Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:127-19-5
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Type:Lab/Research institutions
inquiryN,N-Dimethylacetamide Basic information Outline Chemical Properties Uses Medical Care Test methods Transport requirements Production method Product Name: N,N-Dimethylacetamide Synonyms: Acetic acid dimethylacetamide;N,N-Dimethylacetamide, 99%,
DMAC is best solvent and have kinds of usage Package:190kg/Drum Application:99.00% Transportation:FOB CIF OR OTHERS Port:Any port in China
Cas:127-19-5
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inquiry1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:127-19-5
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inquiryProduct name Dimethylacetamide CAS 127-19-5 MF C4H9NO MW 87.12 EINECS 204-826-4 Melting point -20 °C Boilding point 164.5-166 °C(lit.) Density
Cas:127-19-5
Min.Order:1 Metric Ton
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inquiryProduct description: Product name N,N-Dimethylacetamide (DMAC) CAS number 127-19-5 Assay ≥99% Appearance Colorless transparent liquid Capacity 2000mt/year Application Synthet
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inquirySleeping pills and stability.This product is white or white crystalline powder;Odourless and slightly bitter taste.Almost insoluble in water, soluble in hydrochloric acid.In acid or alkali and heat hydrolysis, oral drug under the action of gastric
Cas:127-19-5
Min.Order:10000 Gram
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inquiryDimethylacetamide English name:Dimethylacetamide Alias:N,N-dimethylacetamide B&J brand 4 L; Dimethylacetamide,(DMA); PROPYLENE CHLORIDE; Acetyldimeethylamine; CBC 510337; CH3CON(CH3)2; More alias :DMAC
Cas:127-19-5
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inquiry1. 99.95%Min 2. 190kg/drum 3. distributer QUALIFED ; EFFICIENCY; RESPONSIBLE Appearance:liquid Storage:in cool Package:225kg/drum Application:excipient Transportation:sea / air both ok Port:any port
Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:127-19-5
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inquiryZorui combines R&D, production and sales into its operations, While continuously providing high-quality raw materials, we also provide and optimize technical solutions for customers to achieve mutual benefit. We adhere to the "quality, integ
Cas:127-19-5
Min.Order:1 Kilogram
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inquiry
Cas:127-19-5
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Manufacturers
inquiryProduct Name: N,N-Dimethylacetamide Synonyms: PROPYLENE CHLORIDE;Acetyldimeethylamine;CBC 510337;CH3CON(CH3)2;dimethylacetamid;dimethylacetoneamide;Dimethylamid kyseliny octove;Dimethylamide acetate CAS: 127-19-5 MF: C4H9NO
Cas:127-19-5
Min.Order:1 Gram
FOB Price: $8900.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:127-19-5
Min.Order:1 Gram
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Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact u
Cas:127-19-5
Min.Order:1 Kilogram
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:127-19-5
Min.Order:10 Gram
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Type:Trading Company
inquiryProduct Name: Dimethylamide acetate Synonyms: PROPYLENE CHLORIDE;Acetyldimeethylamine;CBC 510337;CH3CON(CH3)2;dimethylacetamid;dimethylacetoneamide;Dimethylamid kyseliny octove;N,N-Dimethylacetamide CAS: 127-19-5 MF: C4H9NO MW: 87.12 EINECS:
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Cas:127-19-5
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inquiryProduct Name: N,N-Dimethylacetamide CAS: 127-19-5 MF: C4H9NO MW: 87.12 EINECS: 204-826-4 Mol File: 127-19-5.mol N,N-Dimethylacetamide Structure N,N-Dimethylacetamide Chemical Properties Melting point -20 °C (lit.) Boiling
Cas:127-19-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryN,N-Dimethylacetamide CAS:127-19-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inte
Cas:127-19-5
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:127-19-5
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inquiryProduct Detail Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,
Cas:127-19-5
Min.Order:20 Metric Ton
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Type:Trading Company
inquiryN,N-Dimethylacetamide CAS:127-19-5 Specification Product name N,N-Dimethylacetamide (DMAC) CAS number 127-19-5 Assay ≥99% Appearance Colorless transparent liquid Capacity 2000mt/year
Cas:127-19-5
Min.Order:1 Kilogram
Negotiable
Type:Other
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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Min.Order:10 Kilogram
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
N,N-Dimethylacetamide CAS 127-19-5 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to assembly.
