DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:147-93-3
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:147-93-3
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inquiryItems Standard Result Appearance Light yellow powder or granular Light yellow granular Melting Point
Cas:147-93-3
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:147-93-3
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Cas:147-93-3
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inquiryFactory price Thiosalicylic acid CAS 147-93-3 in stock Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediates (Fluorene,Carb
Cas:147-93-3
Min.Order:1 Gram
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:white or off-white powder Storage:Store in sealed containers
Cas:147-93-3
Min.Order:100 Gram
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inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
Cas:147-93-3
Min.Order:100 Kilogram
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Type:Lab/Research institutions
inquiryThiosalicylic acid CAS:147-93-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed
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Min.Order:1 Gram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryOur company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Cas:147-93-3
Min.Order:1 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:147-93-3
Min.Order:10 Gram
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Product name: Thiosalicylic Acid CAS No.:147-93-3 Molecule Formula:C7H4O2S Molecule Weight:152.17 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:147-93-3
Min.Order:1 Kilogram
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryConditions | Yield |
---|---|
Stage #1: 2-Iodobenzoic acid With copper(l) iodide; potassium carbonate; sulfur In N,N-dimethyl-formamide at 90℃; for 12h; Inert atmosphere; Stage #2: With sodium tetrahydroborate In N,N-dimethyl-formamide at 40℃; Inert atmosphere; Cooling with ice; | 88% |
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen iodide; hypophosphorous acid for 3h; Heating; | 85% |
With hydrogenchloride; diphenylphosphinopolystyrene In tetrahydrofuran for 7h; Heating; | 73% |
With tin; acetic acid weiteres Reagens: konz. Salzsaeure; |
2-phenylbenzo[d]-1,3-oxathiin-4-one
sodium phenoxide
A
diphenyl 2,2'-disulfanediyldibenzoate
B
benzaldehyde
C
Thiosalicylic acid
Conditions | Yield |
---|---|
In benzene for 9h; Heating; | A 51% B n/a C n/a |
2-phenylbenzo[d]-1,3-oxathiin-4-one
sodium ethanolate
A
bis(2-ethoxycarbonylphenyl) disulfide
B
benzaldehyde
C
Thiosalicylic acid
Conditions | Yield |
---|---|
In benzene for 9h; Heating; | A 46% B n/a C n/a |
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline; potassium thioacetate In toluene at 100℃; for 24h; Schlenk technique; Inert atmosphere; | A 27% B 10% |
2-thiocyanatobenzoic acid
Thiosalicylic acid
Conditions | Yield |
---|---|
With sodium sulfide |
Conditions | Yield |
---|---|
With acetic acid; zinc |
1-thioflavone
sodium ethanolate
A
2,2'-dithiobenzoic acid
B
1-(2-mercaptophenyl)ethan-1-one
C
Thiosalicylic acid
D
acetophenone
o-Carboxybenzenediazonium
Thiosalicylic acid
Conditions | Yield |
---|---|
With alkali polysulfide Behandeln der sodaalkalischen Loesung mit Eisen oder Zinkstaub; |
Conditions | Yield |
---|---|
Irradiation; |
3-(3-oxo-3H-benzo[b]thiophen-2-ylidene)-1,3-dihydro-indol-2-one
sodium ethanolate
A
3-formyloxindole
B
Thiosalicylic acid
2-benzoylimino-benzo[b]thiophen-3-one
Thiosalicylic acid
o-(hydroxysulfinyl)benzoic acid
Thiosalicylic acid
Conditions | Yield |
---|---|
With water; zinc weiteres Reagens: Salzsaeure; | |
With ethanol; zinc weiteres Reagens: Salzsaeure; |
2-but-2t-enylmercapto-benzoic acid
B
2-Ethyl-2,3-dihydrobenzothiophene
C
Thiosalicylic acid
Conditions | Yield |
---|---|
at 250℃; |
2-(1,3-dioxo-indan-2-ylidene)-benzo[b]thiophen-3-one
A
2-formylindane-1,3-dione
B
Thiosalicylic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water; sodium nitrite Erwaermen des Reaktionsprodukts mit aethanol. Kalilauge; |
tetrachloromethane
thiophenol
A
Thiosalicylic acid
B
diphenyldisulfane
Conditions | Yield |
---|---|
With potassium hydroxide at 100 - 110℃; im Rohr; |
Conditions | Yield |
---|---|
Irradiation; |
