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Cas:66-71-7
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Items Standard Result Appearance White crystalline powder Confirm Assay 99%min
Cas:66-71-7
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inquiryProduct Name: o-Phenanthroline Synonyms: O-PHENANTHROLINE;ORTHOPHENANTHROLINE;1,10-Fenanthrolin;1,10-o-Phenanthroline;4,5-Diazaphenanthrene;4,5-Phenanthroline;Activ-8 in hexylene g
Hebei yanxi chemical co., LTD is a professional research, development and production 2-phenylacetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carbon environ
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inquiryHigh quality o-Phenanthroline CAS 66-71-7 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additive
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inquiryhigh quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:66-71-7
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inquiryProduct Name: o-Phenanthroline Synonyms: O-PHENANTHROLINE;ORTHOPHENANTHROLINE;1,10-Fenanthrolin;1,10-o-Phenanthroline;4,5-Diazaphenanthrene;4,5-Phenanthroline;Activ-8 in hexylene glycol;beta-Phenanthroline CAS: 66-71-7
Cas:66-71-7
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
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Cas:66-71-7
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inquiryo-Phenanthroline CAS: 66-71-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Cas:66-71-7
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:66-71-7
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inquiry1,10-Phenanthroline CAS: 66-71-7 Specification Items Technical index Product name 1,10-Phenanthroline anhydrate Synonym o-Phenanthroline CAS No
Cas:66-71-7
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryProName: 1,10-Phenanthroline Manufacturer/High ... CasNo: 66-71-7 Molecular Formula: C12H8N2 Appearance: detailed see specifications Application: It is an important raw material and in... DeliveryTime: prompt PackAge: according to the clients
Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquiry{(C12H8N2)((C6H5)3P)Cu(O2CC5H7N2)(H2O)}
A
1,10-Phenanthroline
Conditions | Yield |
---|---|
In acetone byproducts: CO2, H2O, PPh3; N2 bubbled through an acetone suspn. of the Cu-complex (0°C), low ratio Cu complex : acetone; | A n/a B 91% |
In solid byproducts: CO2, H2O, PPh3; maintained at 120°C under vac. (1E-2 Torr); |
Conditions | Yield |
---|---|
With copper(I) oxide; dmap; N-hydroxyphthalimide; oxygen In acetonitrile at 120℃; for 12h; Sealed tube; | 80% |
With potassium tert-butylate In o-xylene at 140℃; for 36h; Inert atmosphere; | 15% |
With platinum; oxygen In methanol at 40℃; under 750.075 Torr; Schlenk technique; Sealed tube; | 100 %Chromat. |
With tert.-butylhydroperoxide In water at 20℃; for 18h; Sealed tube; | 78 %Spectr. |
A
1,10-Phenanthroline
B
{Ru(1,10-phenanthroline)3}(NO3)2*2H2O
Conditions | Yield |
---|---|
With NaNO3 In methanol byproducts: AgCl; heated to reflux for 15 min; cooled, filtered, concd., addn. of an aq. soln. of NaNO3, pptn. filtered off, washed with diethyl ether, recrystn. (water or water-methanol 9:1); elem. anal.; | A n/a B 75% |
{Ag(1,10-phenanthroline)2}ClO4
A
1,10-Phenanthroline
Conditions | Yield |
---|---|
In methanol byproducts: AgCl; heated to reflux for 15 min; cooled, filtered, concd., addn. of an aq. soln. of NaClO4, pptn. filtered off, washed with diethyl ether, recrystn. (water or water-methanol 9:1); elem. anal.; | A n/a B 75% |
