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Cas:75-03-6
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inquiry1 Purity(GC) ≥99.00% 99.8% 2 Appearance Colorless or light yellow liquid Complies Appearance:colorless to slight brown liquid Storage:COOL DRY PLACE Package:50kgs iron drum with plastic lining inside Application:reagent or pharmaceutical inter
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Iodoethane Basic information Product Name: Iodoethane Synonyms: 10doethane(ethyliodide);C2H5I;Ethane, iodo-;Ethane,iodo-;ethaneiodide;Ethyliodid;Ethyljodid;Iodethan CAS:
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Min.Order:1 Kilogram
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Cas:75-03-6
Min.Order:1 Metric Ton
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inquiryChemical Reagent:Iodoethane Molecular Formula:C2H5I Molecular Weight:155.97 Appearance and Properties:A colorless,clear liquid,color changes on being exposed to light,nearly insoluble i
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Iodoethane CAS NO.75-03-6Appearance:powder Storage:Dry and ventilated Package:according to customers' requirements Application:intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect...)or according to y
Product name: Iodethane CAS No.:75-03-6 Molecule Formula:C2H5I Molecule Weight:155.96 Purity: 99% Package: 25kg/drum Description:Colorless clear liquid Manufacture Standards:Enterprise Standard Testing Items
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Cas:75-03-6
Min.Order:1 Kilogram
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Formula: C2H5IMolecular Weight : 155.97 Synonyms: AI3-28593;Ethyl iodide;Ethyljodid;Hydriodic ether;Jodethan;Monoiodoethane;NSC 8825; EINECS: 200-833-1Density: 1.94 g/cm3Melting Point:Boiling Point: 72.8 °C at 760 mmHgFlash Point: 21.1 &d
Cas:75-03-6
Min.Order:0 Metric Ton
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inquiryChangzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
Conditions | Yield |
---|---|
In tetrachloromethane Kinetics; Irradiation (UV/VIS); Kinetics of the reaction of Co(C2H5)(H3CCNOHONCCH3)2(C5H5N) with I2 under irradiation with light at 517 nm is investigated.; MeI and CoI(H3CCNOHONCCH3)2(C5H5N) are the products.; | A n/a B 100% |
ethyl iodide
Conditions | Yield |
---|---|
With iodine In acetonitrile Kinetics; byproducts: {Co(bis(dimethylglyoximato))py(I)}; one-electron oxidn. of Co complex by I2 at 298 K; monitored by (1)H-NMR and UV spect. (361 nm); | 100% |
Conditions | Yield |
---|---|
at 90 - 170℃; for 0.166667h; Arbuzov Reaction; | A n/a B 98% C n/a |
triethyl phosphite
methyl iodide
A
Diethyl methylphosphonate
B
ethyl iodide
Conditions | Yield |
---|---|
at 130℃; for 0.0833333h; Michaelis-Arbuzov reaction; microwave irradiation; | A 97% B n/a |
Conditions | Yield |
---|---|
With iodine In acetonitrile Kinetics; byproducts: I3(1-), {(C2H5)Co(2,2'-bipyridine)2I}(1+); one-electron oxidn. of cis-Co complex by I2 at 298 K; monitored by (1)H-NMR and UV spect. (361 nm); | A <1 B <1 C 97% D 3.2% |
methoxyethene
propargyl alcohol
A
3-(1-methoxy-ethoxy)-propyne
B
ethyl iodide
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid | A 96% B n/a |
iodobenzene
triethyl phosphite
A
diethyl phenylphosphonate
B
ethyl iodide
Conditions | Yield |
---|---|
tetrakis(triethylphosphite)nickel(0) at 160℃; | A 94% B n/a |
at 160℃; Mechanism; var. catalysts, var. temp.; |
diethyl phosphoriodidite
N-(propylidene)-tert-butylamine
A
ethyl iodide
Conditions | Yield |
---|---|
In diethyl ether for 2h; Ambient temperature; | A n/a B 92% |
