CAS No.109-72-8,n-Butyllithium Suppliers

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures

n-Butyllithium

Cas:109-72-8

Min.Order:1 Kilogram

FOB Price: $40.0 / 60.0

Type:Lab/Research institutions

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

n-Butyllithium Manufacturer/High quality/Best price/In stock

Cas:109-72-8

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality N-Butyllithium supplier in China

Cas:109-72-8

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai

n-Butyllithium

Cas:109-72-8

Min.Order:1 Pound

Negotiable

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Butyllithium

Cas:109-72-8

Min.Order:1

Negotiable

Type:Other

inquiry

Enke Pharma-tech Co.,Ltd. （Cangzhou, China ）

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi

n-Butyllithium

Cas:109-72-8

Min.Order:1 Kilogram

FOB Price: $5.0

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Butyllithium

Cas:109-72-8

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei yanxi chemical co.,LTD.

Hebei yanxi chemical co., LTD is a professional research, development and production Cyromazine、lead diacetate trihydrate /Lead acetate trihydrateC、 2-phenylacetamide 、 4-Aminophenyl-1-phenethylpiperidine 、Citric acid monohydrate 、 Citric acid/citr

butyllithium CAS:109-72-8

Cas:109-72-8

Min.Order:1 Metric Ton

FOB Price: $0.1

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

n-Butyllithium CAS 109-72-8

Cas:109-72-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com Product Name n-Butyllithium CAS No. 109-72-8

n-Butyllithium

Cas:109-72-8

Min.Order:1 Gram

FOB Price: $12.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

n-Butyllithium

Cas:109-72-8

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

HPLC 98% CAS 109-72-8 with best quality

Cas:109-72-8

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

inquiry

Wuhan Han Sheng New Material Technology Co.，Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

n-buli/n-Butyllithium 109-72-8

Cas:109-72-8

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

Chemical Name: n-Butyllithium Synonyms: Butyl-lithiu; NBL, BuLi,1-lithiobutane CAS No.: 109-72-8 Molecular Formula: CH3CH2CH2CH2-Li UN: 2445 Properties: Colorless or slightly yellow, suspended solids and transparent liquid, Soluble in Hex

n-Butyllithium manufacturer,CAS:109-72-8

Cas:109-72-8

Min.Order:10 Metric Ton

FOB Price: $1.0

Type:Other

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

n-Butyllithium

Cas:109-72-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta

high quality 109-72-8 n-Butyllithium with best price

Cas:109-72-8

Min.Order:10 Gram

Negotiable

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Lithium, butyl- 109-72-8

Cas:109-72-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: n-Butyllithium CAS: 109-72-8 MF: C4H9Li MW: 64.06 EINECS: 203-698-7 Mol File: 109-72-8.mol n-Butyllithium Structure n-Butyllithium Chemical Properties Melting point -95 °C Boiling point 80 °C density

n-Butyllithium

Cas:109-72-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

catalyst, n-Butyllithium CAS:109-72-8

Cas:109-72-8

Min.Order:1 Kilogram

FOB Price: $21.0 / 24.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

n-Butyllithium CAS: 109-72-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediat

n-Butyllithium CAS: 109-72-8

Cas:109-72-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

cas 109-72-8 n-Butyllithium

Cas:109-72-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:109-72-8

Cas:109-72-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Product Detail Minimum Order Qty. 10 Gram

BUTYLLITHIUM CAS NO.109-72-8

Cas:109-72-8

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Lonwin Chemical Group Limited

n-Butyllithium CAS：109-72-8 Specification mp -95 °c bp 80 °c density 0.68 g/ml at 20 °c fp 10 °f storage temp. 2-8°c form liquid color yellow

Factory supply n-Butyllithium

Cas:109-72-8

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Triumph International Development Limilted

Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:By Sea/Air/Courier Port:Qingdao

n-Butyllithium 109-72-8

Cas:109-72-8

Min.Order:1 Kilogram

FOB Price: $16.0 / 20.0

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

n-buli

Cas:109-72-8

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

n-Butyllithium

Cas:109-72-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

n-Butyllithium

Cas:109-72-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

n-Butyllithium

Cas:109-72-8

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality N-Butyllithium

Cas:109-72-8

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Synthetic route

: 109-72-8
n-butyllithium

: C5H4FeC5H3(CH(CH3)CH2CH(C5H5))(C(H)C12H8)

: C5H4FeC5H3(CH(CH3)CH2CH(C5H4))(CC12H8)(2-)*2Li(1+)=C5H4FeC5H3(CHCH3CH2CHC5H4Li)(CLiC12H8)

Conditions

Conditions	Yield
In toluene; pentane (Ar); 1.6 M n-BuLi in pentane was added at 0°C to soln. of ferrocene in toluene, stirred for 6 h at room temp.; filtered, washed with pentane, dried in vac., elem. anal.;	93%

: 109-72-8
n-butyllithium

: 384378-22-7
(CH3)2Ge(C5(CH3)4H)(C5H5)

: 2Li(1+)*(CH3)2Ge(C5(CH3)4)(C5H4)(2-)=Li2[(CH3)2Ge(C5(CH3)4)(C5H4)]

Conditions

Conditions	Yield
In diethyl ether under N2, Schlenk technique; mixing at -78°C (BuLi in hexane), mixt. was warmed to room temp. and stirred for 15 h; solvent was removed, ppt. was washed with hexane, dried under vac.; elem. anal.;	92%

: 109-72-8
n-butyllithium

: 13292-87-0
dimethyl sulfide borane

A: lithium borohydride

B: 82111-98-6
lithium [butyl(trihydrido)borate]

C: 67335-72-2
LiHB(s-Bu)3

Conditions

Conditions	Yield
In tetrahydrofuran; hexane; dichloromethane under dry N2, hexane soln. of BuLi cooled to -20°C, H3B-SMe2 added to vigorously stirred soln. within 60 min, 2 hours later all volatiles removed in vac.; material suspended in hexane, THF added to form soln., solvents removed, oily material dissolved in CH2Cl2, pentane added to separate LiBH4, repetition of procedure gave slightly purer product;	A n/a B 91% C n/a

...Expand

: 109-72-8
n-butyllithium

: 134939-44-9
bis(tetramethylcyclopentadienyl)dimethylgermanium

: 2Li(1+)*(CH3)2Ge(C5(CH3)4)2(2-)=Li2[(CH3)2Ge(C5(CH3)4)2]

Conditions

Conditions	Yield
In diethyl ether under N2, Schlenk technique; mixing at -78°C (BuLi in hexane), mixt. was warmed to room temp. and stirred for 15 h; solvent was removed, ppt. was washed with hexane, dried under vac.; elem. anal.;	91%

: 109-72-8
n-butyllithium

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 1231953-83-5
trimethylamine borane

A: lithium borohydride

B: Li(tetramethylethylenediamine)BH3(benzyl)

Conditions

Conditions	Yield
In hexane; toluene byproducts: (CH3)3N; under dry N2, hexane soln. of n-BuLi added to soln. of TMEDA in toluene, after 30 min added H3B-NMe3, heated for 1 h to reflux, soln. kept for 3 d at -25°C; elem. anal.;	A 10% B 90%

...Expand

: 109-72-8
n-butyllithium

: 478038-85-6
(CH3)2Ge(C5(CH3)4H)(C5H4CH3)

: 2Li(1+)*(CH3)2Ge(C5(CH3)4)(C5H3CH3)(2-)=Li2[(CH3)2Ge(C5(CH3)4)(C5H3CH3)]

Conditions

Conditions	Yield
In diethyl ether under N2, Schlenk technique; mixing at -78°C (BuLi in hexane), mixt. was warmed to room temp. and stirred for 15 h; solvent was removed, ppt. was washed with hexane, dried under vac.; elem. anal.;	90%

