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EAST CHEMSOURCES LIMITED

Sodium hydride Product Name: Sodium hydride Molecular Weight: 23.99 CAS NO: 7646-69-7 EC NO: 231-587-3 Molecular Formula: NaH

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Sodium hydride Basic information Physical and Chemical Properties Related chemical reaction application Category Explosive hazardous characteristics Flammability hazard characteristics Storage Characteristics extinguishing

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Sodium hydride CAS: 7646-69-7 Specification Item Standard Structural data confirmation 1. H-NMR: The data of structure are identical with reference standard 2. HPLC-MS: Ensure the

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7646-69-7 Application:intermediate

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Synthetic route

: 1333-74-0
hydrogen

: 7440-23-5
sodium

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In tetrahydrofuran heating under increasing H2-pressure (from about 7 to 35atm) to 250-350°C;;	98%
In further solvent(s) heating in mineral oil or in another hydrocarbon (high b.p.) under increasing H2-pressure (from about 7 to 35atm) to 250-350°C;;	98%
In paraffin heating under increasing H2-pressure (from about 7 to 35atm) to 250-350°C;;	98%

: 7440-23-5
sodium

: 7440-21-3
monosilane

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
With naphthalene In 1,2-dimethoxyethane byproducts: H2, SiH2; stirring a mixture of sodium, naphthalene and DME for 1 h, addn. of silane under argon; filtn., washing (ether in a vac. at 288 K for 14 h), elem. anal.;	97.8%

: 1333-74-0
hydrogen

: sodium acetylide

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) heating the powdered carbide in an autoclave (H2 pressure: 500atm)in a H2-stream to 650°C;; 72% NaH;;	86%
In neat (no solvent) heating the powdered carbide in an autoclave (H2 pressure: 500atm)in a H2-stream to 650°C;; 72% NaH;;	86%

: 7440-21-3
monosilane

A: 139508-55-7
sodium disilanyl

B: 139508-56-8
2-sodium trisilanyl

C: 139508-57-9
2-sodium isotetrasilanyl

D: 7646-69-7
sodium hydride

E: sodiumsilanyl

Conditions

Conditions	Yield
With sodium In diethylene glycol Under N2, filling of SiH4 in an evacuated flask with a freshly prepd. Na dispersion at -30 or 25°C under magnetic stirring. End of react. is reached after 3 days.; Concg. in vac. under stirring, filtn. (NaH), addn. of benzylchloride, GC.;	A 17.7% B 1.6% C 0% D 2.1% E 78.6%
With Na on activated charcoal In 1,2-dimethoxyethane Under N2, filling of SiH4 in an evacuated flask with a freshly prepd. Na dispersion at -30 or 25°C under magnetic stirring. End of react. is reached after 3 days.; Concg. in vac. under stirring, filtn. (NaH), addn. of benzylchloride, GC.;	A 30.4% B 4.6% C <1 D 0% E 65%
With sodium In 1,2-dimethoxyethane Under N2, filling of SiH4 in an evacuated flask with a freshly prepd. Na dispersion at -30 or 25°C under magnetic stirring. End of react. is reached after 3 days.; Concg. in vac. under stirring, filtn. (NaH), addn. of benzylchloride, GC.;	A 25.4-28.6 B 1.2-3.5 C <1 D 0-25.1 E 48.3-68.2

...Expand

titanium doped sodium aluminium hydride: titanium doped sodium aluminium hydride

A: 1333-74-0
hydrogen

B: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: Al; dehydrogenation: 160°C, against 0.1 MPa for 3 h; detd. of H2 with Sieverts type volumetric apparatus; XRD;	A 4% B n/a

: sodium alanate

A: 1333-74-0
hydrogen

B: 7646-69-7
sodium hydride

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
titanium(III) chloride at 200 - 250℃; under 760.051 Torr; Product distribution / selectivity; Neat (no solvent); Balled milled;
In neat (no solvent, solid phase) decompd. at heating;

...Expand

: sodium nitride

: 1333-74-0
hydrogen

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: NH3; at about 120°C;;

: sodium azide

: hydrogen

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) reaction of H2 with NaN3 at 300°C (under no circumstances 375°C); using of activated H2 is advantageous;;
In neat (no solvent) reaction of H2 with NaN3 at 300°C (under no circumstances 375°C); using of activated H2 is advantageous;;

: sodium azide

: 1333-74-0
hydrogen

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) heated in a H2-stream;;
In neat (no solvent) heated in a H2-stream;;
In neat (no solvent) byproducts: NH3; begin of react. at about 250°C;;

