Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:120-92-3
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
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Cas:120-92-3
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
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Cyclopentanone Basic information Product Name: Cyclopentanone Synonyms: Adipinketon;Dumasin;Pyran-2,4(3H)-dione, 3-acetyl-6-methyl-;ADIPIC KETONE;AKOS BBS-00004293;KETOCYCLOPENTANE;K
Cas:120-92-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct name Cyclopentanone Synonyms CYCLOPENTANONE REAGENTPLUS(TM) >=99%;CYCLOPENTANONE, REAGENTPLUS, >=99%;CYCLOPENTANONE, STANDARD FOR GC;Cyclopentanone,Certified;Cyclopentanone, pure, 99+%;
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Cas:120-92-3
Min.Order:100 Metric Ton
Negotiable
Type:Lab/Research institutions
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Cas:120-92-3
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
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Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:120-92-3
Min.Order:10 Gram
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Type:Lab/Research institutions
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Cas:120-92-3
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryProduct name: Cyclopentanone CAS No.:120-92-3 Molecule Formula:C5H8O Molecule Weight:84.12 Purity: 99.0% Package: 220kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard TESTIN
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Min.Order:1 Kilogram
Negotiable
Type:Trading Company
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SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of service
Cas:120-92-3
Min.Order:0 Metric Ton
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Hangzhou Dingyan Chem is a leading manufacturer and supplier of chemicals in China.We develop,produce and distribute high quality pharmaceuticals, intermediates, special chemicals and other fine chemicals. We could give you: 1.Best quality in your re
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Cas:120-92-3
Min.Order:1 Kilogram
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1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl
Conditions | Yield |
---|---|
With water; nickel dibromide; dibenzoyl peroxide In N,N-dimethyl acetamide at 60℃; for 3h; | 100% |
With Cp*Ir(6,6'-dionato-2,2'-bipyridine)(H2O) In hexane for 20h; Solvent; Reflux; | 100% |
With allyl methyl carbonate; dihydridotetrakis(triphenylphosphine)ruthenium In toluene at 100℃; for 13h; | 99% |
Conditions | Yield |
---|---|
With oxygen; palladium(II) sulfate; PdSO4-H3PMo6W6O40 In cyclohexane; water at 30℃; for 6h; | 100% |
With oxygen; H3PMo6W6O40 In cyclohexane; water at 29.9℃; under 760 Torr; for 6h; | 100% |
With palladium(II) sulfate; oxygen; H3PMo6W6O40 In cyclohexane; water at 29.9℃; under 760 Torr; for 6h; Product distribution; Rate constant; other time, other Pd(II) salt, other concentration of catalyst; | 100% |
Conditions | Yield |
---|---|
With limonene.; palladium on activated charcoal for 0.5h; Heating; | 100% |
With hydrogen; SC-1 Ni2B In methanol at 25℃; under 760 Torr; for 24h; | 100% |
With diphenylsilane; zinc(II) chloride; tetrakis(triphenylphosphine) palladium(0) In chloroform for 0.5h; Ambient temperature; | 99% |
Conditions | Yield |
---|---|
With bis(1-CH2Ph-3,5,7-3N-1-N(1+)tricyclo[3.3.1.13,7]decaneS2O8 In acetonitrile for 0.0583333h; Oxidation; Heating; | 100% |
