Product Description Product website: http://www.finerchem.com/pro01en/id/763.html Product Name Sodium tetraphenylboron CAS No. 143
Cas:143-66-8
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inquirySodium tetraphenylboron Basic information Product Name: Sodium tetraphenylboron Synonyms: Borate(1-),tetraphenyl-,sodium;kariporuk;sodiumtetraphenylborate(1-)
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inquiryName: Sodium tetraphenylborate Molecular Formula:C24H20BNa Molecular Weight:342.24 CAS No.:143-66-8 Appearance:Similar White Powder Appearance:Similar White Powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Appl
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inquirysodium tetraphenyl borate
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate anschliessendes Behandeln mit H2O und NaCl; | |
With sodium tetrafluoroborate; diethyl ether anschliessendes Behandeln mit wss.NaCl; |
Conditions | Yield |
---|---|
With sodium tetraethylborate In xylene Heating; |
Conditions | Yield |
---|---|
In acetone filtration, evapn. of filtrate; | |
In acetone filtration, evapn. of filtrate; |
trifluoroborane diethyl ether
phenylmagnesium bromide
sodium chloride
sodium tetraphenyl borate
Conditions | Yield |
---|---|
extrn. with dry acetone; | |
In diethyl ether; water ether layer is evapd.; residue dissolved in water; satd. with NaCl; | |
extrn. with dry acetone; | |
In diethyl ether; water ether layer is evapd.; residue dissolved in water; satd. with NaCl; |
sodium tetrafluoroborate
phenylmagnesium bromide
sodium chloride
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In tetrahydrofuran; water THF layer is again treated with aq. NaCl; | |
In tetrahydrofuran C6H5Mg is reacted with Na; poured into satd. soln. of NaCl; extrn. with THF; removing solvent in vac., stirring with CHCl3; | |
In not given organic layer is evapd.; residue freeing from biphenyl by extrn. with CHCl3; recrystn. from ether; |
boron trifluoride
sodium carbonate
phenylmagnesium bromide
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In diethyl ether; water distilling off the ether, adding H2O and calcd. amt. of Na2CO3; | |
In diethyl ether; water distilling off the ether, adding H2O and calcd. amt. of Na2CO3; |
sodium
boron trichloride
chlorobenzene
sodium tetraphenyl borate
Conditions | Yield |
---|---|
With hydrogenchloride In xylene below 30°C; reaction mixture pured into ice, organic layer separated, washed with water, aqueous layers are neutralized with 6N HCl; |
sodium methylate
trifluoroborane diethyl ether
phenylmagnesium bromide
sodium tetraphenyl borate
Conditions | Yield |
---|---|
With ammonium salt |
trifluoroborane diethyl ether
phenylmagnesium bromide
sodium tetraphenyl borate
Conditions | Yield |
---|---|
With sodium carbonate; sodium chloride In diethyl ether water cooling, stirring, adding the BF3*(C2H5)2O soln. drop by drop, evapn. of solvent, taking up the residue with water; precipitation of Mg by adding of Na2CO3, saturation with NaCl, extrn. in Soxlet-equipment with ether; | 55-60 |
With Na2CO3; NaCl In diethyl ether water cooling, stirring, adding the BF3*(C2H5)2O soln. drop by drop, evapn. of solvent, taking up the residue with water; precipitation of Mg by adding of Na2CO3, saturation with NaCl, extrn. in Soxlet-equipment with ether; | 55-60 |
ammonium tetraphenylborate
sodium hydroxide
A
ammonia
B