Cas:127-19-5
Min.Order:1 Kilogram
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Type:Trading Company
inquiryFactory price N,N-Dimethylacetamide CAS 127-19-5 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a stric
Cas:127-19-5
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Type:Trading Company
inquiryConditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride In 1-methyl-pyrrolidin-2-one at 190℃; for 6h; Catalytic behavior; Solvent; Time; Reagent/catalyst; Concentration; | 99.1% |
With cobalt(II) chloride; sodium sulfite; zinc In 1-methyl-pyrrolidin-2-one at 200℃; under 22502.3 Torr; for 7h; Solvent; Reagent/catalyst; Temperature; Pressure; Autoclave; | 98.5% |
With palladium dichloride In 1-methyl-pyrrolidin-2-one at 190℃; for 8h; Catalytic behavior; Temperature; Pressure; |
Conditions | Yield |
---|---|
With self-zirconium modification of the nanoscale solid alkali catalyst In diethyl ether at 20℃; for 5h; Inert atmosphere; | 98.5% |
In diethyl ether | 20% |
With diethyl ether | |
In tetrahydrofuran; dichloromethane at 20℃; Cooling with ice; | |
With triethylamine In dichloromethane at 20℃; for 12h; |
Conditions | Yield |
---|---|
With tertamethylammonium iodide; palladium dichloride In 1-methyl-pyrrolidin-2-one at 20 - 240℃; under 7500.75 - 48754.9 Torr; for 1.96667h; Product distribution / selectivity; Autoclave; | 97% |
2-Dimethylamino-3-methyl-2,4,6-triphenyl-2H-pyran
A
N,N-dimethyl acetamide
B
3-Methyl-2,4,6-triphenylpyryliumchlorid
Conditions | Yield |
---|---|
With acetyl chloride In diethyl ether for 1h; Heating; | A 32% B 94% |
2-Dimethylamino-3-methyl-2,4,6-triphenyl-2H-pyran
acetyl chloride
A
N,N-dimethyl acetamide
B
3-Methyl-2,4,6-triphenylpyryliumchlorid
Conditions | Yield |
---|---|
In diethyl ether for 1h; Heating; | A 32% B 94% |
Conditions | Yield |
---|---|
With [Zn(BH4)2(py)] In tetrahydrofuran for 0.34h; Heating; | 93% |
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
With potassium hydroxide; air In diethyl ether at 20℃; for 90h; | 92% |
carbon monoxide
tertamethylammonium iodide
trimethylamine
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; palladium dichloride In 1-methyl-pyrrolidin-2-one at 20 - 200℃; under 22502.3 Torr; for 8h; Reagent/catalyst; Time; Autoclave; | 90.8% |
metamfepramone
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
With potassium hydroxide; air In diethyl ether at 20℃; for 30h; | 90% |
N,N-Dimethylcarbamidsaeure-trimethylsilylester
acetyl chloride
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
In dichloromethane for 0.25h; Ambient temperature; | 87% |
2-acetoxy-3,3-dimethyl-but-1-ene
(t-C4H9)2SbN(CH3)2
A
N,N-dimethyl acetamide
B
(t-C4H9)2SbCH2COC(CH3)3
Conditions | Yield |
---|---|
under Ar, at 80-90°C, 4 h; | A n/a B 85% |
(t-C4H9)2SbN(CH3)2
1-cyclohexenyl acetate
A
N,N-dimethyl acetamide
B
(t-C4H9)2SbOC6H9
Conditions | Yield |
---|---|
under Ar, at 80-90°C, 4 h; | A n/a B 79% |
3-acetoxy-2-pentene
(t-C4H9)2SbN(CH3)2
A
N,N-dimethyl acetamide
B
(t-C4H9)2SbOC(C2H5)CHCH3
C
(t-C4H9)2SbCH(CH3)COC2H5
Conditions | Yield |
---|---|
under Ar, at 80-90°C, 4 h; | A n/a B n/a C 78% |
under argon, at 80-90°C for 4 h, vac. distn.; |
N,N-Dimethylacetoacetamid
1,3-Dichloro-2-butene
A
N,N-dimethyl acetamide
C
N,N-dimethyl-α-(3-chloro-2-butenyl)acetoacetamide
Conditions | Yield |
---|---|
With potassium hydroxide; Katamin AB at 100℃; for 40h; | A 2.8% B 1.1% C 75% |