(Z)-1,2-di(2-bromopyridin-3-yl)ethene
1,10-Phenanthroline
Conditions | Yield |
---|---|
With copper In N,N-dimethyl-formamide for 5h; Ullmann coupling; Heating; | 67% |
5,6-epoxy-5,6-dihydro-[1,10]phenanthroline
1,10-Phenanthroline
Conditions | Yield |
---|---|
With 2,4,6-trimereaptotriazine, trisodium salt, nonahydrate In ethanol | 65% |
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 8h; Sealed tube; Reflux; | 64% |
A
1,10-Phenanthroline
B
{Ru(1,10-phenanthroline)3}(NO3)2*2H2O
Conditions | Yield |
---|---|
With NaNO3 In methanol byproducts: AgCl; heated to reflux for 30 min; cooled, filtered, concd., addn. of an aq. soln. of NaNO3, pptn. filtered off, washed with diethyl ether, recrystn. (water or water-methanol 9:1); elem. anal.; | A n/a B 55% |
{Ag(1,10-phenanthroline)2}ClO4
A
1,10-Phenanthroline
Conditions | Yield |
---|---|
In methanol byproducts: AgCl; heated to reflux for 30 min; cooled, filtered, concd., addn. of an aq. soln. of NaClO4, pptn. filtered off, washed with diethyl ether, recrystn. (water or water-methanol 9:1); elem. anal.; | A n/a B 55% |
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol at 80℃; for 8h; Schlenk technique; | 47% |
3-acetylpentane-2,4-dione
8-amino-7-quinolinecarbaldehyde
A
1,10-Phenanthroline
B
2-methyl-1,10-phenanthroline
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 8h; Friedlaender reaction; Heating; | A 33% B 39% |
Conditions | Yield |
---|---|
With sulfuric acid; nitrobenzene | |
With sulfuric acid; orthoarsenic acid |
Conditions | Yield |
---|---|
With sulfuric acid; orthoarsenic acid; glycerol | |
With sulfuric acid; orthoarsenic acid; glycerol Reagens 4: HgCl2; |
1-methyl-1,10-phenanthrolinium iodide
1,10-Phenanthroline
Conditions | Yield |
---|---|
With sulfolane; triphenylphosphine at 151℃; Rate constant; |
n-Propyl-Radikal
A
1,10-Phenanthroline
B
propene
C
n-propylacetamide
D
4-propyl-[1,10]phenanthroline
Conditions | Yield |
---|---|
With tris(1,10-phenanthroline)iron(III) tris(hexafluorophosphate) In acetonitrile at 25℃; Rate constant; competition with BrCCL3, other complexes; |
n-propyltrimethyltin
acetonitrile
A
1,10-Phenanthroline
B
propene
C
n-propylacetamide
D
4-propyl-[1,10]phenanthroline
Conditions | Yield |
---|---|
With sodium hydroxide 1.) 22 deg C; Yield given. Multistep reaction. Yields of byproduct given; |
Isopropyl-trimethyl-stannane
acetonitrile
A
1,10-Phenanthroline
B
propene
C
N-isopropylacetamide
D
4-isopropyl-1,10-phenanthroline
Conditions | Yield |
---|---|
With sodium hydroxide 1.) 22 deg C; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
In water Rate constant; Equilibrium constant; Irradiation; HClO4, H2KPO4, Na2HPO4, Na2B2O7, NaOH, t-BuOH; |
Conditions | Yield |
---|---|
In water Rate constant; Equilibrium constant; Irradiation; HClO4, H2KPO4, Na2HPO4, Na2B2O7, NaOH, t-BuOH; |
n-propyltrimethyltin
A
1,10-Phenanthroline
B
propene
C
n-propylacetamide
D
4-propyl-[1,10]phenanthroline
Conditions | Yield |
---|---|
With sodium hydroxide 1.) acetonitrile, 22 deg C; Yield given. Multistep reaction. Yields of byproduct given; |
n-propyltrimethyltin
A
1,10-Phenanthroline
B
propene
C
n-propylacetamide
D
4-propyl-[1,10]phenanthroline
Conditions | Yield |
---|---|
With sodium hydroxide 1.) acetonitrile, 25 deg C; Yield given. Multistep reaction. Yields of byproduct given; |
n-propyltrimethyltin
A
1,10-Phenanthroline
B
propene
C
n-propylacetamide
D
4-propyl-[1,10]phenanthroline
Conditions | Yield |
---|---|