trimethylsilyl iodide
ethyl acetate
A
trimethylsilyl acetate
B
ethyl iodide
Conditions | Yield |
---|---|
at 100℃; for 0.5h; Mechanism; Product distribution; | A n/a B 92% |
4-vinylbenzyl iodide
triethyl phosphite
A
[(4-ethenylphenyl)methyl]phosphonic acid diethyl ester
B
ethyl iodide
Conditions | Yield |
---|---|
at 20℃; for 6h; | A 91% B n/a |
O,O-diethyl-N-butyl-N-isobutenyl aminophosphite
A
ethyl iodide
Conditions | Yield |
---|---|
With methyl iodide at 20℃; | A 90.5% B 87.1% |
O,O-diethyl-N-butyl-N-isobutenyl aminophosphite
methyl iodide
A
ethyl iodide
Conditions | Yield |
---|---|
at 20℃; | A 90.5% B 87.1% |
Conditions | Yield |
---|---|
In diethyl ether for 2h; Ambient temperature; | A n/a B 90% |
Conditions | Yield |
---|---|
In tetrachloromethane Kinetics; byproducts: C4H10, C2H6; Irradiation (UV/VIS); Kinetics of the reaction of Co(C2H5)2(bipy)2ClO4 with I2 under irradiation with light at 517 nm is investigated.; EtI and Co(C2H5)I(bipy)2ClO4 are the main products, C4H10 and C2H6 are byproducts.; | A n/a B 90% |
Conditions | Yield |
---|---|
In tetrachloromethane Irradiation (UV/VIS); Irradiation at 509 nm in CCl4.; Estimation of the quantum yield of the photochemical reaction. Yield of the products estimated by g.l.c.; | A <1 B 90% C 10% |
Conditions | Yield |
---|---|
With lithium chloride; lithium hexamethyldisilazane In tetrahydrofuran at 0℃; | A 88% B n/a |
3-ethyl-2-methylnaphtho[2,1-d]thiazol-3-ium iodide
A
diethyl ether
B
ethene
C
ethyl iodide
Conditions | Yield |
---|---|
With diethyl sulfate at 100℃; for 0.5h; Product distribution; | A n/a B n/a C n/a D 87% |
With diethyl sulfate at 100℃; for 0.5h; | A n/a B n/a C n/a D 87% |
trimethylsilyl iodide
benzoic acid ethyl ester
A
trimethylsilyl benzoate
B
ethyl iodide
Conditions | Yield |
---|---|
at 100℃; for 0.5h; Mechanism; Product distribution; | A n/a B 86% |
(5S,8R,9S,10S,13R,14S,17R)-3-Ethoxy-17-((1R,4R)-4-ethyl-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene
A
ethyl iodide
B
sitostanol
Conditions | Yield |
---|---|
With Methyltrichlorosilane; sodium iodide In acetonitrile at 25℃; for 36h; | A n/a B 86% |
Conditions | Yield |
---|---|
With Methyltrichlorosilane; sodium iodide In acetonitrile at 25℃; for 8h; | A n/a B 85% |
Conditions | Yield |
---|---|
In dichloromethane-d2 (N2); Re complex in CD2Cl2 was reacted with CH3CN for 24 h; monitored by (1)H- and (31)P-NMR; | A 85% B n/a C n/a D 74% |
trimethylsilyl iodide
ethyl ester of p-toluenesulfonic acid
A
4-Methyl-1-benzolsulfonsaeure-trimethylsilylester
B
ethyl iodide
Conditions | Yield |
---|---|
at 100℃; for 0.5h; Mechanism; Product distribution; | A n/a B 84% |
triethyl trithiophosphite
methyl iodide
A
S,S-diethyl methylphosphonodithiothionate
B
ethyl iodide
Conditions | Yield |
---|---|
at 20℃; for 3600h; | A 64% B 80% |
for 288h; Ambient temperature; | A 59% B n/a |
Conditions | Yield |
---|---|
With 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; sodium iodide In acetone Reflux; | 80% |
2-ethoxy-ethanol
acetyl iodide
A
2-hydroxyethyl acetate
B
ethyl iodide
Conditions | Yield |
---|---|
A 79% B n/a |
Conditions | Yield |
---|---|
With Methyltrichlorosilane; sodium iodide In acetonitrile at 25℃; for 8h; | A 75% B n/a |
Conditions | Yield |
---|---|
With hydrogen iodide at 120℃; for 2h; | 72% |
With iodine; aluminium | |
With phosphorus; iodine |
Conditions | Yield |
---|---|
at 20℃; | A n/a B 71% |
Conditions | Yield |
---|---|
In tetrahydrofuran for 4h; Heating; | 100% |
In dichloromethane for 18h; Heating; | 98% |
