Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryTrimethylamine aqueous solution 30% Trimethylamine:colorless gas at room temperature,Anabaena odor, soluble in water, ethanol, ether, flammable, toxic, Relative density(water=1)0.66(-5℃),(Air=1)2.09.Molecular formula: C3H9N,Can be use
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TRIMETHYLAMINE HYDROCHLORIDE Basic information Product Name: TRIMETHYLAMINE HYDROCHLORIDE Synonyms: ai3-15639;dimethylmethaneamine;femanumber:3241;Methanamine, N,N-dimethyl-;Methanamine,
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Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquirySuperior quality, moderate price & quick delivery. Appearance:colourless gas Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:200L metal pail or as per your request Application:Used as a disinfectant, gas alarm
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inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
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75-50-3 TRIMETHYLAMINE HYDROCHLORIDE Application:75-50-3 TRIMETHYLAMINE HYDROCHLORIDE
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inquiry1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
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Min.Order:1 Kilogram
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inquiryN,N-dimethyl-formamide
trimethylamine
Conditions | Yield |
---|---|
With Dimethylphenylsilane; C40H56FeN2Si4(2-) In benzene-d6 at 120℃; for 10h; Reagent/catalyst; Sealed tube; Inert atmosphere; | 99% |
With bis(tetrahydrofuran)calcium di(bis(trimethylsilyl)amide); 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In benzene-d6 at 25℃; for 4h; Inert atmosphere; Schlenk technique; Glovebox; | 99% |
With sodium tetrahydroborate; Bis-(2-bromoethyl)selenium dibromide In tetrahydrofuran at 65℃; for 4h; Product distribution; Mechanism; other temperature (25 deg C), other reaction time, also presence od diethyl selenium dibromide; various other tertiary amides investigated; | 82% |
Conditions | Yield |
---|---|
With C40H56N2RuSi4 at 120℃; for 5h; Reagent/catalyst; Sealed tube; | 99% |
With bis(1,5-cyclooctadiene)dichloro[1,3-bis(1′-butylbenzimidazol-2′-yliden-3′-yl)benzene]dirhodium(I) In benzene-d6 at 100℃; for 2h; Catalytic behavior; Time; Reagent/catalyst; | 89% |
Conditions | Yield |
---|---|
With aluminium(III) triflate; [Ru(Triphos)(TMM)]; hydrogen; ammonium chloride In 1,4-dioxane; water at 150℃; under 67506.8 Torr; for 24h; Solvent; Temperature; Pressure; Autoclave; Schlenk technique; | 99% |
With octane; hydrogen; ammonium bicarbonate In neat (no solvent) at 250℃; for 24h; Catalytic behavior; Reagent/catalyst; Solvent; Autoclave; | 65% |
With aluminium(III) triflate; [Ru(1,1,1-tris(diphenylphosphinomethyl)ethane)(trimethylenemethane)]; ammonia; hydrogen; bis(trifluoromethanesulfonyl)amide In 1,4-dioxane at 150℃; under 60006 Torr; for 24h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Time; Inert atmosphere; Autoclave; | 77 %Spectr. |
C17H18ClN3O
A
5-(4-chlorophenyl)-3-phenyl-1,2,4-oxadiazole
B
trimethylamine
Conditions | Yield |
---|---|
at 215℃; for 0.25h; | A 98% B n/a |
triethylsilane
bis-(dimethylamino)methane
A
1,1,1-triethyl-N,N-dimethylsilylamine
B
trimethylamine
Conditions | Yield |
---|---|
With nickel at 140 - 150℃; | A 97% B n/a |
Conditions | Yield |
---|---|
