Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:585-76-2
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As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:585-76-2
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 3-Bromobenzoic acid CAS No. 585-7
Cas:585-76-2
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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Cas:585-76-2
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inquiryNow we would like to update our product list for you, kindly check the below information: 1. Catalyst series ( such as Noble Metal Catalyst, Phosphorous ligand, etc ) 2. Pharmaceutical Intermediate ( such as diabtes series, Anti
Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:585-76-2
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryAbout Product Details
Cas:585-76-2
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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inquiry3-Bromobenzoic acid Chemical Properties Melting point 155-158 °C(lit.) Boiling point >280 °C density 1,948 g/cm3 refractive index 1.6080 (estimate) storage temp. Sealed in dry,Room Temperature solubility methanol: s
Cas:585-76-2
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:585-76-2
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:585-76-2
Min.Order:1 Kilogram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:585-76-2
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Cas:585-76-2
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inquirySuperior quality, moderate price & quick delivery. Appearance:Colorless needle-like crystals Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:For medicine , pe
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:585-76-2
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryProduct name: 3-Bromobenzoic Acid CAS No.:585-76-2 Molecule Formula:C7H5BrO2 Molecule Weight:201.01 Purity: 99% Package:25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:585-76-2
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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inquiryOur company focuses on the future and the world, and will continue to devote itself to technological progress and the development of new products in the future, hoping to work hand in hand with new and old friends at home and abroad to create a bett
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inquiryConditions | Yield |
---|---|
With sodium hydroxide; carbon monoxide; bis(benzonitrile)palladium(II) dichloride; triphenylphosphine In xylene at 90℃; for 4h; Hydrolysis; | 100% |
With sodium hydroxide |
Conditions | Yield |
---|---|
With Oxone In N,N-dimethyl-formamide at 20℃; for 3h; | 97% |
Stage #1: m-bromobenzoic aldehyde With sodium dihydrogenphosphate In tetrahydrofuran; water at 20℃; for 0.166667h; Stage #2: With sodium chlorite; dihydrogen peroxide In tetrahydrofuran; water at 20℃; for 3h; | 95% |
With sodium chlorite; disodium hydrogenphosphate; dihydrogen peroxide In tetrahydrofuran; water at 20℃; for 3h; Cooling with ice; | 95% |
Conditions | Yield |
---|---|
With iodine; aluminium In acetonitrile at 80℃; for 18h; | 97% |
With potassium hydroxide In methanol at 35℃; for 0.0833333h; | 80% |
Conditions | Yield |
---|---|
With oxygen; pyridinium chlorochromate In water at 120℃; under 45004.5 Torr; for 2h; | 95% |
With Oxone; potassium bromide In dichloromethane; water at 20℃; for 24h; visible light irradiation; | 93% |
With oxygen; Langlois reagent In acetonitrile at 25℃; for 12h; Irradiation; Green chemistry; | 93% |
3-bromo-β-nitro-styrene
