DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryHigh purity Dichloro(p-cymene)ruthenium(II) dimer CAS 52462-29-0 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed addi
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inquiryProduct Name: Dichloro(p-cymene)ruthenium(II) dimer Synonyms: Di-μ-chlorobis(p-cymene)chlororuthenium(II),98%;Dichloro(p-cymene)ruthenium(II) dimmer,98%;Dichloro(p-cymene)ruthenium dimer;Dichloro(p-cymene)ruthenium(II) dimer ,98% [33% Ru];Di
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inquiryProduct name Dichloro(p-cymene)ruthenium(II) dimer Content ≥98% CAS NO. 52462-29-0 Package Structure Formula Appear
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiry(R)-5-isopropyl-2-methylcyclohexa-1,3-diene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In methanol at 140℃; for 0.166667h; Microwave irradiation; | 100% |
In ethanol at 130℃; for 0.0666667h; Microwave irradiation; | 83% |
In ethanol for 24h; Reflux; | 76% |
4-methylisopropylbenzene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In 2-methoxy-ethanol; water at 120℃; for 4h; Product distribution / selectivity; | 98% |
p-mentha-1,5-diene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol for 17h; Schlenk technique; Reflux; Inert atmosphere; | 98% |
In ethanol for 4h; Reflux; Inert atmosphere; | 78% |
In methanol Inert atmosphere; Schlenk technique; Heating; | |
In ethanol for 12h; Reflux; Inert atmosphere; |
p-mentha-1,5-diene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol for 8h; Reflux; | 96% |
In methanol for 4h; Schlenk technique; Inert atmosphere; Reflux; | 85% |
4-methylisopropylbenzene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
for 15h; Inert atmosphere; Reflux; | 94% |
In butan-1-ol at 80℃; for 6h; Solvent; Temperature; | 94% |
In ethanol Reflux; |
ruthenium(III) chloride hydrate
crithmene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol RuCl3*H2O is refluxed in EtOH in presence of the cyclohexadiene under N2 (4 h); ppt. is filtered, a second crop of ppt. is obtained by reducing the filtrate and cooling (-10°C); | 90% |
4-methylisopropylbenzene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol for 24h; Solvent; Inert atmosphere; Reflux; | 90% |
In ethanol for 24h; Reflux; Inert atmosphere; | 90% |
1-methyl-4-isopropyl-1,3-cyclohexadiene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In methanol at 140℃; for 0.00833333h; Inert atmosphere; Microwave irradiation; | 86% |
In methanol Schlenk technique; Inert atmosphere; Reflux; | |
In ethanol at 20℃; for 15h; Schlenk technique; |
ruthenium(III) chloride hydrate
1-methyl-4-isopropyl-1,3-cyclohexadiene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol refluxing for 4 h; crystn. on cooling, filtration, washing (cold MeOH), drying (vac.); second crop on crystn. of filtrate after evapn.; elem. anal.; | 77% |
p-mentha-1,5-diene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol for 4h; Sonication; Reflux; | 76% |
In ethanol at 79℃; for 4h; Heating / reflux; | 35% |
Inert atmosphere; Schlenk technique; | |
Inert atmosphere; Schlenk technique; |
p-mentha-1,5-diene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol in a modified reflux microwave apparatus RuCl3 reacts with α-phellandrene in EtOH (react. time: 10 min); | 67% |
p-mentha-1,5-diene
ruthenium(III)chloride
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol other Radiation; to EtOH added RuCl3 and excess p-mentha-1,5-diene; soln. refluxed under microwave irradiation for 15 min; after cooling to room temp. solvent removed under vac.; residue washed with ether, complex collected by filteration, washed withether and dried; elem. anal.; | 65% |
RuCl3 treated with α-phellandrene in according with early published method (M.A. Bennet, G.B. Robertson, A.K. Smith, J. Organomet. Chem. 43 (1972) C41); |
(R)-5-isopropyl-2-methylcyclohexa-1,3-diene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
Stage #1: ruthenium trichloride In ethanol for 8h; Reflux; Stage #2: (R)-5-isopropyl-2-methylcyclohexa-1,3-diene In ethanol at 20℃; for 12h; | 65% |
p-mentha-1,5-diene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol reflux overnight, under N2; ppt. was filtered off, washed with MeOH, dried in vac.; | 63.5% |
p-mentha-1,5-diene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol for 24h; Schlenk technique; Reflux; | 62% |
p-mentha-1,5-diene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
With ruthenium(III) trichloride hydrate In ethanol for 4h; Reflux; Inert atmosphere; | 11% |
1-methyl-4-isopropyl-1,3-cyclohexadiene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In not given according to: S. B. Jensen, S. J. Rodger, M. D. Spicer, J. Organomet. Chem. 556 (1998) 151; |
chloride
