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Cas:1666-13-3
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inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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Cas:1666-13-3
Min.Order:5 Kiloliter
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:1666-13-3
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inquirySuperior quality Appearance:yellow crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceutical Intermediates Transpo
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:1666-13-3
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inquiryWe are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
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Cas:1666-13-3
Min.Order:1 Kilogram
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Type:Trading Company
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Diphenyl diselenide cas 1666-13-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
we produce and sell good chemicals around the world.Appearance:white power Storage:Keep it in dry,shady and cool place Package:as your requirement Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:SEA OR AIR Port:China Main Po
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
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inquirylow price and high purityAppearance:solid or liquid Storage:in sealed air resistant place Package:As customer require Application:Pharma;Industry;Agricultural Transportation:by sea or by airplane Port:any port in China
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inquiryDiphenyl diselenideAppearance:detailed see specifications Storage:Store in dry, dark and ventilated place Package:according to the clients requirement Application:custom synthesis molecular; API Intermediates;Fluorinating Reagents & Building Blocks f
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
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Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryPhenylselenyl chloride
N,N,N'-tris(trimethylsilyl)benzamidine
A
diphenyl diselenide
B
C26H20N4Se2
Conditions | Yield |
---|---|
In dichloromethane at 23℃; for 3h; | A 100% B 55% |
iodoacetophenone
Benzeneselenol
A
diphenyl diselenide
B
acetophenone
Conditions | Yield |
---|---|
With potassium carbonate In ethanol for 0.25h; Product distribution; Ambient temperature; other iodomethyl ketones; | A 100% B 100% |
A
diphenyl diselenide
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene for 1.5h; Heating; | A 100% B 99% |
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene for 1.5h; Heating; | A 99% B 98% |
Phenylselenyl chloride
Thallous Phenyl Selenide
A
diphenyl diselenide
Conditions | Yield |
---|---|
In diethyl ether for 0.00833333h; Ambient temperature; | A 100% B n/a |
Benzoyl bromide
Thallous Phenyl Selenide
A
diphenyl diselenide
B
phenyl selenobenzoate
Conditions | Yield |
---|---|
In diethyl ether for 1h; | A 1% B 99% |
Conditions | Yield |
---|---|
With GLUTATHIONE In methanol Product distribution; Mechanism; 0.1 M phosphate buffer, pH=6.9; UV spectra; | A 99% B 64% |
1-(naphthalen-2-yl)-2-(phenylselanyl)ethan-1-one
A
diphenyl diselenide
B
methyl 2-naphthyl ketone
Conditions | Yield |
---|---|
With GLUTATHIONE In methanol Product distribution; Mechanism; 0.1 M phosphate buffer, pH=6.9; | A 99% B 91% |
1-(4-nitrophenyl)-2-(phenylselanyl)ethan-1-one
A
diphenyl diselenide
B
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With GLUTATHIONE In methanol Product distribution; Mechanism; 0.1 M phosphate buffer, pH=6.9; differnt quantity of glutathione; relative reactivity to α-(phenylselenenyl)acetophenone; | A 99% B 87% |
A
diphenyl diselenide
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene for 1.5h; Heating; | A 99% B 98% |
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene for 1.5h; Heating; | A 98% B 97% |
A
diphenyl diselenide
B
(Z)-ethyl 2-fluoro-5-phenylpent-2-enoate