m-bromobenzoic acid
Conditions | Yield |
---|---|
With Amberlyst A-26 (OH-); dihydrogen peroxide In 1,4-dioxane at 20℃; for 9h; | 95% |
5-bromo-1H-indole
A
5-bromo-1H-indazole-3-carboxaldehyde
B
m-bromobenzoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water; sodium nitrite In N,N-dimethyl-formamide at 0 - 50℃; for 5h; Inert atmosphere; | A 94% B n/a |
Conditions | Yield |
---|---|
With sodium bromate; potassium sulfate; sulfuric acid In water at 85 - 90℃; for 1.5h; regioselective reaction; | 93.7% |
With sulfuric acid; bromine; mercury(II) oxide In tetrachloromethane for 2.5h; Heating; | 79% |
With N-Bromosuccinimide; sulfuric acid; trifluoroacetic acid at 25℃; for 44h; Bromination; | 78% |
(3-Bromophenyl)methanol
m-bromobenzoic acid
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; Iron(III) nitrate nonahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; acetic acid at 80℃; under 760.051 Torr; for 3h; | 91% |
With Langlois reagent In acetonitrile at 25℃; for 12h; Irradiation; Sealed tube; | 89% |
With tert.-butylhydroperoxide at 100℃; for 5h; | 80% |
3-bromo-N,N-diisopropylbenzamide
A
m-bromobenzoic acid
B
3-bromobenzoic acid isopropylamide
Conditions | Yield |
---|---|
With hydrogenchloride; zinc(II) chloride at 160℃; for 72h; | A 90% B 8% |
benzyl 3-bromobenzoic acid
m-bromobenzoic acid
Conditions | Yield |
---|---|
With methanol; sodium tetrahydroborate; nickel(II) chloride hexahydrate at 20℃; for 0.166667h; chemoselective reaction; | 90% |
1,2-di-(3-bromophenyl)-1,2-ethanediol
m-bromobenzoic acid
Conditions | Yield |
---|---|
With sodium hypochlorite In acetonitrile at 20℃; for 3h; | 89% |
Conditions | Yield |
---|---|
With magnesium In tetrahydrofuran at -78℃; for 0.5h; | 88% |
1,3-dibromobenzene
diphenylmethylsilanecarboxylic acid
A
isophthalic acid
B
m-bromobenzoic acid
Conditions | Yield |
---|---|
With lithium trimethylsilanolate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane at 80℃; for 16h; Glovebox; Overall yield = 40 mg; | A 88% B 7% |
3-bromobenzylamine
m-bromobenzoic acid
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide at 120℃; for 5h; Ionic liquid; | 85% |
Conditions | Yield |
---|---|
With sulfuric acid; bromine; mercury(II) oxide In tetrachloromethane for 2.5h; Heating; | A 80% B n/a |
Conditions | Yield |
---|---|
With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); potassium methanolate In N,N-dimethyl acetamide at 70℃; for 24h; Schlenk technique; Sealed tube; | 79% |
Conditions | Yield |
---|---|
With sulfuric acid; bromine; mercury(II) oxide In tetrachloromethane for 2.5h; Heating; | A 78% B n/a |
2,5-dibromobenzoic acid
A
m-bromobenzoic acid
B
benzoic acid
C
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran | A 78% B 13% C 2% |
Conditions | Yield |
---|---|
With copper(l) iodide; hydroxylamine hydrochloride; oxygen In dimethyl sulfoxide at 100℃; for 10h; | 78% |
With hydroxylamine hydrochloride; iodine In dimethyl sulfoxide at 100℃; for 6h; | 70% |
With 18-crown-6 ether; acetophenone In benzene at 25℃; for 24h; Mechanism; relative reactivity; further oxidative agents; |
carbon monoxide
3-bromo-1-iodylbenzene
A
1-Bromo-3-iodobenzene
B
isophthalic acid
C
m-bromobenzoic acid
Conditions | Yield |
---|---|
With sodium tetrachloropalladate; sodium carbonate In water at 40℃; for 5.5h; Yields of byproduct given; | A n/a B 14% C 76% |
carbon monoxide
3-bromo-1-iodylbenzene
A
3-iodochlorobenzene
B
isophthalic acid
C
m-bromobenzoic acid
Conditions | Yield |
---|---|
With sodium tetrachloropalladate; sodium carbonate In water at 40℃; for 5.5h; Yields of byproduct given; | A n/a B 14% C 76% |
