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Puyang Huicheng Electronic Material Co., Ltd

Puyang Huicheng Electronic Material Co., Ltd was founded in 2002, which is focus on high complex new type intermediates and fine chemical custom synthesis, LED&OLED materials and related intermediates, catalyst design and synthesis.

best quality of 1,3-Bis(diphenylphosphino)propane

Cas:6737-42-4

Min.Order:100 Gram

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 1,3-Bis(Diphenylphosphino)Propane supplier in China

Cas:6737-42-4

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Wuhan Fortuna Chemical Co.,Ltd

High purity 1,3-Bis(diphenylphosphino)propane CAS 6737-42-4 in stock Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed

High purity 1,3-Bis(diphenylphosphino)propane CAS 6737-42-4 in stock

Cas:6737-42-4

Min.Order:10 Kilogram

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Hefei TNJ chemical industry co.,ltd

1. Quality Our products meet MSDS safe standard and we have ISO and other certificate so yan can get high quality products from our company. 2. Price We are the company which is the joint of trade and industry so we cao provide the competiti

1,3-Bis(diphenylphosphino)propane/CAS 6737-42-4

Cas:6737-42-4

Min.Order:25 Kilogram

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Henan Allgreen Chemical Co.,Ltd

high purity Storage:Sealed, dry, microtherm , avoid light and smell. Package:meet customer's demand Application:organic synthesis Transportation:by sea or by air Port:Shanghai, Qingdao

1,3-Bis(diphenylphosphino)propane

Cas:6737-42-4

Min.Order:1 Kilogram

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price OLED 99% 6737-42-4 1,3-Bis(diphenylphosphino)propane Manufacturer

Cas:6737-42-4

Min.Order:1 Gram

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Beijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)

Capability on chemical synthesis 1. Beijing High-Tech Enterprises 2. Strong R&D Team 3. 8 years of experiences in R & D of high-tech Catalyst; 4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on

1,3-Bis(diphenylphosphino)propane,DPPP

Cas:6737-42-4

Min.Order:0 Metric Ton

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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

1,3-Bis(diphenylphosphino)propane Manufacturer/High quality/Best price/In stock

Cas:6737-42-4

Min.Order:1 Kilogram

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1,3-Bis-(diphenylphosphino)-propane

Cas:6737-42-4

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

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Hebei yanxi chemical co.,LTD.

Hebei yanxi chemical co. LTD. has expanded a compositive entity from initially only as a small manufacturer. The company dedicated to the development, production and marketing of chemicals. After many years of efforts, we have established stable

1,3-bis(diphenyphosphino)propane

Cas:6737-42-4

Min.Order:1 Metric Ton

FOB Price: $1.0 / 2.0

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Henan Tianfu Chemical Co., Ltd.

Product Name: 1,3-Bis(diphenylphosphino)propane Synonyms: 1,3-BIS(DIPHENYLPHOSPHINE)PROPANE;1,3-BIS(DIPHENYLPHOSPHINO)PROPANE;DPPP;TRIMETHYLENEBIS(DIPHENYLPHOSPHINE);[3-(Diphenylphosphino)propyl](diphenyl)p

1,3-Bis(diphenylphosphino)propane_

Cas:6737-42-4

Min.Order:1 Kilogram

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

1,3-Bis(diphenylphosphino)propane CAS 6737-42-4

Cas:6737-42-4

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Standard CAS 6737-42-4 with fast shipping

Cas:6737-42-4

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

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Henan Sinotech Import&Export Corporation

Name 1,3-Bis(diphenylphosphino)propane/Propane-1,3-diylbis(diphenylphosphine) CAS NO. 6737-42-4 Molecular Formula C27H26P2 Molecular Weight

1,3-Bis(diphenylphosphino)propane CAS: 6737-42-4

Cas:6737-42-4

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1,3-Bis(diphenylphosphino)propane 6737-42-4

Cas:6737-42-4

Min.Order:1 Kilogram

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Shanghai Minstar Chemical Co., Ltd

1,3-Bis(diphenylphosphino)propane Basic information Product Name: 1,3-Bis(diphenylphosphino)propane Synonyms: 1,3-BIS(DIPHENYLPHOSPHINE)PROPANE;1,3-BIS(DIPHENYLPHOSPHINO)PROPANE;DPPP;TRIMETHYLENEBIS(DIPHENYLPHOSPHINE);[3-(Diphenylphosphino)pro