With potassium permanganate In water; acetonitrile at 25℃; for 1h; | 96% |
With dihydrogen peroxide; tripropylammonium fluorochromate (VI) In acetone at 0 - 10℃; for 2.5h; | 96% |
cyclopentanone
Conditions | Yield |
---|---|
With hydrogenchloride for 0.0416667h; Product distribution; Ambient temperature; pH = 4-6, regeneration of aldehyde; | 100% |
Conditions | Yield |
---|---|
With oxygen; kieselguhr; copper(l) chloride In hexane for 2.5h; Oxidation; Heating; | 99% |
1,1-Bis(phenylthio)cyclopentane
cyclopentanone
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 20 - 25℃; for 2h; Irradiation; | 98% |
Conditions | Yield |
---|---|
With hydrogen In water at 160℃; under 30003 Torr; for 7h; Automated synthesizer; | 98% |
With hydrogen In water at 160℃; under 30003 Torr; for 2.5h; Reagent/catalyst; Temperature; Pressure; Autoclave; | 96% |
With hydrogen In water at 150℃; under 30003 Torr; for 6h; Reagent/catalyst; Autoclave; | 95% |
Conditions | Yield |
---|---|
With hydrogenchloride; FeH6Mo6O24(3-)*3H3N*3H(1+)*7H2O; tetrabutylammomium bromide; dihydrogen peroxide In 1,4-dioxane; water at 85℃; for 24h; | 96% |
With [Fe4III(μ-O)2(μ-acetate)6(2,2'-bipyridine)2(H2O)2](NO3-)(OH-); dihydrogen peroxide; acetic acid In water; acetonitrile at 32℃; for 3h; Catalytic behavior; | 60% |
With dihydrogen peroxide; vanadium phosphorus oxide In acetonitrile at 50℃; for 20h; | 48% |
Conditions | Yield |
---|---|
With sodium perborate at 70℃; for 3h; Ionic liquid; | 95% |
With bis-trimethylsilanyl peroxide; sodium hydride In tetrahydrofuran at 20℃; for 24h; Hydrolysis; | 65% |
1-Methanesulfonyl-1-methylsulfanyl-cyclopentane
cyclopentanone
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 3h; Heating; | 94% |
Conditions | Yield |
---|---|
With Glyoxilic acid; Amberlyst 15 for 0.05h; microwave irradiation; | 94% |
With potassium superoxide; tetraethylammonium bromide In N,N-dimethyl-formamide at 20℃; for 3h; | 88% |
Adipic acid
6-Hydroxyhexanoic acid
A
hexahydro-2H-oxepin-2-one
B
cyclopentanone
Conditions | Yield |
---|---|
at 280 - 300℃; Product distribution / selectivity; | A 7% B 94% |
sodium phosphate at 290℃; Product distribution / selectivity; | A 0.3% B 77% |
tin(IV) oxide at 270℃; Product distribution / selectivity; | A 1% B 73% |
sodium hydroxide at 270 - 290℃; Product distribution / selectivity; | A 25% B 58% |
sodium borate at 290℃; Product distribution / selectivity; | A 0.3% B 39% |
Conditions | Yield |
---|---|
Al2O3#dotK2O In water at 360℃; under 0.750075 Torr; for 500h; | 93% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; methyltrioxorhenium(VII); sodium bromide for 10h; Ambient temperature; | A 8% B 92% |
Conditions | Yield |
---|---|
With tetrabutylammonium tricarbonylnitrosylferrate In hexane at 20 - 80℃; Molecular sieve; Inert atmosphere; | A 92% B n/a |
Conditions | Yield |
---|---|
With hydrogenchloride; dihydrogen peroxide In acetonitrile at 50℃; for 3h; the excess of H2O2 was removed by catalytic hydrogenation using 10percent Pd-C; | A n/a B 91.6% |
Conditions | Yield |
---|---|
With oxygen; palladium matal-containing silica-supported catalyst In various solvent(s) at 59.9℃; for 24h; Product distribution; Mechanism; Pd(0) supported on various zeolites , influence of calcination and reaction temperature and of the solvent; | A 90.1% B n/a |
With oxygen; silica gel; palladium In various solvent(s) at 59.9℃; for 24h; Product distribution; solvent; | A 90.1% B 0.8% |
With oxygen; silica gel; palladium In various solvent(s) at 59.9℃; for 24h; Yields of byproduct given; | A 90.1% B n/a |
