DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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Cas:95-48-7
Min.Order:0 Metric Ton
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Type:Manufacturers
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:95-48-7
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inquiryO-Cresol--99.5% Min CAS No.95-48-7 Appearance: Colorless to yellowish liquid or crystal Purity: 99.5% Min. Appearance:crystal powder Storage:Warehouse ventilation, away from open flame, high temperature, and antioxidant Package:25kg/bag or
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Product Name: o-Cresol Synonyms: O-CRESOL;O-CRESYLIC ACID;O-METHYLPHENOL;O-HYDROXYTOLUENE;FEMA 3480;2-HYDROXYTOLUENE;2-METHYLPHENOL;1-HYDROXY-2-METHYLBENZENE CAS: 95-48-7 MF: C7H8O MW: 108.14 EINECS: 202-423-8
Cas:95-48-7
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryProduct Name: o-Cresol Synonyms: 2-Hydroxytoluene; 2-Methylphenol; 2-Cresol; 2-OH-benzyl; 2-hydroxybenzyl CAS RN.:
Product Name: o-Cresol Synonyms: 2-Hydroxytoluene; 2-Methylphenol; 2-Cresol; 2-OH-benzyl; 2-hydroxybenzyl CAS RN.: 95-48-7;155174-21-3 EINEC
We are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediat
Cas:95-48-7
Min.Order:1 Gram
FOB Price: $4.0 / 5.0
Type:Lab/Research institutions
inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:95-48-7
Min.Order:10 Gram
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Type:Trading Company
inquiryLonwin Industry group limited as a professional manufactor & exporter of chemical materials ,we totally haver more than 270 stuffs, we have been on this line for more than 9 years. Our chemical materials are exported to lot of countries and reg
Cas:95-48-7
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:95-48-7
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:95-48-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct name: O-Cresol CAS No.: 95-48-7 Molecule Formula:C7H8O Molecule Weight:108.14 Purity: 99.0% Package: 25kg/drum Description:Colorless crystals Manufacture Standards:Enterprise Standard TESTING ITEMS
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Appearance Colorless transparent liquid Assay( O-Cresol) 99.0%min Phenol / P-cresol / m-Cresol / Port:Shanghai or Hangzhou port
Superior quality, moderate price & quick delivery. Appearance:white powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediate
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
good quality and cheap price Package:25kg/200kg Application:as intermediates Transportation:by courier/sea/air
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
o-cresol 95-48-7 99.5% min 99.5% min CAS: 95-48-7 High Quality Prompt Delivery Free Sample Production Information : Technical index Items Standards As…Appearance:colorless to yellowish liquid or crystal Storage:Store in a well-closed container away f
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:95-48-7
Min.Order:1 Kilogram
FOB Price: $112.0
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
1.High purity, like 99%, 99.9%, 99.95%, 99.99%, 99.999%2.Quality control, test sample before shipping and keep sample for 3 years after shipping;3. Prompt shipment with professional documents;4. Packing as your request, with photo before shipment;5.
Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
Conditions | Yield |
---|---|
montmorillonite K-10 for 0.0166667h; Solid phase reaction; desilylation; microwave irradiation; | 100% |
With Nanoporous Na+-Montmorillonite Perchloric Acid In ethanol at 20℃; for 0.0833333h; | 90% |
With hydrogenchloride In methanol Ambient temperature; Yield given; |
o-Tolyl N,N,N',N'-tetramethylphosphorodiamidate
ortho-cresol
Conditions | Yield |
---|---|
With formic acid for 1h; Product distribution; Heating; | 100% |
In formic acid for 1h; Heating; Yield given; |
2-Methylphenylboronic acid
ortho-cresol
Conditions | Yield |
---|---|
With 3,3'-dihexyloxy-1,1'-binaphthylidene-4,4'-dione; potassium hydroxide In tetrahydrofuran; water at 20℃; | 100% |
With dihydrogen peroxide at 20℃; for 0.25h; Green chemistry; | 98% |
With water; oxygen; sodium sulfite at 50℃; for 1h; Green chemistry; | 97% |
Conditions | Yield |
---|---|
With hydrogen In para-xylene at 120℃; under 750.075 Torr; for 24h; Glovebox; Sealed tube; chemoselective reaction; | 99% |
With formic acid; C18H14ClN4O2Ru(1+)*Cl(1-); sodium formate In water at 80℃; for 32h; Inert atmosphere; | 70% |
With acetic acid; zinc In ethanol at 180℃; for 0.25h; Solvent; Temperature; Microwave irradiation; | 56% |
Conditions | Yield |
---|---|
platinum; potassium oxide at 360℃; | A 98% B 2% |
platinum; potassium oxide at 360℃; Product distribution; other content of catalyst; | A 98% B 2% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; cobalt(II) chloride In ethanol at 0 - 25℃; for 10h; | 98% |
Conditions | Yield |
---|---|
With hydrogen; nickel-titanium-aluminum In various solvent(s) at 160℃; for 3h; | 97.8% |
With hydrogen; nickel-titanium-aluminum In various solvent(s) at 160℃; for 3h; Product distribution; Rate constant; Thermodynamic data; other temperatures; | 97.8% |
Conditions | Yield |
---|---|
With glycolic Acid; copper hydroxide; sodium hydroxide In water; dimethyl sulfoxide at 120℃; for 6h; Inert atmosphere; Schlenk technique; | 97% |
With copper(l) iodide; 8-quinolinol; potassium hydroxide In water; dimethyl sulfoxide; tert-butyl alcohol at 100℃; for 48h; Inert atmosphere; | 96% |
Stage #1: ortho-methylphenyl iodide With copper(l) iodide; 8-Hydroxyquinoline-N-oxide In dimethyl sulfoxide at 20℃; for 0.166667h; Inert atmosphere; Stage #2: With cesiumhydroxide monohydrate In water; dimethyl sulfoxide at 100℃; for 24h; Inert atmosphere; | 95% |
1,1-dimethylethyl 2-methylphenyl carbonate
ortho-cresol
Conditions | Yield |
---|---|
With erbium(III) triflate In ethanol for 25h; Microwave irradiation; | 97% |
2-hydroxy-3-methylphenyl boronic acid
ortho-cresol
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 120℃; for 24h; | 96% |
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide at 20℃; for 3h; | 95% |
Conditions | Yield |
---|---|
With ammonium bicarbonate In water at 20℃; for 2h; Schlenk technique; | 95% |
Conditions | Yield |
---|---|
With pyridine; hydrogen fluoride for 1.66667h; Decomposition; Fluoro-dediazoniation; Irradiation; | A 93.8% B 1.1% |
Conditions | Yield |
---|---|
Stage #1: 2-methylphenyl bromide With potassium hydroxide; tris-(dibenzylideneacetone)dipalladium(0); 2-((di-adamantan-1-yl)phosphaneyl)-1-(2,6-diisopropylphenyl)-1H-imidazole In 1,4-dioxane; water at 100℃; for 20h; Inert atmosphere; Stage #2: With hydrogenchloride In 1,4-dioxane; water at 20℃; Inert atmosphere; | 93% |
With cesiumhydroxide monohydrate; bis[(trimethylsilyl)methyl](1,5-cyclooctadiene)palladium(II); 2-((di-adamantan-1-yl)phosphaneyl)-1-(2,6-diisopropylphenyl)-1H-imidazole In tetrahydrofuran at 24℃; for 20h; Inert atmosphere; | 92% |
Stage #1: 2-methylphenyl bromide With copper(l) iodide; 8-Hydroxyquinoline-N-oxide In dimethyl sulfoxide at 20℃; for 0.166667h; Inert atmosphere; Stage #2: With cesiumhydroxide monohydrate In water; dimethyl sulfoxide at 110℃; for 18h; Inert atmosphere; | 90% |