: 7446-70-0
aluminium trichloride

: 109-72-8
n-butyllithium

: 443890-22-0
N-(2,6-bis(isopropyl)phenyl)-5-tert-butylpyrrolylaldimine

: 443890-21-9
[N-(2,6-bis(isopropyl)phenyl)-5-tert-butylpyrrolylaldiminato]aluminium(III) dichloride

Conditions

Conditions	Yield
In toluene under N2, Schlenk techques; n-BuLi was added to the soln. of ligand at -35°C, mixt. was warmed to room temp., stirred for 2 h, soln. was cooled to -35°C again and added to suspn. of AlCl3 with stirring,mixt. stirred at room temp. for 36 h; mixt. was filtered, washed with toluene, filtrate was concd., cooled to -35°C; elem. anal.;	88%

...Expand

: 109-72-8
n-butyllithium

: 13292-87-0
dimethyl sulfide borane

A: lithium borohydride

B: 82111-98-6
lithium [butyl(trihydrido)borate]

C: n-butylborane-dimethyl sulfide

D: 15243-31-9
Li{B(n-C4H9)4}

Conditions

Conditions	Yield
In tetrahydrofuran; hexane under dry N2, hexane soln. of n-BuLi cooled to -20°C, H3B-SMe2 added to vigorously stirred soln. within 4 h, resulting suspn. stirred overnight; filtered, detected by NMR;	A 13% B 87% C n/a D n/a
In hexane; dichloromethane; pentane under dry N2, hexane soln. of BuLi cooled to -20°C, H3B*SMe2 added to vigorously stirred soln. within 4 h, stirred overnight, solid filtered, solvent from filtrate removed; residue treated with 1:1 mixt. of CH2Cl2 and pentane, not isolated, detected in CH2Cl2-rich phase by NMR;

...Expand

: 109-72-8
n-butyllithium

: 519005-12-0, 439099-43-1
buta-1,3-dien-2-yltin trichloride

: 2244-38-4
buta-1,3-dien-2-yl-tributylstannane

Conditions

Conditions	Yield
In not given	86%

: 109-72-8
n-butyllithium

: 16390-61-7
1-phenyl-1,2-closo-C2B10H11

: 109-94-4
formic acid ethyl ester

: 16450-20-7
1-(CH(o-CB10H10CC6H5)OH)-2-(C6H5)-1.2-C2B10H10

Conditions

Conditions	Yield
With hydrogenchloride In diethyl ether; benzene nitrogen atmosphere; ether soln. of formate addn. at 50 to 60°C to benzene soln. of Li-salt of carborane (obtained from carborane and BuLi), stirring (1 h), treating with aq. HCl, extracting with ether; extract drying over MgSO4 and evapn., residue recrystn. (hexane);	85%

...Expand

: 109-72-8
n-butyllithium

: 60-29-7
diethyl ether

: 443890-22-0
N-(2,6-bis(isopropyl)phenyl)-5-tert-butylpyrrolylaldimine

: 13499-05-3
hafnium tetrachloride

: 610270-20-7
[Hf(5-tert-butyl-2-[(2,6-diisopropylphenyl)aldimino]pyrrolyl)Cl2(μ-Cl)2Li(OEt2)2]

Conditions

Conditions	Yield
In diethyl ether under N2, Schlenk techques; n-BuLi was added to the soln. of ligand at -35°C, mixt. was warmed to room temp., stirred for 2 h, soln. was cooled to -35°C again and added to suspn. of HfCl4 with stirring,mixt. stirred at room temp. for 20 h; mixt. was filtered, washed with Et2O, ether filtrate was concd., cooled to -35°C; elem. anal.;	85%