With oxygen; silica gel; palladium In various solvent(s) at 59.9℃; for 24h; | A 90.1% B 0.8% |
Conditions | Yield |
---|---|
With formaldehyd; silica gel; iron(III) chloride at 20℃; for 0.0833333h; | 90% |
With chloral hydrate In hexane at 25℃; for 0.5h; Solvent; Temperature; Inert atmosphere; | 83% |
With boron trifluoride diethyl etherate; sodium iodide In acetonitrile for 2h; Heating; | 82% |
With water; β‐cyclodextrin at 20℃; for 16h; | 98 % Chromat. |
2-cyclopentylidene-1,1-dimethylhydrazine
cyclopentanone
Conditions | Yield |
---|---|
With cerium(III) chloride; silica gel for 0.0666667h; Microwave irradiation; | 90% |
With sodium perborate; sodium hydroxide; potassium dihydrogenphosphate; water In tert-butyl alcohol at 60℃; for 24h; | 70% |
With ferric nitrate In dichloromethane 30 min., r.t., then reflux; | 69% |
With silica gel In tetrahydrofuran; water at 25℃; for 10h; | 20% |
Conditions | Yield |
---|---|
With silica gel; iron(III) chloride at 20℃; for 0.333333h; | 90% |
With sulfuric acid In water at 25℃; Rate constant; |
Conditions | Yield |
---|---|
With zirconium hydrogen sulfate; silica gel In hexane for 1.5h; Heating; | 90% |
B
cyclopentanone
Conditions | Yield |
---|---|
With CO In toluene toluene soln. of Mo complex placed in autoclave under 50 atm CO pressure, stirred at 90°C for 12 h; distn., trapping at -78°C; | A 83% B 90% |
cyclopentanone
Conditions | Yield |
---|---|
decompn. at 150°C for 0.5 h; | 88% |
decompn. at 150°C for 0.5 h; | 88% |
Conditions | Yield |
---|---|
With oxygen; silica gel; palladium In various solvent(s) at 59.9℃; for 24h; | A 87.4% B 0.8% |
1-pyrrolidinocyclopent-1-ene
2-((trifluoromethyl)thio)isoindoline-1,3-dione
A
cyclopentanone
Conditions | Yield |
---|---|
In acetonitrile at 25℃; for 48h; Hydrolysis; trifluoromethylthiolation; | A 12.9% B 87.1% |
Conditions | Yield |
---|---|
With water; oxygen; lithium bromide; copper(ll) bromide In tetrahydrofuran at 25℃; under 760.051 Torr; | A 87% B n/a |
Conditions | Yield |
---|---|
With iodo trichloro silane for 1h; Ambient temperature; | A 86% B 39% |
Conditions | Yield |
---|---|
With pyrographite at 450℃; for 0.5h; | 85% |
With calcium hydroxide at 350℃; Product distribution; Further Variations:; Reagents; | 84.2% |
at 290℃; |
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene In dichloromethane at 0 - 20℃; for 0.333333h; Inert atmosphere; Green chemistry; | 85% |
With oxygen; potassium iodide; sodium nitrite In water; acetonitrile for 8h; Reflux; | 75% |
With potassium hydroxide In ethyl acetate at -78℃; Product distribution; | 18% |
2-aminoacetophenone
cyclopentanone
9-methyl-2,3-dihydro-1H-cyclopenta[b]quinoline
Conditions | Yield |
---|---|
With 3-methyl-1-sulfoimidazolium trichloroacetate; trichloroacetic acid In neat (no solvent) at 100℃; Friedlaender Quinoline Synthesis; | 100% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate; N,N-dimethyl-formamide at 90℃; Friedlaender reaction; | 98% |
With ammonium cerium (IV) nitrate In ethanol for 16h; Friedlaender synthesis; Reflux; | 97% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 20℃; Aldol Condensation; | 100% |
With molybdenum(V) chloride In neat (no solvent) for 0.0416667h; Claisen-Schmidt Condensation; Microwave irradiation; Green chemistry; | 99% |
With potassium hydroxide In ethanol at 40℃; for 0.00138889h; | 98% |
4-methoxy-benzaldehyde
cyclopentanone
(2E,5E)-2,5-bis(4-methoxybenzylidene)cyclopentanone
Conditions | Yield |
---|---|