at 210℃; for 0.0833333h; | A 97% B n/a |
Conditions | Yield |
---|---|
at 210℃; for 0.166667h; | A 97% B n/a |
[(E)-4-(Diethoxy-phosphorylsulfanyl)-but-2-enyl]-trimethyl-ammonium; chloride
A
ethyl phosphate
B
ethyl 1,3-butadienyl sulfide
C
trimethylamine
Conditions | Yield |
---|---|
With potassium hydroxide at 110℃; Product distribution; Mechanism; | A 85.4% B 33.3% C 96.3% |
trimethyl-borane; compound with trimethylamine
A
trimethylborane
B
trimethylamine
Conditions | Yield |
---|---|
at 111.3°C, 64.5 Torr equilibrium; | A 96% B 96% |
at 111.3°C, 64.5 Torr equilibrium; | A 96% B 96% |
at 65.8°C, 47.5 Torr equilibrium; | A 63.8% B 63.8% |
1,2-diamino-benzene
A
2-propyl-2,3-dihydro-1H-benzo[1,3,2]diazaborole
B
trimethylamine
Conditions | Yield |
---|---|
In benzene byproducts: H2; by heating at reflux then cooling, adding pentane to the mixture; recrystn. from benzene-pentane; | A 95% B n/a |
1,2-diamino-benzene
A
2-isobutyl-2,3-dihydro-1H-benzo[1,3,2]diazaborole
B
trimethylamine
Conditions | Yield |
---|---|
In benzene byproducts: H2; reflux, then cooling and adding pentane to the mixture; recrystn. from benzene-pentane; | A 95% B n/a |
bis-[(diethoxy-methyl-silanyl)-methyl]-methyl-amine
phenol
A
methyltriphenoxysilane
B
trimethylamine
Conditions | Yield |
---|---|
for 1.5h; Heating; | A 92% B n/a |
1,2-diamino-benzene
A
2-sec-butyl-2,3-dihydro-1H-benzo[1,3,2]diazaborole
B
trimethylamine
Conditions | Yield |
---|---|
In benzene byproducts: H2; by heating at reflux, then cooling and adding pentane to the mixture; recrystn. from benzene-pentane; | A 92% B n/a |
trimethylamine-1-benzylborane
1,2-diamino-benzene
A
2-benzyl-2,3-dihydro-1H-benzo[1,3,2]diazaborole
B
trimethylamine
Conditions | Yield |
---|---|
In benzene byproducts: H2; reflux, cooling then adding pentane to the mixture; crystn. from benzene-pentane; | A 92% B n/a |
Conditions | Yield |
---|---|
With (CH3)3NSO3 In further solvent(s) 12°C, hydrogencarbonatalkal. soln.; cooling the mixture with ice; | A 92% B n/a |
With (CH3)3NSO3 In further solvent(s) 12°C, hydrogencarbonatalkal. soln.; cooling the mixture with ice; | A 92% B n/a |
1,2-diamino-benzene
A
2-isopropyl-2,3-dihydro-1H-1,3,2-benzodiazaborole
B
trimethylamine
Conditions | Yield |
---|---|
In benzene byproducts: H2; by heating at reflux, then cooling and adding pentane to the mixture; recrystn. from benzene-pentane; | A 91% B n/a |
Conditions | Yield |
---|---|
for 1.5h; Heating; | A 89% B n/a |
1,2-diamino-benzene
A
2-cyclohexyl-2,3-dihydro-1H-benzo[1,3,2]diazaborole
B
trimethylamine
Conditions | Yield |
---|---|
In benzene byproducts: H2; by heating at reflux, cooling and adding pentane to the mixture; recrystn. from benzene-pentane; | A 89% B n/a |
acetic acid 15-allyl-3-benzyloxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl ester
A
acetic acid 3-benzyloxy-15-(3-hydroxy-propyl)-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl ester
B
trimethylamine
Conditions | Yield |
---|---|
Stage #1: acetic acid 15-allyl-3-benzyloxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl ester With 9-bora-bicyclo[3.3.1]nonane In tetrahydrofuran at 10 - 20℃; for 4h; Stage #2: With trimethylamine-N-oxide In tetrahydrofuran; ethanol; diethylene glycol dimethyl ether at 150℃; for 1h; | A 89% B n/a |
C12H15Cl2N3O
A
5-(2,4-dichloro-phenyl)-3-methyl-[1,2,4]oxadiazole
B
trimethylamine
Conditions | Yield |
