CAS No.7429-90-5,Aluminium Suppliers,MSDS download

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Synthetic route

: 7446-70-0
aluminium trichloride

: 7429-90-5
aluminium

Conditions

Conditions	Yield
With hydrogen In neat (no solvent) byproducts: HCl; other Radiation; AlCl3 powder placed in quartz tube; tube evacuated and flushed with Ar and then heated under Ar/H2 flow to 90°C; rf discharge ignited for20 min and tube then cooled; XRD;	100%
With potassium In neat (no solvent) heating AlCl3 in a rectangular glass tube and passing the vapor over pieces of K in the horizontal part of the tube;;
With lithium hydride; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride In neat (no solvent) mixed by stirring; deposited at 25-45°C for 15 min - 2 h;

: 12099-15-9
bis(η6-diphenyl)chromium(0)

: 7727-15-3
aluminium bromide

A: {(C6H5C6H5)2Cr}(1+)*AlBr4(1-)*0.25C6H6={(C6H5C6H5)2Cr}AlBr4*0.25C6H6

B: 7429-90-5
aluminium

Conditions

Conditions	Yield
In benzene at room temp.;	A 92% B n/a
In benzene at room temp.;	A 92% B n/a

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: 16842-00-5, 855944-65-9
trimethylamine alane

: 7429-90-5
aluminium

Conditions

Conditions	Yield
With hydrogen In 1,2,5-trimethyl-benzene High Pressure; a soln. of Al complex degassed, pressurized with 3 bar of H2, heated to 150°C for 1 h; allowed to settle, the supernatant removed, washed (n-pentane), dried (vac.); obtained as nanoparticles;	86%
With hydrogen In further solvent(s) byproducts: N(CH3)3; High Pressure; pressurized with 3 bar of H2 in mesitylene-d12, heated to 150°C for 1 h;
byproducts: N(CH3)3, H2; film deposition using CVD method (P<1E-6 Torr, gold covered quartz crystal, Teflon, silicon or gallium arsenide as substrates, laser at 5 or 500mW, cooling with liq. N2); SEM;

: 7446-70-0
aluminium trichloride

: 55527-82-7
bis(η6-toluene)titanium(0)

A: Ti(ηtoluene){(μ-Cl)2(AlCl2)}2

B: 7429-90-5
aluminium

Conditions

Conditions	Yield
In toluene under purified Ar atm.; AlCl3 added to soln. of Ti(η6-MeC6H5)2 in toluene; mixt. stirred for 18 h at room temp.; solid sepd. by filtration; washed (toluene); dried (vac.); identified asAl; soln. evapd. to dryness; solid washed (heptane); dried (vac.); iden tified as Ti-Al complex;	A 80% B 85%

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: 79372-14-8
decamethylsamarocene(II) bis(tetrahydrofurane)

: 75-24-1
trimethylaluminum

A: 109-99-9
tetrahydrofuran

B: 115756-72-4
(C5Me5)2Sm{(μ-Me)AlMe2(μ-Me)}2Sm(C5Me5)2

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
In toluene byproducts: methane; all manipulations conducted under nitrogen excluding air and water; after 24 h standing of the reaction mixt. the formed metallic-like ppt. was removed by filtration and washed with hot toluene, filtrates combined, solvent removed by rotary evapn.;; recrystn. (hot toluene), elem. anal.;;	A n/a B 80% C n/a

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: strontium(II) hydride

: strontium tetrahydroaluminate

A: strontium pentahydroaluminate

B: 1333-74-0
hydrogen

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
In solid SrH2 mechanically treated for 3-4 h, mixed with AlH3 at molar ratio 1:1 in vibrating mechanical load, heated for 3-4 h; DTA-DGV, XRD, IR;	A 80% B n/a C n/a
In solid mechanolysis at 165-220°C; DTA-DGV, IR, XRD;

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: 1333-84-2, 1344-28-1
aluminum oxide

