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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2,6-Diaminotoluene with high purity

Cas:823-40-5

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Jinan Finer Chemical Co., Ltd

Product Description Product Name 1,3-Diamino-2-methylbenzene CAS No. 823-40-5 Appearance Off-white crystal Assay ≥99% Capacity 500mt/year Min.packing 100g

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:1 Gram

FOB Price: $8.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-methyl-m-phenylenediamine

Cas:823-40-5

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei yanxi chemical co.,LTD.

Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:1 Metric Ton

FOB Price: $1.0 / 2.0

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

TIANFUCHEM--28987-59-9--2-CHLORO-4-METHOXYNITROBENZENE factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable bu

TIANFUCHEM--823-40-5--2,6-Diaminotoluene factory price

Cas:823-40-5

Min.Order:1 Metric Ton

FOB Price: $2000.0

Type:Lab/Research institutions

inquiry

Henan Sinotech Import&Export Corporation

Product Name: 2,6-Diaminotoluene Synonyms: TOLYLENE-2,6-DIAMINE;2,6-diamino-toluen;Toluene-2,6-diamine: (2_Methyl-1,2-benzenediamine);2-methyl-m-phenylenediamine 2,6-toluenediamine;2,6-Toluenediamine, 2,6-T

2,6-Diaminotoluene CAS: 823-40-5

Cas:823-40-5

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

inquiry

Hubei Langyou International Trading Co., Ltd

Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s

Changchun Artel lmport and Export trade company

Product Detail Minimum Order Qty. 10 Gram

2,6-Diaminotoluene CAS NO.823-40-5

Cas:823-40-5

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:823-40-5

Cas:823-40-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Kemi-Works Chemical Co., Ltd

English name: 2,6-Diaminotoluene CAS NO.:823-40-5 Molecular formula: C7H10N2 Molecular weight: 122.17 Appearance:- Storage:store in dry and cool place Package:25kg/drum, or as per your request. Application:2,6-Diaminotoluene is an important c

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 2,6-Diaminotoluene

Cas:823-40-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediates Tr

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Siwei Development Group Ltd.

Product name: 2,6-Diaminotoluene CAS No.:823-40-5 Molecule Formula:C7H10N2 Molecule Weight:122.17 Purity: 99.0% Package: 25kg/drum Description:Prism-like crystalline powder Manufacture Standards:Enterprise Standard

Best Quality 2,6-Diaminotoluene

Cas:823-40-5

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

SAGECHEM LIMITED

SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in

SAGECHEM/ 2,6-Diaminotoluene /Manufacturer in China

Cas:823-40-5

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Beijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)

Capability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

2,6-DiaMinotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

factory supply CAS 823-40-5 with competitive price

Cas:823-40-5

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

2,6-DiaMinotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Other

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

2,6-DiaminotolueneAppearance:solid Storage:Shading, sealed and preserved. Package:25 kg/barrels Application:An organic synthetic intermediate used in the synthesis of medicine. Transportation:By express (Door to door) such as FEDEX, DHL, EMS for smal

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

2,6-Diaminotoluene 823-40-5

Cas:823-40-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemsigma International Co.,Ltd.

bulk?production Application:Pharmaceutical intermediates

2,6-Diaminotoluene

Cas:823-40-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

2,6-dinitrotoluene
606-20-2

2,6-dinitrotoluene

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

Conditions
ConditionsYield
With hydrogen In methanol at 50℃; under 1500.15 Torr; for 0.666667h; Inert atmosphere;100%
With Fe3O4Rh; hydrazine hydrate In ethanol at 80℃; for 2h; Inert atmosphere;99%
With hydrogen In ethanol at 20℃; under 760.051 Torr; for 1h;99%
2,6-Toluene diisocyanate
91-08-7

2,6-Toluene diisocyanate

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

Conditions
ConditionsYield
With formic acid; trifluoroborane diethyl ether94%
With water In 1,2-dimethoxyethane at 37℃; for 0.0166667h; Kinetics; Further Variations:; Solvents; Reaction partners; Hydrolysis;10.7%
3-chloro-2-methylbenzenamine
87-60-5