2-(tert-butyldimethylsilyloxy)toluene
ortho-cresol
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol at 20℃; for 1.6h; | 93% |
With zinc tetrafluoroborate In water for 24h; Heating; | 88% |
With sodium cyanide In ethanol; water at 80℃; for 15h; chemoselective reaction; | 84.5% |
With sodium phosphate dodecahydrate In N,N-dimethyl-formamide at 20℃; for 2.5h; | 83% |
Conditions | Yield |
---|---|
With cesiumhydroxide monohydrate; bis[(trimethylsilyl)methyl](1,5-cyclooctadiene)palladium(II); 2-((di-adamantan-1-yl)phosphaneyl)-1-(2,6-diisopropylphenyl)-1H-imidazole In tetrahydrofuran at 24℃; for 20h; Inert atmosphere; | 92% |
With 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; tris-(dibenzylideneacetone)dipalladium(0); cesiumhydroxide monohydrate In tetrahydrofuran at 24℃; Inert atmosphere; Glovebox; Sealed tube; | 91% |
With aluminum (III) chloride; choline chloride; urea; sodium hydroxide at 180℃; for 6h; Reagent/catalyst; Green chemistry; | 86.2% |
With trans-di(μ-acetato)bis[o-(di-o-tolyl-phosphino)benzyl]dipalladium(II); C29H45Pt; potassium carbonate In water; N,N-dimethyl-formamide at 115℃; for 0.5h; Inert atmosphere; Microwave irradiation; | 63% |
ortho-cresol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In benzene at 70℃; | 91% |
3,3-diethyl-1-(o-tolyl)triaz-1-ene
ortho-cresol
Conditions | Yield |
---|---|
With water; sulfonic acid resin (H+ form) In acetonitrile for 0.166667h; Heating; | 90% |
methyl 2-methylphenoxy acetate
A
o-methylphenoxyacetic acid
B
ortho-cresol
Conditions | Yield |
---|---|
With lithium chloride In N,N-dimethyl-formamide for 22h; Heating; | A 90% B 5% |
ortho-cresol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride; dihydrogen peroxide; potassium hydrogencarbonate In tetrahydrofuran; methanol; water at 20℃; for 16h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With iodine at 20℃; | 89% |
Conditions | Yield |
---|---|
With selenium(IV) oxide; dihydrogen peroxide In tetrahydrofuran for 10h; Heating; | A 88% B 9 % Chromat. |
With dihydrogen peroxide; methyltrioctylammonium tetrakis(oxodiperoxotungsto)phosphate at 90℃; for 1.5h; | A 23% B 10% |
methanol
phenol
A
2.6-dimethylphenol
B
methoxybenzene
C
ortho-cresol
Conditions | Yield |
---|---|
zirconium(IV) oxide at 320℃; under 112509 Torr; for 1.5h; Product distribution; Kinetics; Further Variations:; Catalysts; Pressures; Temperatures; | A 87% B 0.5% C 6% |
aluminum oxide at 290℃; under 195.02 - 600.05 Torr; Kinetics; Product distribution; Rate constant; | |
samarium(III) oxide; tin(IV) oxide at 349.85℃; for 1h; Product distribution; Further Variations:; Catalysts; Alkylation; |
Conditions | Yield |
---|---|
With trimethylsilyl iodide at 105 - 114℃; for 0.25h; Microwave irradiation; Inert atmosphere; | 85% |
With pyridine hydrochloride for 0.233333h; demethylation; microwave irradiation; | 82% |
With pyridinium p-toluenesulfonate for 0.0333333h; microwave irradiation; | 70% |
With boron tribromide-dimethyl sulfide complex In 1,2-dichloro-ethane at 83.5℃; for 12h; | 67.2% |
With hydrogen In dodecane; hexane at 270℃; under 22502.3 Torr; for 8h; Autoclave; |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; iron(III) chloride hexahydrate at 110℃; for 4h; Sealed tube; | 84% |
Conditions | Yield |
---|---|
Stage #1: o-toluidine With sulfuric acid at 20℃; Cooling with ice; Stage #2: With sodium nitrite In water Reflux; | 83% |
Stage #1: o-toluidine With sodium nitrite In water at 20℃; Milling; Green chemistry; Stage #2: With water at 60℃; for 0.416667h; Neutral conditions; Green chemistry; | 78% |
With sulfuric acid Diazotization.Verkochen des Diazoniumsulfats mit Wasser; |
Conditions | Yield |
---|---|
With hydrogen In toluene at 629.9℃; Mechanism; Kinetics; Rate constant; other temperature 760-1110 K; | A n/a B 83% |