: beryllium

A

B: 7429-90-5
aluminium

Conditions

Conditions	Yield
In neat (no solvent) heating a 1:1 mixture up to 1280°C for 3h; formation of a mixture of the metals and oxides;;	A 64% B n/a

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: 7446-70-0
aluminium trichloride

: 137013-38-8
(pentamethylcyclopentadienyl)Al

A: {(η5-C5Me5)2Al}{(η1-C5Me5)AlCl3}

B: 7429-90-5
aluminium

Conditions

Conditions	Yield
In toluene under N2, after 3 days heated at 100°C for 15 h; slowly cooled;	A 50% B n/a

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: [1,3-(tBu)2(C5H3)]2Sm

: 7784-21-6
aluminium hydride

: aluminium hydride*TMEDA

A: (C5H3(C(CH3)3)2)5Sm4(AlH4)4H3((CH3)2NC2H4N(CH3)2)2

B: 7429-90-5
aluminium

Conditions

Conditions	Yield
In diethyl ether byproducts: H2; dropwise addn. of AlH3 in ether to soln. of Sm-compd. in diethyl ether, addn. of AlH3*TMEDA, stirred for 24 h; pptn. filtered off, filtrate concd., sepn. after 48 h, washed with pentane, dried in vac.; elem. anal.;	A 35% B n/a

...Expand

: aluminum(I) chloride

: 60-29-7
diethyl ether

: 108-88-3
toluene

: 4039-32-1
lithium hexamethyldisilazane

A: 54Al*15Al(1+)*18N(SiC3H9)2(1-)*2Li(OC4H10)3(1+)*Li(OC4H10)4(1+)*1.5C6H5CH3=[Al69N18Si36C108H324](C40H100Li3O10)*1.5C7H8

B: 17634-40-1
diethyl ether ; compound with aluminium trichloride

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
In diethyl ether; toluene byproducts: LiCl*3Et2O; soln. of AlCl in toluene/Et2O (3/1) was added to LiN(SiMe3)2 at -78°C; soln. was warmed to room temp. within 1 d; heated at 60°C for 1 h; filtered; soln. was left at 60°C for 2 mo; pptd.;	A 7% B n/a C n/a

...Expand

: aluminium hydride*(dibutyl ether)0.3

A: AlH2OC3H6CH3

B: 7429-90-5
aluminium

Conditions

Conditions	Yield
In neat (no solvent) Kinetics; byproducts: O(C4H9)2, H2; thermal decompn. at 50-100°C; identification of products by IR;	A 5% B n/a

: aluminum(I) chloride

: 60-29-7
diethyl ether

: 108-88-3
toluene

: 4039-32-1
lithium hexamethyldisilazane

A: 54Al*15Al(1+)*18N(Si(CH3)3)2(1-)*3Li(O(C2H5)2)4(1+)*6C6H5CH3=[Al69(N(Si(CH3)3)2)18](Li(O(C2H5)2)4)3*6C6H5CH3

B: 17634-40-1
diethyl ether ; compound with aluminium trichloride

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
In diethyl ether; toluene byproducts: LiCl3Et2O; gaseous AlCl were condensed with toluene and diethyl ether at -196°C; soln. of AlClEt2O was added to LiN(SiMe3)2 at 25°C; mixt. was left for 1 h; filtered; soln. was heated at 60°C for 1.5 h; pptd.;	A 5% B n/a C n/a

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Na/K alloy: Na/K alloy

: 97-93-8
triethylaluminum

A: potassium tetraethylaluminate

B: 2397-68-4
sodium tetraethylaluminate

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
Stage #1: Na/K alloy; triethylaluminum at 85 - 90℃; for 1.25h; Stage #2: triethylaluminum In toluene at 60 - 80℃; for 4h; Product distribution / selectivity;
Stage #1: Na/K alloy; triethylaluminum at 87 - 95℃; for 3.5h; Stage #2: triethylaluminum In toluene at 20 - 88℃; for 1h; Product distribution / selectivity;
In toluene at 20 - 35℃; for 9.25h; Product distribution / selectivity;