1,3-Bis(diphenylphosphino)propane

Cas:6737-42-4

Min.Order:1 Kilogram

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

catalyst, 1,3-Bis(diphenylphosphino)propane CAS:6737-42-4

Cas:6737-42-4

Min.Order:1 Kilogram

FOB Price: $30.4 / 36.2

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Qingdao Beluga Import and Export Co., LTD

1,3-Bis(diphenylphosphino)propane CAS:6737-42-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality

1,3-Bis(diphenylphosphino)propane CAS:6737-42-4

Cas:6737-42-4

Min.Order:1 Gram

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1,3-Bis(diphenylphosphino)propane

Cas:6737-42-4

Min.Order:1 Kilogram

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:6737-42-4

Cas:6737-42-4

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

1,3-Bis(Diphenylphosphino)Propane

Cas:6737-42-4

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

1,3-Bis(diphenylphosphino)propane

Cas:6737-42-4

Min.Order:4 Kilogram

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Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS 6737-42-4 1,3-Bis(diphenylphosphino)propane

Cas:6737-42-4

Min.Order:1 Kilogram

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1,3-Bis(diphenylphosphino)propane

Cas:6737-42-4

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 1,3-bis(diphenyphosphino)propane

Cas:6737-42-4

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Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products 1,3-Bis(diphenylphosphino)propane

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

1,3-Bis(diphenylphosphino)propane/High quality/Best price

Cas:6737-42-4

Min.Order:1 Gram

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 1,3-bis(diphenyphosphino)propane

Cas:6737-42-4

Min.Order:10 Gram

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Siwei Development Group Ltd.

Product name: 1,3-Bis(Diphenylphosphino)Propane CAS No.:6737-42-4 Molecule Formula:C27H26P2 Molecule Weight:412.44 Purity: 98.0% Package: 25kg/drum Description:Light yellow crystalline powder Manufacture Standards:Enterprise Standard

High Quality 1,3-Bis(Diphenylphosphino)Propane in stock

Cas:6737-42-4

Min.Order:1 Kilogram

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

1,3-Bis(diphenylphosphino)propane

Cas:6737-42-4

Min.Order:1 Gram

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Synthetic route

methanol
67-56-1

methanol

(propane-1,3-diyl)bis(diphenylphosphane)-borane(1:2)
100809-49-2

(propane-1,3-diyl)bis(diphenylphosphane)-borane(1:2)

A

Trimethyl borate
121-43-7

Trimethyl borate

B

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

Conditions
ConditionsYield
In toluene at 100℃; Inert atmosphere;A n/a
B 98%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

Conditions
ConditionsYield
Stage #1: chloro-diphenylphosphine With sodium In dibutyl ether at 105℃; for 2h;
Stage #2: 1.3-chlorobromopropane In dibutyl ether at 105℃; for 2h;
95%
(propane-1,3-diyl)bis(diphenylphosphane)-borane(1:2)
100809-49-2

(propane-1,3-diyl)bis(diphenylphosphane)-borane(1:2)

ethanol
64-17-5

ethanol

A

triethyl borate
150-46-9

triethyl borate

B

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

Conditions
ConditionsYield
Inert atmosphere; Reflux;A n/a
B 94%
1,3-bis(diphenylphosphoryl)propane
16524-41-7

1,3-bis(diphenylphosphoryl)propane

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

Conditions
ConditionsYield
With diisobutylaluminium hydride In toluene at 150℃; for 12h; Inert atmosphere;93%
With 1,1,3,3-Tetramethyldisiloxane; titanium(IV) isopropylate In various solvent(s) at 100℃; for 7h;91%
With diethoxymethylane; Bis(p-nitrophenyl) phosphate In toluene at 110℃; Inert atmosphere; chemoselective reaction;82%
With indium(III) bromide; 1,1,3,3-Tetramethyldisiloxane In toluene at 100℃; for 22h; Inert atmosphere; Sealed tube;80%
With hexylsilane; trifluorormethanesulfonic acid In toluene at 70℃; for 24h; Inert atmosphere; Sealed tube; chemoselective reaction;72 %Spectr.
1,3-dibromo-propane
109-64-8

1,3-dibromo-propane

diphenylphosphane
829-85-6

diphenylphosphane

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

Conditions
ConditionsYield
With cesium hydroxide; 4 Angstroem MS In N,N-dimethyl-formamide at 23℃; for 45h;83%
With cesium hydroxide; 4 A molecular sieve In N,N-dimethyl-formamide at 23℃; for 45h;83%
With tert-butylimino-tris(dimethylamino)phosphorane In tetrahydrofuran; diethyl ether for 24h; Ambient temperature;60%
C21H14N2O8
1273415-58-9