: 7732-18-5
water

: 7440-23-5
sodium

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) with over-heated H2O-vapor between 250 and 400°C;;
In neat (no solvent) with over-heated H2O-vapor between 250 and 400°C;;

: 1333-74-0
hydrogen

: 20611-81-8
disodium cyanamide

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) heating the powdered Na-compound in an autoclave (H2 pressure: 500atm)in a H2-stream to 650°C;;
In neat (no solvent) heating the powdered Na-compound in an autoclave (H2 pressure: 500atm)in a H2-stream to 650°C;;

: triphenyl boron sodium

A: 960-71-4
triphenylborane

B: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
With methanol In diethyl ether byproducts: CH3ONa; on addn. of ether/methanol to suspension of ((C6H5)3B)Na in ether;;
With methanol In diethyl ether byproducts: CH3ONa; on addn. of ether/methanol to suspension of ((C6H5)3B)Na in ether;;

Hg(b),Na(0.1-0.8) (W%): Hg(b),Na(0.1-0.8) (W%)

: 1333-74-0
hydrogen

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) anodic decompn. of Na-amalgame (prepared by electrolysis of aq. Na-salt solns. at 80-90°C), at 250-300°C in a Na-halogenide/NaOH-melt (cathode: Ni or Fe or Ni-alloy or Fe-alloy), react. of Na with H2;;
In neat (no solvent) anodic decompn. of Na-amalgame (prepared by electrolysis of aq. Na-salt solns. at 80-90°C), at 250-300°C in a Na-halogenide/NaOH-melt (cathode: Ni or Fe or Ni-alloy or Fe-alloy), react. of Na with H2;;

: 1822-71-5
NaC5H11-n

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In n-heptane decompn. at ambient temp., N2-atmosphere;;
In n-heptane decompn. at ambient temp., N2-atmosphere;;

: 7647-14-5
sodium chloride

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
With hydrogen byproducts: HCl; ΔH = 62.04 cal/mol;

: 34557-54-5
methane

: 7647-14-5
sodium chloride

A: 7647-01-0
hydrogenchloride

B: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent)

...Expand

: Na3AlH6, α

A: 1333-74-0
hydrogen

B: 7646-69-7
sodium hydride

C: 7429-90-5
aluminium

Conditions

Conditions	Yield
In neat (no solvent, solid phase) above 180°C; powder XRD;
In neat (no solvent, solid phase) heating; 228°C; DSC;

...Expand

: 7439-96-5
manganese

: 1310-73-2
sodium hydroxide

A: 7440-23-5
sodium

B: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
600-700°C, N2 or H2 flow; the product was separated;

...Expand

: 7440-23-5
sodium

A: sodium acetylide

B: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
With methane In gas Kinetics; (gas space temp.: 500 and 465°, Na temp.: 500 and 450° orgas space temp.: 340 - 445°, Na temp.: 395°); gas chromy.;

: hydrogen

: 7440-23-5
sodium

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) free Na reacts in H-atmosphere during glow discharge;;
calcium In neat (no solvent) passing H over pure Na in a Fe-ship in a refractory glass tube; addition of Ca-splinters accelerates the process;; NaH smoke floculates between two condensers; not pure;;
In neat (no solvent) Electrolysis; Na anode;Ni cathode;;

: 7440-23-5
sodium

: 1310-73-2
sodium hydroxide

A: sodium oxide

B: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
in system NaOH-K-Na-KOH;
In neat (no solvent) at 400°C in a closed Ni-tube;;
In neat (no solvent) at 400°C in a closed Ni-tube;;

...Expand

: 7440-23-5
sodium

: 74-86-2
acetylene

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) catalytic decomposition of C2H2 by molten Na leads to the formation of H; this reacts with Na at 100-550°C;;
In neat (no solvent) catalytic decomposition of C2H2 by molten Na leads to the formation of H; this reacts with Na at 100-550°C;;

: 74-85-1
ethene

: 7440-23-5
sodium

A: sodium carbide

B: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: polyethylene; polymerization of C2H4 during reaction of ethine with molten Na;;

...Expand

: 7647-01-0
hydrogenchloride

: 7440-23-5
sodium

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In gas in highly dild. flames of Na-vapor and hydrogen halide;;
In gas in highly dild. flames of Na-vapor and hydrogen halide;;

: 67-56-1
methanol

: 7440-23-5
sodium

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
byproducts: hydroxy-methyl radicals;