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: 16853-85-3
lithium aluminium tetrahydride

A: 1333-74-0
hydrogen

B: lithium hydride

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
titanium(III) chloride at 90℃; for 5h; Product distribution / selectivity; Neat (no solvent); Balled milled;
In solid Kinetics; thermal decomposition of ball milled for various times or as-received LiAlH4; powder XRD;
chromium(VI) oxide In diethyl ether; toluene Kinetics; Catalytic decompn. of LiAlH4 in solution;

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: 16853-85-3
lithium aluminium tetrahydride

A: lithium hexahydroaluminate

B: 1333-74-0
hydrogen

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
titanium(III) chloride at 50 - 150℃; under 760.051 Torr; Product distribution / selectivity; Neat (no solvent); Balled milled;
at 100 - 200℃; under 760.051 Torr; Product distribution / selectivity; Neat (no solvent); Balled milled;
In neat (no solvent) 170°C - 220°C;
With magnesium hydride; titanium(II) hydride In neat (no solvent) at 54 - 171℃; Kinetics; Inert atmosphere;

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: magnesium hydride

A: 1333-74-0
hydrogen

B: 7439-95-4
magnesium

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
titanium(III) chloride at 250 - 350℃; under 760.051 Torr; Product distribution / selectivity; Neat (no solvent); Balled milled;

...Expand

: sodium aluminum tetrahydride

A: sodium alanate

B: 1333-74-0
hydrogen

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
titanium(III) chloride at 50 - 200℃; under 760.051 Torr; Product distribution / selectivity; Neat (no solvent); Balled milled;
In neat (no solvent) in stainless steel reactor, at 480-490 K for 3 h, according to: E. C. Ashby, P. Kobertz, Inorg. Chem., 1966, 5, 1615.; XRD;
In neat (no solvent) on heating;
at 210℃;

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: sodium alanate

A: 1333-74-0
hydrogen

B: 7646-69-7
sodium hydride

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
titanium(III) chloride at 200 - 250℃; under 760.051 Torr; Product distribution / selectivity; Neat (no solvent); Balled milled;
In neat (no solvent, solid phase) decompd. at heating;

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: lithium hexahydroaluminate

A: 1333-74-0
hydrogen

B: lithium hydride

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
titanium(III) chloride at 150 - 250℃; under 760.051 Torr; Product distribution / selectivity; Neat (no solvent); Balled milled;
at 200 - 250℃; under 760.051 Torr; Product distribution / selectivity; Neat (no solvent); Balled milled;
In solid 220°C - 275°C;

...Expand

A: magnesium hydride

B: 1333-74-0
hydrogen

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
titanium(III) chloride at 50 - 250℃; under 760.051 Torr; Product distribution / selectivity; Neat (no solvent); Balled milled;
at 100℃; under 760.051 Torr; Product distribution / selectivity; Neat (no solvent); Balled milled;
at 145 - 305℃;

...Expand

: Al12Mg17

: 1333-74-0
hydrogen

: 7439-95-4
magnesium

A: magnesium hydride

B: 7429-90-5
aluminium

Conditions

Conditions	Yield
hydrogenation at 30 bar H2 at 350°C for 0 to 24 h; detd. by XRD;

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: aluminum sulfide

: 7429-90-5
aluminium

Conditions

Conditions	Yield
With iron In neat (no solvent) Al2S3 is decomposed on Fe;; not isolated;;
With iron In neat (no solvent) Al2S3 is molten with iron shavings;;
With H2 or hydrocarbons reduction of Al2S3 by hydrogen or hydrocarbons;;

: 1333-84-2, 1344-28-1
aluminum oxide

: aluminum sulfide

: 7429-90-5
aluminium

Conditions

Conditions	Yield
byproducts: SO2;
With pyrographite In neat (no solvent) fractionated reduction; first portion: Al alloy with contaminating metalls (Si, Fe, Ti), second portion (using charcoal as reducing reagent):pure Al;;
With pyrographite In neat (no solvent) fractionated reduction; first portion: Al alloy with contaminating metalls (Si, Fe, Ti), second portion (using charcoal as reducing reagent):pure Al;;