3-chloro-2-methylbenzenamine

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

Conditions
ConditionsYield
With ammonium hydroxide; urea; copper(l) chloride at 160℃; under 17251.7 Torr; for 20h; Reagent/catalyst; Temperature; Pressure; Autoclave;85.5%
3-nitro-o-tolylamine
603-83-8

3-nitro-o-tolylamine

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

Conditions
ConditionsYield
With hydrogenchloride; tin; tin(ll) chloride auf dem Wasserbade;
With formic acid In ethanol; water at 20℃; for 1h;
With sodium tetrahydroborate In ethanol; water at 25℃; for 0.5h;
With hydrazine hydrate In ethanol at 80℃; for 0.483333h; Catalytic behavior;
With hydrazine hydrate In ethanol at 90℃; for 14h; Catalytic behavior; Green chemistry;
hydrogenchloride
7647-01-0

hydrogenchloride

3-nitro-o-tolylamine
603-83-8

3-nitro-o-tolylamine

tin

tin

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

ethanol
64-17-5

ethanol

2,6-dinitrotoluene
606-20-2

2,6-dinitrotoluene

palladium charcoal

palladium charcoal

A

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

B

2-hydroxylamino-6-nitrotoluene
5805-95-8

2-hydroxylamino-6-nitrotoluene

Conditions
ConditionsYield
Hydrogenation;
sulfuric acid
7664-93-9

sulfuric acid

2,6-dinitrotoluene
606-20-2

2,6-dinitrotoluene

vanadium compound

vanadium compound

A

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

B

3-nitro-o-tolylamine
603-83-8

3-nitro-o-tolylamine

C

6,6'-Dinitro-2,2'-azoxytoluene
5806-00-8

6,6'-Dinitro-2,2'-azoxytoluene

Conditions
ConditionsYield
bei der elektrolytischen Reduktion;
2,6-dinitrotoluene
606-20-2

2,6-dinitrotoluene

A

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

B

3-nitro-o-tolylamine
603-83-8

3-nitro-o-tolylamine

Conditions
ConditionsYield
In phosphate buffer pH=2; Electrochemical reaction;
(S)-2-Amino-4-[(R)-2-{3-[(R)-2-((S)-4-amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethylsulfanylcarbonylamino]-2-methyl-phenylcarbamoylsulfanyl}-1-(carboxymethyl-carbamoyl)-ethylcarbamoyl]-butyric acid
188910-15-8

(S)-2-Amino-4-[(R)-2-{3-[(R)-2-((S)-4-amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethylsulfanylcarbonylamino]-2-methyl-phenylcarbamoylsulfanyl}-1-(carboxymethyl-carbamoyl)-ethylcarbamoyl]-butyric acid

A

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

B

2-amino-6-isocyanatotoluene

2-amino-6-isocyanatotoluene

C

(S)-2-Amino-4-[(R)-2-(3-amino-2-methyl-phenylcarbamoylsulfanyl)-1-(carboxymethyl-carbamoyl)-ethylcarbamoyl]-butyric acid

(S)-2-Amino-4-[(R)-2-(3-amino-2-methyl-phenylcarbamoylsulfanyl)-1-(carboxymethyl-carbamoyl)-ethylcarbamoyl]-butyric acid

D

(S)-2-Amino-4-[(R)-1-(carboxymethyl-carbamoyl)-2-(3-isocyanato-2-methyl-phenylcarbamoylsulfanyl)-ethylcarbamoyl]-butyric acid

(S)-2-Amino-4-[(R)-1-(carboxymethyl-carbamoyl)-2-(3-isocyanato-2-methyl-phenylcarbamoylsulfanyl)-ethylcarbamoyl]-butyric acid

Conditions
ConditionsYield
With Hank's balanced salts solution at 25℃; for 72h; Kinetics; Product distribution; Further Variations:; Temperatures;
2,4-dinitrotoluene
121-14-2