: 10035-10-6, 12258-64-9
hydrogen bromide

: 7440-23-5
sodium

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In gas in highly dild. flames of Na-vapor and hydrogen halide;;
In gas in highly dild. flames of Na-vapor and hydrogen halide;;

: 10034-85-2
hydrogen iodide

: 7440-23-5
sodium

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In gas in highly dild. flames of Na-vapor and hydrogen halide;;
In gas in highly dild. flames of Na-vapor and hydrogen halide;;

: hydrogen

: 25681-79-2
disodium

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent, gas phase) byproducts: Na; reacn. in crossing region of Na2 molecular beam and H-atom beam; QMS, LIF;

: sodium amide

: hydrogen

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: NH3; reaction of dry H2 with NaNH2 at 300°C;;
In neat (no solvent) byproducts: NH3; reaction of dry H2 with NaNH2 at 300°C;;

: sodium oxide

: hydrogen

: 7646-69-7
sodium hydride

Conditions

Conditions	Yield
In neat (no solvent) reduction of Na2O with H at 170-180°C;;

: 7646-69-7
sodium hydride

: 7440-05-3
palladium

: sodium palladium hydrate

Conditions

Conditions	Yield
In neat (no solvent) 2:1 molar mixture of educts, 700K;	100%
In neat (no solvent, solid phase) according to: W. Bronger, P. Mueller, D. Schmitz, H. Spittank, Z. anorg. allg. Chem. 516 (1984) 35; heating reaction mixt. (molar ratio NaH:Pd=4:1) in H2 atmosphere (360°C, 6 h); X-ray anal.;

: 7789-78-8
calcium hydride

: magnesium hydride

: potassium metaborate

: 7646-69-7
sodium hydride

A: potassium borohydride

B: magnesium oxide

Conditions

Conditions	Yield
In neat (no solvent, solid phase) ball milled at room temp., 120 min; extd. (ethylenediamine) under Ar; filtered; ethylenediamine evapd. at room temp. under 0.05 MPa; XRD;	A 100% B n/a

...Expand

: 63115-77-5
arachno-6,8-S2B7H9

: 7646-69-7
sodium hydride

: 75-05-8
acetonitrile

: hypho-CH3CNS2B7H8Na

Conditions

Conditions	Yield
In tetrahydrofuran byproducts: H2; distn. of THF into mixt. of NaH and B-complex, warming to room temp., filtration and conc. after H2 evolution (vac.), addn. of predried CH3CN, refluxing overnight; evapn. (vac.);	100%

...Expand

: tris(triphenylphosphinegold)oxonium fluoroborate

: 33836-49-6
1,3-diphenyl-2,8-dihydrocyclopenta[a]indene

: 7646-69-7
sodium hydride

: 2,4-dihydro-1,3-diphenyl(triphenylphosphinegold)cyclopenta{b}indene

Conditions

Conditions	Yield
In tetrahydrofuran Ar atmosphere; stirring suspn. of Au-complex, org. ligand and NaH at 0 to -10°C for 1 h 45 min; addn. of several crystals of PPh3; filtration, evapn. to dryness (vac.); residue washing (pentane), dissoln. (THF), addn. to cold pentane (stirring), pptn.; ppt. sepn., washing (pentane), drying; elem. anal.;	100%

...Expand

: tris(triphenylphosphinegold)oxonium fluoroborate

: 7646-69-7
sodium hydride

: 670-54-2
ethenetetracarbonitrile

A: 2P(C6H5)3*Au(1+)*BF4(1-)=(P(C6H5)3)2AuBF4

B: 506-65-0
gold(I) cyanide

Conditions

Conditions	Yield
In tetrahydrofuran stirring suspn. of all substances in abs. THF for 4 h; ppt. sepn., washing (THF, water and ether) and drying gave AuCN; soln. dild. with petroleum ether and cooled to 0°C; ppt. sepn. and washing with petroleum ether gave Au-complex;	A 100% B 67%

...Expand

: {(C5H5)Fe(C5H4C3H3N2)}*B((C3H2N2C5H4)Fe(C5H5))(C8H14)

: 7646-69-7
sodium hydride

: Na(1+)*{((C5H5)Fe(C5H4C3H2N2))2B(C8H14)}(1-)=Na{((C5H5)Fe(C5H4C3H2N2))2B(C8H14)}

Conditions

Conditions	Yield
In benzene to soln. of Fe-B-compd. was added NaH, stirred for 2 h at room temp.; filtn., evapn.;	100%