: 1333-84-2, 1344-28-1
aluminum oxide

A: aluminium nitride

B: 1299-86-1
aluminium carbide

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
With pyrographite In neat (no solvent) byproducts: graphite; Electric Arc; on heating in an electric arc; formation of Al4C3 containing Al2O3, AlN, Al and graphite;; yield of Al (at best: 30%) increases with decreasing cooling velocity;;
With pyrographite In neat (no solvent) on heating in an electric furnace; formation of Al4C3 containing Al2O3, AlN and Al;; yield of Al (at best: 30%) increases with decreaseing cooling velocity;;

...Expand

: 1333-84-2, 1344-28-1
aluminum oxide

A: 1299-86-1
aluminium carbide

B: 7429-90-5
aluminium

Conditions

Conditions	Yield
With caebon In neat (no solvent) byproducts: CO; heating Al2O3 with carbon; formation of solid Al, Al2O3, and Al4C3 as product mixture with residual carbon; reaction mechanism discussed;;
With pyrographite In neat (no solvent) byproducts: CO; Electric Arc; reaction temp. above b.p. of Al at 1 atm; favouring by pressure or by elimination of CO by flushing with H or city gas;; best yield about 49g Al per 106g Al4C3;;
With pyrographite; calcium oxide In neat (no solvent) byproducts: CO; Electric Arc; heating with BaO or Sr-compunds; requirement of energy: 5kWh;;

: 1333-84-2, 1344-28-1
aluminum oxide

: 7429-90-5
aluminium

Conditions

Conditions	Yield
With pyrographite In melt byproducts: CO, CO2; Electrolysis; in molten cryolite; coal-electrodes; decompn. voltage 1.2 V;;
Electrolysis; if Al2O3 contaminated with 0.45% (Fe2O3+SiO2), purity of product 99%, if with 0.15-0.25%, then 99.5%; other impurities: water (<1%), alkali (0.5-2%);
Electrolysis; impurities of Al2O3: water 0.18%, Fe2O3 0.04%, SiO2 0.05%, Na2O 0.18 %;

: cadmium sulfate

: 7429-90-5
aluminium

A: aluminum(III) sulfate

B: 7440-43-9
cadmium

Conditions

Conditions	Yield
In water Al powder activated with HCl; pptn. of Cd;	A n/a B 100%
In water Al powder activated with HCl; pptn. of Cd;	A n/a B 100%
In water Al wire; incomplete pptn. of Cd; pptn. within some minutes in presence of sodium potassium tartrate;
In water Al wire; incomplete pptn. of Cd; pptn. within some minutes in presence of sodium potassium tartrate;

...Expand

: 7439-93-2
lithium

: 7429-90-5
aluminium

: 7440-21-3
silicon

: lithium aluminium silicide

Conditions

Conditions	Yield
In melt in a tantalum tube weld-seald under Ar and protected from air by a silica jacket sealed under vac.; mixt. Li, Al, Si (15:3:6 mol) heated at 1223K, 10 h in vertical furnace and shaken several times;; cooled at rate of 6 K h**-1; elem. anal.;	100%

...Expand

: (C4H9)4N(1+)*F(1-)*14HF*7H2O = (C4H9)4NF*14HF*7H2O

: 7429-90-5
aluminium

: 115631-72-6
(C4H9)4N(1+)*AlF4(1-) = (C4H9)4NAlF4

Conditions

Conditions	Yield
In acetonitrile Electrolysis; galvanostatic conditions (300 mA, 10-70 V, 1.7 Ah), aluminum anode, platinum cathode; filtn., evapn. (reduced pressure), recrystn. (Et2O/CHCl3 1:4); elem. anal.;	100%