...Expand

: 109-72-8
n-butyllithium

: 4181-91-3
(R)-(-)-benzyl-α-d chloride

: 688-73-3
tri-n-butyl-tin hydride

: 108-18-9
diisopropylamine

: 84369-11-9
(S)-(-)-(.alfa.-deuteriobenzyl)tributyltin

Conditions

Conditions	Yield
In tetrahydrofuran; hexane to THF soln. of (i-Pr)2NH at 0°C added hexane soln. of BuLi, stirred at 0°C for 30 min, Bu3SnH added, stirred at 0°C for 30 min, soln. added to THF soln. of (R)-PhCHDCl at 0°C over 30 min, mixt. kept at 0°C for 5 h; added water, mixt. extd. with ether, sepd., washed with water and brine, extract dried with MgSO4, concd., chromd.;	84%

...Expand

: 109-72-8
n-butyllithium

: 1231953-83-5
trimethylamine borane

A: lithium borohydride

B: 82111-98-6
lithium [butyl(trihydrido)borate]

C: 84280-42-2
lithium [(dimethylamino)methyl]trihydroborate

D: 84280-43-3
lithium benzyltrihydroborate

Conditions

Conditions	Yield
In hexane; toluene under dry N2, refluxing for 30 min;	A 4% B 80% C 4% D 2%
In hexane; toluene under dry N2, refluxing for 2 d;	A 15% B 64% C 15% D 6%

...Expand

: 109-72-8
n-butyllithium

: borane tetrahydrofuran

A: lithium borohydride

B: 84280-32-0
lithium di-n-butylborohydride

C: 67335-72-2
LiHB(s-Bu)3

D: 15243-31-9
Li{B(n-C4H9)4}

Conditions

Conditions	Yield
In tetrahydrofuran; hexane under dry N2, soln. of BH3 in THF cooled to -78°C, hexane soln. of n-BuLi added with stirring, mixt. allowed to warm to -30°C within 1 h; not isolated, detected by NMR;	A 77% B 3% C 13% D 7%

...Expand

: 109-72-8
n-butyllithium

: 13292-87-0
dimethyl sulfide borane

A: lithium borohydride

B: 82111-98-6
lithium [butyl(trihydrido)borate]

C: 15243-31-9
Li{B(n-C4H9)4}

Conditions

Conditions	Yield
In hexane under dry N2, hexane soln. of n-BuLi cooled to -10°C, H3B-SMe2 added with stirring for few minutes, after 20 min all volatile material stripped in vac.; residue dissolved in THF, not isolated, detected by NMR;	A 18% B 77% C 5%
In hexane under dry N2, hexane soln. of n-BuLi added over period of 10 min to H3B-SMe2 with stirring; residue dissolved in minimum THF, not isolated, detected by NMR;	A 44% B 41% C 15%

...Expand

: 109-72-8
n-butyllithium

: (2S, 5R, 7S, 8R, 2E, 4E)-tricarbonyliron[(η4-2-5)-8-(tert-butoxycarbonylamino)-7-methoxynona-2,4-dienal]

: 21406-61-1
pentyltriphenylphosphonium bromide

: (2R, 3S, 5R, 8S, 5E, 7E, 9Z)-tricarbonyliron[(η4-5-8)-2-(tert-butoxycarbonylamino)-3-methoxytetradodeca-5,7,9-triene]

Conditions

Conditions	Yield
In hexane; toluene (N2 atmosphere); addn. of BuLi to susp. of C5H11PPh3Br (stirring, 0°C), addn. of soln. of Fe complex (after 5 min, -78°C), stirring (-78°C, 30 min, 0°C, 30 min), addn. of H2O (0°C),extraction (EtOAc), drying (MgSO4); evapn. (in vacuo), chromatography (SiO2 hexane/EtOAc);	73%

...Expand

: 109-72-8
n-butyllithium

C20H8N4(BCl)2(C6H4CH3)4*(n)C6H5CH3 n:0.5-1;: C20H8N4(BCl)2(C6H4CH3)4*(n)C6H5CH3 n:0.5-1;

