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Cas:2637-34-5
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 2-Pyridinethiol CAS No. 2637-34-5 Appearance
Cas:2637-34-5
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryTianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationship
Cas:2637-34-5
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:2637-34-5
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:2637-34-5
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inquiryName 2-Mercaptopyridine Synonyms 2-Pyridinethiol; 2-Pyridyl mercaptan CAS NO. 2637-34-5 Molecular Formula C5H5NS M
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:2637-34-5
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inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
Cas:2637-34-5
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inquiry2-Pyridinethione Chemical Properties Melting point 127-130 °C(lit.) Boiling point 184.9±23.0 °C(Predicted) density 1.161 (estimate) refractive index 1.5605 (estimate) Fp 125°C storage temp. 2-8°C solubil
2-Pyridinethione CAS:2637-34-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
Cas:2637-34-5
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:2637-34-5
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:2637-34-5
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Our Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual
Cas:2637-34-5
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:2637-34-5
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Cas:2637-34-5
Min.Order:1 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:2637-34-5
Min.Order:10 Gram
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inquiryHangzhou Verychem Science And Technology Co. Ltd. was set up in year 2004, it’s a young but fast growing company. In the twelve years history, it invested two pharmaceutical raw material production plants, one researching company, and several
We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:2637-34-5
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inquiryProduct name: 2-Mercaptopridine CAS No.: 2637-34-5 Molecule Formula:C5H5NS Molecule Weight:111.17 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:2637-34-5
Min.Order:1 Kilogram
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:2637-34-5
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:2637-34-5
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inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
L-leucine
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
A
2-Mercaptopyridine
B
N-tert-butoxycarbonyl-L-leucine
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 12h; Ambient temperature; | A n/a B 95% |
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
L-proline
A
2-Mercaptopyridine
B
1-(tert-butoxycarbonyl)-L-proline
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 4h; Ambient temperature; | A n/a B 95% |
methanol
pyridin-2-yl 1-thio-β-D-glucopyranoside
A
2-Mercaptopyridine
B
methyl beta-D-glucopyranoside
Conditions | Yield |
---|---|
With citrate-phosphate buffer; almond β-D-glucosidase at 25℃; for 1h; pH=5.0; | A n/a B 95% |
1-phenyl-2-(pyridin-2-ylthio)ethan-1-one
2-Mercaptopyridine
Conditions | Yield |
---|---|
With magnesium; acetic acid In methanol at 20℃; | 94% |
2,2'-dipyridyldisulphide
2,4-dimethylbenzenesulfonic acid
triphenylphosphine
A
2-Mercaptopyridine
B
2,4-dimethyl-thiophenol
C
Triphenylphosphine oxide
Conditions | Yield |
---|---|
In benzene for 2h; Product distribution; Mechanism; Heating; further reaction partners - various diaryl disulfides; | A n/a B 92% C 88% |