: 13536-79-3
lanthanum(III) bromide

: 7429-90-5
aluminium

: La4Br2Al5

Conditions

Conditions	Yield
In neat (no solvent, solid phase) all manipulations under Ar atm.; stoich. mixt. of compds. sealed in Ta tubes then tubes sealed inside silica ampoules under vac. (ca. 1E-2 mbar), heated at 900°C for 10 d;	100%

: [Ni(ammonia)6](2+)

: 7429-90-5
aluminium

A: Al(3+)*4OH(1-)=Al(OH)4(1-)

: nickel

Conditions

Conditions	Yield
With Sulfate In further solvent(s) Kinetics; byproducts: NH3, H2; ammine Ni complex reacted with metallic Al in aq. soln. at pH 11.0-12.0; unreacted Al is removed by dissoln. in alkaline soln.;	A n/a B 99.9%
With Nitrate In further solvent(s) Kinetics; byproducts: NH3, H2; ammine Ni complex reacted with metallic Al in aq. soln. at pH 11.0-12.0;	A n/a B 0%

...Expand

: 587-85-9
diphenylmercury(II)

: 7429-90-5
aluminium

: 7440-66-6
zinc

A: 1078-58-6
diphenylzinc

B: 841-76-9
triphenylaluminium

Conditions

Conditions	Yield
In neat (no solvent)	A 1% B 99%

...Expand

: 7647-01-0
hydrogenchloride

: 7429-90-5
aluminium

: aluminum(I) chloride

Conditions

Conditions	Yield
In neat (no solvent) liquid Al reacted with HCl gas in graphite furnace in high vac. at 750°C (by Schnoeckel, H. Z. Naturforsch. 1976, 31b, 1291);	99%
In neat (no solvent) passing HCl gas over liq. Al at 1000°C and 1E-5 mbar;
In neat (no solvent) passing HCl over Al in graphite cell heated to 900°C;

: 67-63-0
isopropyl alcohol

: 7429-90-5
aluminium

: AlCl3*4(CH3)2CHOH

Conditions

Conditions	Yield
With hydrogen chloride org. compd. cooling to -80°C, satn. with hydrogen chloride for 3 h, metal turnings addn., mixt. heating under reflux condenser for 5-6 h,crystn. at room temp.; crystals sepn. from mother liquor, washing (isopropyl alcohol), recrystn. from alcohol; elem. anal.; X-ray diffraction;	99%

: strontium

: 7429-90-5
aluminium

: SrAl2

Conditions

Conditions	Yield
In melt under Ar atm. mixt. Sr and Al was pressed into pellets and arc-melted;	99%
In melt Electric Arc; remelted several times; XRD;
In melt Electric Arc; arc melting of elements with 3 wt. % excess of Sr, remelting four times;

: 7440-56-4
germanium

: rubidium pentasulfide

: 7704-34-9
sulfur

: 7429-90-5
aluminium

: Rb3(AlS2)3(GeS2)7

Conditions

Conditions	Yield
In neat (no solvent) stoich. amt. of Rb2S5, Al, Ge and S sealed in fused silica tube; heated at 850°C for 3 d; cooled to 400°C over 4 d; detd. by energy-dispersive X-ray analysis;	99%

...Expand

: 378784-00-0, 7440-16-6
rhodium

: 7429-90-5
aluminium

: Al0733Rh0267

Conditions

Conditions	Yield
Stage #1: rhodium; aluminium In melt Electric arc; Inert atmosphere; Stage #2: at 999.84℃; for 72h; Sealed tube; Inert atmosphere; Stage #3: at 999.84℃; under 675068 Torr; for 0.333333h; Inert atmosphere;	99%

: 378784-00-0, 7440-16-6
rhodium

: iridium

: 7429-90-5
aluminium

: Al0.733(Rh0.75Ir0.25)0.267

Conditions

Conditions	Yield
Stage #1: rhodium; iridium; aluminium In melt Electric arc; Inert atmosphere; Stage #2: at 999.84℃; for 72h; Sealed tube; Inert atmosphere; Stage #3: at 999.84℃; under 675068 Torr; for 0.333333h; Inert atmosphere;	99%