C21H14N2O8

chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

Conditions
ConditionsYield
With [Ir(ppy)2bpy]PF6; N-ethyl-N,N-diisopropylamine In 1,2-dichloro-ethane at 22℃; for 8h; Irradiation;82%
phenylmagnesium bromide
100-58-3

phenylmagnesium bromide

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium triflate / tetrahydrofuran / 2.25 h / 0 °C / Inert atmosphere; Reflux
2: diisobutylaluminium hydride / toluene / 12 h / 150 °C / Inert atmosphere
View Scheme
n-butyllithium
109-72-8, 29786-93-4

n-butyllithium

1,3-dibromo-propane
109-64-8

1,3-dibromo-propane

diphenylphosphane
829-85-6

diphenylphosphane

A

diphenyl(3-bromopropyl)phosphine

diphenyl(3-bromopropyl)phosphine

B

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

Conditions
ConditionsYield
Stage #1: n-butyllithium; diphenylphosphane In tetrahydrofuran; hexane at 20℃; for 0.833333h; Inert atmosphere;
Stage #2: 1,3-dibromo-propane In tetrahydrofuran; hexane at 20℃; for 0.333333h; Inert atmosphere; Overall yield = 396.6 mg;
latter phosphonate

latter phosphonate

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

dimethyl 1-octen-2-yl-phosphonate
174781-89-6

dimethyl 1-octen-2-yl-phosphonate

dimethyl (E)-octenylphosphonate

dimethyl (E)-octenylphosphonate

Conditions
ConditionsYield
In palladium diacetate100%
In 1,3-bis(dimethylphosphino)propane85%
(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonylmolybdenum(0)
12146-37-1, 124717-04-0

(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonylmolybdenum(0)

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

A

tetracarbonyl-1,3-bis(diphenylphosphino)propane-molybdenum(0)
15553-68-1

tetracarbonyl-1,3-bis(diphenylphosphino)propane-molybdenum(0)

B

bicyclo[2.2.1]hepta-2,5-diene
121-46-0

bicyclo[2.2.1]hepta-2,5-diene

Conditions
ConditionsYield
In tetrahydrofuran reaction in a calorimeter under argon;A 100%
B n/a
[Rh(dppp)(CO)2]2

[Rh(dppp)(CO)2]2

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

hydrogen
1333-74-0

hydrogen

RhH(CO)(C6H5)2PCH2CH2CH2P(C6H5)2(C6H5)2P(CH2)3P(C6H5)2
81524-37-0

RhH(CO)(C6H5)2PCH2CH2CH2P(C6H5)2(C6H5)2P(CH2)3P(C6H5)2

Conditions
ConditionsYield
In dichloromethane-d2 total pressure: 1 atm; 1.0-6.0 h; room temperature; dpp:Rh2 ratio=6.2:1;; no isolation; NMR-spectroscopic characterization;;100%
In dichloromethane-d2 total pressure: 1 atm; 10 h; room temperature; dpp:Rh2 ratio=19.8:1;; no isolation; NMR-spectroscopic characterization;;80%
In dichloromethane-d2 total pressure: 1 atm; 0.2 h; room temperature; dpp:Rh2 ratio=6.2:1; about 20-25 % unknown hydrides;; no isolation; NMR-spectroscopic characterization;;60%
With carbon monoxide In dichloromethane-d2 total pressure: 1 atm; 0.2 h; room temperature; dpp:Rh2 ratio=6.1:1;H2:CO=1:1; about 20-25 % unknown hydrides detected;; no isolation; NMR-spectroscopic characterization;;14%
chloromethyl(1,5-cyclooctadiene)palladium(II)

chloromethyl(1,5-cyclooctadiene)palladium(II)

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

[PdCl(CH3)(bis(diphenylphosphino)propane)]
139168-06-2

[PdCl(CH3)(bis(diphenylphosphino)propane)]

Conditions
ConditionsYield
In dichloromethane under N2 at room temp. in darkness, 1:1 mixt., stirred for 1.5 h; pptd., filtered, washed (ether), dried (vac.), NMR;100%
chlorobis(1,3-diphenylphosphinopropane)-exo-nido-[10-hydroorthocarborane-5,6,10-tris(hydrido)]ruthenium

chlorobis(1,3-diphenylphosphinopropane)-exo-nido-[10-hydroorthocarborane-5,6,10-tris(hydrido)]ruthenium