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
A
2-Mercaptopyridine
B
Boc-Thr-OH
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 12h; Ambient temperature; | A n/a B 92% |
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
A
2-Mercaptopyridine
B
Boc-Tyr-OH
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 16h; Ambient temperature; | A n/a B 92% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; zirconium(IV) chloride In tetrahydrofuran at 35℃; for 0.166667h; Reduction; | 90% |
With sodium citrate; titanium(III) chloride In ethanol; water; acetic acid pH 4.5 to 6.O; | 40% |
With water; titanium(IV) oxide In acetonitrile at 22℃; Irradiation; |
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
A
2-Mercaptopyridine
B
N-tert-butoxycarbonyl-L-methionine
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 8h; Ambient temperature; | A n/a B 90% |
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
A
2-Mercaptopyridine
B
N-tert-butoxycarbonyl-L-phenylalanine
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 16h; Ambient temperature; | A n/a B 89% |
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
L-Tryptophan
A
2-Mercaptopyridine
B
Boc-Trp-OH
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 8h; Ambient temperature; | A n/a B 89% |
triisopropylsilyl 4-(pyridine-2-yldisulfanyl)pentanoate
alpha-mercaptophenylacetic acid
A
2-Mercaptopyridine
B
[2-({5-oxo-5-[(triisopropylsilyl)oxy]pentan-2-yl}disulfanyl)phenyl]acetic acid
Conditions | Yield |
---|---|
In tetrahydrofuran at -10 - 20℃; for 1.5h; Inert atmosphere; | A n/a B 88% |
Conditions | Yield |
---|---|
With Dimethylphenylsilane In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; | 88% |
Stage #1: 2-mercaptopyridine N-oxide With bis(pinacol)diborane In water at 110℃; for 10h; Stage #2: With ethylenediamine In water at 20℃; for 1h; | 72% |
N-palmitoxy-2-pyridinethione
thiophenol
A
2-Mercaptopyridine
B
pentadecane
C
diphenyldisulfane
Conditions | Yield |
---|---|
With tetrachloromethane for 0.333333h; Product distribution; Mechanism; Ambient temperature; sonication; | A 87% B 85% C 70% |
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
A
2-Mercaptopyridine
B
(S)-N-(tert-butoxycarbonyl)serine
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 10h; Ambient temperature; | A n/a B 85% |
L-alanin
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
A
2-Mercaptopyridine
B
L-N-Boc-Ala
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 16h; Ambient temperature; | A n/a B 84% |
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
A
2-Mercaptopyridine
B
N-(tert-Butyloxycarbonyl)-L-cysteine
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 12h; Ambient temperature; | A n/a B 84% |
L-cystine
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
A
2-Mercaptopyridine
B
di-t-butoxycarbonyl-L-cystine
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 20h; Ambient temperature; | A n/a B 83% |
L-valine
O-(tert-butyl) S-(pyridin-2-yl)carbonothioate
A
2-Mercaptopyridine
B
t-Boc-L-valine
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide for 12h; Ambient temperature; | A n/a B 80% |
pyridin-2-yl 1-thio-β-D-glucopyranoside
ethanol
A
2-Mercaptopyridine
B
(2R,3R,4S,5S,6R)-2-Ethoxy-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol
Conditions | Yield |
---|---|
With citrate-phosphate buffer; almond β-D-glucosidase at 25℃; for 1h; pH=5.0; | A n/a B 79% |
Conditions | Yield |
---|---|
With sodiumsulfide nonahydrate; copper; ethane-1,2-dithiol In dimethyl sulfoxide at 100℃; for 20h; Inert atmosphere; Green chemistry; | 76% |