2,4-dinitrotoluene

3,5-dinitrotoluene
618-85-9

3,5-dinitrotoluene

2,6-dinitrotoluene
606-20-2

2,6-dinitrotoluene

1-methyl-2,3-dinitrobenzene
602-01-7

1-methyl-2,3-dinitrobenzene

3,4-Dinitrotoluene
610-39-9

3,4-Dinitrotoluene

2,5-dinitrotoluene
619-15-8

2,5-dinitrotoluene

A

3,5-diaminotoluene
108-71-4

3,5-diaminotoluene

B

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

C

4-methylbenzene-1,3-diamine
95-80-7

4-methylbenzene-1,3-diamine

D

4-methyl-1,2-diaminobenzene
496-72-0

4-methyl-1,2-diaminobenzene

E

2-methyl-p-phenylenediamine
95-70-5

2-methyl-p-phenylenediamine

F

3-methyl-1,2-benzenediamine
2687-25-4

3-methyl-1,2-benzenediamine

Conditions
ConditionsYield
With hydrogen; nickel at 120 - 140℃; under 11251.1 - 22502.3 Torr; Product distribution / selectivity;
1-methyl-4-nitrobenzene
99-99-0

1-methyl-4-nitrobenzene

2,4-dinitrotoluene
121-14-2

2,4-dinitrotoluene

3,5-dinitrotoluene
618-85-9

3,5-dinitrotoluene

2,6-dinitrotoluene
606-20-2

2,6-dinitrotoluene

1-methyl-2,3-dinitrobenzene
602-01-7

1-methyl-2,3-dinitrobenzene

2,5-dinitrotoluene
619-15-8

2,5-dinitrotoluene

A

methylcyclohexylamine

methylcyclohexylamine

B

methylcyclohexyldiamine

methylcyclohexyldiamine

C

toluidine

toluidine

D

3,5-diaminotoluene
108-71-4

3,5-diaminotoluene

E

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

F

4-methylbenzene-1,3-diamine
95-80-7

4-methylbenzene-1,3-diamine

G

2-methyl-p-phenylenediamine
95-70-5

2-methyl-p-phenylenediamine

H

3-methyl-1,2-benzenediamine
2687-25-4

3-methyl-1,2-benzenediamine

Conditions
ConditionsYield
With hydrogen at 170 - 215.6℃; under 67.5068 Torr;
2,4-dinitrotoluene
121-14-2

2,4-dinitrotoluene

2,6-dinitrotoluene
606-20-2

2,6-dinitrotoluene

A

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

B

4-methylbenzene-1,3-diamine
95-80-7

4-methylbenzene-1,3-diamine

Conditions
ConditionsYield
With hydrogen; Ni hydrogenation catalyst In water at 120 - 122℃; under 18751.9 Torr;
With hydrogen; nickel In water at 180℃; under 19502 Torr; for 18 - 215h; Product distribution / selectivity;
With hydrogen; nickel on SiO2 and ZrO2 mixture In water at 116 - 126℃; under 18751.9 Torr; Product distribution / selectivity; Inert atmosphere; Industry scale;
1,2-dichloro-4-methyl-3,5-dinitro-benzene
53278-85-6

1,2-dichloro-4-methyl-3,5-dinitro-benzene

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

Conditions
ConditionsYield
With sodium hydroxide; calcium carbonate; aluminum nickel In methanol
2,6-diamino-3,4-dichlorotoluene

2,6-diamino-3,4-dichlorotoluene

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

Conditions
ConditionsYield
With calcium oxide In palladium on charcoal; isopropyl alcohol
2,6-dichlorotoluene
118-69-4

2,6-dichlorotoluene

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

Conditions
ConditionsYield
With ammonium hydroxide; C30H42NOP*C9H9ClPd In ethanol at 80℃; under 760.051 Torr; for 8h; Catalytic behavior; Temperature;58.3 g
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

chloroformic acid ethyl ester
541-41-3

chloroformic acid ethyl ester

ethyl N-(3-ethoxycarbonylamino-2-methylphenyl)carbamate
16648-51-4

ethyl N-(3-ethoxycarbonylamino-2-methylphenyl)carbamate

Conditions
ConditionsYield
With TEA In tetrahydrofuran for 1h; Heating;98%
In chloroform
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