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

bis(1,3-diphenylphosphinopropane)chlororuthenium(II) nido-7,8-dicarbaundecaborate dichloromethane

bis(1,3-diphenylphosphinopropane)chlororuthenium(II) nido-7,8-dicarbaundecaborate dichloromethane

Conditions
ConditionsYield
In benzene benzene added to equimolar mixt. of Ru-carborane-complex and (PPh2)2(CH2)3, stirred at 22°C for 2-3 h; ppt. filtered off, washed (C6H6), recrystd. (CH2Cl2-hexane); elem. anal.;100%
chlorobis(1,3-diphenylphosphinopropane)-exo-nido-[7,8-dimethyl-10-hydroorthocarborane-5,6,10-tris(hydrido)]ruthenium(II) semidichloromethane

chlorobis(1,3-diphenylphosphinopropane)-exo-nido-[7,8-dimethyl-10-hydroorthocarborane-5,6,10-tris(hydrido)]ruthenium(II) semidichloromethane

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

bis(1,3-diphenylphosphinopropane)chlororuthenium(II) nido-7,8-dimethyl-7,8-dicarbaundecaborate dichloromethane

bis(1,3-diphenylphosphinopropane)chlororuthenium(II) nido-7,8-dimethyl-7,8-dicarbaundecaborate dichloromethane

Conditions
ConditionsYield
In benzene benzene added to equimolar mixt. of Ru-carborane-complex and (PPh2)2(CH2)3, stirred at 22°C for 2-3 h; ppt. filtered off, washed (C6H6), recrystd. (CH2Cl2-hexane); elem. anal.;100%
Pt(Sn(CH3)3)2(P(CH3C6H4)3)2

Pt(Sn(CH3)3)2(P(CH3C6H4)3)2

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

Pt(Sn(CH3)3)2(C6H5)2P(CH2)3P(C6H5)2

Pt(Sn(CH3)3)2(C6H5)2P(CH2)3P(C6H5)2

Conditions
ConditionsYield
99%
dichloro(1,5-cyclooctadiene)palladium(II)
12107-56-1

dichloro(1,5-cyclooctadiene)palladium(II)

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

[1,3-bis(diphenylphosphino)propane]dichloridepalladium(II)
59831-02-6

[1,3-bis(diphenylphosphino)propane]dichloridepalladium(II)

Conditions
ConditionsYield
In dichloromethane for 2h; Inert atmosphere;99%
1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

N-(2-cyclopropylideneethyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide

N-(2-cyclopropylideneethyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide

cobalt(II) bromide

cobalt(II) bromide

C42H44CoNO2P2S

C42H44CoNO2P2S

Conditions
ConditionsYield
With zinc(II) iodide; zinc In acetonitrile at 20 - 25℃; for 2h; Inert atmosphere; Sealed tube;99%
2-trifluoromethanesulfonyloxy-8-acetylaminonaphthalene
168901-50-6

2-trifluoromethanesulfonyloxy-8-acetylaminonaphthalene

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

palladium diacetate
3375-31-3

palladium diacetate

8-acetylamino-2-naphthoic acid, methyl ester

8-acetylamino-2-naphthoic acid, methyl ester

Conditions
ConditionsYield
With dimethyl sulfoxide; triethylamine In methanol98.5%
hydrogenchloride
7647-01-0

hydrogenchloride

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

palladium
7440-05-3

palladium

bis(diphenylphosphino)propanepalladium(II) dichloride
59831-02-6

bis(diphenylphosphino)propanepalladium(II) dichloride

Conditions
ConditionsYield
Stage #1: hydrogenchloride; palladium With nitric acid In water
Stage #2: 1,3-bis-(diphenylphosphino)propane In water; N,N-dimethyl-formamide at 50℃; for 1h;
98.1%
di(pyridin-2-yl)amine
1202-34-2

di(pyridin-2-yl)amine

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

silver perchlorate

silver perchlorate

[Ag2(bis(2-pyridyl)amine)2(dppp)(ClO4)2]
936008-61-6

[Ag2(bis(2-pyridyl)amine)2(dppp)(ClO4)2]

Conditions
ConditionsYield
In acetonitrile stoich. mixt. in CH3CN stirred for 12 h at room temp.; evapd., washed (Et2O), elem. anal.;98%
2,2':6,2''-terpyridine
1148-79-4

2,2':6,2''-terpyridine

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

silver perchlorate

silver perchlorate

[Ag2(2,2':6',6''-terpyridyl)2(dppp)][ClO4]2

[Ag2(2,2':6',6''-terpyridyl)2(dppp)][ClO4]2

Conditions
ConditionsYield
In acetonitrile stoich. mixt. in CH3CN stirred for 12 h at room temp.; evapd., washed (Et2O), elem. anal.;98%
(C8H12)Pt(CH3C(O)NCH2COO)
142316-59-4

