixed with hydroquinone inacetic acid, pptn. of KReOCl5, to mother liquor addn. of phenanthrolinen AcOH contg. (Ac)2O, pptn.; filtered, washed (acetic acid), kept in vacuo for 5 h; elem. anal.;	A 100% B 100%

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