2,5-hexanedione
110-13-4

2,5-hexanedione

2,6-di(2,5-dimethyl-1H-pyrrol-1-yl)toluene

2,6-di(2,5-dimethyl-1H-pyrrol-1-yl)toluene

Conditions
ConditionsYield
montmorillonite K-10 at 90℃; for 0.05h; modified Paal-Knorr synthesis; microwave heating;97%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

dimethyl acetylenedicarboxylate
762-42-5

dimethyl acetylenedicarboxylate

2,6-bis(1,2-dicarbomethoxyvinylamino)toluene
49635-43-0

2,6-bis(1,2-dicarbomethoxyvinylamino)toluene

Conditions
ConditionsYield
In methanol; chloroform standing overnight;95%
In methanol at 0 - 20℃;
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

dimethyl acetylenedicarboxylate
762-42-5

dimethyl acetylenedicarboxylate

C19H22N2O8

C19H22N2O8

Conditions
ConditionsYield
In methanol; chloroform at 0 - 20℃; for 16h; Inert atmosphere; Schlenk technique;95%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

4-formylphenyl 4-(dodecyloxy)benzoate
56800-36-3

4-formylphenyl 4-(dodecyloxy)benzoate

N,N'-bis[4-(4-n-dodecyloxybenzoyloxy)benzylidene]-(2-methyl-1,3-phenylene)diamine
1373878-22-8

N,N'-bis[4-(4-n-dodecyloxybenzoyloxy)benzylidene]-(2-methyl-1,3-phenylene)diamine

Conditions
ConditionsYield
With acetic acid In ethanol at 20℃; for 24h;93%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

2-ethoxymethylene-3-oxobutanoic acid ethyl ester
3788-94-1

2-ethoxymethylene-3-oxobutanoic acid ethyl ester

C21H26N2O6

C21H26N2O6

Conditions
ConditionsYield
In ethanol at 70℃; for 0.333333h; Microwave irradiation; Inert atmosphere;93%
diisobutyl carbonate
539-92-4

diisobutyl carbonate

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

2,4-TDA
1187831-01-1

2,4-TDA

Conditions
ConditionsYield
With sodium isobutoxide at 120℃; for 0.5h; Inert atmosphere;92%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

2-methyl-1,3-diaminocyclohexane

2-methyl-1,3-diaminocyclohexane

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen; sodium sulfate In 1,4-dioxane at 220℃; under 105011 Torr; for 6h; Solvent; Pressure; Temperature; Reagent/catalyst; Autoclave;91%
Hydrogenation;
With 5 wt% ruthenium/carbon; hydrogen; sodium nitrite In isopropyl alcohol at 170℃; under 62256.2 Torr; for 4h; Temperature; Autoclave;
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

Ethyl oxalyl chloride
4755-77-5

Ethyl oxalyl chloride

diethyl N,N'-[1,3-(2-methyl)phenyl]dioxalamate
47300-42-5

diethyl N,N'-[1,3-(2-methyl)phenyl]dioxalamate

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran for 1h; Reflux;90%
With triethylamine In N,N-dimethyl-formamide
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

diethyl 2-ethoxymethylenemalonate
87-13-8

diethyl 2-ethoxymethylenemalonate

diethyl 2-{[3-(2,2-bisethoxycarbonylvinylamino)-2-methylphenylamino]methylene}malonate
39595-13-6

diethyl 2-{[3-(2,2-bisethoxycarbonylvinylamino)-2-methylphenylamino]methylene}malonate

Conditions
ConditionsYield
In ethanol for 5h; Heating;90%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

trifluoroacetic anhydride
407-25-0

trifluoroacetic anhydride

N-[3-(2,2-dimethylpropionylamino)-2-methylphenyl]-2,2-dimethylpropionamide
25116-07-8