(C8H12)Pt(CH3C(O)NCH2COO)

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

((C6H5)2P(CH2)3P(C6H5)2)Pt(CH3C(O)NCH2COO)
142316-57-2

((C6H5)2P(CH2)3P(C6H5)2)Pt(CH3C(O)NCH2COO)

Conditions
ConditionsYield
In dichloromethane N2; stirred for 20 min at room temp.; evapd. to dryness under reduced pressure, crystd. from CH2Cl2/light petroleum; NMR;98%
(C8H12)Pt(CH3C(O)NCH(CH2C6H5)COO)

(C8H12)Pt(CH3C(O)NCH(CH2C6H5)COO)

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

((C6H5)2P(CH2)3P(C6H5)2)Pt(CH3C(O)NCH(CH2C6H5)COO)*H2O

((C6H5)2P(CH2)3P(C6H5)2)Pt(CH3C(O)NCH(CH2C6H5)COO)*H2O

Conditions
ConditionsYield
In dichloromethane N2; stirred for 15 min at room temp.; evapd. to dryness under reduced pressure, crystd. from CH2Cl2/light petroleum; NMR;98%
cis-dichloro(dimethylaminomethylene)(triphenylarsine)platinum(II)

cis-dichloro(dimethylaminomethylene)(triphenylarsine)platinum(II)

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

[1,3-bis(diphenylphosphino)propane](dimethylaminomethylene)(chloro)platinum(II) chloride - H2O (2/1)

[1,3-bis(diphenylphosphino)propane](dimethylaminomethylene)(chloro)platinum(II) chloride - H2O (2/1)

Conditions
ConditionsYield
With H2O In chloroform-d1 CDCl3; evapd., the residue was washed with pentane, crystd. from CH2Cl2-hexane (elem. anal.);98%
1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

nickel(II) acetate tetrahydrate
6018-89-9

nickel(II) acetate tetrahydrate

Thiosalicylic acid
147-93-3

Thiosalicylic acid

[Ni(SC6H4CO2)(C27H26P2)]
195049-36-6

[Ni(SC6H4CO2)(C27H26P2)]

Conditions
ConditionsYield
With pyridine In methanol dissoln. of the Ni salt and the ligand in MeOH with warming, addn. of thiosalicylic acid, then pyridine, short reflux; filtration, washing (cold MeOH; Et2O), drying, recrystn. (CH2Cl2/Et2O); elem. anal.;98%
[(COD)Rh(μ-,kappa.O,O'-HCO2)]2
125979-15-9

[(COD)Rh(μ-,kappa.O,O'-HCO2)]2

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

Rh(η(3)-cyclooctenyl)(Ph2P(CH2)3PPh2)
177283-23-7

Rh(η(3)-cyclooctenyl)(Ph2P(CH2)3PPh2)

Conditions
ConditionsYield
In tetrahydrofuran Ar-atmosphere; slow addn. of 1 equiv. of phosphine to Rh-complex soln. at -78°C, stirring for 20 min, slow warming to room temp., stirring for 30 min; solvent removal, drying (vac., 1 d);98%
nickel(II) chloride hexahydrate

nickel(II) chloride hexahydrate

dimercaptomaleonitrile disodium salt hydrate

dimercaptomaleonitrile disodium salt hydrate

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

(maleonitriledithilato)(1,3-bis(diphenylphosphino)propane)nickel(II)
635315-48-9

(maleonitriledithilato)(1,3-bis(diphenylphosphino)propane)nickel(II)

Conditions
ConditionsYield
In acetone mixt. of solids NiCl2*6H2O (1 mmol) and Ph2PCH2CH2CH2P(Ph)2 (0.41 g) in acetone stirred for 1 h; pptd. by H2O addn. with stirring; ppt. filtered off; washed (H2O, EtOH, Et2O); dried at room temp.; elem. anal.;98%
potassium tetrachloroplatinate(II)
10025-99-7

potassium tetrachloroplatinate(II)

1,3-bis-(diphenylphosphino)propane
6737-42-4

1,3-bis-(diphenylphosphino)propane

{1,3-bis(diphenylphosphino)propane}platinumCl2
59329-00-9

{1,3-bis(diphenylphosphino)propane}platinumCl2

Conditions
ConditionsYield
With hydrogenchloride In ethanol; water at 90℃; for 3h;98%

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