ortho-cresol
Conditions | Yield |
---|---|
With 6,6'-dimethyl-2,2'-bipyridine; (1,2-dimethoxyethane)dichloronickel(II); bis(pinacol)diborane; lithium tert-butoxide In methanol; N,N-dimethyl acetamide; water at 30℃; for 24h; Inert atmosphere; Glovebox; Sealed tube; | 83% |
With [2,2]bipyridinyl; (1,2-dimethoxyethane)dichloronickel(II); water; bis(pinacol)diborane; lithium tert-butoxide In methanol; N,N-dimethyl acetamide at 30℃; for 24h; Schlenk technique; | 63% |
Conditions | Yield |
---|---|
at 20℃; for 0.666667h; | 100% |
With triethylamine In dichloromethane at 20℃; | 99% |
With silver trifluoromethanesulfonate at 60℃; for 0.116667h; neat (no solvent); | 99% |
Conditions | Yield |
---|---|
With benzyltriphenylphosphonium peroxodisulfate; potassium bromide In acetonitrile for 4.5h; Heating; | 100% |
With dihydrogen peroxide; vanadia; potassium bromide In chloroform; water at 24.84℃; under 760.051 Torr; | 99% |
With hydrogen bromide; acetic acid In water; dimethyl sulfoxide at 20℃; for 16h; | 99% |
Conditions | Yield |
---|---|
With (NH4)2Ce(NO3)6 on pillared bentonite In methanol at 25℃; for 48h; | 100% |
With thionyl chloride; bismuth subnitrate In dichloromethane at 20℃; for 2h; | 83% |
With cupric nitrate trihydrate supported on K 10 montmorillonite clay; nitric acid; acetic anhydride In tetrachloromethane for 1h; Ambient temperature; | 80% |
Conditions | Yield |
---|---|
With triethylamine In ethyl acetate at 0 - 20℃; for 0.166667h; Green chemistry; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; | 89% |
With pyridine | 85% |
With pyridine In dichloromethane at 0 - 20℃; Inert atmosphere; | 74% |
With pyridine |
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran | 100% |
With potassium carbonate In acetone Reflux; | 100% |
Stage #1: ortho-cresol With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 0.5h; Inert atmosphere; Stage #2: propargyl bromide In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With potassium carbonate In butanone for 5.5h; Heating; | 100% |
With potassium carbonate In acetone Ambient temperature; | 100% |
With caesium carbonate In acetonitrile at 25℃; | |
With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 3h; | |
With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 3h; |
methyl 3,3,3-trifluoropyruvate
ortho-cresol
Conditions | Yield |
---|---|
With triethylamine In tetrachloromethane for 24h; Ambient temperature; | 100% |
With tert-butylamine In tetrachloromethane for 3h; Ambient temperature; other substituted phenols, other polyfluorinated carbonyl compounds, other amines and solvents; nucleophilic catalysis in C-hydroxyalkylation; |
Conditions | Yield |
---|---|
With Trimethylacetic acid In toluene for 20h; Heating; | 100% |
ortho-cresol
Ethyl 2-bromopropionate
ethyl 2-(2-methylphenyl)oxypropionate
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide | 100% |
With potassium iodide In N,N-dimethyl-formamide; acetone Heating; | 83% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 1h; Etherification; | 100% |
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 0 - 20℃; for 16h; | 99% |
Stage #1: ortho-cresol With N-ethyl-N,N-diisopropylamine In 1,2-dichloro-ethane for 0.166667h; Stage #2: chloromethyl methyl ether In 1,2-dichloro-ethane at 20℃; for 10h; | 98% |
tert-butyldimethylsilyl chloride
ortho-cresol
2-(tert-butyldimethylsilyloxy)toluene
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 3h; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide at 23℃; for 15h; Inert atmosphere; Schlenk technique; | 99% |
With 1H-imidazole; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate at 20℃; for 2h; | 98% |
ortho-cresol
ortho-nitrofluorobenzene
1-methyl-2-(2-nitrophenoxy)benzene
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 95℃; for 20h; | 100% |