: anti-C20H8N4(BC4H9)2(C6H4CH3)4

Conditions

Conditions	Yield
In hexane byproducts: LiCl, toluene; C4H9Li soln. added to suspn. of C20H8N4(BCl)2(C6H5CH3)4*(n)C6H5CH3 in hexane (-78 °C), warmed up to room temp., stirred (16 h); ppt. filtered, washed with hexane, extd. with CH2Cl2; detd. by MAS, UV, (1)H NMR, (11)B NMR;	71%

: iron(II) chloride tetrahydrate

: 109-72-8
n-butyllithium

: 100-44-7
benzyl chloride

: 17534-15-5
1,2-benzenedithiole

: 116089-38-4
2-(Benzylthio)thiophenol

Conditions

Conditions	Yield
With hydrogenchloride; carbon monoxide In tetrahydrofuran under N2; reaction of dithiol and BuLi at -78 °C; addn. of Fe-salt at room temp.; CO introduced for 2h; benzyl chloride added; stirring for 1h at room temp.; evapn.; excess of benzyl chloride removed by hexane; HCl and THF added; refluxed for 2h;; evapn.; treatment with H2O/CCl4; organic layer dried (Na2SO4), filtered and evapd.; distn. (180-220 °C, vacuum); elem. anal.;;	70%

Yield

With hydrogenchloride; carbon monoxide In tetrahydrofuran under N2; reaction of dithiol and BuLi at -78 °C; addn. of Fe-salt at room temp.; CO introduced for 2h; benzyl chloride added; stirring for 1h at room temp.; evapn.; excess of benzyl chloride removed by hexane; HCl and THF added; refluxed for 2h;; evapn.; treatment with H2O/CCl4; organic layer dried (Na2SO4), filtered and evapd.; distn. (180-220 °C, vacuum); elem. anal.;;

70%

...Expand

: 109-72-8
n-butyllithium

: 53268-50-1
chloro(trifluoromethyl)disulfane

: 1-Trifluoromethyldisulfanyl-butane

Conditions

Conditions	Yield
	68%
	68%

: 109-72-8
n-butyllithium

: 131498-79-8
1-trimethylsiloxy-3,7,10-trimethylgermatrane

: 1067-42-1
tetrabutylgermanium

Conditions

Conditions	Yield
In tetrahydrofuran byproducts: LiOSi(CH3)3; a suspn. of germatrane in THF was treated with an excess of n-BuLi in n-hexane at room temp. for 4 h; evap., filtered;	65%

: 1271-86-9
N,N-dimethylaminomethylferrocene

: 109-72-8
n-butyllithium

: 68-12-2, 33513-42-7
N,N-dimethyl-formamide

: 162762-18-7, 212901-69-4, 174225-69-5
2-(N,N-dimethylaminomethyl)ferrocenecarboxaldehyde

Conditions

Conditions	Yield
In not given addn. of LiBu (1 equiv., room temp.), stirring (24 h), addn. of DMF (-78°C), stirring (4 h, room temp.), hydrolysis; extn. (Et2O), chromy. (alumina, Et2O/pentane 1:2); elem. anal.;	62%

...Expand

: 109-72-8
n-butyllithium

: 70559-35-2
1-bromogermatrane

: 1067-42-1
tetrabutylgermanium

Conditions

Conditions	Yield
In tetrahydrofuran a suspn. of germatrane in THF was treated with an excess of n-BuLi in n-hexane at room temp. for 4 h;	61%

: 109-72-8
n-butyllithium

: 1231953-83-5
trimethylamine borane

: lithium borohydride

Conditions

Conditions	Yield
In hexane under dry N2, refluxing for 20 h;	60%

: 26743-81-7
tetracarbonyl-bis(diphenylphosphino)methane-molybdenum(0)

: 109-72-8
n-butyllithium

: 115-09-3
methylmercury(II) chloride

: Mo(CO)4((C6H5)2PCH(HgCH3)P(C6H5)2)