---|---|
at 170℃; for 0.5h; | A 88% B n/a |
A
ZrCl4Ti(N(CH3)2)4
B
trimethylamine
Conditions | Yield |
---|---|
In pentane under N2, Ti(NMe2)4 in n-pentane added dropwise to suspn. of ZrCl4*2NMe3 in n-pentane, stirred for 24 h; ppt. collected, washed with n-hexane, dried in vac. for 3 h at room temp.; elem. anal.; | A 85.7% B n/a |
Conditions | Yield |
---|---|
for 1.5h; Heating; | A 85% B n/a |
1,2-diamino-benzene
A
2-butyl-2,3-dihydro-1H-benzo[1,3,2]diazaborole
B
trimethylamine
Conditions | Yield |
---|---|
In benzene byproducts: H2; reflux, then cooling and adding pentane to the mixture; recrystn. from benzene-pentane; | A 85% B n/a |
trimethylamine-N-oxide dihydrate
A
(μ-hydrido)(μ-pyridyl)(trimethylamine N-oxide)dirhenium heptacarbonyl
B
trimethylamine
Conditions | Yield |
---|---|
In dichloromethane Re complex dissolved in CH2Cl2, excess Me3NO*2H2O added, stirred vigorously at room temp. for 10 h; filtered, filtrate washed with water, hexane added, slowly evapd.; elem. anal.; | A 84% B n/a |
Conditions | Yield |
---|---|
With C55H43P3Rh(1+)*C32H12BF24(1-); isopropyl alcohol at 80℃; for 24h; Reagent/catalyst; Inert atmosphere; | 82% |
biochemische Reduktion durch gaerende Zucker-Loesungen; | |
With zinc |
diazomethane
methylammonium 1-methylcaffolide
A
3,6,8-trimethyl-1-oxa-3,6,8-triaza-spiro[4.4]nonane-2,4,7,9-tetraone
B
trimethylamine
Conditions | Yield |
---|---|
In diethyl ether for 48h; | A 80% B n/a |
diazomethane
ammonium caffolide
A
3,6,8-trimethyl-1-oxa-3,6,8-triaza-spiro[4.4]nonane-2,4,7,9-tetraone
B
trimethylamine
Conditions | Yield |
---|---|
In diethyl ether for 48h; | A 80% B n/a |
diazomethane
ammonium 1,3-dimethylcaffolide
A
3,6,8-trimethyl-1-oxa-3,6,8-triaza-spiro[4.4]nonane-2,4,7,9-tetraone
B
trimethylamine
Conditions | Yield |
---|---|
In diethyl ether for 48h; | A 80% B n/a |
Conditions | Yield |
---|---|
A 80% B n/a C n/a |
1,2-diamino-benzene
A
2-hexyl-2,3-dihydro-1H-benzo[1,3,2]diazaborole
B
trimethylamine
Conditions | Yield |
---|---|
In benzene byproducts: H2; reflux, then cooling and adding pentane to the mixture; recrystn. from benzene-pentane; | A 79% B n/a |
4-Methylbenzyl bromide
trimethylamine
(4-methylbenzyl)trimethylammonium bromide
Conditions | Yield |
---|---|
In diethyl ether at 0 - 20℃; | 100% |
In tetrahydrofuran; ethanol at 25℃; for 24h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
In water; acetonitrile at 140℃; for 5.5h; | 100% |
In ethanol at 180℃; for 2.5h; | 93% |
at 95℃; |
1,3-propanesultone
trimethylamine
N-(3-sulfonatopropyl)-N,N,N-trimethylammonium
Conditions | Yield |
---|---|
In ethanol; acetone at 0 - 20℃; for 24h; | 100% |
In acetone at 35℃; for 2h; | 86% |
In benzene |
dichloromethanesulphonyl chloride
methanesulfonyl chloride
trimethylamine
A
trichloromethanesulfinyl chloride
B
Trimethylammonium-(methylsulfonyl)methansulfonat
Conditions | Yield |
---|---|
In tetrahydrofuran at -70℃; | A 55% B 100% |
Conditions | Yield |
---|---|
at 20℃; for 24h; | 100% |
dichloromethanesulphonyl chloride
trimethylamine
trimethylammonium trichloromethanesulfinate
Conditions | Yield |
---|---|
In tetrahydrofuran at -70℃; | 100% |
tert-butyl N-[4-(2-bromoethoxy)-3-methoxybenzyl]carbamate
trimethylamine
Conditions | Yield |
---|---|
In methanol for 18h; Heating; | 100% |
trimethylamine
Conditions | Yield |
---|---|
In ethanol at 80℃; for 14h; Substitution; | 100% |