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In 1,2-dichloro-ethane at 83℃; for 0.166667h; | A 13% B 99% |
B
diphenyl diselenide
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In 1,2-dichloro-ethane at 20℃; for 0.166667h; | A 99% B 31% |
Se-phenyl butaneselenoate
diphenyl diselenide
Conditions | Yield |
---|---|
With iodine In methanol at 20℃; for 4.5h; | 99% |
Conditions | Yield |
---|---|
at 60 - 70℃; for 0.5h; Reduction; oxidation; | A 5.4% B 98.6% |
at 100 - 120℃; for 5h; Reduction; oxidation; | A 92.5% B 95.6% |
Conditions | Yield |
---|---|
With dihydrogen peroxide In ethanol at 0℃; for 0.3h; | 98% |
With dimethyl 2,3-dicyanofumarate In dichloromethane at 0 - 20℃; for 12h; Inert atmosphere; | 98% |
With sodium perborate In ethanol at 20℃; for 6h; | 97% |
Conditions | Yield |
---|---|
With selenium; potassium hydroxide In dimethyl sulfoxide at 90℃; for 4h; Time; Solvent; Concentration; | 98% |
With selenium; potassium hydroxide In water at 130℃; for 5h; Green chemistry; | 98% |
With selenium; copper(II) oxide; potassium hydroxide In dimethyl sulfoxide at 90℃; for 1h; Inert atmosphere; | 96% |
benzyl phenyl selenide
A
diphenyl diselenide
B
1,1'-(1,2-ethanediyl)bisbenzene
Conditions | Yield |
---|---|
at 600℃; under 20 Torr; | A 98% B 92% |
phenyl trimethylsilyl selenide
A
trimethylsilyl iodide
B
diphenyl diselenide
Conditions | Yield |
---|---|
With iodine | A 98% B 96% |
Conditions | Yield |
---|---|
In ethanol at 0℃; for 1h; | 98% |
benzoyl chloride
Thallous Phenyl Selenide
A
diphenyl diselenide
B
phenyl selenobenzoate
Conditions | Yield |
---|---|
In diethyl ether for 2.5h; | A 1% B 98% |
Thallous Phenyl Selenide
acetyl chloride
A
acetyl phenyl selenide
B
diphenyl diselenide
Conditions | Yield |
---|---|
In diethyl ether for 1h; | A 98% B 1% |
aniline
Se-phenyl 4-methylbenzenecarboselenothioate
A
diphenyl diselenide
B
4-methylthiobenzanilide
Conditions | Yield |
---|---|
In hexane for 24h; Heating; | A 98% B 68% |
2-phenylethanol
1,2-diphenyl-1-phenylseleno-2-ethanone
A
phenyl benzyl ketone
B
diphenyl diselenide
C
(2-phenyl-ethyl) phenyl selenide
Conditions | Yield |
---|---|
With tributylphosphine In benzene for 4h; Ambient temperature; | A 98% B 8% C 72% |
p-tolyl benzeneselenosulfonate
Triethylgerman
A
triethylgermyl p-toluenesulfonate
B
diphenyl diselenide
Conditions | Yield |
---|---|
With air; 2,2'-azobis(isobutyronitrile) In not given | A 93% B 98% |
piperidine
Se-phenyl 4-methylbenzenecarboselenothioate
A
diphenyl diselenide
B
piperidinium 4-methylbenzenecarbodithiolate
Conditions | Yield |
---|---|
In hexane at 20℃; for 0.5h; | A 97% B 31% |
Phenylselenyl chloride
phenyl trimethylsilyl selenide
A
chloro-trimethyl-silane
B
diphenyl diselenide
Conditions | Yield |
---|---|
In acetonitrile at 9℃; | A 97% B 93% |
Acetyl bromide
Thallous Phenyl Selenide
A
acetyl phenyl selenide
B
diphenyl diselenide
Conditions | Yield |
---|---|
In diethyl ether for 1h; | A 97% B 1% |
tert-butyl phenyl selenide
diphenyl diselenide
Conditions | Yield |
---|---|
sodium perchlorate In acetonitrile | 97% |
phenylselenium trichloride
diphenyl diselenide
Conditions | Yield |
---|---|
With sodium L-ascorbate In methanol; water for 24h; | 97% |
trans-2-<1-(Phenylseleno)benzyl>cyclohexanol
A
diphenyl diselenide
B
2-hydroxybenzylidenecyclohexane
Conditions | Yield |
---|---|
With N-chloro-succinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene In toluene 1.) 1h 0 deg C, 2.) 7h room temperature; | A 40% B 97% |
Thallous Phenyl Selenide
1-chloroacetophenone
A
α-(phenylseleno)acetophenone
B
diphenyl diselenide
Conditions | Yield |
---|---|
In diethyl ether for 10h; | A 97% B 1% |
Conditions | Yield |
---|---|
With RhCl(PPh3)3; hydrogen; triethylamine In tetrahydrofuran at 50℃; under 760 Torr; for 24h; | 100% |
With ruthenium trichloride; zinc In N,N-dimethyl-formamide at 100℃; for 1h; | 98% |
Stage #1: diphenyl diselenide With 1-butyl-3-methylimidazolium Tetrafluoroborate; zinc at 20℃; Inert atmosphere; Stage #2: benzyl chloride at 20℃; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With indium(III) bromide; zinc In N,N-dimethyl-formamide at 100℃; for 1h; | 100% |
