Product description: Product name 1-Bromo-3-chloropropane CAS number 109-70-6 Assay ≥99% Appearance Colorless transparent liquid Capacity 500mt/year Application Pharmaceutica
Cas:109-70-6
Min.Order:1 Kilogram
FOB Price: $12.0
Type:Lab/Research institutions
inquiry1-Bromo-3-chloropropane CAS:109-70-6 Specification Product name 1-Bromo-3-chloropropane CAS number 109-70-6 Assay ≥99% Appearance Colorless transparent liquid Capacity 500mt/year
Cas:109-70-6
Min.Order:1 Kilogram
Negotiable
Type:Other
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
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Cas:109-70-6
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryName: 1-Bromo-3-chloropropane Synonyms: 1-bromo-3-chloro-propan;3-Bromo-1-chloropropane;3-Chloro-1Chemicalbook-bromopropane;omega-Chlorobromopropane;Propane,1-bromo-3-chloro-;Trimethylenebromidechloride;trimethylenebromidechloride;TRIMETHYLENECHLOROB
Conditions | Yield |
---|---|
With hydrogen bromide; dibenzoyl peroxide In benzene at 20℃; for 6h; | 92% |
With hydrogen bromide | |
With hydrogen bromide |
3-chloropropyl p-toluenesulfonate
diethyl ether
A
1-Chloropentane
B
1,3-chlorobromopropane
3-chloropropyl p-toluenesulfonate
diethyl ether
A
decyl chloride
B
1,3-chlorobromopropane
Conditions | Yield |
---|---|
With sulfuryl dichloride; dibenzoyl peroxide | |
With sulfuryl dichloride; dilauryl peroxide | |
With sulfuryl dichloride; dilauryl peroxide | |
With sulfuryl dichloride; dibenzoyl peroxide | |
With chlorine at 25 - 180℃; |
Conditions | Yield |
---|---|
With ethyl bromide; aluminum tri-bromide at 2 - 5℃; |
Conditions | Yield |
---|---|
With ethyl bromide; aluminum tri-bromide at 2 - 5℃; |
3-chloroprop-1-ene
A
2-bromo-1-chloropropane
B
1,3-chlorobromopropane
Conditions | Yield |
---|---|
With hydrogen bromide | |
With hydrogen bromide | |
With hydrogen bromide |
Conditions | Yield |
---|---|
With sulfuric acid; hydrogen bromide dann Destillieren; | |
With phosphorus tribromide | |
With phosphorus tribromide |
hydrogen bromide
bromine
3-chloroprop-1-ene
1,3-chlorobromopropane
Conditions | Yield |
---|---|
in Gegenwart von Feuchtigkeit; |
Conditions | Yield |
---|---|
in Gegenwart von Feuchtigkeit; |
Conditions | Yield |
---|---|
in Gegenwart von Feuchtigkeit; |
1,3-chlorobromopropane
Conditions | Yield |
---|---|
With diethyl ether |
sulfuryl dichloride
dilauryl peroxide
propyl bromide
A
1-bromo-2-chloropropane
B
1,3-chlorobromopropane
sulfuryl dichloride
propyl bromide
dibenzoyl peroxide
A
1-bromo-2-chloropropane
B
1,3-chlorobromopropane
hydrogen bromide
3-chloroprop-1-ene
A
2-bromo-1-chloropropane
B
1,3-chlorobromopropane
Conditions | Yield |
---|---|
at -18 - 18℃; | |
unter verschiedenen Bedingungen; | |
unter verschiedenen Bedingungen; |
hydrogen bromide
acetic acid
3-chloroprop-1-ene
A
2-bromo-1-chloropropane
B
1,3-chlorobromopropane
Conditions | Yield |
---|---|
at -18 - 18℃; |
ethyl bromide
aluminium bromide
1,3-Dichloropropane
A
1,3-chlorobromopropane
B
1,3-dibromo-propane
Conditions | Yield |
---|---|
at 2 - 5℃; |
Conditions | Yield |
---|---|
With hydrogen bromide at 100℃; |
Conditions | Yield |
---|---|
With mercury dichloride |
Conditions | Yield |
---|---|
beim Kochen; |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 25℃; for 12h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 1h; | 98% |
Stage #1: thiophenol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 1h; Inert atmosphere; Stage #2: 1.3-chlorobromopropane In tetrahydrofuran at 0 - 20℃; for 24h; Inert atmosphere; | 95% |
Isobutyronitrile
1,3-chlorobromopropane
5-chloro-2,2-dimethylpentanenitrile
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane at 70℃; for 16h; | 100% |