With lithium perchlorate; triethylamine at 20℃; for 0.0166667h; | 100% |
With trichloro(trifluoromethanesulfonato)titanium(IV) at 20℃; for 2h; aldol condensation; | 97% |
With animal bone meal catalyst modified with Na In water for 0.25h; Reflux; | 97% |
cyclopentanone
ethyl 2-cyanoacetate
ethyl 2-cyano-2-cyclopentylideneacetate
Conditions | Yield |
---|---|
piperidine at 23℃; under 750.06 Torr; for 2h; Knoevenagel condensation; | 100% |
With morpholine; bis(acetylacetonate)oxovanadium at 40℃; for 1h; Reagent/catalyst; Temperature; Time; Knoevenagel Condensation; | 99% |
With ammonium acetate; acetic acid In toluene Knoevenagel Condensation; Reflux; | 93% |
Conditions | Yield |
---|---|
With iodine; mercury dichloride In dichloromethane for 1h; Ambient temperature; | 100% |
With N-chloro-succinimide In various solvent(s) at 20℃; for 0.5h; | 91% |
With N-chloro-succinimide In dimethyl sulfoxide at 20℃; for 0.25h; | 87% |
Conditions | Yield |
---|---|
With N,O-bis(trimethylsilyl)hydroxylamine; potassium hydride In tetrahydrofuran for 1.5h; Ambient temperature; - 78 deg C to room temp.; | 100% |
With sodium hydroxide; hydroxylamine hydrochloride at 20℃; for 0.5h; grinding; | 100% |
With hydroxylamine hydrochloride; sodium acetate In methanol Heating; | 100% |
Conditions | Yield |
---|---|
With zirconium dioxide hydrate; isopropyl alcohol at 130℃; for 0.666667h; Meerwein-Ponndorf-Verley Reduction; | 100% |
Stage #1: cyclopentanone With tetrabutylammonium tricarbonylnitrosylferrate; tricyclohexylphosphine In 1,4-dioxane at 50℃; Inert atmosphere; Stage #2: With water; sodium hydroxide In 1,4-dioxane; methanol at 20℃; for 1.5h; Inert atmosphere; chemoselective reaction; | 99% |
With C15H18BF3; hydrogen; tert-butylimino-tri(pyrrolidino)phosphorane In tetrahydrofuran at 75℃; under 75007.5 Torr; for 20h; Glovebox; | 99% |
chloro-trimethyl-silane
cyclopentanone
1-(trimethylsilyloxy)cyclopentene
Conditions | Yield |
---|---|
With triethylamine; sodium iodide In acetonitrile at 23℃; for 1.5h; Inert atmosphere; | 100% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 40℃; for 0.5h; | 98% |
With magnesium In N,N-dimethyl-formamide at 15 - 25℃; | 94% |
4-penten-1-ylmagnesium bromide
cyclopentanone
1-(pent-4'-enyl)cyclopentan-1-ol
Conditions | Yield |
---|---|
100% | |
at 0℃; | 90% |
In diethyl ether for 2h; Ambient temperature; | 72% |
nitromethane
cyclopentanone
phenylmethanethiol
1-benzylthio-1-nitromethylcyclopentane
Conditions | Yield |
---|---|
With piperidine In benzene | 100% |
With piperidine In acetonitrile for 4h; Heating; | 94% |
With piperidine In benzene Heating; |
benzoic acid hydrazide
cyclopentanone
N'-cyclopentylidene benzohydrazide
Conditions | Yield |
---|---|
at 143℃; under 2100.21 Torr; for 0.05h; Microwave irradiation; neat (no solvent); | 100% |
for 0.05h; Microwave irradiation; | 100% |
at 20℃; for 0.05h; Microwave irradiation; | 100% |
3,4-dimethoxy-benzaldehyde
cyclopentanone
2,5-Bis<(3,4-dimethoxyphenyl)methylen>cyclopentanon
Conditions | Yield |
---|---|
With lithium perchlorate; triethylamine at 20℃; for 96h; | 100% |
With hydrogenchloride; acetic acid at 25 - 30℃; for 2h; | 85% |
With hydrogenchloride In acetic acid at 25 - 30℃; for 2h; | 85% |
Conditions | Yield |
---|---|
With ammonium acetate; zinc In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; | 100% |
With zinc; bis(cyclopentadienyl)titanium dichloride In tetrahydrofuran for 0.0833333h; Ambient temperature; | 98% |
With ammonium chloride; zinc In tetrahydrofuran; water at 20℃; for 10h; | 90% |