With ruthenium trichloride; zinc In N,N-dimethyl-formamide at 100℃; for 1h; | 98% |
With RhCl(PPh3)3; hydrogen; triethylamine In tetrahydrofuran at 50℃; under 760 Torr; for 24h; | 97% |
pent-4-enoic acid
diphenyl diselenide
5-phenylselanylmethyl-dihydro-furan-2-one
Conditions | Yield |
---|---|
With copper(I) trifluoromethanesulfonate benzene; calcium carbonate In dichloromethane at 30℃; for 8h; | 100% |
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 30℃; | 95% |
With carbon tetrabromide In dichloromethane for 4h; Irradiation; | 95% |
Conditions | Yield |
---|---|
With 4-tert-butylpyridine; hydrogen sulfide; oxygen; iron(II) chloride In acetonitrile for 4h; Ambient temperature; | 100% |
With 4-tert-butylpyridine; 2-Picolinic acid; dihydrogen peroxide; triphenylphosphine; iron(II) chloride In acetonitrile at 0℃; | 99% |
With di-tert-butyl peroxide at 120℃; for 18h; Reagent/catalyst; | 96% |
(cyclopent-2-eneyl)acetic acid
diphenyl diselenide
(3aα,6a,6aα)-hexahydro-6-(phenylseleno)-2H-cyclopentafuran-2-one
Conditions | Yield |
---|---|
With copper(I) trifluoromethanesulfonate benzene; calcium carbonate In dichloromethane at 30℃; for 7.5h; other acids; | 100% |
With copper(I) trifluoromethanesulfonate benzene; calcium carbonate In dichloromethane at 30℃; for 7.5h; | 100% |
With iodine In acetonitrile at 20℃; for 16h; regioselective reaction; | 81% |
With iodosylbenzene In dichloromethane at 20℃; | 72% |
With ammonium persulfate In acetonitrile at 70℃; for 2h; | 70% |
diphenyl diselenide
phenylselenium trichloride
Phenylselenyl chloride
Conditions | Yield |
---|---|
In tetrachloromethane at 20℃; for 2h; | 100% |
diphenyl diselenide
trans-2-(2-phenylethynyl)-1-cyclohexanol
Conditions | Yield |
---|---|
With tributylphosphine In tetrahydrofuran | 100% |
diphenyl diselenide
6-benzyloxy-4-methyl-4Z-hexen-1-ol p-toluenesulfonate
(Z)-6-benzyloxy-4-methyl-1-phenylseleno-4-hexene
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol for 2h; Ambient temperature; | 100% |
diphenyl diselenide
C16H25ClHgO2
Conditions | Yield |
---|---|
In benzene for 0.216667h; Irradiation; | 100% |
diphenyl diselenide
C15H23ClHgO3
(1R,4aR,8aS)-5,5,8a-Trimethyl-2-oxo-6-phenylselanyl-decahydro-naphthalene-1-carboxylic acid methyl ester
Conditions | Yield |
---|---|
In benzene for 0.216667h; Irradiation; | 100% |
diphenyl diselenide
C17H27ClHgO4
(1'R,4'aS,8'aR)-5',5',8'a-Trimethyl-6'-phenylselanyl-octahydro-spiro[[1,3]dioxolane-2,2'-naphthalene]-1'-carboxylic acid methyl ester
Conditions | Yield |
---|---|
In benzene for 0.216667h; Irradiation; | 100% |
Conditions | Yield |
---|---|
In benzene for 0.216667h; Irradiation; | 100% |
diphenyl diselenide
Tellurobenzoic acid Te-(4-fluoro-phenyl) ester
phenyl selenobenzoate
Conditions | Yield |
---|---|
In benzene at 8℃; for 1.5h; Irradiation; | 100% |
In benzene at 8℃; for 1.5h; Mechanism; Irradiation; other acyl tellurides; other radical traps; other termolysis conditions; | 100% |
In benzene at 8℃; for 1.5h; Irradiation; | 93% |
diphenyl diselenide
(1S,2R,4R)-7,7-Dimethyl-1-phenylselanylmethyl-bicyclo[2.2.1]heptan-2-ol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol Heating; | 100% |
With sodium tetrahydroborate In ethanol for 6h; Heating; | 100% |
Conditions | Yield |
---|---|
With sodium dihydrogenphosphate; zinc In water; acetonitrile for 1h; | 100% |
With indium In tetrahydrofuran; water at 25℃; for 24h; | 98% |
Stage #1: diphenyl diselenide With zinc In acetonitrile at 65℃; for 1h; Stage #2: benzyl bromide In water; acetonitrile at 65℃; for 0.2h; | 98% |
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; zinc In water; acetonitrile for 1h; | 100% |
With dipotassium hydrogenphosphate; zinc In water; acetonitrile for 1h; Product distribution; Further Variations:; Reaction partners; Reagents; Solvents; | 100% |
With sodium tetrahydroborate In acetonitrile for 0.0833333h; pH=7; pH-value; | 100% |
diphenyl diselenide
chloroacetic acid ethyl ester