With 4-Methoxybenzenethiol; potassium tert-butylate; bis[2-(diphenylphosphino)phenyl] ether In toluene at 100℃; for 2h; | 7% |
di-2-pyridyl sulfide
phenol
A
2-Mercaptopyridine
B
2-phenoxypyridine
Conditions | Yield |
---|---|
at 200℃; for 1h; | A 47.5 mg B 72% |
With potassium tert-butylate In propan-1-ol at 200℃; for 0.5h; Mechanism; further solvents; |
A
2-Mercaptopyridine
Conditions | Yield |
---|---|
In neat (no solvent) melting in a porcelain crucible; mlet is cooled and dissolved in CH2Cl2 and eluted through a 5% deactivated alumina column; recrystn. from CHCl3/benzene/light petroleum; elem. anal.; | A n/a B 70% |
2,2'-dipyridyldisulphide
4-chloro-benzenesulfonic acid
triphenylphosphine
A
2-Mercaptopyridine
B
p-Chlorothiophenol
C
Triphenylphosphine oxide
Conditions | Yield |
---|---|
In benzene for 4h; Product distribution; Mechanism; Heating; further reaction partners - various diaryl disulfides; | A n/a B 53% C 65% |
Conditions | Yield |
---|---|
With sodium thiosulfate In ethanol; water for 22h; Heating; starting pH=3.2, (85percent H3PO4, NaH2PO4); | 63% |
With propylene glycol; potassium hydrosulfide at 150 - 175℃; |
3-carboxy-2-mercaptopyridine
A
2-Mercaptopyridine
B
2,2'-dipyridyldisulphide
Conditions | Yield |
---|---|
at 800℃; under 0.01 Torr; | A 58% B 11% |
2-bromo-pyridine
benzyl alcohol
A
2-Mercaptopyridine
B
2-(benzylthio)pyridine
Conditions | Yield |
---|---|
With water; sodium thiosulfate In neat (no solvent) at 150℃; for 24h; Reagent/catalyst; Sealed tube; Green chemistry; chemoselective reaction; | A n/a B 40% |
Conditions | Yield |
---|---|
With sodium citrate; titanium(III) chloride In ethanol; water; acetic acid pH 4.5 to 6.O; | 38% |
(4R,5S)-5-(3-Cyano-indol-1-ylmethyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid 2-thioxo-2H-pyridin-1-yl ester
A
2-Mercaptopyridine
Conditions | Yield |
---|---|
In tetrahydrofuran at -78℃; for 1.25h; Irradiation; | A 6.9 mg B 11% C 9% D 34% |
Conditions | Yield |
---|---|
With phosphorous (V) sulfide at 160℃; |
Conditions | Yield |
---|---|
With 2,2'-dipyridyl disulfide bis-N-oxide In chloroform for 1h; Ambient temperature; | 100% |
With oxygen In water at 80℃; under 2250.23 Torr; for 1h; | 99% |
With manganese(II)carbonate; 3,4,5-trihydroxybenzoic acid; oxygen; sodium carbonate In water at 80℃; under 2250.23 Torr; for 4h; pH=9; Schlenk technique; Green chemistry; | 99% |
2-Mercaptopyridine
n-octanoic acid chloride
S-(pyridin-2-yl)octanethioate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; Cooling with ice bath; | 100% |
With TEA In dichloromethane at 0℃; | |
Stage #1: 2-Sulfanylpyridine With triethylamine In dichloromethane at 0℃; Stage #2: n-octanoic acid chloride at 20℃; for 1.5h; |
2-Mercaptopyridine
4-azidobutanoyl chloride
Conditions | Yield |
---|---|
In dichloromethane for 1.5h; from 4 deg C to RT; | 100% |
2-Mercaptopyridine
2-chlorothiphenol
methanethiosulfonic acid S-methyl ester
S-ethyl methanethiosulfonate
S-isopropyl methanethiosulfonate
S-propyl methanethiosulfonate
S-butyl methanethiosulfonate
3,4-dimethylthiophenol
o-hydroxymethyl thiophenol
3,4-difluorobenzenethiol
3-ethoxybenzenethiol
para-nitrobenzenethiol
4-aminotiophenol
A
2-(isopropyldisulfanyl)pyridine
B
2-(methyldisulfanyl)pyridine
C
2-(ethyldisulfaneyl)pyridine
D
2-pyridyl 1-methylpropyl disulfide
E
4-methyldisulfanyl-phenylamine
F
m-ethoxyphenyl methyl disulfide
G
o-chlorophenyl ethyl disulfide
H
3,4-dimethylphenyl methyl disulfide
I
o-chlorophenyl isopropyl disulfide
J
o-(hydroxymethyl)phenyl methyl disulfide
K
3,4-difluorophenyl methyl disulfide
L
3,4-dimethylphenyl ethyl disulfide
M