...Expand

: 378784-00-0, 7440-16-6
rhodium

: iridium

: 7429-90-5
aluminium

: Al0.733(Rh0.5Ir0.5)0.267

Conditions

Conditions	Yield
Stage #1: rhodium; iridium; aluminium In melt Electric arc; Inert atmosphere; Stage #2: at 999.84℃; for 72h; Sealed tube; Inert atmosphere; Stage #3: at 999.84℃; under 675068 Torr; for 0.333333h; Inert atmosphere;	99%

...Expand

: 378784-00-0, 7440-16-6
rhodium

: iridium

: 7429-90-5
aluminium

: Al0.733(Rh0.25Ir0.75)0.267

Conditions

Conditions	Yield
Stage #1: rhodium; iridium; aluminium In melt Electric arc; Inert atmosphere; Stage #2: at 999.84℃; for 72h; Sealed tube; Inert atmosphere; Stage #3: at 999.84℃; under 675068 Torr; for 0.333333h; Inert atmosphere;	99%

...Expand

: iridium

: 7429-90-5
aluminium

: Al0733Ir0267

Conditions

Conditions	Yield
Stage #1: iridium; aluminium In melt Electric arc; Inert atmosphere; Stage #2: at 999.84℃; for 72h; Sealed tube; Inert atmosphere; Stage #3: at 999.84℃; under 675068 Torr; for 0.333333h; Inert atmosphere;	99%

: 74-85-1
ethene

: 7429-90-5
aluminium

: 97-93-8
triethylaluminum

Conditions

Conditions	Yield
With Na; Al2(C2H5)3Cl3 In not given byproducts: NaCl; NMR spect. anal.;	98.7%
With titanium; hydrogen at 120 - 130℃; under 2250.23 - 75007.5 Torr; for 13h;

: 7429-90-5
aluminium

: barium(II) oxide

: 7440-39-3
barium

Conditions

Conditions	Yield
5h in vac. at 1300-1340 °C; Metal distilles off. Repeated distn. gives 99.5% purity;	98.5%
4h in vac. at 1010-1030 °C; opening of apparatus under CO2, crushing of product under desiccated toluene to avoid self inflammation; Metal sublimes off. Repeated distn. gives 99.48% purity;
sublimation in vac.; 99.9% Ba;
sublimation in vac.; 99.9% Ba;

: 74-96-4
ethyl bromide

: 7429-90-5
aluminium

: 97-93-8
triethylaluminum

Conditions

Conditions	Yield
With Mg; Na In not given byproducts: MgBr2, NaBr; NMR spect. anal.;	98.2%

: 7440-55-3
gallium

: 7429-90-5
aluminium

: aluminum gallium

Conditions

Conditions	Yield
In neat (no solvent) Al and Ga metals were heated in sealed quartz tube to 700° and then cooled to room temp.;	98%
In neat (no solvent)
In neat (no solvent)
In neat (no solvent) melting Ga and Al in a porcelain tube in vac.;;

: 7553-56-2
iodine

: 7429-90-5
aluminium

: 7784-23-8
aluminium(III) iodide

Conditions

Conditions	Yield
In hexane thin foil of Al was suspended in degassed n-hexane under argon, 1.5 equiv. I2 was added, mixt. was boiled under reflux for 1-3 h; filtered into a heated receiver; elem. anal.;	96%
In further solvent(s) sheet aluminium in I2/ethyl iodide soln.;; impurities of I2;;
In neat (no solvent) addn. of Al to molten I2, ignition and melting of the metal;;

: 109-99-9
tetrahydrofuran

: 7429-90-5
aluminium

: C12H24O3Al2

Conditions

Conditions	Yield
With catalyst: HgCl2-ZnCl2-MeI In tetrahydrofuran refluxing (60°C, 5 h); addn. of benzene, filtration, evapn.; elem. anal.;	96%