ethyl 2-(phenylselanyl)acetate
Conditions | Yield |
---|---|
Stage #1: diphenyl diselenide With sodium tetrahydroborate In ethanol at 0℃; for 0.166667h; Inert atmosphere; Stage #2: chloroacetic acid ethyl ester In ethanol for 1h; Inert atmosphere; | 100% |
Stage #1: diphenyl diselenide With sodium tetrahydroborate; ethanol at 0 - 25℃; for 1h; Stage #2: chloroacetic acid ethyl ester at 25℃; for 2h; | 98% |
Stage #1: diphenyl diselenide With sodium tetrahydroborate In ethanol for 0.166667h; Stage #2: chloroacetic acid ethyl ester In ethanol at 50 - 55℃; for 0.75h; | 94% |
diphenyl diselenide
1-phenyl-2-bromoethane
(2-phenyl-ethyl) phenyl selenide
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol for 2h; Ambient temperature; | 100% |
With zinc In N,N-dimethyl-formamide at 100℃; for 2h; Inert atmosphere; | 94% |
With indium iodide In dichloromethane at 20℃; for 1h; | 89% |
With sodium tetrahydroborate In ethanol; 1,2-dichloro-ethane at 20℃; Reduction; alkylation; | 79% |
With triphenylphosphine; 1-pentyl-3-methylimidazolium bromide at 75℃; for 5.5h; | 75% |
Conditions | Yield |
---|---|
With sodium dihydrogenphosphate; zinc In water; acetonitrile for 1h; | 100% |
With sodium tetrahydroborate; ethanol In tetrahydrofuran at 0℃; for 0.416667h; Inert atmosphere; | 98% |
Stage #1: diphenyl diselenide With indium iodide; 1-butyl-3-methylimidazolium Tetrafluoroborate at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: allyl bromide at 20℃; | 97% |
diphenyl diselenide
1-chloro-2,4-dinitro-benzene
(2,4-dinitrophenyl)(phenyl)selane
Conditions | Yield |
---|---|
With borax; N-Acetylcysteine In methanol; water for 1h; Ambient temperature; | 100% |
With sodium hydroxide; cetyltrimethylammonim bromide; Aminoiminomethanesulfinic acid In tetrahydrofuran for 4h; Heating; | 87% |
With sodium hydroxide; Aminoiminomethanesulfinic acid; cetyltrimethylammonim bromide In tetrahydrofuran; water for 4h; Heating; | 87% |
Stage #1: diphenyl diselenide With sodium tetrahydroborate In ethanol Inert atmosphere; Stage #2: 1-chloro-2,4-dinitro-benzene In ethanol; dimethyl sulfoxide for 12h; Reflux; Inert atmosphere; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In 1,2-dimethoxyethane at 20℃; for 12h; Inert atmosphere; | 100% |
With indium iodide In dichloromethane at 20℃; for 1h; | 80% |
With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide In tetrahydrofuran for 3h; Heating; | 78% |
With triphenylphosphine; 1-pentyl-3-methylimidazolium bromide at 75℃; for 6h; | 72% |
diphenyl diselenide
(1S,6R,8R,10S)-8-(3-Chloropropyl)-10-methoxy-3,3,9,9-tetramethyl-2,4,7-trioxabicyclo[4.4.0]decane
(1S,6R,8R,10S)-10-Methoxy-3,3,9,9-tetramethyl-8-(3-phenylselenylpropyl)-2,4,7-trioxabicyclo[4.4.0]decane
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol for 0.666667h; Substitution; Heating; | 100% |
Conditions | Yield |
---|---|
With zinc In acetonitrile for 0.0833333h; pH=14; Barbier Coupling Reaction; | 100% |
With zinc In dichloromethane at 20℃; for 5h; | 87% |
With indium iodide In dichloromethane at 20℃; for 0.416667h; | 85% |
Conditions | Yield |
---|---|
With potassium dihydrogenphosphate; zinc In water; acetonitrile for 1h; | 100% |
diphenyl diselenide
[4-(tert-butyldimethylsiloxy)-5-methoxy-3-(3',7'-dimethyl-6'-epoxy-2'-octenyl)benzyloxy]-tert-butyldimethylsilane
[4-(tert-butyldimethylsiloxy)-5-methoxy-3-(3',7'-dimethyl-7'-hydroxy-6'-phenylselenyl-2'-octenyl)benzyloxy]-tert-butyldimethylsilane
Conditions | Yield |
---|---|
With sodium tetrahydroborate | 100% |
Stage #1: diphenyl diselenide With sodium tetrahydroborate In ethanol at 0℃; for 0.4h; Stage #2: [4-(tert-butyldimethylsiloxy)-5-methoxy-3-(3',7'-dimethyl-6'-epoxy-2'-octenyl)benzyloxy]-tert-butyldimethylsilane In ethanol at 0℃; for 48h; Further stages.; | 100% |
diphenyl diselenide
1-(5-O-tert-butyldimethylsilyl-2,3-O-isopropylidene-β-D-ribofuranosyl)-4-ethoxy-1H-pyrimidin-2-one
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -80℃; for 1h; | 100% |
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