s-butyl o-chlorophenyl disulfide
N
3,4-dimethylphenyl isopropyl disulfide
O
o-chlorophenyl n-propyl disulfide
P
3,4-dimethylphenyl n-propyl disulfide
Q
n-butyl o-chlorophenyl disulfide
R
3,4-difluorophenyl ethyl disulfide
S
3,4-difluorophenyl isopropyl disulfide
T
sec-butyl 3,4-dimethylphenyl disulfide
U
sec-butyl 3,4-difluorophenyl disulfide
V
3,4-difluorophenyl n-propyl disulfide
W
n-butyl 3,4-dimethylphenyl disulfide
X
n-butyl 3,4-difluorophenyl disulfide
Y
methyl 4-nitrophenyl disulphide
Conditions | Yield |
---|---|
In methanol for 1h; Combinatorial reaction / High throughput screening (HTS); | A 10% B 35% C 25% D 15% E 82% F 28% G 59% H 53% I 80% J 44% K 50% L 66% M 100% N 19% O 37% P 48% Q 76% R 42% S 53% T 38% U 65% V 54% W 79% X 43% Y 76% |
2-Mercaptopyridine
4-(difluoromethoxy)benzoyl chloride
Conditions | Yield |
---|---|
In tetrahydrofuran for 0.5h; | 100% |
2-Mercaptopyridine
2-mercaptopyridine sodium salt
Conditions | Yield |
---|---|
With sodium In ethanol at 20℃; for 3h; Inert atmosphere; | 100% |
With sodium In ethanol at 20℃; Inert atmosphere; | |
With sodium In ethanol | |
With sodium hydride In tetrahydrofuran Inert atmosphere; Glovebox; |
Conditions | Yield |
---|---|
With copper(l) iodide; (S,S)-1,2-diaminocyclohexane In water at 120℃; | 99.9% |
Conditions | Yield |
---|---|
With potassium carbonate; triethylamine In dichloromethane at 0℃; | 99% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran; acetonitrile at 0 - 20℃; Inert atmosphere; | 98% |
Stage #1: 2-Sulfanylpyridine With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran; acetonitrile at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran; acetonitrile at 0 - 20℃; Inert atmosphere; | 98% |
2-Mercaptopyridine
2-(3-bromopropyl)isoindole-1,3-dione
2-[3'-(pyridin-2''-ylsulfanyl)propyl]-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 6h; Inert atmosphere; | 99% |
With potassium carbonate In acetone for 4h; Reflux; | 94% |
With potassium carbonate In acetone Heating; |
2-Mercaptopyridine
α-bromoacetophenone
1-phenyl-2-[2]pyridylmercapto-ethanone; hydrobromide
Conditions | Yield |
---|---|
In diethyl ether for 0.5h; | 99% |
2-Mercaptopyridine
O-(2-deoxy-2-azido-3,4,6-tri-O-benzyl-α-D-galactopyranosyl) trichloroacetimidate
2-((2S,3R,4R,5R,6R)-3-Azido-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-ylsulfanyl)-pyridine
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve In dichloromethane at -20℃; for 1h; other reagent: BF3*Et2O; | 99% |
Conditions | Yield |
---|---|
With potassium phosphate; (1,10-phenanthroline)bis(triphenylphosphine)copper(I) nitrate In toluene at 110℃; for 24h; | 99% |
2-Mercaptopyridine
Methoxycarbonylsulfenyl chloride
3-mercaptopropionic acid
3-(2-pyridyldithio)propionic acid
Conditions | Yield |
---|---|
In dichloromethane | 99% |
In dichloromethane | 99% |
2-Mercaptopyridine
(triphenylarsine)gold(I) chloride
triphenylarsinegold(I)-2-pyridinethiolato
Conditions | Yield |
---|---|
With sodium hydroxide In methanol addn. of NaOH and gold complex to pyridine soln. under N2; stirring, room temp., overnight; evapn.; washing (hexane); recrystn. (benzene); elem. anal.; | 99% |
2-Mercaptopyridine
1-adamantyl bromomethyl ketone
1-(adamantan-1-yl)-2-(pyridin-2-ylsulfanyl)ethan-1-one
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 20℃; | 99% |
With triethylamine In acetonitrile at 20℃; | 99% |
2-Mercaptopyridine
2-bromo-1-(2,4,6-trimethylphenyl)ethanone
2-(pyridin-2-ylsulfanyl)-1-(2,4,6-trimethyl-phenyl)-ethanone
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 20℃; | 99% |
2-Mercaptopyridine
Trimethylacetic acid