With lithium hexamethyldisilazane at 70℃; for 16h; | 100% |
With lithium hexamethyldisilazane at 70℃; for 16h; | 100% |
1,3-chlorobromopropane
para-thiocresol
γ-chloropropyl 4-methylphenyl sulphide
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; | 100% |
With sodium hydroxide In ethanol at 100℃; | 65% |
With potassium hydroxide |
2,3-dihydro-2H-furan
1,3-chlorobromopropane
5-(3-chloropropyl)-2,3-dihydrofuran
Conditions | Yield |
---|---|
Stage #1: 2,3-dihydro-2H-furan With tert.-butyl lithium In tetrahydrofuran; pentane at -78 - 0℃; for 3h; Inert atmosphere; Stage #2: 1.3-chlorobromopropane In tetrahydrofuran; pentane at -78℃; for 14h; Inert atmosphere; | 100% |
With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium 1.) THF, from -78 deg C to 0 deg C, 1.25 h, 2.) THF, from 0 deg C to 25 deg C, 7.33 h; Yield given. Multistep reaction; |
2,6-dihydroxylacetophenone
1,3-chlorobromopropane
2-(3-chlorophenoxy)-6-hydroxyacetophenone
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 24h; Heating; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 70℃; for 4h; | 46% |
With potassium carbonate In acetone |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 24h; Williamson Ether Synthesis; Reflux; | 100% |
With potassium carbonate In acetone for 24h; Heating; | 71% |
With potassium carbonate In acetone for 24h; Heating; | 70% |
1,3-chlorobromopropane
4-Hydroxyacetophenone
1-[4-(3-chloropropoxy)phenyl]ethanone
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 65℃; for 18h; | 100% |
With potassium carbonate In acetone at 65℃; | 99% |
With potassium carbonate In acetone at 65℃; | 99% |
1,3-chlorobromopropane
meta-hydroxyacetanilide
N-<3-(3-chloropropoxy)phenyl>acetamide
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 16h; Heating; | 100% |
With sodium hydroxide In ethanol for 8h; Heating; | 65% |
1,3-chlorobromopropane
N-(3,3-dimethoxy-2-butylidene)isopropylamine
N-(7-chloro-2,2-dimethoxy-3-heptylidene)isopropylamine
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran; hexane 1.) 0 deg C, 3 h, 2.) rt, 20 h; | 100% |
Stage #1: N-(3,3-dimethoxy-2-butylidene)isopropylamine With lithium diisopropyl amide In tetrahydrofuran; hexane at 0℃; for 3h; Stage #2: 1.3-chlorobromopropane In tetrahydrofuran; hexane at 0 - 20℃; for 20h; | 98% |
1,3-chlorobromopropane
2-nitro-10H-indolo[3,2-b]quinoline
2-nitro-10-chloropropylindolo[3,2-b]quinoline
Conditions | Yield |
---|---|
With sodium hydroxide; dimethyl sulfoxide at 20℃; for 4h; Substitution; | 100% |
benzoimidazole
1,3-chlorobromopropane
1-(Benzimidazol-1-yl)-3-chloropropane
Conditions | Yield |
---|---|
Stage #1: benzoimidazole With sodium hydride In 1-methyl-pyrrolidin-2-one at 20℃; for 0.5h; Stage #2: 1.3-chlorobromopropane In 1-methyl-pyrrolidin-2-one at 20 - 100℃; for 76h; | 100% |
With tetrabutylammomium bromide; sodium hydroxide In water at 60℃; for 2.08333h; | 62% |
With sodium hydride 1) acetonitrile, reflux, 1 h; 2) acetonitrile, reflux, 2 h; Yield given; Multistep reaction; | |
With potassium carbonate In acetone for 12h; Reflux; |
methyl 4'-hydroxy-4-biphenylcarboxylate
1,3-chlorobromopropane
Methyl 4'-(3-chloropropoxy)[1,1'-biphenyl]-4-carboxylate
Conditions | Yield |
---|---|
With potassium carbonate In butanone for 24h; Heating; | 100% |
With potassium carbonate In butanone | 92% |
With potassium carbonate In butanone | 92% |
2-fluoro-4-hydroxybenzonitrile
1,3-chlorobromopropane
4-(3-chloropropoxy)-2-fluorobenzonitrile
Conditions | Yield |
---|---|
With potassium carbonate In butanone Heating; | 100% |
1,3-chlorobromopropane
1-(3,5-difluoro-4-hydroxyphenyl)ethanone
1-[4-(3-chloro-propoxy)-3,5-difluoro-phenyl]-ethanone
