Iodoethane supplier | CasNO.75-03-6

Name
Ethyl iodide
EINECS 200-833-1
CAS No. 75-03-6
Article Data308
CAS DataBase
Density 1.94 g/cm³
Solubility 4 g/L in water at 20 °C
Melting Point -108 °C
Formula C₂H₅I
Boiling Point 72.8 °C at 760 mmHg
Molecular Weight 155.966
Flash Point 21.1 °C
Transport Information
Appearance Colorless to yellow liquid
Safety 23-26-45-16-36/37/39-27
Risk Codes 20-36/37/38-42/43-10-23/24/25
Molecular Structure
Hazard Symbols Xn,T
Synonyms AI3-28593;Ethyl iodide;Ethyljodid;Hydriodic ether;Jodethan;Monoiodoethane;NSC 8825;
PSA 0.00000
LogP 1.44130

Synthetic route

: [CoEt(dimethylglyoximate(1-))2(pyridine)]

: 7553-56-2
iodine

A: iodobisdimethylglyoximepyridine cobalt(III)

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
In tetrachloromethane Kinetics; Irradiation (UV/VIS); Kinetics of the reaction of Co(C2H5)(H3CCNOHONCCH3)2(C5H5N) with I2 under irradiation with light at 517 nm is investigated.; MeI and CoI(H3CCNOHONCCH3)2(C5H5N) are the products.;	A n/a B 100%

...Expand

: [CoEt(dimethylglyoximate(1-))2(pyridine)]

: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
With iodine In acetonitrile Kinetics; byproducts: {Co(bis(dimethylglyoximato))py(I)}; one-electron oxidn. of Co complex by I2 at 298 K; monitored by (1)H-NMR and UV spect. (361 nm);	100%

: ethyl 4-(diethoxyphosphorylmethyl)-5-(iodomethyl)furan-3-carboxylate

: 122-52-1
triethyl phosphite

A: 78-38-6
ethylphosphonic acid diethyl ester

B: ethyl 4,5-bis-(diethoxyphosphorylmethyl)furan-3-carboxylate

C: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
at 90 - 170℃; for 0.166667h; Arbuzov Reaction;	A n/a B 98% C n/a

...Expand

: 122-52-1
triethyl phosphite

: 74-88-4
methyl iodide

A: 683-08-9
Diethyl methylphosphonate

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
at 130℃; for 0.0833333h; Michaelis-Arbuzov reaction; microwave irradiation;	A 97% B n/a

...Expand

: cis-{(C2H5)2Co(2,2'-bipyridine)2}(ClO4)

A: 74-84-0
ethane

B: 74-85-1
ethene

C: 75-03-6
ethyl iodide

D: 106-97-8
n-butane

Conditions

Conditions	Yield
With iodine In acetonitrile Kinetics; byproducts: I3(1-), {(C2H5)Co(2,2'-bipyridine)2I}(1+); one-electron oxidn. of cis-Co complex by I2 at 298 K; monitored by (1)H-NMR and UV spect. (361 nm);	A <1 B <1 C 97% D 3.2%

...Expand

: 107-25-5
methoxyethene

: 107-19-7
propargyl alcohol

A: 38987-67-6
3-(1-methoxy-ethoxy)-propyne

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
With toluene-4-sulfonic acid	A 96% B n/a

...Expand

: 591-50-4
iodobenzene

: 122-52-1
triethyl phosphite

A: 1754-49-0
diethyl phenylphosphonate

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
tetrakis(triethylphosphite)nickel(0) at 160℃;	A 94% B n/a
at 160℃; Mechanism; var. catalysts, var. temp.;

...Expand

: 20502-50-5
diethyl phosphoriodidite

: 7020-81-7
N-(propylidene)-tert-butylamine

A: 75-03-6
ethyl iodide

B: 1,4-di-tert-butyl-2-ethoxy-3,5-diethyl-1,4,2-diazaphospholidine 2-oxide

Conditions

Conditions	Yield
In diethyl ether for 2h; Ambient temperature;	A n/a B 92%

...Expand

: 16029-98-4
trimethylsilyl iodide

: 141-78-6
ethyl acetate

A: 2754-27-0
trimethylsilyl acetate

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
at 100℃; for 0.5h; Mechanism; Product distribution;	A n/a B 92%