S-2'-pyridyl 2,2-dimethylpropanthioate
Conditions | Yield |
---|---|
With magnesium hydroxide; lithium hydroxide monohydrate; di-tert-butyl dicarbonate In dichloromethane at 25℃; for 24h; | 99% |
2-Mercaptopyridine
[tris(dimethylamino)phosphane]gold(I) chloride
Conditions | Yield |
---|---|
Stage #1: 2-Sulfanylpyridine With potassium hydroxide In ethanol at 20℃; for 0.5h; Stage #2: [tris(dimethylamino)phosphane]gold(I) chloride In ethanol at 20℃; for 24h; | 99% |
Conditions | Yield |
---|---|
With C55H43O4P In acetonitrile at 20℃; | 99% |
2-Mercaptopyridine
propynoic acid ethyl ester
(Z)-3-(pyridin-2-ylsulfanyl)-acrylic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: 2-Sulfanylpyridine With potassium hydroxide In ethanol at 20℃; for 0.166667h; Stage #2: propynoic acid ethyl ester In ethanol at 20℃; for 8h; | 98% |
With sodium hydroxide In ethanol at -18 - 20℃; for 22h; stereoselective reaction; | 98% |
In methanol at 100℃; for 0.133333h; Microwave irradiation; stereoselective reaction; | 83% |
With triethylamine In dichloromethane; dimethyl sulfoxide | 82% |
2-Mercaptopyridine
Chloromethyltrimethylsilane
2-(trimethylsilylmethylmercapto)pyridine
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In ethanol for 1h; Heating; | 98% |
Conditions | Yield |
---|---|
With triethylamine In methanol for 18h; 0 deg C to r.t.; | 98% |
2-Mercaptopyridine
(6-amino-5-bromopyridin-3-yl)phosphonate de diethyle
Conditions | Yield |
---|---|
With potassium tert-butylate In ammonia for 1.5h; Irradiation; | 98% |
Conditions | Yield |
---|---|
Stage #1: 2-Sulfanylpyridine With hydrogenchloride; sodium hypochlorite In dichloromethane; water at -10 - -5℃; for 0.25h; Stage #2: benzylamine In dichloromethane at 0℃; for 0.5h; | 98% |
Stage #1: 2-Sulfanylpyridine With hydrogenchloride; sodium hypochlorite In dichloromethane; water at -10 - -5℃; for 0.25h; Stage #2: benzylamine In dichloromethane; water at -78 - 0℃; for 0.5h; |
2-Mercaptopyridine
S-pyridin-2-yl (S)-3-methylpentanethioate
Conditions | Yield |
---|---|
Stage #1: (3S)-methylvaleric acid With oxalyl dichloride In dichloromethane at 25℃; for 2h; Stage #2: 2-Sulfanylpyridine With triethylamine In dichloromethane at 0 - 25℃; for 2h; | 98% |
2-Mercaptopyridine
(3S)-methylvaleric acid
S-pyridin-2-yl (S)-3-methylpentanethioate
Conditions | Yield |
---|---|
Stage #1: (3S)-methylvaleric acid With oxalyl dichloride In dichloromethane at 25℃; for 2h; Stage #2: 2-Sulfanylpyridine With triethylamine In dichloromethane at 0 - 25℃; for 2h; Further stages.; | 98% |
2-Mercaptopyridine
5-methoxylindole
3-(2-pyridylthio)-5-methoxyindole
Conditions | Yield |
---|---|
With oxone In methanol at 20℃; for 6h; | 98% |
2-Mercaptopyridine
Os(triphenylphosphine)3Br2
cis-trans-cis-{bis(pyridine-2-thiolato)bis(triphenylphosphine)osmium(II)}
Conditions | Yield |
---|---|
In ethanol refluxing (1 h); crystn. on cooling, filtration off, washing (EtOH), drying (vca.); elem. anal.; | 98% |
2-Mercaptopyridine
dichloro(2,2'-bipyridine)platinum(II)
Conditions | Yield |
---|---|
In water heated at 70°C for 24 h, an excess of NH4PF6 added; elem. anal.; | 98% |
2-Mercaptopyridine
fac-(acetonitrile){bis(diphenylphosphino)methane}tricarbonylmolydenum
[Mo(CO)3(η1-SC5H4NH)(η2-bis(diphenylphosphino)methane)]
Conditions | Yield |
---|---|
In methanol under N2; a soln. of Mo-contg. compd. (1.0 mmol) in MeOH was treated with pyridine-2-thione (1.0 mmol) in MeOH at room temp.; after 1 h the solid was isolated by filtration, washed with n-hexane, and dried under vac.; elem. anal.; | 98% |
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