: tantalum(V) oxide

: hafnium(IV) oxide

: 7429-90-5
aluminium

Hf(b),Ta(185-19) (W%): Hf(b),Ta(185-19) (W%)

Conditions

Conditions	Yield
With Al; KClO3; CaO In melt Electric Arc; thermit smelting; ball-milled powdered mixt. HfO2, Ta2O5, CaO, CaF2, KClO3 (10:1.2:4:3:6.5 wt.), 15% excess Al was poured inside MgO-lined steelreactor; ignition with burning Mg of trigger mixt. (KClO3:Al=2:1); also in Ar in copper double wall reactor; remelting by electron beam (2.7 kW, 1 h, vac. 3.9E-4 Pa) or arc melting (under Ar, tungsten electrode) to evap. Al excess; elem. anal.;	95.5%
With Al; KClO3; CaO In melt Electric Arc; thermit smelting; ball-milled powdered mixt. HfO2, Ta2O5, CaO, CaF2, KClO3 (10:1.2:4:3:6.5 wt.), 10% excess Al was poured inside MgO-lined steelreactor; ignition with burning Mg of trigger mixt. (KClO3:Al=2:1); also in Ar in copper double wall reactor; remelting by electron beam (2.7 kW, 1 h, vac. 3.9E-4 Pa) or arc melting (under Ar, tungsten electrode) to evap. Al excess; elem. anal.;	95%
With Al; KClO3; CaO In melt Electric Arc; thermit smelting; ball-milled powdered mixt. HfO2, Ta2O5, CaO, CaF2, KClO3 (10:1.2:4:3:6.5 wt.), 5% excess Al was poured inside MgO-lined steel reactor; ignition with burning Mg of trigger mixt. (KClO3:Al=2:1); also in Ar in copper double wall reactor; remelting by electron beam (2.7 kW, 1 h, vac. 3.9E-4 Pa) or arc melting (under Ar, tungsten electrode) to evap. Al excess; elem. anal.;	85%

...Expand

: 7429-90-5
aluminium

: 108-95-2
phenol

: 15086-27-8
aluminium(III) phenoxide

Conditions

Conditions	Yield
With mercury dichloride In tetrahydrofuran for 24h; Reflux; Inert atmosphere;	95%

: 7440-32-6
titanium

: graphite

: 7429-90-5
aluminium

: titanium-aluminium carbide

Conditions

Conditions	Yield
With Sn In neat (no solvent) other Radiation; mixt. milled for 2 h; coldly pressed into rods; combustion reaction carried out in CO2 laser; XRD;	95%
In solid self-propagating high-temperature synthesis;

...Expand

: 97-93-8
triethylaluminum

: 7429-90-5
aluminium

A: 75-24-1
trimethylaluminum

B: 2040-00-8
diethylaluminum iodide

Conditions

Conditions	Yield
With iodine; methyl iodide In ethanol Sonication; N2; CH3I, I2 and Al introduced in a condenser with C2H5OH at -20°C, ultrasonic acceleration at room temp. for 2 h, Et3Al (ratio MeI/Et3Al = 1.50) dropped into soln. within 10 min, sonication for 30 min; distilled (vac.);	A 86% B 95%

...Expand

: 7440-47-3
chromium

: 7440-02-0
nickel

: 7429-90-5
aluminium

: 7440-33-7
tungsten

A Ni(77.1),Cr(2.0),Al(17.9),W(3.0) (A%): Ni(77.1),Cr(2.0),Al(17.9),W(3.0) (A%)

B Ni(79.8),Cr(5.8),Al(12.2),W(2.2) (A%): Ni(79.8),Cr(5.8),Al(12.2),W(2.2) (A%)