N-[3-(2,2-dimethylpropionylamino)-2-methylphenyl]-2,2-dimethylpropionamide

Conditions
ConditionsYield
In tetrahydrofuran Cooling with ice;90%
dipropyl acetylenedicarboxylate
14447-02-0

dipropyl acetylenedicarboxylate

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

C27H38N2O8

C27H38N2O8

Conditions
ConditionsYield
In methanol; chloroform at 0 - 20℃; for 16h; Schlenk technique; Inert atmosphere;90%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

C28H50O4

C28H50O4

C63H110N2O8

C63H110N2O8

Conditions
ConditionsYield
In methanol; chloroform at 0 - 20℃; for 16h; Schlenk technique; Inert atmosphere;88%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

acetylenedicarboxylic acid di-n-hexyl ester

acetylenedicarboxylic acid di-n-hexyl ester

C39H62N2O8

C39H62N2O8

Conditions
ConditionsYield
In methanol; chloroform at 0 - 20℃; for 16h; Schlenk technique; Inert atmosphere;86%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

ethyl acetoacetate
141-97-9

ethyl acetoacetate

(Z)-3-[3-((Z)-2-Ethoxycarbonyl-1-methyl-vinylamino)-2-methyl-phenylamino]-but-2-enoic acid ethyl ester
182410-18-0

(Z)-3-[3-((Z)-2-Ethoxycarbonyl-1-methyl-vinylamino)-2-methyl-phenylamino]-but-2-enoic acid ethyl ester

Conditions
ConditionsYield
With calcium sulfate; acetic acid In ethanol at 80℃; for 2h;85%
With copper(II) sulfate In ethanol at 80℃; for 4h;
methanol
67-56-1

methanol

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

N2,N2,N6,N6-tetrakis(methoxymethyl)-2,6-diaminotoluene

N2,N2,N6,N6-tetrakis(methoxymethyl)-2,6-diaminotoluene

Conditions
ConditionsYield
With oxygen at 120℃; under 7500.75 Torr; for 10h; Reagent/catalyst; Autoclave;85%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

pivaloyl chloride
3282-30-2

pivaloyl chloride

N-[3-(2,2-dimethylpropionylamino)-2-methylphenyl]-2,2-dimethylpropionamide
25116-07-8

N-[3-(2,2-dimethylpropionylamino)-2-methylphenyl]-2,2-dimethylpropionamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran for 0.5h;84%
With pyridine
With triethylamine
1-bromo-4-tert-butylbenzene
3972-65-4

1-bromo-4-tert-butylbenzene

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

N1,N3-bis(4-tert-butylphenyl)-2-methylbenzene-1,3-diamine

N1,N3-bis(4-tert-butylphenyl)-2-methylbenzene-1,3-diamine

Conditions
ConditionsYield
With chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)]palladium (II); sodium t-butanolate In toluene at 90℃; for 12h; Inert atmosphere;81%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

propynoic acid ethyl ester
623-47-2

propynoic acid ethyl ester

2,6-bis(2'-carboethoxyvinylamino)toluene

2,6-bis(2'-carboethoxyvinylamino)toluene

Conditions
ConditionsYield
In methanol for 24h; Ambient temperature;80%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

indole-2,3-dione
91-56-5

indole-2,3-dione

3,3'-[(2-methyl-1,3-phenylene)dinitrilo]bis[1,3-dihydro-2H-indole-2-one]

3,3'-[(2-methyl-1,3-phenylene)dinitrilo]bis[1,3-dihydro-2H-indole-2-one]

Conditions
ConditionsYield
With acetic acid In ethanol for 19h; Heating;80%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