: 132939-86-7
IrOs(H)2(CO)3((C6H5)2PCH2P(C6H5)2)2(1+)*BF4(1-) = {IrOs(H)2(CO)3(((C6H5)2P)2CH2)2}BF4

: 7646-69-7
sodium hydride

: 132959-03-6
IrOs(H)2(CO)3((C6H4)C6H5PCH2P(C6H5)2)((C6H5)2PCH2P(C6H5)2)

Conditions

Conditions	Yield
In tetrahydrofuran (Ar); added THF to NaH and Ir-complex; stirred vigorously for 1 h; evapd. (vac.); (31)P NMR, IR;	100%

: 15038-48-9, 17731-95-2
tris(acetonitrile)tricarbonylmolybdenum(0)

: 7646-69-7
sodium hydride

: 161202-62-6
3-diphenylphosphanyl-2-diphenylphosphanylmethyl-2-methyl-1-propanethiol

: Na(1+)*(CO)3Mo(C29H29P2S)(1-)*2C4H8O=Na[(CO)3Mo(C29H29P2S)]*2C4H8O

Conditions

Conditions	Yield
In tetrahydrofuran Ar atmosphere, addn. of NaH to soln. of ligand at 0°C, stirring (30 min), addn. of solid Mo complex, stirring (30 min); concn., washing (petroleum ether (40/60), ultrasonication), removement of solvent (vacuum);	100%

...Expand

: 17653-38-2
C2B7H13

: 7646-69-7
sodium hydride

: 107-13-1
acrylonitrile

: 679838-36-9, 680224-29-7
endo/exo-6-(NCCH2CH2)-arachno-6,8-C2B7H12

Conditions

Conditions	Yield
In 1,2-dimethoxyethane under N2 atm. arachno-6,8-C2B7H13 was dissolved in DME and cooled to 0°C, NaH was added, react. mixt. was warmed to room temp., filtered,cooled to 0°C, acrylonitrile was added dropwise and stirred for 12 h; HCl-Et2O was added at 0°C, allowed to warm to room temp., soln. was filtered, were evapd. in vacuo, and dried in vacuo; elem. anal.;	100%

...Expand

: 15038-48-9, 17731-95-2
tris(acetonitrile)tricarbonylmolybdenum(0)

: 215854-12-9
(CH3OCH2)C(CH2P(C6H5)2)(CH2SH)2

: 7646-69-7
sodium hydride

: 2Na(1+)*(CO)3Mo(C18H21OPS2)(2-)*2C4H8O=Na2[(CO)3Mo(C18H21OPS2)]*2C4H8O

Conditions

Conditions	Yield
In tetrahydrofuran Ar atmosphere, addn. of NaH to soln. of ligand at 0°C, stirring (30 min), addn. of solid Mo complex, stirring (30 min); concn., washing (petroleum ether (40/60), ultrasonication), removement of solvent (vacuum);	100%

...Expand

: 109-99-9
tetrahydrofuran

: 1428144-91-5
1,8-bis(2-hydroxy-3,5-di-tert-butylbenzyl)-4,11-dimethyl-1,4,8,11-tetraazacyclotetradecane

: 7646-69-7
sodium hydride

: 1428144-92-6
Na2{(tBu2PhO)2Me2Cyclam}

Conditions

Conditions	Yield
at 20℃; Inert atmosphere;	100%

...Expand

: 109-99-9
tetrahydrofuran

: 1607013-48-8
B-(2-pyridyl)-9-borabicyclo[3.3.1]nonane hydrogen chloride salt

: 7646-69-7
sodium hydride

: Na[B-(2-pyridyl)-9-borabicyclo[3.3.1]nonane]*2THF

Conditions

Conditions	Yield
for 12h; Inert atmosphere; Schlenk technique; Glovebox;	100%

...Expand

: 288-13-1
NH-pyrazole

: 7646-69-7
sodium hydride

: 98-80-6
phenylboronic acid

: 80583-77-3
sodium phenyltris(pyrazolyl)borate

Conditions

Conditions	Yield
at 200℃; for 0.25h; Microwave irradiation; Inert atmosphere;	100%

...Expand

: 121-43-7
Trimethyl borate

: 7646-69-7
sodium hydride

: 16940-66-2
sodium tetrahydroborate

Conditions

Conditions	Yield
Heating;	99.5%
In neat (no solvent) 1mol B(OCH3)3, 4mol NaH, 225-275°C;; 90-96% NaBH4;;	94%
In neat (no solvent) 1mol B(OCH3)3, 4mol NaH, 225-275°C;; 90-96% NaBH4;;	94%