2-(dimethylamino)propan-1-ol
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
With potassium hydroxide; air In diethyl ether at 20℃; for 90h; | 73% |
Conditions | Yield |
---|---|
In methanol for 8h; Heating; | A 71% B 52% |
2-oxo-2-dimethylamino-4-methyl-1,3,2-dioxaphosphorinane
A
2-chloro-2-oxo-2-mercapto-4-methyl-1,3,2-dioxaphosphorinane
B
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
With acetyl chloride In benzene for 1h; Heating; | A n/a B 70% |
N,N,N,N,N,N-hexamethylphosphoric triamide
A
N,N-dimethyl acetamide
B
N,N,N',N'-Tetramethylphosphorodiamidic chloride
Conditions | Yield |
---|---|
With acetyl chloride In benzene for 1h; Heating; | A n/a B 67% |
4-chloropropiophenone enol acetate
(t-C4H9)2SbN(CH3)2
A
(t-C4H9)2SbCH(CH3)COC6H4-4-Cl
B
N,N-dimethyl acetamide
C
(t-C4H9)2SbOC(C6H4-4-Cl)CHCH3
Conditions | Yield |
---|---|
under Ar, at 80-90°C, 8 h; | A 66% B n/a C n/a |
Conditions | Yield |
---|---|
With sodium tetracarbonyl cobaltate In 1-methyl-pyrrolidin-2-one at 200℃; under 22502.3 Torr; for 14h; Autoclave; | 64.5% |
With palladium dichloride In 1-methyl-pyrrolidin-2-one at 190℃; for 12h; Catalytic behavior; |
(t-C4H9)2SbN(CH3)2
1-acetoxycyclopentene
A
C13H25OSb
B
N,N-dimethyl acetamide
C
(t-C4H9)2SbOC5H7
Conditions | Yield |
---|---|
under Ar, at 80-90°C, 4 h; | A 64% B n/a C n/a |
Conditions | Yield |
---|---|
With triphenyltin(IV) hydroxide In benzene-d6 at 90℃; for 36h; | 64% |
With 6H(1+)*Mo9O40PV3(6-); oxygen In acetonitrile at 60℃; under 760.051 Torr; for 2h; Inert atmosphere; Glovebox; | 53 %Chromat. |
maleiimide
2-dimethylamino-5-ethyl-4-methyloxazole
A
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
In acetic acid for 3h; Cyclization; ring cleavage; Heating; | A n/a B 63% |
1,1,1-triethyl-N,N-dimethylsilylamine
trimethylsilyl acetate
A
Hexamethyldisiloxane
B
N,N-dimethyl acetamide
C
1,1,1-triethyl-3,3,3-trimethyl-disiloxane
D
hexaethyl disiloxane
Conditions | Yield |
---|---|
With N-Methylformamide at 50 - 75℃; for 21h; | A n/a B 60% C n/a D n/a |
With N-Methylformamide at 50 - 75℃; for 21h; Product distribution; Mechanism; other amides as catalysts; | A n/a B 60% C n/a D n/a |
1,1,1-triethyl-N,N-dimethylsilylamine
A
Hexamethyldisiloxane
B
N,N-dimethyl acetamide
C
1,1,1-triethyl-3,3,3-trimethyl-disiloxane
D
hexaethyl disiloxane
Conditions | Yield |
---|---|
With N-Methylformamide; trimethylsilyl acetate at 50 - 75℃; for 21h; | A n/a B 60% C n/a D n/a |
trimethylsilyl acetate
A
Hexamethyldisiloxane
B
N,N-dimethyl acetamide
C
1,1,1-triethyl-3,3,3-trimethyl-disiloxane
D
hexaethyl disiloxane
Conditions | Yield |
---|---|
With N-Methylformamide; 1,1,1-triethyl-N,N-dimethylsilylamine at 50 - 75℃; for 21h; | A n/a B 60% C n/a D n/a |
2-methyl-1-phenyl-1-acetoxy-1-propene
(t-C4H9)2SbN(CH3)2
A
N,N-dimethyl acetamide
B
(t-C4H9)2SbOC(C6H5)C(CH3)2
Conditions | Yield |
---|---|
under Ar, at 80-90°C, 8 h; | A n/a B 58% |
Conditions | Yield |
---|---|
In dichloromethane for 5h; | 57% |
1-phenylprop-1-enyl acetate
(t-C4H9)2SbN(CH3)2
A
(t-C4H9)2SbCH(CH3)COC6H5
B
N,N-dimethyl acetamide
C
(t-C4H9)2SbOC(C6H5)CHCH3
Conditions | Yield |
---|---|
under Ar, at 80-90°C, 8 h; | A 57% B n/a C n/a |
under argon, at 80-90°C, 8 h; |
trans-geranyl bromide
N,N-dimethyl acetamide
Geranylessigsaeure-N,N-dimethylamid
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide In tetrahydrofuran at -78℃; | 100% |