In tetrahydrofuran at 20℃; for 1h; Cooling with ice; | 97% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 70℃; for 24h; | 100% |
With potassium carbonate In acetonitrile for 8h; Reflux; | 90% |
With sodium acetate In o-xylene for 3h; Reflux; | 74% |
1-methylquinoline-2(1H)-thione
ethyl iodide
2-ethylthio-1-methylquinolinium iodide
Conditions | Yield |
---|---|
In benzene for 6h; Heating; | 100% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 15h; | 100% |
With sodium hydroxide at 120℃; |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 20℃; for 15h; | 100% |
With sodium hydroxide In ethanol at 20℃; for 15h; | 100% |
With sodium hydroxide In ethanol; water for 72h; | 98% |
ethyl iodide
Dimethyl(phenyl)phosphine
dimethylethylphenylphosphonium iodide
Conditions | Yield |
---|---|
In benzene at 20℃; for 12h; Inert atmosphere; Schlenk technique; | 100% |
glyoxalic acid ethylthioacetal
ethyl iodide
2,2-bis(ethylthio)butanoic acid
Conditions | Yield |
---|---|
With oxonium; potassium hexamethylsilazane In tetrahydrofuran at 25℃; for 2.5h; Product distribution; reactant; | 100% |
(i) HN(SiMe3)2, KH, THF, (ii) /BRN= 505934/, (iii) aq. HCl; Multistep reaction; | |
With hydrogenchloride; potassium hydride; 1,1,1,3,3,3-hexamethyl-disilazane 1.) THF, 0 deg C, 15 min; THF, 25 deg C, 2.5 h.; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile for 2h; Heating; | 100% |
With cesium fluoride In acetonitrile for 1h; Heating; | 99% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In benzene | |
With potassium carbonate In acetone for 16h; Heating; | |
With cesium fluoride In N,N-dimethyl-formamide at 10 - 15℃; for 24h; | 88 % Chromat. |
Conditions | Yield |
---|---|
Stage #1: indole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Inert atmosphere; Stage #2: ethyl iodide for 1h; | 100% |
Stage #1: indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere; Stage #2: ethyl iodide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere; | 98% |
Stage #1: indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 0.5h; Stage #2: ethyl iodide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; | 98% |
2,3-dihydrobenzimidazol-2-thione
ethyl iodide
1-ethyl-2-(ethylthio)-1H-benzo[d]imidazole
Conditions | Yield |
---|---|
With sodium naphthalenide In tetrahydrofuran for 5h; Ambient temperature; | 100% |
1-(tert-butoxycarbonyl)-L-proline
ethyl iodide
(2S)-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester 2-ethyl ester
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 16h; Ambient temperature; | 100% |
With 18-crown-6 ether; potassium carbonate In tetrahydrofuran for 21h; Inert atmosphere; Reflux; |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 72h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide for 0.05h; microwave irradiation; | 90% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 12h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
Stage #1: ortho-methylbenzoic acid With sec.-butyllithium In tetrahydrofuran; 1-hexene; cyclohexane at -78 - 20℃; Stage #2: ethyl iodide In tetrahydrofuran; 1-hexene; cyclohexane at -78 - 20℃; Stage #3: With hydrogenchloride; water In tetrahydrofuran; cyclohexane | 100% |
With sec.-butyllithium In cyclohexane for 8h; Ambient temperature; | 82% |
With sec.-butyllithium 1.) THF, cyclohexane, -78 deg C, 1 h, 2.) THF, cyclohexane, RT, 4 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0℃; for 1h; Stage #2: In tetrahydrofuran at 0℃; | 100% |
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0 - 20℃; Stage #2: With citric acid In water pH=2 - 3; | 100% |