Conditions | Yield |
---|---|
hydroxide In water; dimethyl sulfoxide at 25℃; Rate constant; elimination; |
Conditions | Yield |
---|---|
With n-butyllithium; N,N,N,N,-tetramethylethylenediamine 1.) cyclohexane, hexane, 0 deg C, 30 min, r.t., 22 h, 2.) cyclohexane, 0 deg C, 30 min, r.t., 24 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane; water at 30℃; Kinetics; Rate constant; Mechanism; other temperature, other pH; |
Thiosalicylic acid
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane; water at 30℃; further temperature; |
Thiosalicylic acid
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane; water at 30℃; further temperature; | |
With sodium hydroxide In 1,4-dioxane; water at 30℃; Kinetics; Rate constant; Mechanism; other temperature, other pH; |
Conditions | Yield |
---|---|
2-amino-2-hydroxymethyl-1,3-propanediol In water; dimethyl sulfoxide at 25℃; Rate constant; other base; |
Thiosalicylic acid
Conditions | Yield |
---|---|
With buffer (pH=11) at 20℃; | |
With buffer (pH=11) at 20℃; Rate constant; |
ortho-chlorobenzoic acid
A
2,2'-dithiobenzoic acid
B
Thiosalicylic acid
C
benzoic acid
D
salicylic acid
Conditions | Yield |
---|---|
With sulfur In melt at 270℃; Product distribution; effect of various molten salts, amount of sulfur, molar ratio of sulfur to molten salts, composition of molten salt and various mercaptylation agents; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; sulfur 1.) 270 deg C, NaOH-KOH melt, 3 min.; 2.) water; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
Yield given. Multistep reaction; | |
With hydrogenchloride; sodium disulfide; acetic acid; zinc; sodium nitrite Multistep reaction; | |
Multi-step reaction with 2 steps 1.1: hydrogenchloride; sodium nitrite / water 1.2: 80 °C 2.1: hydrogenchloride; sodium hydroxide; sodium dithionite / water View Scheme |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 20℃; for 15h; | 100% |
With sodium hydroxide In ethanol at 20℃; for 15h; | 100% |
With sodium hydroxide In ethanol; water for 72h; | 98% |
Conditions | Yield |
---|---|
With boric acid In water at 100℃; for 0.25h; Heating / reflux; | 100% |
Conditions | Yield |
---|---|
With sulfuric acid In toluene for 6h; Heating / reflux; | 100% |
Conditions | Yield |
---|---|
With potassium hydroxide; copper In water Heating; | 100% |
Thiosalicylic acid
p-methoxybenzyl chloride
2-(4-methoxy-benzylsulfanyl)-benzoic acid
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 10h; Heating; | 99.7% |
Thiosalicylic acid
α-bromoacetophenone
2-[(2-oxo-2-phenylethyl)thio]-benzoic acid
Conditions | Yield |
---|---|
With sodium acetate In methanol at 20℃; for 1h; | 99.1% |
With potassium hydroxide In ethanol for 2h; Heating; | 39.9% |
Stage #1: Thiosalicylic acid; α-bromoacetophenone With potassium hydroxide In ethanol for 2h; Inert atmosphere; Reflux; Stage #2: With hydrogenchloride In ethanol; water Cooling with ice; |
Conditions | Yield |
---|---|
With xenon difluoride In dichloromethane at 25℃; | 99% |
With 1-oxa-2-azaspiro[2.5]octane In toluene | 99% |
With polyvinylpolypyrrolidonium tribromide In ethanol at 20℃; for 1.5h; Green chemistry; | 99% |
Thiosalicylic acid
1-Bromo-2-bromomethyl-benzene
2‑(2‑bromobenzylsulfanyl)benzoic acid
Conditions | Yield |
---|---|
With potassium carbonate In water; acetone for 8h; Reflux; Inert atmosphere; | 99% |
With potassium hydroxide In ethanol; water at 50 - 60℃; for 4h; | 8 g |
Conditions | Yield |
---|---|
With sodium hydroxide for 1h; Ambient temperature; | 99% |
3-phenyl-5-chloro-4-chloromethyl-1-methyl-1H-pyrazole
Thiosalicylic acid
2-(3-phenyl-5-chloro-1-methyl-1H-pyrazol-4-ylmethylsulphanyl)benzoic acid
Conditions | Yield |
---|---|
Stage #1: 3-phenyl-5-chloro-4-chloromethyl-1-methyl-1H-pyrazole; Thiosalicylic acid With potassium carbonate In ethanol; water for 2h; Heating / reflux; Stage #2: With hydrogenchloride In water pH=2; | 99% |
Conditions | Yield |
---|---|
Stage #1: Thiosalicylic acid With sodium hydroxide In methanol; water at 20℃; for 0.333333h; Stage #2: isopropyl bromide In methanol; water at 70℃; | 99% |
With potassium carbonate In ethanol at 78℃; for 12h; | 46% |
With potassium hydroxide In ethanol for 6h; | 30% |
N-Benzylidenemethylamine
Thiosalicylic acid