N,N-dimethyl acetamide
4-bromobenzenecarbonitrile
2-(4-cyanophenyl)-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With potassium In ammonia | 100% |
Stage #1: N,N-dimethyl acetamide With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78℃; for 1h; Stage #2: With zinc(II) chloride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Stage #3: 4-bromobenzenecarbonitrile With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; cyclohexane at 20℃; for 4h; | 89% |
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
With perchloric acid; trichlorophosphate at 60 - 70℃; | 100% |
N,N-dimethyl acetamide
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
at 20℃; for 0.0833333h; | 100% |
N,N-dimethyl acetamide
D-3,6-di-O-trifluoromethanesulfonyl-1,2:4,5-di-O-isopropylidene-myo-inositol
(D)-2,5-di-O-acetyl-1,6:3,4-di-O-isopropylidene-allo-inositol
Conditions | Yield |
---|---|
With potassium acetate at 70℃; | 100% |
2,5-dibromopyridine
N,N-dimethyl acetamide
1-(5-bromopyridin-2-yl)ethanone
Conditions | Yield |
---|---|
With n-butyllithium In hexane; toluene at -40 - 20℃; for 2h; Inert atmosphere; | 100% |
Stage #1: 2,5-dibromopyridine With n-butyllithium In hexane; toluene at -40℃; for 0.666667h; Stage #2: N,N-dimethyl acetamide In hexane; toluene at 20℃; for 1h; Further stages.; | 83% |
Stage #1: 2,5-dibromopyridine With n-butyllithium In toluene Inert atmosphere; Stage #2: N,N-dimethyl acetamide In toluene Inert atmosphere; | 83% |
N,N-dimethyl acetamide
C13H10N2O4S
N,N-dimethyl-3-phenyl-3-(2-nitrobenezenesulfonylamino)propanamide
Conditions | Yield |
---|---|
With triisopropylsilyl trifluoromethanesulfonate; triethylamine In toluene at 20℃; for 12h; Mannich type reaction; | 100% |
N,N-dimethyl acetamide
N-(benzylidene)-p-methylbenzenesulfonamide
N,N-dimethyl-3-((4-methylphenyl)sulfonamido)-3-phenylpropanamide
Conditions | Yield |
---|---|
With triisopropylsilyl trifluoromethanesulfonate; triethylamine In toluene at 20℃; for 12h; Mannich type reaction; | 100% |
N,N-dimethyl acetamide
4-methyl-N-(3-nitrobenzylidene)benzenesulfonamide
N,N-dimethyl-3-(3-nitrophenyl)-3-(tosylamino)propanamide
Conditions | Yield |
---|---|
With triisopropylsilyl trifluoromethanesulfonate; triethylamine In toluene at 20℃; for 12h; Mannich type reaction; | 100% |
N,N-dimethyl acetamide
N-(p-chlorobenzylidene)-p-toluenesulfonamide
3-(4-chlorophenyl)-N,N-dimethyl-3-(tosylamino)propanamide
Conditions | Yield |
---|---|
With triisopropylsilyl trifluoromethanesulfonate; triethylamine In toluene at 20℃; for 12h; Mannich type reaction; | 100% |
N,N-dimethyl acetamide
N-(2-naphthylidene)-4-methylbenzenesulfonamide
N,N-dimethyl-3-(naphthalen-2-yl)-3-(tosylamino)propanamide
Conditions | Yield |
---|---|
With triisopropylsilyl trifluoromethanesulfonate; triethylamine In toluene at 20℃; for 12h; Mannich type reaction; | 100% |
N,N-dimethyl acetamide
N-(2,2-dimethylpropylidene)-p-toluenesulfonamide
N,N,4,4-tetramethyl-3-(tosylamino)pentanamide
Conditions | Yield |
---|---|
With triisopropylsilyl trifluoromethanesulfonate; triethylamine In toluene at 20℃; for 12h; Mannich type reaction; | 100% |
N,N-dimethyl acetamide
3-cyclopropyl-N,N-dimethyl-3-(tosylamino)propanamide
Conditions | Yield |
---|---|
With triisopropylsilyl trifluoromethanesulfonate; triethylamine In toluene at 20℃; for 12h; Mannich type reaction; | 100% |