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0 - 20℃; Stage #2: With citric acid In water pH=2 - 3; | 100% |
Conditions | Yield |
---|---|
With silver perchlorate In acetonitrile for 48h; Ambient temperature; | 100% |
methyl (2-nitrophenyl)acetate
ethyl iodide
methyl 2-ethyl-2-(2-nitrophenyl)butanoate
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 4.5h; | 100% |
With potassium tert-butylate; 18-crown-6 ether In tetrahydrofuran 1) -78 deg C to RT, 2 h, 2) -78 deg C; | 76% |
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; zinc In water; acetonitrile for 1h; | 100% |
With dipotassium hydrogenphosphate; zinc In water; acetonitrile for 1h; Product distribution; Further Variations:; Reaction partners; Reagents; Solvents; | 100% |
With sodium tetrahydroborate In acetonitrile for 0.0833333h; pH=7; pH-value; | 100% |
5-hydroxy-5-(trifluoromethyl)imidazolidine-2,4-dione
ethyl iodide
3-Ethyl-5-hydroxy-5-trifluoromethyl-imidazolidine-2,4-dione
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol Ambient temperature; | 100% |
With potassium carbonate In acetone Heating; | 60 % Turnov. |
1-(tert-butoxycarbonylamino)-2,3-difluorobenzene
ethyl iodide
N-(tert-Butoxycarbonyl)-N-ethyl-2,3-difluoroaniline
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide for 2h; | 100% |
ethyl iodide
2-phenyl-4-ethyl-1,3,4-thiadiazol-5(4H)-one
Conditions | Yield |
---|---|
In acetonitrile for 5h; Heating; | 100% |
imidazo[1,5-a]pyridine-3-thiol
ethyl iodide
3-ethylsulfanyl-imidazo[1,5-a]pyridine
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 45℃; | 100% |
With potassium carbonate In acetone at 45℃; for 12h; | |
With potassium carbonate In acetone Inert atmosphere; |
1-benzyl-3-carbethoxy-5-methyl-7-phenyl-1,4-dihydro-4-oxopyrrolo<3,4-b>pyridine
ethyl iodide
1-Benzyl-6-ethyl-5-methyl-4-oxo-7-phenyl-4,6-dihydro-1H-pyrrolo[3,4-b]pyridine-3-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With sodium methylate In N,N-dimethyl-formamide r.t., overnight; | 100% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 6h; | 100% |
With N-ethyl-N,N-diisopropylamine In acetone at 20℃; for 0.333333h; Sonication; | 90% |
With potassium hydroxide In 1,4-dioxane at 70℃; for 1.5h; | 58% |
ethyl iodide
2-methyl-3-trifluoroacetylpyrrole
1-ethyl-3-trifluoroacetyl-2-methylpyrrole
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 40℃; for 20h; | 100% |
ethyl iodide
(S)-2-hydroxy-4-pentenoic acid
(S)-3-hydroxy-4-pentenoic acid ethyl ester
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In N,N-dimethyl-formamide for 5h; | 100% |
ethyl iodide
3-trifluoroacetyl-2-phenylpyrrole
1-ethyl-3-trifluoroacetyl-2-phenylpyrrole
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 70℃; for 20h; | 100% |
Conditions | Yield |
---|---|
With sodium hydride In acetonitrile at 0℃; for 7h; | 100% |
With sodium methylate In methanol for 6h; Reflux; | 97% |
Stage #1: 2-amino-benzenethiol With potassium tert-butylate In ethanol at 0℃; for 0.75h; Stage #2: ethyl iodide In ethanol at 0 - 20℃; for 0.75h; Further stages.; | 85% |
ethyl iodide
Conditions | Yield |
---|---|
In acetonitrile for 0.366667h; | 100% |
ethyl iodide
O,O-diethyltrimethylsilylchloromethylphosphonate α-lithie
(1-Chloro-1-trimethylsilanyl-propyl)-phosphonic acid diethyl ester
Conditions | Yield |
---|---|
In tetrahydrofuran; hexane for 1h; Ambient temperature; | 100% |
ethyl iodide
4,6-dimethyl-1-phenyl-2-oxopyrimidine
4-methyl-1-phenyl-6-propylpyrimidin-2(1H)-one
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide for 1h; | 100% |
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