...Expand

: 45817-37-6
4-vinylbenzyl iodide

: 122-52-1
triethyl phosphite

A: 726-61-4
[(4-ethenylphenyl)methyl]phosphonic acid diethyl ester

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
at 20℃; for 6h;	A 91% B n/a

...Expand

: 79948-06-4
O,O-diethyl-N-butyl-N-isobutenyl aminophosphite

A: 75-03-6
ethyl iodide

B: ethyl N-butyl-N-isobutenylamidomethylphosphonate

Conditions

Conditions	Yield
With methyl iodide at 20℃;	A 90.5% B 87.1%

: 79948-06-4
O,O-diethyl-N-butyl-N-isobutenyl aminophosphite

: 74-88-4
methyl iodide

A: 75-03-6
ethyl iodide

B: ethyl N-butyl-N-isobutenylamidomethylphosphonate

Conditions

Conditions	Yield
at 20℃;	A 90.5% B 87.1%

...Expand

: 20502-50-5
diethyl phosphoriodidite

: 622-29-7
N-Benzylidenemethylamine

A: 75-03-6
ethyl iodide

B: 2-ethoxy-1,4-dimethyl-3,5-diphenyl-1,4,2-diazaphospholidine 2-oxide

Conditions

Conditions	Yield
In diethyl ether for 2h; Ambient temperature;	A n/a B 90%

...Expand

: cis-{(C2H5)2Co(2,2'-bipyridine)2}(ClO4)

: 7553-56-2
iodine

: cis-ethyl iodo bis(2,2'-bipyridyl) cobalt(III) perchlorate

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
In tetrachloromethane Kinetics; byproducts: C4H10, C2H6; Irradiation (UV/VIS); Kinetics of the reaction of Co(C2H5)2(bipy)2ClO4 with I2 under irradiation with light at 517 nm is investigated.; EtI and Co(C2H5)I(bipy)2ClO4 are the main products, C4H10 and C2H6 are byproducts.;	A n/a B 90%

...Expand

: cis-{Et2Co(bpy)2}(1+)

: 7553-56-2
iodine

A: 74-84-0
ethane

B: 75-03-6
ethyl iodide

C: 106-97-8
n-butane

Conditions

Conditions	Yield
In tetrachloromethane Irradiation (UV/VIS); Irradiation at 509 nm in CCl4.; Estimation of the quantum yield of the photochemical reaction. Yield of the products estimated by g.l.c.;	A <1 B 90% C 10%

...Expand

: C26H39NO5Si

A: C28H43NO5Si

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
With lithium chloride; lithium hexamethyldisilazane In tetrahydrofuran at 0℃;	A 88% B n/a

: 54581-48-5
3-ethyl-2-methylnaphtho[2,1-d]thiazol-3-ium iodide

A: 60-29-7
diethyl ether

B: 74-85-1
ethene

C: 75-03-6
ethyl iodide

D: 2-methyl-3-ethylnaphtho<2,1-d>thiazolium bisulfate

Conditions

Conditions	Yield
With diethyl sulfate at 100℃; for 0.5h; Product distribution;	A n/a B n/a C n/a D 87%
With diethyl sulfate at 100℃; for 0.5h;	A n/a B n/a C n/a D 87%

...Expand

: 16029-98-4
trimethylsilyl iodide

: 93-89-0
benzoic acid ethyl ester

A: 2078-12-8
trimethylsilyl benzoate

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
at 100℃; for 0.5h; Mechanism; Product distribution;	A n/a B 86%

...Expand

: 78371-07-0
(5S,8R,9S,10S,13R,14S,17R)-3-Ethoxy-17-((1R,4R)-4-ethyl-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene

A: 75-03-6
ethyl iodide

B: 204638-28-8
sitostanol

Conditions

Conditions	Yield
With Methyltrichlorosilane; sodium iodide In acetonitrile at 25℃; for 36h;	A n/a B 86%

: 932-92-3
cyclohexyl ethyl ether

A: 75-03-6
ethyl iodide

B: 108-93-0
cyclohexanol

Conditions

Conditions	Yield
With Methyltrichlorosilane; sodium iodide In acetonitrile at 25℃; for 8h;	A n/a B 85%

: {(η5-C5H5)Re(NO)(PPh3)(IC2H5)}BF4

: 75-05-8
acetonitrile

A: {(η5-C5H5)Re(NO)(PPh3)(NCCH3)}BF4

: (RR,SS)-{(η5-C5H5)Re(NO)(PPh3)}2I(BF4)

: (SS,RR)-{(η5-C5H5)Re(NO)(PPh3)}2Cl(BF4)

D: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
In dichloromethane-d2 (N2); Re complex in CD2Cl2 was reacted with CH3CN for 24 h; monitored by (1)H- and (31)P-NMR;	A 85% B n/a C n/a D 74%

...Expand

: 16029-98-4
trimethylsilyl iodide

: 80-40-0
ethyl ester of p-toluenesulfonic acid

A: 17872-98-9
4-Methyl-1-benzolsulfonsaeure-trimethylsilylester

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
at 100℃; for 0.5h; Mechanism; Product distribution;	A n/a B 84%

...Expand

: 688-62-0
triethyl trithiophosphite

: 74-88-4
methyl iodide

A: 31650-57-4
S,S-diethyl methylphosphonodithiothionate

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
at 20℃; for 3600h;	A 64% B 80%
for 288h; Ambient temperature;	A 59% B n/a

...Expand

: 121-44-8
triethylamine

: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
With 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; sodium iodide In acetone Reflux;	80%

: 110-80-5
2-ethoxy-ethanol

: 507-02-8
acetyl iodide

A: 542-59-6
2-hydroxyethyl acetate

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
	A 79% B n/a

...Expand

: 77067-57-3
4-Ethoxy-octane

A: 589-62-8
octan-4-ol

B: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
With Methyltrichlorosilane; sodium iodide In acetonitrile at 25℃; for 8h;	A 75% B n/a

: 64-17-5
ethanol

: 75-03-6
ethyl iodide

Conditions

Conditions	Yield
With hydrogen iodide at 120℃; for 2h;	72%
With iodine; aluminium
With phosphorus; iodine

: 507-02-8
acetyl iodide

: 103-73-1
Phenetole

A: 75-03-6
ethyl iodide

B: 122-79-2
Phenyl acetate

Conditions

Conditions	Yield
at 20℃;	A n/a B 71%

...Expand

: 616-47-7
1-methyl-1H-imidazole

: 75-03-6
ethyl iodide

: 35935-34-3
1-ethyl-3-methylimidazolium iodide

Conditions

Conditions	Yield
In tetrahydrofuran for 4h; Heating;	100%
In dichloromethane for 18h; Heating;	98%
In tetrahydrofuran at 20℃; for 1h; Cooling with ice;	97%

: 51-17-2
benzoimidazole

: 75-03-6
ethyl iodide

: 24351-22-2
1,3-diethyl-1H-benzo[d]imidazol-3-ium iodide

Conditions

Conditions	Yield
With potassium carbonate In acetonitrile at 70℃; for 24h;	100%
With potassium carbonate In acetonitrile for 8h; Reflux;	90%
With sodium acetate In o-xylene for 3h; Reflux;	74%

: 4800-27-5
1-methylquinoline-2(1H)-thione

: 75-03-6
ethyl iodide

: 95875-55-1
2-ethylthio-1-methylquinolinium iodide

Conditions

Conditions	Yield
In benzene for 6h; Heating;	100%

: 104-94-9
4-methoxy-aniline

: 75-03-6
ethyl iodide

: 15144-80-6
N,N-diethyl-4-methoxyaniline

Conditions

Conditions	Yield
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 15h;	100%
With sodium hydroxide at 120℃;