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 20h; Heating / reflux; | 100% |
4-(5-methyl-4, 5,6,7-tetrahydro[1,3]oxazolo[4,5-c]pyridin-2-yl)phenol
1,3-chlorobromopropane
Conditions | Yield |
---|---|
With potassium carbonate In butanone for 4h; Heating / reflux; | 100% |
4-(4-acetyl-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-b]azepin-2-yl)phenol
1,3-chlorobromopropane
Conditions | Yield |
---|---|
With potassium carbonate In butanone for 20h; Heating / reflux; | 100% |
In ethyl acetate for 20h; Reflux; | 100% |
1,3-chlorobromopropane
5-hydroxy-1,3-dihydro-1-isoindolone
5-(3-chloro-propoxy)-2,3-dihydro-isoindol-1-one
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetonitrile for 18h; Heating / reflux; | 100% |
1,3-chlorobromopropane
potassium thioacetate
thioacetic acid S-(3-chloropropyl) ester
Conditions | Yield |
---|---|
In tetrahydrofuran for 1h; Heating; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 20h; Heating / reflux; | 100% |
With potassium carbonate In acetone | 100% |
With potassium carbonate In acetone Heating / reflux; | 98% |
1,3-chlorobromopropane
7-hydroxy-6-methoxy-3-pivaloyloxymethyl-3,4-dihydroquinazolin-4-one
7-(3-chloropropoxy)-6-methoxy-3-((pivaloyloxy)methyl)-3,4-dihydroquinazolin-4-one
Conditions | Yield |
---|---|
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 20℃; | 100% |
1,3-chlorobromopropane
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide; acetone; mineral oil | 100% |
1,3-chlorobromopropane
1,3-bis(2,2-dimethyl-5-chloropentanoyloxy)-propane
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran; water | 100% |
1,3-chlorobromopropane
2-fluoro-4-hydroxybenzoic acid
3-chloropropyl 4-(3-chloropropoxy)-2-fluorobenzoate
Conditions | Yield |
---|---|
With potassium carbonate In butanone at 80℃; | 100% |
4-bromo-2-fluorophenol
1,3-chlorobromopropane
4-bromo-1-(3-chloro-propoxy)-2-fluoro-benzene
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 3h; Product distribution / selectivity; Heating / reflux; | 100% |
1,3-chlorobromopropane
Conditions | Yield |
---|---|
Stage #1: 8-[2-(6,6-dimethyl-bicyclo[3.1.1]hept-2-yl)-ethyl]-1-phenyl-1,3,8-triaza-spiro[4.5]decan-4-one With potassium tert-butylate In tetrahydrofuran at 0℃; for 0.5h; Stage #2: 1.3-chlorobromopropane In tetrahydrofuran at 0 - 50℃; for 4h; | 100% |
tert-butyl 1H-indole-2-carboxylate
1,3-chlorobromopropane
tert-butyl 1-(3-chloropropyl)-1H-indole-2-carboxylate
Conditions | Yield |
---|---|
Stage #1: tert-butyl 1H-indole-2-carboxylate With sodium hydride In N,N-dimethyl-formamide Stage #2: 1.3-chlorobromopropane In N,N-dimethyl-formamide at 60℃; for 16h; | 100% |
1,3-chlorobromopropane
3,3-difluoro-1,3-dihydro-2H-indol-2-one
1-(3-chloropropyl)-3,3-difluoroindolin-2-one
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 16h; | 100% |
1,3-chlorobromopropane
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 3h; Reflux; | 100% |
With potassium carbonate In acetonitrile for 3h; Reflux; | 96% |
With potassium carbonate In acetonitrile for 3h; Reflux; | 96% |
4-(4-hydroxy-phenyl)-piperidine-1-carboxylic acid tert-butyl ester
1,3-chlorobromopropane
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 80℃; for 16h; | 100% |
With potassium carbonate In acetone at 90℃; for 40h; |
1-tert-butyl 3-ethyl 4-oxopiperidine-1,3-dicarboxylate
1,3-chlorobromopropane
Conditions | Yield |
---|---|
Stage #1: 1-tert-butyl 3-ethyl 4-oxopiperidine-1,3-dicarboxylate With potassium tert-butylate In tetrahydrofuran at -20℃; for 0.5h; Stage #2: 1.3-chlorobromopropane In tetrahydrofuran at 15℃; Inert atmosphere; | 100% |
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