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In water little excess of NaOH, boiling; | |
In water little excess of NaOH, boiling; |
sodium tetrafluoroborate
phenylmagnesium bromide
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In diethyl ether heating on water bath; | |
With sodium chloride In diethyl ether; water 2 h stirring, addn. of reaction mixture to a satd. aq. NaCl soln.; extrn. the aq. layer with ether two times, evapn. in vac.; recrystn. in ether at 0°C; | |
In diethyl ether heating on water bath; | |
With NaCl In diethyl ether; water 2 h stirring, addn. of reaction mixture to a satd. aq. NaCl soln.; extrn. the aq. layer with ether two times, evapn. in vac.; recrystn. in ether at 0°C; |
tris(2-methoxyethyl)borate
sodium carbonate
phenylmagnesium bromide
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In water converted to the ammonium salt with NH4Cl solution (after removing the biaryls with benzene) and is then reconverted; |
phenylmagnesium chloride
sodium carbonate
tris(2-(2-methoxyethoxy)ethyl) borate
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In water converted to the ammonium salt with NH4Cl solution (after removing the biaryls with benzene) and is then reconverted; |
Conditions | Yield |
---|---|
In methanol refluxed equimolar amts. of educts under N2, solvent is subsequently evapd. and residue crystd. from ether; recrystn. from CHCl3; |
Conditions | Yield |
---|---|
In acetone with cation-exchanger called Levatit S 100 or Permutit RS; | |
In water; acetone passing the soln. through a Na form cation exchanger; | |
In water; acetone passing the soln. through a Na form KU-2 resin cation exchanger; | |
In acetone with cation-exchanger called Levatit S 100 or Permutit RS; |
Conditions | Yield |
---|---|
With sodium In 1,2-dimethoxyethane byproducts: NaCl; Sonication; allowed to react with 2 equivs. of Na in DME with ultrasonic promotion; |
Conditions | Yield |
---|---|
Stage #1: bromobenzene With magnesium In diethyl ether Reflux; Stage #2: With sodium tetrafluoroborate In diethyl ether for 48h; |
Conditions | Yield |
---|---|
Stage #1: sodium tetrafluoroborate With magnesium In tetrahydrofuran; ethylene dibromide for 0.0166667h; Sealed tube; Inert atmosphere; Schlenk technique; Stage #2: phenyl halide In tetrahydrofuran; ethylene dibromide at 20℃; for 12h; Sealed tube; Inert atmosphere; Schlenk technique; |
Conditions | Yield |
---|---|
With magnesium In tetrahydrofuran at 0 - 20℃; for 12h; Inert atmosphere; |
2,2-diiodo-5,6-dimethyl-1,3-dihydro-2-telluraindene
sodium tetraphenyl borate
2-phenyl-2-iodo-5,6-dimethyl-1,3-dihydro-2-telluraindene
Conditions | Yield |
---|---|
In ethanol for 0.25h; Heating; | 100% |
sodium tetraphenyl borate
tetraisopropylphosphonium iodide
tetraisopropylphosphonium tetraphenylborate
Conditions | Yield |
---|---|
In methanol at 52℃; the structure of the product was investigated by X-ray spectroscopy; | 100% |
1-methyl-1H-imidazole
2,4,6-trichloropyrimidine
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In ethyl acetate Ambient temperature; | 100% |
Conditions | Yield |
---|---|
In ethyl acetate Ambient temperature; | 100% |
In ethyl acetate | 100% |
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In dichloromethane -40 deg C. then room temp., 1 h; | 100% |
Conditions | Yield |
---|---|
With sodium carbonate; palladium dichloride In water at 100℃; for 4h; other reagent, temperature, reaction time; | 100% |