: 75-03-6
ethyl iodide

: 147-93-3
Thiosalicylic acid

: 21101-79-1
2-ethylsulfanylbenzoic acid

Conditions

Conditions	Yield
With sodium hydroxide In ethanol at 20℃; for 15h;	100%
With sodium hydroxide In ethanol at 20℃; for 15h;	100%
With sodium hydroxide In ethanol; water for 72h;	98%

: 75-03-6
ethyl iodide

: 672-66-2
Dimethyl(phenyl)phosphine

: 72153-49-2
dimethylethylphenylphosphonium iodide

Conditions

Conditions	Yield
In benzene at 20℃; for 12h; Inert atmosphere; Schlenk technique;	100%

: 10490-06-9
glyoxalic acid ethylthioacetal

: 75-03-6
ethyl iodide

: 71535-44-9
2,2-bis(ethylthio)butanoic acid

Conditions

Conditions	Yield
With oxonium; potassium hexamethylsilazane In tetrahydrofuran at 25℃; for 2.5h; Product distribution; reactant;	100%
(i) HN(SiMe3)2, KH, THF, (ii) /BRN= 505934/, (iii) aq. HCl; Multistep reaction;
With hydrogenchloride; potassium hydride; 1,1,1,3,3,3-hexamethyl-disilazane 1.) THF, 0 deg C, 15 min; THF, 25 deg C, 2.5 h.; Yield given. Multistep reaction;

: 480-63-7
mesitylenecarboxylic acid

: 75-03-6
ethyl iodide

: 1754-55-8
ethyl 2,4,6-trimethylbenzoate

Conditions

Conditions	Yield
With caesium carbonate In acetonitrile for 2h; Heating;	100%
With cesium fluoride In acetonitrile for 1h; Heating;	99%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In benzene
With potassium carbonate In acetone for 16h; Heating;
With cesium fluoride In N,N-dimethyl-formamide at 10 - 15℃; for 24h;	88 % Chromat.

: 120-72-9
indole

: 75-03-6
ethyl iodide

: 10604-59-8
N-Ethylindole

Conditions

Conditions	Yield
Stage #1: indole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Inert atmosphere; Stage #2: ethyl iodide for 1h;	100%
Stage #1: indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere; Stage #2: ethyl iodide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere;	98%
Stage #1: indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 0.5h; Stage #2: ethyl iodide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃;	98%

: 583-39-1
2,3-dihydrobenzimidazol-2-thione

: 75-03-6
ethyl iodide

: 124530-66-1
1-ethyl-2-(ethylthio)-1H-benzo[d]imidazole

Conditions

Conditions	Yield
With sodium naphthalenide In tetrahydrofuran for 5h; Ambient temperature;	100%

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 75-03-6
ethyl iodide

: 135097-23-3
(2S)-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester 2-ethyl ester

Conditions

Conditions	Yield
With potassium carbonate In acetone for 16h; Ambient temperature;	100%
With 18-crown-6 ether; potassium carbonate In tetrahydrofuran for 21h; Inert atmosphere; Reflux;

: 91-56-5
indole-2,3-dione

: 75-03-6
ethyl iodide

: 4290-94-2
N-ethylisatin

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 72h;	100%
With potassium carbonate In N,N-dimethyl-formamide for 0.05h; microwave irradiation;	90%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 12h; Inert atmosphere;	90%

: 118-90-1
ortho-methylbenzoic acid

: 75-03-6
ethyl iodide

: 2438-03-1
2-(n-Propyl)-benzoesaeure

Conditions

Conditions	Yield
Stage #1: ortho-methylbenzoic acid With sec.-butyllithium In tetrahydrofuran; 1-hexene; cyclohexane at -78 - 20℃; Stage #2: ethyl iodide In tetrahydrofuran; 1-hexene; cyclohexane at -78 - 20℃; Stage #3: With hydrogenchloride; water In tetrahydrofuran; cyclohexane	100%
With sec.-butyllithium In cyclohexane for 8h; Ambient temperature;	82%
With sec.-butyllithium 1.) THF, cyclohexane, -78 deg C, 1 h, 2.) THF, cyclohexane, RT, 4 h; Yield given. Multistep reaction;

