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Cas:7446-70-0
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Product Description Name Aluminium chloride CAS 7446-70-0 Assay 99% Appearance
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inquiryAluminium chloride Basic information Product Name: Aluminium chloride Synonyms: epapesticidechemicalcode013901;NSC 143016;PAC (salt);Pearsall;Praestol K2001;Trichloroaluminum;trichloroal
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inquiryEnglish Name: Aluminum Chloride Molecular formula: ALCL3 Molecular weight: 133.34 CAS number:7446-70-0 EINECS number:231-208-1 Physical and chemical properties: white to pale yellow crystalline powder, relative density of 2.44 (25 ℃), the a
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inquirySynonyms: epapesticidechemicalcode013901;NSC 143016;PAC (salt);Pearsall;Praestol K2001;Trichloroaluminum;trichloroaluminum,anhydrous;trichloroaluminumsolutions CAS: 7446-70-0 MF: AlCl3 MW: 133.34 EINECS: 231-208-1 Product Categories: Industria
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Aluminium chloride CAS: 7446-70-0 Specification aluminium chloride product name aluminium chloride synonyms aluminium trichloride cas no. 7446-70-0
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryProduct name: Aluminium Chloride CAS No.:7446-70-0 Molecule Formula:AlCl3 Molecule Weight:133.3422 Purity: 99.3% Package: 50kg/drum Description:Colorless or yellow powder Manufacture Standards:Enterprise Standard T
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Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
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Cas:7446-70-0
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Conditions | Yield |
---|---|
In neat (no solvent) passing a flow of Cl2 over Al in a combustion tube;; | 80% |
In neat (no solvent) heating Al shavings in a flow of chlorine; distd. in vac.; | |
at 600 K; |
phosgene
aluminium bromide
A
aluminium trichloride
B
carbonyl bromide chloride
Conditions | Yield |
---|---|
equil. amts of educts in tube, cooling than 140-145°C, 7-8h; distn., addn. Hg, distn. 24.5-25.5°C atmospheric pressure; | A n/a B 50% |
equil. amts of educts in tube, cooling than 140-145°C, 7-8h; distn., addn. Hg, distn. 24.5-25.5°C atmospheric pressure; | A n/a B 50% |
lithium aluminium tetrahydride
phosphorus trichloride
A
aluminium trichloride
B
phosphan
Conditions | Yield |
---|---|
In diethyl ether reduction of PCl3 with LiAlH4 in ether at 0 °C;; | |
In diethyl ether reduction of PCl3 with LiAlH4 in ether at 75 °C;; | A n/a B 0.25% C n/a |
In diethyl ether reduction of PCl3 with LiAlH4 in ether at 75 °C;; | A n/a B 0.25% C n/a |
In diethyl ether reduction of PCl3 with LiAlH4 in ether at 0 °C;; |
8-chloro-1-methoxy-phenazine
A
aluminium trichloride
B
8-chloro-phenazin-1-ol
Conditions | Yield |
---|---|
With benzene |
methylbutane
tertiary butyl chloride
aluminium bromide
A
aluminium trichloride
B
Isobutane
C
2-bromo-2-methylbutane
D
3-bromo-2-methylbutane
hydrogenchloride
ethyl 2-ethoxy-2-iminoacetate
A
aluminium trichloride
B
oxalic acid diethyl ester
2,2-diphenylpropane
2-methyl-2-phenylpropanoyl chloride
A
aluminium trichloride
B
benzene
2,4,6-Trimethylacetophenone
propionyl chloride
A
aluminium trichloride
B
1,3-dipropionyl-2,4,6-trimethylbenzene
propionyl chloride
1,3,5-trimethyl-benzene
A
aluminium trichloride
B
1,3-dipropionyl-2,4,6-trimethylbenzene
6-Acetyl-1,2,3,4-tetrahydronaphthalene
diethyl ether
acetyl chloride
A
aluminium trichloride
B
2,5-diacetyl-7-ethyl-1-methyl-indene
A
aluminium trichloride
B
1-benzoyl-2,4-dibromo-5-(2,4-dimethyl-benzoyl)-benzene
Conditions | Yield |
---|---|
With m-xylene |
phosgene
chlorine
A
aluminium trichloride
B
trichlorophosphate
Conditions | Yield |
---|---|
In neat (no solvent) reaction at at temperatures higher than 300°C;; |
carbon monoxide
chlorine
A
aluminium trichloride
B
trichlorophosphate
Conditions | Yield |
---|---|
In neat (no solvent) reaction at at temperatures higher than 300°C;; |
chlorine
A
aluminium trichloride
B
trichlorophosphate
Conditions | Yield |
---|---|
With pyrographite In neat (no solvent) reaction at temperatures higher than 300°C;; |