Conditions

Conditions	Yield
In melt Electric Arc; ingots by arc melting of Ni(75)-Cr(2.5)-Al(20)-W(2.5) (at%), several remelts, sealed in silica tube under vac. with partial pressure of Ar, 1573K (2 weeks), furnace cooled to 1523K, 4 weeks, 1273K (6 weeks), quenched in iced water; electron microscopy, electron probe microanalysis, x-ray diffraction;	A 95% B 5%

...Expand

: 13955-96-9
dicyclopropylmercury

: 7429-90-5
aluminium

: {((CH2)2CH)3Al}2

Conditions

Conditions	Yield
In neat (no solvent) The reactants in sealed tube were heated in an oil bath to 75°C for 1 week;; sublimed at 50°C and 10E-6 torr;;	95%

: 2216-51-5
(-)-menthol

: 7429-90-5
aluminium

: aluminium tri(-)-menthylate

Conditions

Conditions	Yield
In toluene byproducts: H2; (inert atmosphere); reflux (12-15 h); decantation, extn., centrifugation, distn., recrystn. (benzene); elem. anal.;	95%
In benzene byproducts: H2; (inert atmosphere); reflux (25-30 h); decantation, extn., centrifugation, distn., recrystn. (benzene); elem. anal.;	87%

: 67-63-0
isopropyl alcohol

: 7429-90-5
aluminium

: aluminum tris(iso-propoxide)

Conditions

Conditions	Yield
With mercury dichloride for 9h; Reflux; Inert atmosphere;	95%

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Raw Materials

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CAS No.:7429-90-5
Name:Aluminium
Article Data:675
Molecular Structure:
Formula:Al
Molecular Weight:27.9895
Synonyms:0100MSR;0670TS;0870MSO;0900X;102B;102C;1100H24;1110W;130W;13T;1440YL;1N99;20B2C-M;210EA;350F;4690NS;5207N;550N;5654NS;6050T5;66NLB;716ON;725EA;725N;7640NS;8F02A;900M;91-2343T;97-4071RE;A 1H03P02;A 1H5;A 3303H;A 36 (metal);A95;A 999;A 99N;AA 15;AA 15(metal);AB 1003;AC 1003;AC 5000;ACG 1/2;ACG 3/8;ADS 1;AL 101;AL 885-20;AL-AT 250;ALBO 615;ALC Fine;ALE 06PB;ALE 11PB;APV;APV (metal);ASB (metal);AW 600;AW 666C;AW 808;Aisin Metal Fiber;Al 050P;Al18000;Al-At 500F;AlN 30H0;Alcan 105;Alcan 2000;Alcan 5754;Alcan7100;Alcan XI 1391;Alcoa 7468;Alex;Almi-Paste SSP 303AR;Alpaste 0100M;Alpaste0100MA;Alpaste 0200M;Alpaste 0230M;Alpaste 0230T;Alpaste0241M;Alpaste 0300M;Alpaste 0500M;Alpaste 0539X;Alpaste 0620MS;Alpaste 0780M;Alpaste 0900M;Alpaste 100MS;Alpaste 1100MA;Alpaste 1100NA;Alpaste 1100TA;Alpaste 1109MA;Alpaste1200M;Alpaste1810YL;Alpaste 1830YL;Alpaste 1900XS;Alpaste 1950M;Alpaste1950N;Alpaste 2172EA;Alpaste 240T;Alpaste 241M;Alpaste 4-621;Alpaste 4919;Alpaste50-63;Alpaste 51-148B;Alpaste 51-231;Alpaste 52-509;Alpaste 5301N;Aluminium lngot;
EINECS:231-072-3
Density:2.7 g/mL at 25 °C(lit.)
Melting Point:660.37 °C(lit.)
Boiling Point:2460oC
Flash Point:400 °C
Solubility:Soluble in hot water
Appearance:silver foil, shot or powder
Hazard Symbols:F,Xi,Xn
Risk Codes17-15-36/38-10-67-65-62-51/53-48/20-38-11
Safety: 7/8-43A-43-26-62-61-36/37-33-29-16-9
Transport Information:
PSA:0.00000
LogP:0.33750

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