: boric acid trimethylester tetrahydrofuranate

: Tetrahydro-furan; compound with trifluoroborane

: 7646-69-7
sodium hydride

: 16940-66-2
sodium tetrahydroborate

Conditions

Conditions	Yield
In tetrahydrofuran byproducts: NaF; addn. of B(OCH3)3THF to NaH at 60-65°C (stirring, N2-atmosphere), NaH dissolves, boiling, cooling to ambient temp., addn. of BF3THF, distn. of THF and B(OCH3), extractn. of residue with isopropyl amine;; pure product;;	99%
In tetrahydrofuran byproducts: NaF; addn. of B(OCH3)3THF to NaH at 60-65°C (stirring, N2-atmosphere), NaH dissolves, boiling, cooling to ambient temp., addn. of BF3THF, distn. of THF and B(OCH3), extractn. of residue with isopropyl amine;; pure product;;	99%

...Expand

: 91686-41-8
2,3-bis(trimethylsilyl)-2,3-dicarba-nido-hexaborane(8)

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 7646-69-7
sodium hydride

: Na(1+)*(CH3)2NCH2CH2N(CH3)2*B4H5C2(Si(CH3)3)2(1-) = Na(((CH3)2NCH2)2)(Si(CH3)3)2C2B4H5

Conditions

Conditions	Yield
In further solvent(s) byproducts: H2; addn. of B-compd. in TMEDA to mixt. of NaH and TMEDA (-78°C, vac.); filtration (vac.), solvent removal (vac.); recrystn. (hexane); elem. anal.;	99%

...Expand

: 464926-60-1
(1,2-bis[1,3-dioxan-2-yl]-3,4-bis[trimethylsilyl]cyclobutadiene)cyclopentadienylcobalt

: 7646-69-7
sodium hydride

: 406498-73-5
(1,2-bis[1,3-dioxan-2-yl]cyclobutadiene)cyclopentadienylcobalt

Conditions

Conditions	Yield
With Me4NF In dimethyl sulfoxide under inert atmosphere, Schlenk techniques; Co complex, NaH and Me4NF (molar ratio 2.4:1:19.3) dissolved in dry Me2SO; heated to 50°C overnight; aq. workup with ethyl ether; chromd. (silica gel, hexanes-ethyl acetate);	99%

: 471255-34-2
Ir(H)(Cl)CH3OC6H2(CH2P(C4H9)2)2

: Ir(Cl)CH3OC6H2(CH2P(C4H9)2)CH2P(C4H9)C(CH3)2CH2

: 1333-74-0
hydrogen

: 7646-69-7
sodium hydride

: 471255-35-3
(p-OMetBu4PCP)IrH4

Conditions

Conditions	Yield
With NaH In tetrahydrofuran Sonication; complexes in THF were treated with 100% excess of NaH, the mixt. was stirred at room temp. for 1 h under H2 atm., sonicated for 6 h with intermittent cooling and stirring, stirred for 24 h at room temp.; filtered, THF was removed by a stream of H2;	99%

...Expand

: 109-99-9
tetrahydrofuran

: La2(O-2,6-i-Pr2C6H3)6

: 2078-54-8
2,6-diisopropylphenol

: 7646-69-7
sodium hydride

: 172918-17-1
(THF)La(O-2,6-i-Pr2C6H3)2(μ-O-2,6-i-Pr2C6H3)2Na(THF)2

Conditions

Conditions	Yield
In tetrahydrofuran; toluene Ar-atmosphere; addn. of La-compd. (in PhMe) to mixt. of diisopropylphenol and NaH (in THF) with stirring, stirring for 72 h at room temp.; filtration (Celite), removal of volatiles (vac.), washing (hexane), extn. into PhMe, filtration (Celite), vol. reduction (vac.), crystn. (-40°C, overnight); elem. anal.;	99%