Conditions | Yield |
---|---|
In neat (no solvent) calcination of NH4Cl and Al2O3;; |
Conditions | Yield |
---|---|
In neat (no solvent) mixture contg. 45-50 weight-% Al-powder, 45 weight-% Al2O3 and 5-10 weight-% NH4Cl is heated to 600-830 °C yielding AlCl3 vapors;; not isolated;; |
Conditions | Yield |
---|---|
260°C; distillation of AlCl3; | |
In neat (no solvent) calcination of NH4Cl and Al2(SO4)3;; |
aluminium trichloride
Conditions | Yield |
---|---|
With sodium chloride heating; | |
With hydrogenchloride HCl vapor; | |
With potassium chloride byproducts: K2S; |
Conditions | Yield |
---|---|
500°C; | |
500°C; |
Conditions | Yield |
---|---|
95°C; | |
95°C; |
Conditions | Yield |
---|---|
With hydrogen In neat (no solvent) byproducts: HCl; other Radiation; AlCl3 powder placed in quartz tube; tube evacuated and flushed with Ar and then heated under Ar/H2 flow to 90°C; rf discharge ignited for20 min and tube then cooled; XRD; | 100% |
With potassium In neat (no solvent) heating AlCl3 in a rectangular glass tube and passing the vapor over pieces of K in the horizontal part of the tube;; | |
With lithium hydride; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride In neat (no solvent) mixed by stirring; deposited at 25-45°C for 15 min - 2 h; |
Conditions | Yield |
---|---|
In benzene under N2, dropwise addn. of thiol soln. to a suspension of AlCl3 in benzene, dissoln.of AlCl3, stirred for 15 min at room temp.; evapn. of solvent, dried in vac. at room temp. for 3h, elem. anal.; | 100% |
Conditions | Yield |
---|---|
In acetonitrile (inert atmosphere); condensing MeCN onto AlCl3 and PrCl3, reflux until aclear soln. is obtained; solvent removal (vac.); elem. anal.; | 100% |
aluminium trichloride
ethanethiol
aluminiumtrichloride*ethanediol
Conditions | Yield |
---|---|
In benzene slow addn. of ethanethiol to a suspn. of an equimolar amt. of AlCl3 in benzene; mixt. stirred for 1 h at room temp.; solvent distd. off in vac. at 60°C; residual oil distd. at 86°C (0.5 Torr); elem. anal.; | 100% |
In benzene under N2, dropwise addn. of thiol soln. to a suspension of AlCl3 in benzene, dissoln.of AlCl3, stirred for 15 min at room temp.; evapn. of solvent, dried in vac. at room temp. for 3h, elem. anal.; | 100% |
aluminium trichloride
Conditions | Yield |
---|---|
In benzene mixt. stirred until AlCl3 completely dissolved (ca 10h); evapn. under reduced pressure at room temp., dried (50°C, 0.4 mm, 3h); | 100% |
aluminium trichloride
Conditions | Yield |
---|---|
In benzene mixt. stirred until AlCl3 completely dissolved (ca 10h); evapn. under reduced pressure at room temp., dried (50°C, 0.4 mm, 3h); elem. anal.; | 100% |
Conditions | Yield |
---|---|
In benzene | 100% |
Conditions | Yield |
---|---|
In benzene | 100% |
Conditions | Yield |
---|---|
In benzene under N2, CH3SH introduced in a suspension of AlCl3 for 5 min, dissoln.of AlCl3, stirred for 15 min at room temp.; evapn. of solvent, dried in vac. at room temp. for 3h, elem. anal.; | 100% |
aluminium trichloride
Trimethyl(methylthio)silane
aluminium trichloride*trimethylsilyl methyl sulphide
Conditions | Yield |
---|---|
In benzene a benzene soln. of Me3SiSMe was added dropwise under N2 to a suspn. of AlCl3 in benzene, mixt. was stirred for 15 min at room temp.; solvent was evapd.; elem. anal.; | 100% |
aluminium trichloride
(ethylthio)trimethylsilane
aluminium trichloride*trimethylsilyl ethyl sulphide
Conditions | Yield |
---|---|
In benzene a benzene soln. of Me3SiSEt was added dropwise under N2 to a suspn. of AlCl3 in benzene, mixt. was stirred for 15 min at room temp.; solvent was evapd.; elem. anal.; | 100% |
aluminium trichloride
phenylthiotrimethylsilane
aluminium trichloride*trimethylsilyl phenyl sulphide
Conditions | Yield |
---|---|
In benzene a benzene soln. of Me3SiSPh was added dropwise under N2 to a suspn. of AlCl3 in benzene, mixt. was stirred for 15 min at room temp.; solvent was evapd.; elem. anal.; | 100% |
Conditions | Yield |
---|---|
In further solvent(s) byproducts: MeCl; slow heating in neat Ph(Me)P(O)OMe until complete pptn.; particle size and polymerization degree depending on heating rate; | 100% |
aluminium trichloride