With sodium hydroxide 1.) acetonitrile, 25 deg C; Yield given. Multistep reaction. Yields of byproduct given; |
tetramethylstannane
A
1,10-Phenanthroline
B
4-methyl-1,10-phenanthroline
Conditions | Yield |
---|---|
With sodium hydroxide 1.) acetonitrile, 70 deg C, 2 h; Yield given. Multistep reaction; |
Ethyltrimethylstannan
A
4-ethyl-[1,10]phenanthroline
B
1,10-Phenanthroline
C
4-methyl-1,10-phenanthroline
D
N-ethylacetamide
Conditions | Yield |
---|---|
With sodium hydroxide 1.) acetonitrile, 22 deg C; Yield given. Multistep reaction. Yields of byproduct given; |
Ethyltrimethylstannan
acetonitrile
A
4-ethyl-[1,10]phenanthroline
B
1,10-Phenanthroline
C
4-methyl-1,10-phenanthroline
D
N-ethylacetamide
Conditions | Yield |
---|---|
With sodium hydroxide 1.) 22 deg C; Yield given. Multistep reaction. Yields of byproduct given; |
Isopropyl-trimethyl-stannane
A
1,10-Phenanthroline
B
propene
C
N-isopropylacetamide
D
4-isopropyl-1,10-phenanthroline
Conditions | Yield |
---|---|
With sodium hydroxide 1.) acetonitrile, 22 deg C; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
at 21.85℃; Equilibrium constant; |
Conditions | Yield |
---|---|
In ethanol; dichloromethane |
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid at 160℃; for 3h; | 100% |
With sulfuric acid; nitric acid at 160℃; | 99% |
With sulfuric acid; nitric acid at 160℃; for 3h; | 99% |
1,10-Phenanthroline
1,10-phenanthroline-5,6-dione
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid; sodium bromide at 90℃; for 2h; | 100% |
With sulfuric acid; nitric acid; potassium bromide at 130℃; for 3h; | 98.1% |
With sulfuric acid; nitric acid; potassium bromide at 95℃; for 3h; Cooling with ice; Sealed tube; Schlenk technique; | 97% |
1,10-Phenanthroline
1,3-dibromo-propane
6,7-dihydro-5H-[1,4]diazepino[1,2,3,4-l,m,n][1,10]phenanthroline-4,8-diium dibromide
Conditions | Yield |
---|---|
In chlorobenzene at 70 - 120℃; | 100% |
In nitrobenzene at 120℃; | 100% |
for 12h; Reflux; | 99% |
1,10-Phenanthroline
(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonylmolybdenum(0)
A
(1,10-phenanthroline)molybdenum tetracarbonyl
B
bicyclo[2.2.1]hepta-2,5-diene
Conditions | Yield |
---|---|
In tetrahydrofuran reaction in a calorimeter under argon; | A 100% B n/a |
hydrogenchloride
1,10-Phenanthroline
potassium perrhenate
B
o-phenanthrolinium oxopentachlororhenate(V)
Conditions | Yield |
---|---|
With hydroquinone In acetic anhydride; acetic acid under N2 at room temp.; passing HCl gas through soln. of KReO4 in acetic acid and (Ac)2O till clear soln. (rhenate), mixed with hydroquinone inacetic acid, pptn. of KReOCl5, to mother liquor addn. of phenanthrolinen AcOH contg. (Ac)2O, pptn.; filtered, washed (acetic acid), kept in vacuo for 5 h; elem. anal.; | A 100% B 100% |
1,10-Phenanthroline
potassium perrhenate
o-phenanthrolinium oxopentachlororhenate(V)
Conditions | Yield |
---|---|
With hydroquinone In hydrogenchloride under N2 at room temp.; KReO4 suspended in concd. HCl, shaken, addn. ofhydroquinone in concd. HCl, yellow soln. obtained, addn. of phenanthroline, pptn.; filtered, washed (acetic acid), kept in vacuo for 5 h; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran (Ar); stirring (5 h); washing (hexane), drying (vac.); elem. anal.; | 100% |
1,10-Phenanthroline
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
chloro(p-cymene)(η2-1,10-phenanthroline-κ2N)ruthenium
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 3h; Inert atmosphere; Schlenk technique; | 100% |