Conditions

Conditions	Yield
In tetrahydrofuran addn. of LiBu (hexane soln.) to soln. of Mo-complex (0°C), stirring (2 h), addn. of Hg-compd., warming (room temp.), stirring (2 h); THF removal (reduced pressure), recrystn. (CH2Cl2-methanol);	60%

...Expand

: 16743-46-7
tetracarbonyl-bis(diphenylphosphino)methane-chromium(0)

: 109-72-8
n-butyllithium

: 115-09-3
methylmercury(II) chloride

: Cr(CO)4((C6H5)2PCH(HgCH3)P(C6H5)2)

Conditions

Conditions	Yield
In tetrahydrofuran addn. of LiBu (hexane soln.) to soln. of Cr-complex (0°C), stirring (2 h), addn. of Hg-compd., warming (room temp.), stirring (2 h); THF removal (reduced pressure), recrystn. (CH2Cl2-methanol);	60%

...Expand

: 109-72-8
n-butyllithium

: 41830-14-2
tetracarbonyl-bis(diphenylphosphino)methane-tungsten(0)

: 115-09-3
methylmercury(II) chloride

: W(CO)4((C6H5)2PCH(HgCH3)P(C6H5)2)

Conditions

Conditions	Yield
In tetrahydrofuran addn. of LiBu (hexane soln.) to soln. of W-complex (0°C), stirring (2 h), addn. of Hg-compd., warming (room temp.), stirring (2 h); THF removal (reduced pressure), recrystn. (CH2Cl2-methanol);	60%

...Expand

: 26743-81-7
tetracarbonyl-bis(diphenylphosphino)methane-molybdenum(0)

: 109-72-8
n-butyllithium

: 107-27-7
ethylmercury(II) chloride

: Mo(CO)4((C6H5)2PCH(HgCH2CH3)P(C6H5)2)

Conditions

Conditions	Yield
In tetrahydrofuran addn. of LiBu (hexane soln.) to soln. of Mo-complex (0°C), stirring (2 h), addn. of Hg-compd., warming (room temp.), stirring (2 h); THF removal (reduced pressure), recrystn. (CH2Cl2-methanol);	60%

...Expand

: 16743-46-7
tetracarbonyl-bis(diphenylphosphino)methane-chromium(0)

: 109-72-8
n-butyllithium

: 107-27-7
ethylmercury(II) chloride

: Cr(CO)4((C6H5)2PCH(HgCH2CH3)P(C6H5)2)

Conditions

Conditions	Yield
In tetrahydrofuran addn. of LiBu (hexane soln.) to soln. of Cr-complex (0°C), stirring (2 h), addn. of Hg-compd., warming (room temp.), stirring (2 h); THF removal (reduced pressure), recrystn. (CH2Cl2-methanol);	60%

...Expand

: 109-72-8
n-butyllithium

: 41830-14-2
tetracarbonyl-bis(diphenylphosphino)methane-tungsten(0)

: 107-27-7
ethylmercury(II) chloride

: W(CO)4((C6H5)2PCH(HgCH2CH3)P(C6H5)2)

Conditions

Conditions	Yield
In tetrahydrofuran addn. of LiBu (hexane soln.) to soln. of W-complex (0°C), stirring (2 h), addn. of Hg-compd., warming (room temp.), stirring (2 h); THF removal (reduced pressure), recrystn. (CH2Cl2-methanol);	60%

...Expand

: 26743-81-7
tetracarbonyl-bis(diphenylphosphino)methane-molybdenum(0)

: 109-72-8
n-butyllithium

: 100-56-1
phenylmercury(II) chloride

: Mo(CO)4((C6H5)2PCH(HgC6H5)P(C6H5)2)

Conditions

Conditions	Yield
In tetrahydrofuran addn. of LiBu (hexane soln.) to soln. of Mo-complex (0°C), stirring (2 h), addn. of Hg-compd., warming (room temp.), stirring (2 h); THF removal (reduced pressure), recrystn. (CH2Cl2-methanol);	60%

...Expand