1-butyl-3-methylimidazolium chloride
Conditions | Yield |
---|---|
In neat (no solvent) 1-butyl-3-methylimidazolium chloride was mixed with AlCl3 under N2 for 5min.; | 100% |
E.J. Angueira, M.G. White, J. Mol. Catal. A Chem. 227 (1-2) (2005) 51-58; 238 (2005) 163-174; |
aluminium trichloride
triethyl(trimethylsilylimino)phosphorane
Conditions | Yield |
---|---|
In acetonitrile byproducts: Me3SiCl; Ar atm.; equivalent amts., refluxing; evapn. (vac., to dryness); elem. anal.; | 100% |
aluminium trichloride
syn-AlCl[PhP(CH2SiMe2NSiMe2CH2)2PPh]
Conditions | Yield |
---|---|
In toluene byproducts: LiCl; inert atmosphere; stirring for 12 h; filtration off of LiCl (Celite), solvent removal (vac.), recrystn. (PhMe, slow evapn.); | 100% |
[N-(2-diphenylphosphinophenyl)-2,6-dimethylanilide]Li(THF)2
aluminium trichloride
[N-(2-diphenylphosphinophenyl)-2,6-dimethylanilide]AlCl2
Conditions | Yield |
---|---|
In toluene under N2 atm. AlCl3 was added at -35°C to soln. (N-(2-phenylphosphinophenyl)-2,6-dimethylanilide)Li(THF)2 in toluene and stirred at room temp. for 4 days; react. mixt. was filtered, solvent was stripped; | 100% |
Conditions | Yield |
---|---|
In neat (no solvent) the educts were warmed with stirring to 40°C, cooled to 20°C;; distn. in vac. (removal of excess boroxine and by-products), residue sublimed in high vac. at about 130 °C; elem. anal.;; | A 99.9% B n/a |
aluminium trichloride
trans-1,2-bis[(trimethylsilyl)oxy]cyclohexane
{C6H10(O)(OSi(CH3)3)}2{AlCl2}2
Conditions | Yield |
---|---|
In dichloromethane a stirred suspn. of AlCl3 in CH2Cl2 at -78°C was treated dropwise under dry Ar with a soln. of the ether in CH2Cl2, the mixture was kept at 25°C for 20 h; removal of the volatiles by evapn. in vacuo; | 99.2% |
Conditions | Yield |
---|---|
With methylmagnesium bromide In not given react. of AlCl3 with MeMgBr; | 99% |
Conditions | Yield |
---|---|
697°C,in N2; | 99% |
697°C,in N2; | 99% |
With oxygen glowing in O2-stream; |
aluminium trichloride
bis(triphenylphosphine)iminium chloride
N(P(C6H5)3)2(1+)*AlCl4(1-)=N(P(C6H5)3)2[AlCl4]
Conditions | Yield |
---|---|
In tetrahydrofuran inert atmosphere; stirring equimolar amts. (room temp., 4 h); solvent removal (vac.); elem. anal.; | 99% |
Conditions | Yield |
---|---|
With C2Cl6 In acetonitrile Sonication; (N2); addn. of MeCN to Pr, AlCl3 and C2Cl6, sonication for 3 h; solvent removal (vac.); elem. anal.; | 99% |
aluminium trichloride
potassium hydridotris(3,5-dimethylpyrazolyl)borate
{(tris(3,5-dimethyl-1-pyrazolyl)hydridoborate)2Al}(AlCl4)
Conditions | Yield |
---|---|
In dichloromethane stirring (18 h, room temp.), solvent removal (vacuum); extraction (CH2Cl2), recrystn. (MeCN); | 99% |
Conditions | Yield |
---|---|
In toluene byproducts: LiCl; treatment of LiBH4 with AlCl3 in toluene; pptn.; distn.; | 99% |
freezing-thawing (vac., 20 to -78°C); |
hydrogenchloride
aluminium trichloride
(P((CH3)2C6H5))3Cl2Re(N-pyrrolyl)
mer-trichlorotris(dimethylphenylphosphine)rhenium(III)
Conditions | Yield |
---|---|
99% |
hydrogenchloride
aluminium trichloride
mer-(PMe2Ph)3Cl2Re(3,4-NC4H2Me2)
mer-trichlorotris(dimethylphenylphosphine)rhenium(III)
Conditions | Yield |
---|---|
In chloroform-d1 N2-atmosphere; excess of HCl, 1 equiv. of AlCl3, standing for 1-2 days; not sepd.; NMR-spectroscopy; | 99% |
hydrogenchloride
aluminium trichloride
mer-trichlorotris(dimethylphenylphosphine)rhenium(III)
Conditions | Yield |
---|---|
99% |
aluminium trichloride
1-[(1-chloro-1-methylethyl)azo]-2,4,6-trichlorobenzene
1,3-Diphenylcarbodiimide
Conditions | Yield |
---|---|
In dichloromethane inert atmosphere; soln. of N-compounds added dropwise to suspension of AlCl3 at -60°C; stirred for 1 h at -60°C, then for 1 h at 0°C;; evapd.; pptd. from CH2Cl2/pentane; elem. anal.;; | 99% |
aluminium trichloride
W(O)(CHC(CH3)3)Cl2(P(C2H5)3)2
[W(O)(CHC(CH3)3)(P(C2H5)3)2](2+)*2AlCl4(1-)=[W(O)(CHC(CH3)3)(P(C2H5)3)2](AlCl4)2
Conditions | Yield |
---|---|
In dichloromethane AlCl3 was added to stirred soln. of W compd. in CH2Cl2 in ca. 2:1 molarratio; filtered, vol. of filtrate halved in vac., equal vol. of pentane was added, crystd., elem. anal.; | 99% |
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