In dichloromethane inert atm.; 2 equiv of phenanthroline was added to a suspn. of complex in CH2Cl2, the mixt. was stirred for 3 h at room temp.; evapd. to dryness, dissolved in water, filtered, evapd. to dryness; elem. anal.; | 99% |
In dichloromethane at 20℃; for 0.5h; | 51% |
1,10-Phenanthroline
Conditions | Yield |
---|---|
In toluene Ar atm.; stirring; concn., addn. of hexane, crystn. (-30°C, overnight), filtn., drying (vac., 40°C); | 100% |
1,10-Phenanthroline
tetrakis(actonitrile)copper(I) hexafluorophosphate
2,9-bis(2,6-dimethoxyphenyl)-3-ethynyl-[1,10]-phenanthroline
Cu(C12H6N2(C6H3(OCH3)2)2)(C12H8N2)(1+)*PF6(1-)=CuC40H32N4O4PF6
Conditions | Yield |
---|---|
In [D3]acetonitrile | 100% |
1,10-Phenanthroline
niobium pentafluoride
trimethylsilylazide
[Nb(N3)4(1,10-phen)2][Nb(N3)6]
Conditions | Yield |
---|---|
In acetonitrile at -196 - 20℃; for 6h; | 100% |
1,10-Phenanthroline
tantalum pentafluoride
trimethylsilylazide
[Ta(N3)4(1,10-phen)2][Ta(N3)6]
Conditions | Yield |
---|---|
In acetonitrile at -196 - 20℃; for 6h; | 100% |
1,10-Phenanthroline
tetrakis(actonitrile)copper(I) hexafluorophosphate
Conditions | Yield |
---|---|
In dichloromethane-d2 | 100% |
1,10-Phenanthroline
2-(6-(2,4,6-trimethylphenyl)pyridin-2-yl)-9-(2,4,6-trimethylphenyl)[1,10]phenanthroline
zinc trifluoromethanesulfonate
Conditions | Yield |
---|---|
In dichloromethane-d2; [D3]acetonitrile | 100% |
1,10-Phenanthroline
2-(6-(2,4,6-trimethylphenyl)pyridin-2-yl)-9-(2,4,6-trimethylphenyl)[1,10]phenanthroline
Conditions | Yield |
---|---|
In dichloromethane-d2; [D3]acetonitrile | 100% |
bromobenzene
1,10-Phenanthroline
6,7-dihydro-5H-[1,4]diazepino[1,2,3,4-lmn][1,10]phenanthroline-4,8-diium
Conditions | Yield |
---|---|
at 115℃; for 4h; | 100% |
1,10-Phenanthroline
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 30h; Inert atmosphere; Schlenk technique; | 100% |
1,10-Phenanthroline
Conditions | Yield |
---|---|
In dichloromethane for 30h; Inert atmosphere; Schlenk technique; | 100% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; | 100% |
1,10-Phenanthroline
1,1,1,3,3,3-hexafluoro-2-phenylisopropyl alcohol
C30H37N3W
Conditions | Yield |
---|---|
Stage #1: 1,1,1,3,3,3-hexafluoro-2-phenylisopropyl alcohol; C30H37N3W In benzene at 20℃; for 0.5h; Stage #2: 1,10-Phenanthroline In benzene at 20℃; for 1h; | 100% |
1,10-Phenanthroline
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide for 0.0833333h; | 100% |
Conditions | Yield |
---|---|
In acetonitrile at -196 - 20℃; for 16h; | 100% |
1,10-Phenanthroline
tris(p-trifluoromethylphenyl)phosphine gold bis(trifluoromethanesulfonyl)imidate
Conditions | Yield |
---|---|
In dichloromethane Inert atmosphere; | 100% |
1,10-Phenanthroline
Conditions | Yield |
---|---|
In dichloromethane Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In dichloromethane Inert atmosphere; | 100% |
1,10-Phenanthroline
[(Cy3P)Au]N(trifluoromethylsulfonyl)2
Conditions | Yield |
---|---|
In dichloromethane Inert atmosphere; | 100% |
1,10-Phenanthroline
(p-tolyl)3PAuN(trifluoromethanesulfonyl)2
Conditions | Yield |
---|---|
In dichloromethane Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In dichloromethane Inert atmosphere; | 100% |
1,10-Phenanthroline
[bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I)
Conditions | Yield |
---|---|
In dichloromethane Inert atmosphere; | 100% |
1,10-Phenanthroline
A
tris(1,10-phenanthroline)iron(II) triflate
Conditions | Yield |
---|---|
In [D3]acetonitrile | A 100% B n/a |
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