Conditions | Yield |
---|---|
With trimethyl orthoformate at 40℃; under 6000480 Torr; for 8h; | 100% |
Irradiation; | 25% |
Ce(3+)-mont at 25℃; for 0.5h; Yield given; |
t-butoxycarbonylhydrazine
cyclopentanone
tert-butyl 2-cyclopentylidenehydrazine carboxylate
Conditions | Yield |
---|---|
In methanol at 20℃; for 2h; | 100% |
In methanol at 20℃; for 3h; Inert atmosphere; | 98% |
In hexane for 0.333333h; Heating; | 96% |
Conditions | Yield |
---|---|
With iodine; magnesium In diethyl ether for 3h; Grignard reaction; Heating; | 100% |
With iodine; magnesium 1.) ether, reflux, 2.) ether, benzene, RT, 2 h; Yield given. Multistep reaction; | |
Stage #1: 1-Bromonaphthalene With magnesium In diethyl ether Stage #2: cyclopentanone In diethyl ether for 3h; Grignard reaction; | |
Stage #1: 1-Bromonaphthalene With magnesium In diethyl ether for 0.5h; Reflux; Stage #2: cyclopentanone In diethyl ether at 0℃; for 1h; |
2,4,6-trimethylbenzenesulfonohydrazide
cyclopentanone
N'-cyclopentylidene-2,4,6-trimethylbenzenesulfonohydrazide
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
In methanol 1.) 50 deg, 2.) room temperature; | 88% |
t-butyldimethylsiyl triflate
cyclopentanone
1-tert-butyldimethylsilyloxycyclopentene
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 0.0833333h; | 100% |
With 2,6-dimethylpyridine In tetrahydrofuran at 0℃; for 1h; | 71% |
With triethylamine In dichloromethane at 0℃; |
ethyl hydrogen (5,6-dihydro-p-dioxin-2-yl)ethylphosphonite
cyclopentanone
Conditions | Yield |
---|---|
for 600h; Ambient temperature; | 100% |
cyclopentanone
1,2-diamino-benzene
2,3-cyclopentano-3,4-dihydro-5H-4-spirocyclopentano-1,5-benzodiazepine
Conditions | Yield |
---|---|
With mesoporous aluminosilicate MCM-41(14) at 100℃; for 1h; | 100% |
With ytterbium(III) triflate at 20℃; for 4h; | 99% |
With octadecafluorodecahydronaphthalene (cis+trans) at 60℃; for 2h; | 99% |
cyclopentanone
toluene-4-sulfonic acid hydrazide
cyclopentanone p-tolylsulfonylhydrazone
Conditions | Yield |
---|---|
In ethanol at 100℃; for 1h; | 100% |
In ethanol at 100℃; for 1.66667h; Inert atmosphere; | 100% |
In methanol at 20℃; Inert atmosphere; | 99.5% |
cyclopentanone
2-amino-1-benzylamine
3',4'-dihydro-1'H-spiro[cyclopentane-1,2'-quinazoline]
Conditions | Yield |
---|---|
In chloroform at 60℃; for 24h; | 100% |
With acetic acid In ethanol for 3h; Heating; | 82% |
cyclopentanone
4-flourophenylmagnesium bromide
1-cyclopent-1-enyl 4-fluorobenzene
Conditions | Yield |
---|---|
Stage #1: cyclopentanone; 4-flourophenylmagnesium bromide In tetrahydrofuran at 0℃; Reflux; Stage #2: With hydrogenchloride In tetrahydrofuran; water | 100% |
In tetrahydrofuran; diethyl ether at 0℃; for 2h; Reflux; | 100% |
Stage #1: cyclopentanone; 4-flourophenylmagnesium bromide In tetrahydrofuran at 0℃; for 2h; Reflux; Stage #2: With hydrogenchloride; water In tetrahydrofuran Cooling with ice; | 100% |
In diethyl ether Grignard reaction; Reflux; | 61% |
(i), (ii) KHSO4; Multistep reaction; |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 0.0166667h; microwave irradiation; | 100% |
With aluminum oxide; potassium fluoride In methanol at 35 - 40℃; for 0.5h; Claisen-Schmidt condensation; ultrasound irradiation; | 96% |
With sodium-modified hydroxyapatite In water for 0.5h; Aldol condensation; Reflux; | 96% |
nitromethane
thiophenol
cyclopentanone
1-nitromethyl-1-phenylthiocyclopentane
Conditions | Yield |
---|---|
With piperidine In benzene for 61h; Heating; | 100% |
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