: 4530-20-5
BOC-glycine

: 75-03-6
ethyl iodide

: 149794-10-5
N-(tert-buytoxycarbonyl)-N-ethylglycine

Conditions

Conditions	Yield
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0℃; for 1h; Stage #2: In tetrahydrofuran at 0℃;	100%
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0 - 20℃; Stage #2: With citric acid In water pH=2 - 3;	100%
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0 - 20℃; Stage #2: With citric acid In water pH=2 - 3;	100%

: 139-66-2
diphenyl sulfide

: 75-03-6
ethyl iodide

: 10504-65-1
diphenylethylsulfonium perchlorate

Conditions

Conditions	Yield
With silver perchlorate In acetonitrile for 48h; Ambient temperature;	100%

: 30095-98-8
methyl (2-nitrophenyl)acetate

: 75-03-6
ethyl iodide

: 136764-89-1
methyl 2-ethyl-2-(2-nitrophenyl)butanoate

Conditions

Conditions	Yield
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 4.5h;	100%
With potassium tert-butylate; 18-crown-6 ether In tetrahydrofuran 1) -78 deg C to RT, 2 h, 2) -78 deg C;	76%

: 1666-13-3
diphenyl diselenide

: 75-03-6
ethyl iodide

: 17774-38-8
ethyl phenyl selenide

Conditions

Conditions	Yield
With dipotassium hydrogenphosphate; zinc In water; acetonitrile for 1h;	100%
With dipotassium hydrogenphosphate; zinc In water; acetonitrile for 1h; Product distribution; Further Variations:; Reaction partners; Reagents; Solvents;	100%
With sodium tetrahydroborate In acetonitrile for 0.0833333h; pH=7; pH-value;	100%

: 105480-41-9
5-hydroxy-5-(trifluoromethyl)imidazolidine-2,4-dione

: 75-03-6
ethyl iodide

: 105480-43-1
3-Ethyl-5-hydroxy-5-trifluoromethyl-imidazolidine-2,4-dione

Conditions

Conditions	Yield
With sodium ethanolate In ethanol Ambient temperature;	100%
With potassium carbonate In acetone Heating;	60 % Turnov.

: 129589-65-7
1-(tert-butoxycarbonylamino)-2,3-difluorobenzene

: 75-03-6
ethyl iodide

: 129589-69-1
N-(tert-Butoxycarbonyl)-N-ethyl-2,3-difluoroaniline

Conditions

Conditions	Yield
With sodium hydride In N,N-dimethyl-formamide for 2h;	100%

: sel de potassium de la 2-phenyl-1,3,4-oxadiazol-5(4H)-one

: 75-03-6
ethyl iodide

: 82476-09-3
2-phenyl-4-ethyl-1,3,4-thiadiazol-5(4H)-one

Conditions

Conditions	Yield
In acetonitrile for 5h; Heating;	100%

: 76259-00-2
imidazo[1,5-a]pyridine-3-thiol

: 75-03-6
ethyl iodide

: 76266-04-1
3-ethylsulfanyl-imidazo[1,5-a]pyridine

Conditions

Conditions	Yield
With potassium carbonate In acetone at 45℃;	100%
With potassium carbonate In acetone at 45℃; for 12h;
With potassium carbonate In acetone Inert atmosphere;

: 100856-26-6
1-benzyl-3-carbethoxy-5-methyl-7-phenyl-1,4-dihydro-4-oxopyrrolo<3,4-b>pyridine

: 75-03-6
ethyl iodide

: 100856-34-6
1-Benzyl-6-ethyl-5-methyl-4-oxo-7-phenyl-4,6-dihydro-1H-pyrrolo[3,4-b]pyridine-3-carboxylic acid ethyl ester