methanol
m-bromobenzoic aldehyde
A
methyl 3-bromobenzoate
B
m-bromobenzoic acid
Conditions | Yield |
---|---|
With 3,3'-dimethyl-1,1'-(hexane-1,6-diyl)diimidazolium glutarate; 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 55℃; for 16h; Molecular sieve; | A 72% B 10% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide; sodium nitrite In N,N-dimethyl-formamide at 20℃; for 6h; | 72% |
Conditions | Yield |
---|---|
With ethanol In water at 85℃; for 60h; Time; von Richter Aromatic Carboxylation; Ionic liquid; | 67% |
3-bromobenzoyl cyanide
m-bromobenzoic acid
Conditions | Yield |
---|---|
With sulfuric acid; water at 103℃; for 0.5h; | 67% |
m-bromobenzoic acid
Conditions | Yield |
---|---|
With ferrocene; tert-Butyl peroxybenzoate In 1,2-dichloro-ethane at 80℃; for 12h; Sealed tube; | 66% |
1-Bromo-3-iodobenzene
carbon dioxide
A
isophthalic acid
B
m-bromobenzoic acid
Conditions | Yield |
---|---|
Stage #1: carbon dioxide With o-phenylenebis(diphenylphosphine); copper(II) acetate monohydrate In 1,4-dioxane at 65℃; for 0.333333h; Schlenk technique; Stage #2: 1-Bromo-3-iodobenzene With palladium diacetate; triethylamine; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane; toluene at 100℃; for 16h; Schlenk technique; Sealed tube; | A 62% B 20% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; copper(ll) bromide In acetic anhydride | A 19% B 59% |
Conditions | Yield |
---|---|
Stage #1: carbon dioxide With o-phenylenebis(diphenylphosphine); copper(II) acetate monohydrate In 1,4-dioxane at 65℃; for 0.333333h; Schlenk technique; Stage #2: 1-Bromo-3-iodobenzene With palladium diacetate; triethylamine; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane; toluene at 100℃; for 2h; Schlenk technique; Sealed tube; | 52% |
With copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; diethylzinc In N,N-dimethyl acetamide at 70℃; under 760.051 Torr; | 51% |
Stage #1: 1-Bromo-3-iodobenzene With copper In tetrahydrofuran at 25℃; for 0.5h; Stage #2: carbon dioxide In tetrahydrofuran for 24h; | 49% |
m-bromobenzoic aldehyde
A
m-bromobenzoic acid
B
bis-(3-bromo-benzoyl)-peroxide
C
3-Bromperoxobenzoesaeure
Conditions | Yield |
---|---|
With oxygen; ozone; lithium chloride In tetrachloromethane at 50℃; | A n/a B 50.4% C n/a |
Conditions | Yield |
---|---|
With thionyl chloride at 90℃; for 3h; | 100% |
Stage #1: m-bromobenzoic acid With thionyl chloride at 70℃; for 5h; Stage #2: methanol With sodium hydrogencarbonate at 20℃; for 4h; Cooling with ice; | 98% |
With sulfuric acid for 0.3h; Reflux; Microwave irradiation; | 94% |
Conditions | Yield |
---|---|
Stage #1: m-bromobenzoic acid With N,N-dimethyl-formamide In dichloromethane at 0℃; for 0.0833333h; Stage #2: With oxalyl dichloride In dichloromethane at 20℃; for 12h; | 100% |
With thionyl chloride Reflux; | 97% |
With thionyl chloride |
Conditions | Yield |
---|---|
With sodium carbonate; palladium dichloride In water at 100℃; for 4h; other reagent, temperature, reaction time; | 100% |
With palladium on activated charcoal; sodium carbonate for 3h; Heating; | 90% |
With palladium on activated charcoal; sodium carbonate at 20℃; for 24h; Product distribution; influence of catalyst, reaction time, temperature; | 61% |
With palladium diacetate; sodium hydroxide In water at 25℃; for 2h; Product distribution; other reagent, reaction time, temperature; | 100 % Chromat. |
With sodium carbonate; palladium on activated charcoal In water for 1h; Suzuki reaction; Heating; | 97 % Chromat. |
m-bromobenzoic acid