...Expand

: [diruthenium(μ-CN(Me)2)(μ-CO)(CO)(NHCCMe3CC(Ph)(Cp)2]CF3SO3

: 7646-69-7
sodium hydride

: [diruthenium(μ-CN(Me)2)(μ-CO)(CO)(NNaCCMe3CC(Ph))(Cp)2]CF3SO3

Conditions

Conditions	Yield
In not given (N2), mixed; not isolated, detected by IR;	99%

: [diruthenium(μ-CN(Me)(benzyl))(μ-CO)(CO)(NHCCMe3CCH)(Cp)2]CF3SO3

: 7646-69-7
sodium hydride

: [diruthenium(μ-CN(Me)(benzyl))(μ-CO)(CO)(NNaCCMe3CCH)(Cp)2]CF3SO3

Conditions

Conditions	Yield
In not given (N2), mixed; not isolated, detected by IR;	99%

: [diruthenium(μ-CN(Me)2)(μ-CO)(CO)(NHCCMe3CC(p-tolyl))(Cp)2]CF3SO3

: 7646-69-7
sodium hydride

: [diruthenium(μ-CN(Me)2)(μ-CO)(CO)(NNaCCMe3CC(p-tolyl))(Cp)2]CF3SO3

Conditions

Conditions	Yield
In not given (N2), mixed; not isolated, detected by IR;	99%

: [diruthenium(μ-CN(Me)(benzyl))(μ-CO)(CO)(NHCCMe3CC(Ph)(Cp)2]CF3SO3

: 7646-69-7
sodium hydride

: [diruthenium(μ-CN(Me)(benzyl))(μ-CO)(CO)(NNaCCMe3CC(Ph))(Cp)2]CF3SO3

Conditions

Conditions	Yield
In not given (N2), mixed; not isolated, detected by IR;	99%

: [diruthenium(μ-CN(Me)(xylyl))(μ-CO)(CO)(NHCCMe3CCC(Me)CH2(Cp)2]CF3SO3

: 7646-69-7
sodium hydride

: [diruthenium(μ-CN(Me)(xylyl))(μ-CO)(CO)(NNaCCMe3CCC(Me)CH2)(Cp)2]CF3SO3

Conditions

Conditions	Yield
In not given (N2), mixed; not isolated, detected by IR;	99%

: [diruthenium(μ-CN(Me)(benzyl))(μ-CO)(CO)(NHCCMe3CC(p-tolyl))(Cp)2]CF3SO3

: 7646-69-7
sodium hydride

: [diruthenium(μ-CN(Me)(benzyl))(μ-CO)(CO)(NNaCCMe3CC(p-tolyl))(Cp)2]CF3SO3

Conditions

Conditions	Yield
In not given (N2), mixed; not isolated, detected by IR;	99%

: [diruthenium(μ-CN(Me)(xylyl))(μ-CO)(CO)(NHCCMe3CCBu)(Cp)2]CF3SO3

: 7646-69-7
sodium hydride

: diruthenium(μ-CN(Me)(xylyl)(μ-CO)(CO)(NNaCCMe3CCBu)(Cp)2]CF3SO3

Conditions

Conditions	Yield
In not given (N2), mixed; not isolated, detected by IR;	99%

: [diruthenium(μ-CN(Me)(xylyl))(μ-CO)(CO)(NHCCMe3CC(Ph)(Cp)2]CF3SO3

: 7646-69-7
sodium hydride

: [diruthenium(μ-CN(Me)(xylyl))(μ-CO)(CO)(NNaCCMe3CC(Ph))(Cp)2]CF3SO3

Conditions

Conditions	Yield
In not given (N2), mixed; not isolated, detected by IR;	99%

: [diruthenium(μ-CN(Me)(xylyl))(μ-CO)(CO)(NHCCMe3CC(p-tolyl))(Cp)2]CF3SO3

: 7646-69-7
sodium hydride

: [diruthenium(μ-CN(Me)(xylyl))(μ-CO)(CO)(NNaCCMe3CC(p-tolyl))(Cp)2]CF3SO3

Conditions

Conditions	Yield
In not given (N2), mixed; not isolated, detected by IR;	99%

: [Bu3NH][1-ammonia-closo-dodecaborate]

: 7646-69-7
sodium hydride

: sodium amino-closo-dodecaborate

Conditions

Conditions	Yield
In tetrahydrofuran refluxed; filtered, evapd., washed (Et2O);	99%
In tetrahydrofuran refluxing (Bu3NH)(B12H11NH3) with 2 equiv. NaH in THF; solvent was evapd., residue was washed with Et2O;	99%

: [Ph(pz)Bt(tBu)]H

: 7646-69-7
sodium hydride

: sodium phenyl(pyrazolyl)bis((tert-butylthio)methyl)borate

Conditions

Conditions	Yield
In tetrahydrofuran NaH added to soln. of Ph(pz)Bt(tBu)H;	99%

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