Conditions

Conditions	Yield
With sodium methylate In N,N-dimethyl-formamide r.t., overnight;	100%

: 75-03-6
ethyl iodide

: 149-30-4
2-Mercaptobenzothiazole

: 2757-92-8
2-(ethylthio)benzothiazole

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 20℃; for 6h;	100%
With N-ethyl-N,N-diisopropylamine In acetone at 20℃; for 0.333333h; Sonication;	90%
With potassium hydroxide In 1,4-dioxane at 70℃; for 1.5h;	58%

: 75-03-6
ethyl iodide

: 142991-74-0
2-methyl-3-trifluoroacetylpyrrole

: 144219-84-1
1-ethyl-3-trifluoroacetyl-2-methylpyrrole

Conditions

Conditions	Yield
With potassium hydroxide In dimethyl sulfoxide at 40℃; for 20h;	100%

: 75-03-6
ethyl iodide

: 38996-05-3
(S)-2-hydroxy-4-pentenoic acid

: 349649-09-8
(S)-3-hydroxy-4-pentenoic acid ethyl ester

Conditions

Conditions	Yield
With sodium hydrogencarbonate In N,N-dimethyl-formamide for 5h;	100%

: 75-03-6
ethyl iodide

: 144219-80-7
3-trifluoroacetyl-2-phenylpyrrole

: 144219-86-3
1-ethyl-3-trifluoroacetyl-2-phenylpyrrole

Conditions

Conditions	Yield
With potassium hydroxide In dimethyl sulfoxide at 70℃; for 20h;	100%

: 75-03-6
ethyl iodide

: 137-07-5
2-amino-benzenethiol

: 13920-91-7
2-(ethylthio)aniline

Conditions

Conditions	Yield
With sodium hydride In acetonitrile at 0℃; for 7h;	100%
With sodium methylate In methanol for 6h; Reflux;	97%
Stage #1: 2-amino-benzenethiol With potassium tert-butylate In ethanol at 0℃; for 0.75h; Stage #2: ethyl iodide In ethanol at 0 - 20℃; for 0.75h; Further stages.;	85%

: 75-03-6
ethyl iodide

: C10H21N4PS2

: 1-Ethylsulfanylthiocarbonyl-2,8,9-trimethyl-2,5,8,9-tetraaza-1-phosphonia-bicyclo[3.3.3]undecane; iodide

Conditions

Conditions	Yield
In acetonitrile for 0.366667h;	100%

: 75-03-6
ethyl iodide

: 176100-94-0
O,O-diethyltrimethylsilylchloromethylphosphonate α-lithie

: 118512-68-8
(1-Chloro-1-trimethylsilanyl-propyl)-phosphonic acid diethyl ester

Conditions

Conditions	Yield
In tetrahydrofuran; hexane for 1h; Ambient temperature;	100%

: 75-03-6
ethyl iodide

: 21139-18-4
4,6-dimethyl-1-phenyl-2-oxopyrimidine

: 61404-63-5
4-methyl-1-phenyl-6-propylpyrimidin-2(1H)-one

Conditions

Conditions	Yield
With sodium hydride In N,N-dimethyl-formamide for 1h;	100%

Iodoethane Consensus Reports

Reported in EPA TSCA Inventory.

Iodoethane Specification

The Ethane, iodo-, with the CAS registry number 75-03-6, is also known as Monoiodoethane. Its EINECS number is 200-833-1. This chemical's molecular formula is C₂H₅I and molecular weight is 155.97. What's more, its systematic name is iodoethane. Its classification code is Mutation data. Ethyl iodide is very good with alkylation reactions. It is used as organic reagents and pharmaceutical intermediates. It is also used as the hydrogen radical promoter. It should be sealed and stored in a cool, ventilated and dry place. Moreover, it should be protected from light, heat and fire.