4-methoxyphenylboronic acid
4'-methoxy-(1,1'-biphenyl)-3-carboxylic acid
Conditions | Yield |
---|---|
With potassium carbonate; dichlorobis(4-pyridinaldoxime)palladium(II) In water for 1h; Suzuki reaction; Heating; | 100% |
With 2C2H5NO2*Pd(2+)*2Cl(1-); potassium carbonate In water at 20℃; for 1.5h; Suzuki-Miyaura Coupling; Green chemistry; | 98% |
With C26H24Cl4N8O4Pd2; potassium carbonate In methanol; water; N,N-dimethyl-formamide at 20 - 100℃; for 0.25h; Catalytic behavior; Reagent/catalyst; Temperature; Time; Solvent; Suzuki-Miyaura Coupling; Green chemistry; | 98% |
m-bromobenzoic acid
Conditions | Yield |
---|---|
With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 3h; | 100% |
Conditions | Yield |
---|---|
With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 0 - 20℃; for 16h; | 100% |
Conditions | Yield |
---|---|
With nickel dibromide | 100% |
Conditions | Yield |
---|---|
With sulfated zirconia at 130℃; for 1h; Microwave irradiation; | 99.2% |
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydrogencarbonate In water at 90℃; for 24h; tri-n-butyltin hydride mediated dehalogenation of various organohalides in aqueous medium; | 99% |
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydrogencarbonate In water at 90℃; for 24h; | 95% |
With tri-n-butyl-tin hydride; sodium hydrogencarbonate In water for 24h; Ambient temperature; Irradiation; | 93% |
m-bromobenzoic acid
4-fluoroboronic acid
4’-fluoro-[1,1’-biphenyl]-3-carboxylic acid
Conditions | Yield |
---|---|
With 2C2H5NO2*Pd(2+)*2Cl(1-); potassium carbonate In water at 20℃; for 1.5h; Suzuki-Miyaura Coupling; Green chemistry; | 99% |
With potassium carbonate In water at 20℃; for 4h; Suzuki-Miyaura Coupling; Green chemistry; | 96% |
With palladium diacetate; sodium hydroxide In water for 0.166667h; Ambient temperature; | 95% |
With sodium hydroxide; palladium dichloride In water at 25℃; for 0.166667h; | 95% |
With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate In 1,4-dioxane; water at 95℃; Suzuki-Miyaura Coupling; Inert atmosphere; | 78% |
Conditions | Yield |
---|---|
With sodium carbonate; Pd-complex on fluorous reversed silica gel In water at 80℃; for 16h; Suzuki reaction; | 99% |
With potassium hydroxide; potassium carbonate; palladium-carbon In water | 98% |
With 2C2H5NO2*Pd(2+)*2Cl(1-); potassium carbonate In water at 20℃; for 1.5h; Suzuki-Miyaura Coupling; Green chemistry; | 97% |
Conditions | Yield |
---|---|
With palladium diacetate; sodium carbonate In water at 20℃; for 0.5h; | 99% |
m-bromobenzoic acid
4-methylphenylboronic acid
4'-methylbiphenyl-3-carboxylic acid
Conditions | Yield |
---|---|
With 4C3H6N6*Pd(2+)*2C2H3O2(1-); sodium carbonate In water at 80℃; for 2h; Suzuki-Miyaura Coupling; Green chemistry; | 99% |
Stage #1: m-bromobenzoic acid With palladium diacetate In water at 20℃; for 0.0833333h; Suzuki-Miyaura Coupling; Inert atmosphere; Stage #2: 4-methylphenylboronic acid With potassium hydroxide In water for 5h; Suzuki-Miyaura Coupling; Inert atmosphere; Reflux; | 98% |
With 2C2H5NO2*Pd(2+)*2Cl(1-); potassium carbonate In water at 20℃; for 1.5h; Suzuki-Miyaura Coupling; Green chemistry; | 96% |
Conditions | Yield |
---|---|
Stage #1: m-bromobenzoic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: aniline In N,N-dimethyl-formamide at 25℃; for 16h; | 99% |
With oxygen; lithium hydroxide In water at 20℃; for 14h; Sonication; | 90% |
Conditions | Yield |
---|---|
With tetraethylammonium bromide; potassium carbonate In dichloromethane at 20℃; Molecular sieve; | 99% |
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