With palladium on activated charcoal; sodium carbonate for 3h; Heating; | 90% |
With palladium on activated charcoal; sodium carbonate at 20℃; for 24h; Product distribution; influence of catalyst, reaction time, temperature; | 61% |
With palladium diacetate; sodium hydroxide In water at 25℃; for 2h; Product distribution; other reagent, reaction time, temperature; | 100 % Chromat. |
With sodium carbonate; palladium on activated charcoal In water for 1h; Suzuki reaction; Heating; | 97 % Chromat. |
Conditions | Yield |
---|---|
With palladium diacetate; sodium carbonate In acetone at 20℃; for 0.0833333h; | 100% |
With sodium carbonate; palladium diacetate In acetone at 20℃; for 0.0833333h; Suzuki reaction; | 98% |
sodium tetraphenyl borate
1,4,7-tri(4-hexynyl)-1,4,7-triazacyclononane
Conditions | Yield |
---|---|
In methanol | 100% |
sodium tetraphenyl borate
Conditions | Yield |
---|---|
With trifluoroacetic acid | 100% |
Conditions | Yield |
---|---|
With water; acetic acid; bis-triphenylphosphine-palladium(II) chloride at 20℃; for 6h; | 100% |
With bis-triphenylphosphine-palladium(II) chloride; water; acetic acid at 20℃; for 6h; Catalytic behavior; Reagent/catalyst; Temperature; Inert atmosphere; Sealed tube; | 94% |
copper(l) iodide
sodium tetraphenyl borate
copper
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane Irradiation (UV/VIS); under Ar; mole ratio NaBPh4 : CuI = 1 : 1; irradn. (254 nm) for 1 h gave deposition of Cu; deposit sepd., washed with acetone and water, and dried in vac. to give pure Cu; | 100% |
sodium tetraphenyl borate
copper(II) acetylacetonate
zinc(II) acetylacetonate
A
copper
B
zinc
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane Irradiation (UV/VIS); under Ar; mole ratios NaBPh4 : Zn(acac)2 : Cu(acac)2 = 20 : 7 : 3; irradn. (254 nm) for 18 h gave deposition only of Cu; | A 100% B 0% |
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane Irradiation (UV/VIS); under Ar; mole ratio NaBPh4 : ZnI2 = 2 : 1; irradn. (254 nm) for 2 h gave deposition of Zn; deposit sepd., washed with acetone and water, and dried in vac. to give pure Zn; | 100% |
trans-acetonitrile-bis(1,2-bis(dimethylphosphino)ethane)chloroiron(II) chloride
sodium tetraphenyl borate
trans-{iron(II)Cl(MeNC)(Me2PCH2CH2PMe2)2}{BPh4}
Conditions | Yield |
---|---|
In acetonitrile 1 equiv. NaBPh4 added to a soln. of (FeCl(NCMe)(dmpe)2)Cl;; filtration; elem. anal.;; | 100% |
sodium tetraphenyl borate
ReO2(C5H5N)4(1+)*B(C6H5)4(1-)
Conditions | Yield |
---|---|
With pyridine In acetone NaBPh4 in acetone was added to a soln. of Re-compound in pyridine with 2 drops of pyridine;; H2O was added, ppt. was collected, dried, recrystd. from acetone-ether;elem. anal.;; | 100% |
bis(triphenylphosphine)iridium(I) carbonyl chloride
sodium tetraphenyl borate
[Ir(CO)3(triphenylphosphine)2]BPh4
Conditions | Yield |
---|---|
With carbon monoxide In tetrahydrofuran a portion of NaBPh4 was added to a soln. of Ir-complex in THF that has been satd. with CO, mixt. was stirred for 30 min; THF was removed, residue extd. with CH2Cl2, filtered into a Schlenk flask, stirred under CO for 15 min, pentane was added to form a ppt. which can be recrystd. from CH2Cl2-pentane; | 100% |
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In methanol stirred for 4 h, addn. of Na(BPh4); | 100% |