Stage #1: ortho-cresol With sodium hydride In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; Stage #2: ortho-nitrofluorobenzene In N,N-dimethyl-formamide at 20 - 50℃; for 13h; Inert atmosphere; | 93% |
Stage #1: ortho-cresol With potassium tert-butylate In tetrahydrofuran for 1h; Stage #2: ortho-nitrofluorobenzene In tetrahydrofuran |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 50℃; | 100% |
In tetrahydrofuran; (2S)-N-methyl-1-phenylpropan-2-amine hydrate | 59.1 g (94%) |
In tetrahydrofuran; (2S)-N-methyl-1-phenylpropan-2-amine hydrate | 59.1 g (94%) |
1-(tert-Butoxycarbonyl)-4-cyano-4-(methanesulfonyloxymethyl)piperidine
ortho-cresol
1-(tert-Butoxycarbonyl)-4-cyano-4-(2-methylphenoxymethyl)piperidine
Conditions | Yield |
---|---|
In water; ethyl acetate; N,N-dimethyl-formamide | 100% |
(4R)-1,2,3-oxathiazolidine-3-carboxylic acid, 4-phenyl 1,1-dimethylethyl ester-2,2-dioxide
ortho-cresol
Conditions | Yield |
---|---|
Stage #1: tert-butyl (R)-4-phenyl-1,2,3-oxathiazolidine-3-carboxylate 2,2-dioxide; ortho-cresol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 2h; Inert atmosphere; Stage #2: With trifluoroacetic acid In dichloromethane at 20℃; for 3h; optical yield given as %ee; enantioselective reaction; | 100% |
cycl-isopropylidene malonate
ortho-cresol
3-(2-methylphenoxy)-3-oxo-propanoic acid
Conditions | Yield |
---|---|
at 110℃; for 3h; | 100% |
at 100℃; for 3h; Neat (no solvent); | |
at 110℃; for 3h; Inert atmosphere; | |
at 90℃; |
ortho-cresol
[2H]-o-cresol
Conditions | Yield |
---|---|
With perchloric acid; d(4)-methanol at 75℃; for 144h; Inert atmosphere; | 100% |
With water-d2; sodium hydroxide at 180℃; for 0.25h; Reagent/catalyst; pH-value; Microwave irradiation; regioselective reaction; | 94% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 1.5h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: ortho-cresol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.0833333h; Stage #2: C16H11I In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 12h; | 100% |
Conditions | Yield |
---|---|
With Magnesium-Aluminum layered double oxides catalyst at 149.84℃; under 760.051 Torr; for 12h; Autoclave; Inert atmosphere; Irradiation; Green chemistry; | 99.4% |
With dimanganese decacarbonyl at 180℃; for 1h; Reagent/catalyst; | 30% |
N,N,N',N'-tetrabutyl-N''-methylguanidine at 180℃; for 4.5h; | 90 % Chromat. |
ortho-cresol
2-cyanobenzyl chloride
2-(2-methylphenoxymethyl)benzonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 110℃; for 6h; | 99.3% |
Conditions | Yield |
---|---|
With Mo2P5-MCM-48 at 120℃; for 3h; | 99.2% |
Conditions | Yield |
---|---|
With hydrogen In water at 20℃; under 7500.75 Torr; for 6h; Autoclave; | 99.1% |
With hydrogen at 100℃; under 3750.38 Torr; for 3h; Reagent/catalyst; Pressure; Temperature; | 99% |
With nickel(II) oxide; hydrogen; palladium In hexane at 80℃; under 7500.75 Torr; for 10h; | 98% |
formaldehyd
Octanethiol
ortho-cresol
methyl iodide
2,4-bis(n-octylthiomethyl)-6-methylphenol
Conditions | Yield |
---|---|
Stage #1: formaldehyd; Octanethiol; ortho-cresol With hydrogenchloride; 2,2'-iminobis[ethanol] In water for 8h; pH=Ca. 3 - 4; Reflux; Stage #2: methyl iodide With copper(l) iodide at 95℃; for 4h; Temperature; | 99.1% |
Conditions | Yield |
---|---|
With potassium carbonate; 1-Butylimidazole; copper(l) chloride In tetradecane; toluene at 120℃; for 16h; Product distribution / selectivity; | 99% |
With 2-Picolinic acid; potassium phosphate; copper(l) iodide In dimethyl sulfoxide at 90℃; for 24h; Inert atmosphere; | 95% |
With 2-Picolinic acid; potassium phosphate; copper(l) iodide In dimethyl sulfoxide at 90℃; for 24h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In acetonitrile at 20℃; for 1h; | 99% |
With trifluorormethanesulfonic acid In acetonitrile at 20℃; | 96% |
at 130℃; for 3h; | 95% |
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