4-chloro-6,7-dimethoxyquinoline-3-carbonitrile
214470-55-0

4-chloro-6,7-dimethoxyquinoline-3-carbonitrile

10,11-dimethoxy-4-methyldibenzo[c,f]-2,7-naphthyridine-3,6-diamine
936833-38-4

10,11-dimethoxy-4-methyldibenzo[c,f]-2,7-naphthyridine-3,6-diamine

Conditions
ConditionsYield
With pyridine hydrochloride In 2-ethoxy-ethanol at 210℃; under 1034.32 Torr; for 1h; Product distribution / selectivity; Microwave irradiation;80%
With pyridine hydrochloride In 2-ethoxy-ethanol at 130℃; for 8h; Product distribution / selectivity;65%
In 2-ethoxy-ethanol for 15h; Heating;
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

4-chloro-6,7-dimethoxyquinoline-3-carbonitrile
214470-55-0

4-chloro-6,7-dimethoxyquinoline-3-carbonitrile

A

10,11-dimethoxy-4-methyldibenzo[c,f]-2,7-naphthyridine-3,6-diamine
936833-38-4

10,11-dimethoxy-4-methyldibenzo[c,f]-2,7-naphthyridine-3,6-diamine

B

4-[(3-amino-2-methylphenyl)amino]-6,7-dimethoxyquinoline-3-carbonitrile

4-[(3-amino-2-methylphenyl)amino]-6,7-dimethoxyquinoline-3-carbonitrile

Conditions
ConditionsYield
With pyridine hydrochloride In 2-ethoxy-ethanol at 210℃; for 1h; Temperature; Time; Concentration; Microwave irradiation;A 79%
B n/a
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

2-dimethylaminomethylene-1,3-bis(dimethylimmonio)propane bistetrafluoroborate

2-dimethylaminomethylene-1,3-bis(dimethylimmonio)propane bistetrafluoroborate

7-amino-8-methylquinoline-3-carboxaldehyde
521074-55-5

7-amino-8-methylquinoline-3-carboxaldehyde

Conditions
ConditionsYield
Stage #1: 2,6-toluenediamine; 2-dimethylaminomethylene-1,3-bis(dimethylimmonio)propane bistetrafluoroborate In isopropyl alcohol for 16h; Reflux;
Stage #2: With hydrogenchloride In water at 20 - 70℃; for 5h;
Stage #3: With potassium carbonate In water; ethyl acetate at 90℃; for 16h;
77%
Stage #1: 2,6-toluenediamine; 2-dimethylaminomethylene-1,3-bis(dimethylimmonio)propane bistetrafluoroborate In isopropyl alcohol for 16h; Heating / reflux;
Stage #2: With hydrogenchloride; water In isopropyl alcohol at 70℃; for 5h;
Stage #3: With potassium carbonate In water; ethyl acetate at 90℃;
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

acetylenedicarboxylic acid diethyl ester
762-21-0

acetylenedicarboxylic acid diethyl ester

C23H30N2O8

C23H30N2O8

Conditions
ConditionsYield
In methanol; chloroform at 0 - 20℃; for 16h; Schlenk technique; Inert atmosphere;77%
2-methylphenyl bromide
95-46-5

2-methylphenyl bromide

2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

2-methyl-N1,N3-di-o-tolylbenzene-1,3-diamine

2-methyl-N1,N3-di-o-tolylbenzene-1,3-diamine

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In 1,4-dioxane at 110℃; Inert atmosphere;76.06%
2,6-Diaminotoluene
823-40-5

2,6-Diaminotoluene

4-formyl-3-hydroxyphenyl 4-n-dodecyloxy-3-fluorobenzoate
1363404-49-2

4-formyl-3-hydroxyphenyl 4-n-dodecyloxy-3-fluorobenzoate

N,N'-bis[4-(4-n-dodecyloxy-3-fluorobenzoyloxy)-2-hydroxybenzylidene]-(2-methyl-1,3-phenylene)diamine
1373878-32-0

N,N'-bis[4-(4-n-dodecyloxy-3-fluorobenzoyloxy)-2-hydroxybenzylidene]-(2-methyl-1,3-phenylene)diamine

Conditions
ConditionsYield
With acetic acid In ethanol at 20℃; for 24h;76%
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