cis,trans-[dicarbonylbis(trimethylphosphine)(methyl)iodoiron(II)]
sodium tetraphenyl borate
Dimethyl(phenyl)phosphine
(CO)2CH3Fe(P(CH3)3)2P(CH3)2C6H5(1+)*B(C6H5)4(1-)
Conditions | Yield |
---|---|
In methanol at -30°C; | 100% |
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In methanol room temperature; | 100% |
Conditions | Yield |
---|---|
In methanol; water (air); addn. of the ligand in MeOH to a soln. of the Cu salt in H2O, stirring (5 min), filtration, addn. of aq. NaBPh4, stirring (10 min); filtration, washing (H2O), drying (vac.), stirring with Et2O, filtration, repeating this extn., drying (vac.); elem.anal.; | 100% |
Pd(P(C6H5)3)2(Cl)CH2CC(C6H5)
PdCl(P(C6H5)3)2(C(C6H5)CCH2)
sodium tetraphenyl borate
Pd(P(C6H5)3)2(CH2CHCHC6H5)(1+)*B(C6H5)4(1-)=[Pd(P(C6H5)3)2(CH2CHCHC6H5)]B(C6H5)4
Conditions | Yield |
---|---|
In chloroform-d1; [(2)H6]acetone stoich. amts.; room temp., 5 min.; (1)H NMR monitoring; | 100% |
PdCl(P(C6H5)3)2(CH2CCSi(CH3)3)
sodium tetraphenyl borate
Pd(P(C6H5)3)2(CH2CHCHSi(CH3)3)(1+)*B(C6H5)4(1-)=[Pd(P(C6H5)3)2(CH2CHCHSi(CH3)3)]B(C6H5)4
Conditions | Yield |
---|---|
In chloroform-d1; [(2)H6]acetone stoich. amts.; room temp., 5 min.; (1)H NMR monitoring; | 100% |
ethene
[1,2-bis(diisopropylphosphino)ethane]chloro(pentamethylcyclopentadienyl)ruthenium(II)
sodium tetraphenyl borate
((CH3)5C5)Ru(C2H4)((((CH3)2CH)2PCH2)2)(1+)*B(C6H5)4(1-)=[((CH3)5C5)Ru(C2H4)((((CH3)2CH)2PCH2)2)][B(C6H5)4]
Conditions | Yield |
---|---|
In methanol C2H4-atmosphere; stirring (10 min); filtering, washing (EtOH, petroleum ether), drying (vac.); elem. anal.; | 100% |
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In water stirring (1 h, room temp.); washing (H2O, iPrOH, Et2O), drying (vac.); | 100% |
sodium tetraphenyl borate
phenyl[tri(tert-butyl)phosphine]gold(I)
Conditions | Yield |
---|---|
In ethanol byproducts: NaBF4, PhBO; N2-atmosphere; excess NaBPh4, stirring at room temp. in absence of direct light for 15 d (crystn.); | 100% |
dichloro(benzene)ruthenium(II) dimer
sodium tetraphenyl borate
(η(6)-benzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium tetraphenylborate
Conditions | Yield |
---|---|
In water; acetonitrile N2-atmosphere; stirring Ru-complex with excess TlCp (in dark, in MeCN, 5h), filtration, addn. of H2O, filtration, addn. of excess NaBPh4 (in H2 O), stirring for 30 min; pptn. on concn., filtration, washing (H2O), drying (vac.); can be recrystallized (MeCN/Et2O); elem. anal.; | 100% |
sodium tetraphenyl borate
Conditions | Yield |
---|---|
In methanol under N2 atm. soln. ligand and ((Cp*RhCl)2(μ-Cl))2 in MeOH was stirred at room temp. for 30 min, NaBPh4 was added and stirred for 2 h; solvent was removed in vacuo, residue was dissolved in CH2Cl2 and filtered through Celite, solvent was removed; elem. anal.; | 100% |
(η(5)-C5H5)2Ti(η(2)-CO(i-Pr))I
sodium tetraphenyl borate
ethenetetracarbonitrile
(η(5)-C5H5)2Ti(η(2)-CO(i-Pr))(NCBPh3)
Conditions | Yield |
---|---|
In methanol Ar-atmosphere; mixing equimolar amts. of Ti-complex and TCNE, addn. of 2equiv. NaBPh4; | 100% |
sodium tetraphenyl borate
N,N'-dimethylimidazolium-2-carboxylate
1,3-dimethylimidazolium tetraphenylborate
Conditions | Yield |
---|---|
With water In tetrahydrofuran Inert atmosphere; | 100% |
sodium tetraphenyl borate
Conditions | Yield |
---|---|
With water In tetrahydrofuran Inert atmosphere; | 100% |
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