3-methyl-2-phenyl-2H-benzo[e][1,3]thiazin-4(3H)-one
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In toluene at 90℃; for 20h; Inert atmosphere; | 99% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In toluene at 90℃; for 20h; | 99% |
p-nitrobenzene iodide
Thiosalicylic acid
2-((4-nitrophenyl)thio)benzoic acid
Conditions | Yield |
---|---|
With [Ce((L)-proline)2]2(oxalate); potassium carbonate In ethanol at 80℃; for 6h; | 99% |
Thiosalicylic acid
Conditions | Yield |
---|---|
With chlorine | 98.5% |
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile) In xylene | 98% |
2,4-dichloro-N-hydroxybenzenecarboximidoyl chloride
Thiosalicylic acid
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran Ambient temperature; | 98% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; for 2h; | 98% |
With potassium carbonate In acetone at 25℃; for 1h; | 97% |
Stage #1: Thiosalicylic acid With potassium carbonate In acetone Stage #2: methyl iodide In acetone at 20℃; for 1h; | 96% |
Conditions | Yield |
---|---|
With potassium carbonate; copper In water at 130 - 140℃; for 3h; Product distribution / selectivity; Ullmann Condensation; | 98% |
With copper; potassium carbonate In water at 130 - 140℃; for 3h; | 96% |
With potassium carbonate In water | 52.8 g (97%) |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 3h; | 98% |
With lithium aluminium tetrahydride | 97% |
With lithium aluminium tetrahydride In tetrahydrofuran; diethyl ether for 1h; | 96% |
Aliquat 336
Thiosalicylic acid
tricaprylmethylammonium thiosalicylate
Conditions | Yield |
---|---|
With sodium hydroxide at 60℃; for 4h; | 98% |
With sodium hydroxide In water at 40℃; for 4h; Inert atmosphere; | 98% |
1,3-bis-(diphenylphosphino)propane
nickel(II) acetate tetrahydrate
Thiosalicylic acid
[Ni(SC6H4CO2)(C27H26P2)]
Conditions | Yield |
---|---|
With pyridine In methanol dissoln. of the Ni salt and the ligand in MeOH with warming, addn. of thiosalicylic acid, then pyridine, short reflux; filtration, washing (cold MeOH; Et2O), drying, recrystn. (CH2Cl2/Et2O); elem. anal.; | 98% |
pyridine
dichloro( 1,5-cyclooctadiene)platinum(ll)
sodium tetraphenyl borate
Thiosalicylic acid
triphenylphosphine
[(triphenylphosphine)2Pt(thiosalicylate)...pyridinium][tetraphenylborate]
Conditions | Yield |
---|---|
In methanol mixt. (PtCl2(cod)), PPh3, thiosalicylic acid, and pyridine in MeOH was heated to reflux for 10 min, Na(BPh4) was added to refluxing soln.; elem. anal.; | 98% |
Conditions | Yield |
---|---|
Stage #1: tris-(trifluoroacetylacetonato)iron(III); Thiosalicylic acid In ethylene glycol at 120℃; Inert atmosphere; Stage #2: With hydrogenchloride In water; ethylene glycol at 20℃; Inert atmosphere; | 98% |
2-ethynylpyridine
Thiosalicylic acid
2-(pyridin-2-ylmethyl)-4H-3,1-benzoxathiin-4-one
Conditions | Yield |
---|---|
With palladium diacetate In toluene at 120℃; for 1h; Inert atmosphere; regioselective reaction; | 98% |
Conditions | Yield |
---|---|
Stage #1: Thiosalicylic acid With trichloroisocyanuric acid In acetonitrile at -20℃; Green chemistry; Stage #2: 3-mercaptopropionic acid In acetonitrile at -20℃; for 0.0833333h; Green chemistry; | 98% |
With trichloroisocyanuric acid In acetonitrile at -20℃; for 0.0833333h; | 97.8% |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; iron(II) acetylacetonate In toluene at 120℃; for 16h; Inert atmosphere; Glovebox; | 98% |
With potassium phosphate In toluene at 110℃; for 20h; Inert atmosphere; Schlenk technique; Green chemistry; | 90% |
1-(tert-butyl)-4-(3,3,3-trifluoroprop-1-yn-1-yl)-benzene
Thiosalicylic acid
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; iron(II) acetylacetonate In toluene at 120℃; for 16h; Inert atmosphere; Glovebox; | 98% |
Conditions | Yield |
---|---|
With sodium acetate In methanol at 23℃; for 0.5h; | 98% |
With sodium acetate In methanol at 23℃; for 0.5h; |
2-Mercaptopyridine
Thiosalicylic acid
2-(pyridin-2-yl-disulfanyl) benzoic acid
Conditions | Yield |
---|---|
With thionyl chloride | 98% |
With thionyl chloride In chloroform at 20℃; for 1h; | 82.4% |
Conditions | Yield |
---|---|
Stage #1: Thiosalicylic acid With sodium hydroxide In water Stage #2: mercury dichloride In water at 20℃; for 3h; | 98% |
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