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In tetrahydrofuran Electrochem. Process; electrochemically generated Ru-complex-ion (voltammetric step), Ar atmosphere, supporting electrolyte 0.2 M Bu4NPF6; not isolated; voltammetric monitoring; |
A
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
B
{CH3NC4H3(CH3)4}(1+)
Conditions | Yield |
---|---|
With HCl In dichloromethane under N2, standard Schlenk techniques; degassing a soln. of Ru-compd.in CH2Cl2 via three freeze/pump/thaw cycles, addn. of 1.6 equiv. HCl and stirring for 9 h; in air; evapn. of solvent, NMR; |
[(RuCl2(p-cymene))2(μ-1,2-bis(ethylsulfinyl)ethane)]
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In chloroform-d1 byproducts: EtS(O)C2H4S(O)Et; Ru complex was dissolved in CDCl3; NMR monitoring; |
A
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In dichloromethane-d2 equil. in soln.; not isolated, detected by NMR; |
[(RuCl2(p-cymene))2(μ-1,3-bis(ethylsulfinyl)propane)]
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In chloroform-d1 byproducts: EtS(O)C2H4S(O)Et; Ru complex was dissolved in CDCl3; NMR monitoring; |
[RuCl2(p-cymene)(SOCCN(Mes)CH=CHN(Mes))]
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In dichloromethane-d2 byproducts: SOCCN(Mes)CH=CHN(Mes); (N2); std. Schlenk technique; soln. of Ru complex in CD2Cl2 was heated at 40°C for few h; NMR monitoring; |
1-methyl-4-isopropyl-1,3-cyclohexadiene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol for 6h; Reflux; | |
In ethanol for 6h; Reflux; | |
In ethanol for 6h; Reflux; |
crithmene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol for 6h; Reflux; | |
In ethanol for 6h; Reflux; | |
In ethanol for 6h; Reflux; |
crithmene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol for 6h; Concentration; Reflux; |
(R)-5-isopropyl-2-methylcyclohexa-1,3-diene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In methanol for 5h; Reflux; Inert atmosphere; Schlenk technique; | |
In methanol Inert atmosphere; |
1-methyl-4-isopropyl-1,3-cyclohexadiene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
at 50℃; for 0.5h; Microwave irradiation; | |
In methanol Reflux; |
crithmene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol at 80 - 85℃; for 12h; | 1.85 g |
In ethanol at 80℃; for 24h; Inert atmosphere; |
p-mentha-1,5-diene
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol at 90 - 130℃; | |
In ethanol Inert atmosphere; Reflux; |
1,2-bis(2,5-diphenylphospholano)methane
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In ethanol; dichloromethane at 70℃; for 2h; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
sodium acetylacetonate
Conditions | Yield |
---|---|
In acetone for 0.666667h; Inert atmosphere; Schlenk technique; | 100% |
In acetone at 20℃; for 0.833333h; | 59% |
(+)-(R)-2,2'bis(di-para-tolylphosphanyl)-1,1'binaphthyl
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
diethyl amine hydrochloride
Conditions | Yield |
---|---|
In toluene (Ar); heating a soln. of ruthenium complex with ammonium salt and phosphine in toluene at 50°C for 2 h with stirring, refluxing for 12 hwith stirring; cooling, evapn.; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Hg(C6H2-2,3-(OCH2O)-6-CH2NMe2)2
[(η(6)-1-Me-4-(i)Pr-C6H4)Ru(C6H3-2,3-(OCH2O)-6-CH2NMe2)Cl]
Conditions | Yield |
---|---|
In dichloromethane byproducts: HgCl2; N2-atmosphere; stirring equimolar amts. at room temp. for 3 d; filtration off of HgCl2, concn., pptn. on Et2O addn.; elem. anal.; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
[η5-C5H4(CH2)2PPh2]Ti(O(i)Pr)3
Conditions | Yield |
---|---|
In dichloromethane (Ar); stirring a mixt. of ruthenium and titanium complexes in CH2Cl2 for4 h at room temp.; evapn., washing with pentane; elem. anal.; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
[η5-C5H4(CH2)2PCy2]Ti(O(i)Pr)3
Conditions | Yield |
---|---|
In dichloromethane (Ar); stirring a mixt. of ruthenium and titanium complexes in CH2Cl2 for4 h at room temp.; evapn., washing with pentane; elem. anal.; | 100% |
1,10-Phenanthroline
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
chloro(p-cymene)(η2-1,10-phenanthroline-κ2N)ruthenium
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 3h; Inert atmosphere; Schlenk technique; | 100% |
In dichloromethane inert atm.; 2 equiv of phenanthroline was added to a suspn. of complex in CH2Cl2, the mixt. was stirred for 3 h at room temp.; evapd. to dryness, dissolved in water, filtered, evapd. to dryness; elem. anal.; | 99% |
In methanol for 1h; | 84% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
dichloromethane
Conditions | Yield |
---|---|