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl acetamide With trichlorophosphate at 0 - 5℃; for 1h; Stage #2: C26H44N2O3 In ISOPROPYLAMIDE; water at 10℃; for 2h; Stage #3: With sodium hydroxide In ISOPROPYLAMIDE; water at 20℃; for 2h; pH=9 - 10; | 100% |
3-bromo-4-methyl-5-nitro-6-methoxypyridine
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 80 - 95℃; for 5h; | 100% |
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
In ethanol for 0.0833333h; | 100% |
Conditions | Yield |
---|---|
In diethyl ether | 100% |
Conditions | Yield |
---|---|
In diethyl ether | 100% |
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
at 50℃; for 1h; | 100% |
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
With acetic acid In N,N-dimethyl-formamide; toluene at 105℃; for 3h; | 100% |
N,N-dimethyl acetamide
ethyl acetoacetate
ethyl 2-[(dimethylamino)methylene]-3-oxobutanoate
Conditions | Yield |
---|---|
In ethanol; N,N-dimethyl-formamide at 60℃; for 2h; | 100% |
N,N-dimethyl acetamide
Conditions | Yield |
---|---|
With butoxytributylazanium sulfate In chloroform at 60℃; for 2h; | 99.5% |
Cyclopropyl methyl ketone
N,N-dimethyl acetamide
2-cyclopropyl-2-oxoethyl acetate
Conditions | Yield |
---|---|
Stage #1: Cyclopropyl methyl ketone; N,N-dimethyl acetamide With trifluorormethanesulfonic acid; thallium(III) acetate at 60℃; for 0.333333h; Stage #2: With water for 0.166667h; Further stages.; | 99% |
N,N-dimethyl acetamide
4-benzyloxypropiophenone
Acetic acid 2-(4-benzyloxy-phenyl)-1-methyl-2-oxo-ethyl ester
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl acetamide; 4-benzyloxypropiophenone With trifluorormethanesulfonic acid; thallium(III) acetate at 60℃; for 0.333333h; Stage #2: With water for 0.166667h; Further stages.; | 99% |
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl acetamide; cyclohexanone With trifluorormethanesulfonic acid; thallium(III) acetate at 60℃; for 0.333333h; Stage #2: With water for 0.166667h; Further stages.; | 99% |
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl acetamide; inden-1-one With trifluorormethanesulfonic acid; thallium(III) acetate at 60℃; for 0.333333h; Stage #2: With water for 0.166667h; Further stages.; | 99% |
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl acetamide; cyclopentanone With trifluorormethanesulfonic acid; thallium(III) acetate at 60℃; for 0.333333h; Stage #2: With water for 0.166667h; Further stages.; | 99% |
N,N-dimethyl acetamide
[chloro-(p-tolylsulfinyl)methylidene]cyclopentadecane
2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}-N,N-dimethylacetamide
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl acetamide With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.166667h; Stage #2: [chloro-(p-tolylsulfinyl)methylidene]cyclopentadecane In tetrahydrofuran at -78 - -50℃; for 0.666667h; Further stages.; | 99% |
Stage #1: N,N-dimethyl acetamide With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.166667h; Stage #2: [chloro-(p-tolylsulfinyl)methylidene]cyclopentadecane In tetrahydrofuran at -78℃; for 3h; |
N,N-dimethyl acetamide
D-3-O-trifluoromethanesulfonyl-1,2:4,5-di-O-isopropylidene-myo-inositol
1L-1-O-acetyl-2,3:5,6-di-O-isopropylidene-chiro-inositol
Conditions | Yield |
---|---|
With potassium acetate at 70℃; | 99% |
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