Physical properties of Ethane, iodo- are: (1)ACD/LogP: 2.03; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): 2.03; (4)ACD/LogD (pH 7.4): 2.03; (5)ACD/BCF (pH 5.5): 20.48; (6)ACD/BCF (pH 7.4): 20.48; (7)ACD/KOC (pH 5.5): 302.23; (8)ACD/KOC (pH 7.4): 302.23; (9)Index of Refraction: 1.516; (10)Molar Refractivity: 24.28 cm³; (11)Molar Volume: 80.3 cm³; (12)Polarizability: 9.62×10^-24cm³; (13)Surface Tension: 28.5 dyne/cm; (14)Density: 1.94 g/cm³; (15)Flash Point: 21.1 °C; (16)Enthalpy of Vaporization: 29.44 kJ/mol; (17)Boiling Point: 72.8 °C at 760 mmHg; (18)Vapour Pressure: 128 mmHg at 25°C.

Preparation: this chemical can be prepared by ethanol and PI₃ by heating and reflux.

2P + 3I₂→ 2PI₃

3C₂H₅OH + PI₃ →3CH₃CH₂I + H₃PO₄

Uses of Ethane, iodo-: it can be used to produce 1-ethyl-3-nitro-2-phenyl-indole by heating. It will need reagent Na and solvent ethanol with the reaction time of 2 hours. The yield is about 59%.

Ethane, iodo- can be used to produce 1-ethyl-3-nitro-2-phenyl-indole by heating

When you are using this chemical, please be cautious about it as the following:
This chemical is flammable, so you should keep it away from sources of ignition - No smoking. It is harmful by inhalation. It is toxic by inhalation, in contact with skin and if swallowed. It is irritating to eyes, respiratory system and skin. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. You must not breathe gas/fumes/vapour/spray (appropriate wording to be specified by the manufacturer). You should take off immediately all contaminated clothing. When using it, you need wear suitable protective clothing, gloves and eye/face protection. In case of accident or if you feel unwell, you must seek medical advice immediately (show the label where possible).

You can still convert the following datas into molecular structure:
(1)InChI: InChI=1S/C2H5I/c1-2-3/h2H2,1H3
(2)InChIKey: HVTICUPFWKNHNG-UHFFFAOYSA-N
(3)Canonical SMILES: CCI

The toxicity data is as follows:

Organism	Test Type	Route	Reported Dose (Normalized Dose)	Effect	Source
guinea pig	LD50	intraperitoneal	322mg/kg (322mg/kg)		"Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects, GKNT, 1982Vol. -, Pg. 68, 1982.
mouse	LD50	intraperitoneal	560mg/kg (560mg/kg)		"Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects, GKNT, 1982Vol. -, Pg. 68, 1982.
mouse	LD50	subcutaneous	1gm/kg (1000mg/kg)	PERIPHERAL NERVE AND SENSATION: FLACCID PARALYSIS WITHOUT ANESTHESIA (USUALLY NEUROMUSCULAR BLOCKAGE) LUNGS, THORAX, OR RESPIRATION: RESPIRATORY STIMULATION LUNGS, THORAX, OR RESPIRATION: OTHER CHANGES	Japanese Journal of Pharmacology. Vol. 3, Pg. 99, 1954.
rabbit	LDLo	oral	300mg/kg (300mg/kg)		"Patty's Industrial Hygiene and Toxicology," 3rd rev. ed., Clayton, G.D., and F.E. Clayton, eds., New York, John Wiley & Sons, Inc., 1978-82. Vol. 3 originally pub. in 1979; pub. as 2n rev. ed. in 1985.Vol. 2B, Pg. 3487, 1981.
rat	LC50	inhalation	65gm/m³/30M (65000mg/m³)		Fiziologicheski Aktivnye Veshchestva. Physiologically Active Substances. Vol. 7, Pg. 35, 1975.
rat	LD50	intraperitoneal	330mg/kg (330mg/kg)		"Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects, GKNT, 1982Vol. -, Pg. 68, 1982.

Product Name

Ethyl iodide

Synthetic route

Iodoethane Consensus Reports

Iodoethane Specification

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