In dichloromethane (under N2, Schlenk); soln. of Ru-complex in CH2Cl2 added dropwise to soln. of ligand in CH2Cl2, stirred for 1 h; concd., hexane added; elem. anal.; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In dichloromethane (under N2, Schlenk); soln. of Ru-complex in CH2Cl2 added dropwise to soln. of ligand in CH2Cl2, stirred for 2 h; concd., pentane added; elem. anal.; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
2-{[4-phenyl-1H-1,2,3-triazol-1-yl]methyl}pyridine
[Ru(η6-p-cymene)Cl(1-(2-picolyl)-4-phenyl-1H-1,2,3-triazole)]Cl
Conditions | Yield |
---|---|
In ethanol mixt. ligand and Ru complex in EtOH was stirred at room temp. for 2 days; hexane was added and left to stand at 4°C for 2 h, soln. was filtered and evapd.; | 100% |
triethylsilane
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
dichloro(μ-chloro)(μ-hydrido)bis(η-p-cymene)diruthenium(II)
Conditions | Yield |
---|---|
In benzene-d6 at 20℃; Inert atmosphere; Glovebox; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
4-bromopyridine hydrochloride
[RuCl2(p-cymene)(4-BrNC5H4)]
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 100% |
In dichloromethane at 20℃; | 97% |
pyridine
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
η-p-cymene dichloro(pyridine)ruthenium(II)
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 24h; | 100% |
In dichloromethane at 20℃; | 89% |
In toluene at 20℃; for 4h; Inert atmosphere; Schlenk technique; Reflux; | 80.2% |
In toluene for 3h; Inert atmosphere; Schlenk technique; Reflux; | 79% |
In acetone at 20℃; | 69% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
4,4'-dinonyl-2,2'-bipyridine
Conditions | Yield |
---|---|
In ethanol for 4h; Reflux; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; Inert atmosphere; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In dichloromethane for 0.5h; Inert atmosphere; Schlenk technique; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In dichloromethane for 0.5h; Inert atmosphere; Schlenk technique; | 100% |
3,5-Lutidine
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 24h; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl
(2,2'-bis(diphenylphosphino)-1,1'-binaphathalene)chloro(p-cymene)ruthenium chloride
Conditions | Yield |
---|---|
In ethanol; dichloromethane at 65℃; for 1.5h; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
In isopropyl alcohol at 85℃; for 5h; Schlenk technique; Inert atmosphere; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
With triethylamine In toluene at 20℃; for 3h; Schlenk technique; | 100% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
2-amino-5,10-dihydro-5,10-dioxo-4(pyridine-3-yl)-4H-benzo[g]chromene-3-carbonitrile
Conditions | Yield |
---|---|
In acetone at 20℃; for 0.5h; | 100% |
(4-(trifluoromethyl)phenyl)methanethiol
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
Conditions | Yield |
---|---|
at 0℃; for 4h; Inert atmosphere; Schlenk technique; | 100% |
In ethanol Inert atmosphere; Reflux; |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
dichloromethane
1,1’-((2,3,5,6-tetramethyl-1,4-phenylene)bis(methylene))bis(1H-imidazole)
Conditions | Yield |
---|---|
at 99.84℃; for 24h; Sealed tube; | 99.8% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
3-(diphenylphosphino)propionic acid
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 3h; Inert atmosphere; Schlenk technique; | 99.7% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
phosphorous acid trimethyl ester
[Ru(η6-p-cymene)Cl2{P(OMe)3}]
Conditions | Yield |
---|---|
In hexane under N2, reflux for 4 h; solvent was removed in vac., crystn. at -30 °C from CH2Cl2-petroleum ether overnight, elem. anal.; | 99.6% |
In tetrahydrofuran at 20℃; for 3h; Inert atmosphere; | 90% |
In dichloromethane under N2, Schlenk techniques; soln. of Ru complex in CH2Cl2 stirred at room temp., P(OMe)3 added, mixt. stirred at room temp. for 2 h; soln. concd. under vac., hexanes added, filtered, solid washed with pentane, dried under vac.; | 76.1% |
In dichloromethane Ar or N2-atmosphere; stirring (room temp., 15 min); evapn. (vac.), washing (hexane), filtering, drying (vac.); elem. anal.; | 63% |
In methanol; dichloromethane |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
2-(4-bromophenyl)-1H-imidazo(4,5-f)[1,10]phenanthroline
Conditions | Yield |
---|---|
at 60℃; for 0.5h; Microwave irradiation; | 99.3% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
(diphenylphosphino)acetophenone
{(η6-p-cymene)Cl2(η1-PPh2CH2COPh)ruthenium(II)}
Conditions | Yield |
---|---|
In chloroform (under Ar or N2, Schlenk techniques); stirred for 1 h; filtd., the filtrate is covered with hexane, elem. anal.; | 99% |
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
dichloromethane
Conditions | Yield |
---|---|
In dichloromethane under dry N2, 2:1 mixt., stirred for 1-2 h; evapd., dried (vac.), elem. anal.; | 99% |
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