In ethanol; chloroform Reflux; | 91% |
In ethanol at 80℃; for 14h; | 49% |
Toluene-4-sulfonic acid (2R,4R,5R)-5-[1,3]dioxolan-2-yl-4-hydroxy-tetrahydro-furan-2-ylmethyl ester
trimethylamine
Conditions | Yield |
---|---|
In ethanol at 80℃; for 24h; Substitution; | 100% |
trimethylamine
Conditions | Yield |
---|---|
With water for 1h; Reduction; | 100% |
trimethylamine
Conditions | Yield |
---|---|
With water for 1h; Reduction; | 100% |
N-tert-Butyloxycarbonyl-L-glutaminyl-L-threonine 2-bromoethyl ester
trimethylamine
Conditions | Yield |
---|---|
In acetone at 20℃; for 72h; Alkylation; | 100% |
Conditions | Yield |
---|---|
In water at 20℃; | 100% |
2-Amino-6-chloropurin
trimethylamine
2-amino-N,N,N-trimethyl-9H-purine-6-ylammonium chloride
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; | 100% |
In ethanol; dimethyl sulfoxide at 20℃; for 12h; | 76% |
In dimethyl sulfoxide for 12h; | 72% |
2-(N-acetylanilino)-4-chloromethyl-1,3-selenazole
trimethylamine
Conditions | Yield |
---|---|
In benzene at 20℃; for 2h; | 100% |
2-(N-acetylanilino)-4-iodomethyl-1,3-selenazole
trimethylamine
Conditions | Yield |
---|---|
In benzene at 20℃; for 2h; | 100% |
1,4-anhydro-2,3-O-isopropylidene-5-O-toluene-p-sulphonyl-DL-ribitol
trimethylamine
Conditions | Yield |
---|---|
In ethanol at 70℃; for 0.25h; | 100% |
trimethylamine
Conditions | Yield |
---|---|
In tetrahydrofuran at -78 - 20℃; for 24h; | 100% |
1,4-bis(3',5'-bis(6''-bromohexyl)styryl)benzene
trimethylamine
Conditions | Yield |
---|---|
In tetrahydrofuran at -78 - 20℃; for 24h; | 100% |
trimethylamine
Conditions | Yield |
---|---|
In tetrahydrofuran at -78 - 20℃; for 24h; | 100% |
In tetrahydrofuran; water at -78 - 20℃; for 24h; | 92% |
1-(bromomethyl)-2,5-dichloro-4-methylbenzene
trimethylamine
Conditions | Yield |
---|---|
In diethyl ether at 0 - 20℃; | 100% |
In diethyl ether at 0 - 20℃; |
Conditions | Yield |
---|---|
In ethanol | 100% |
4,4'-bis(bromomethyl)-2,2'-bipyridine
trimethylamine
Conditions | Yield |
---|---|
In dichloromethane; water at 20℃; for 24h; | 100% |
In ethanol; water at 20℃; for 1h; Inert atmosphere; | 100% |
In ethanol; water at 20℃; for 1h; | |
In dichloromethane; water at 20℃; for 24h; | |
In dichloromethane at 20℃; for 24h; |
trimethylamine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 50℃; under 750.075 - 1500.15 Torr; for 17h; Autoclave; Industry scale; | 100% |
Conditions | Yield |
---|---|
In not given react. of the Al compd. with an excess of NMe3; | 100% |
6-methylbenzofuran-3-ylmethyl bromide
trimethylamine
Br(1-)*C13H18NO(1+)
Conditions | Yield |
---|---|
In tetrahydrofuran; chloroform at 20℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran; chloroform at 20℃; Inert atmosphere; | 100% |
Methyl 4-(bromomethyl)benzoate
trimethylamine
1-(4-(methoxycarbonyl)phenyl)-N,N,N-trimethylmethanammonium bromide
Conditions | Yield |
---|---|
In water; acetonitrile at 80℃; for 15h; Sealed flask; | 100% |
In acetonitrile at 50℃; for 12h; |
1-(2,3-dioleyl-5-O-tosyl-α-D-ribofuranosyl)-4-nitroimidazole
trimethylamine
1-(2,3-dioleyl-5-trimethylammonium-α-D-ribofuranosyl)-4-nitroimidazole tosylate
Conditions | Yield |
---|---|
In tetrahydrofuran; acetonitrile at 50℃; for 48h; | 100% |
1-(2,3-dioleyl-5-O-tosyl-α-D-ribofuranosyl)-5-nitroindole
trimethylamine
1-(2,3-dioleyl-5-trimethylammonium-α-D-ribofuranosyl)-5-nitroindole tosylate
Conditions | Yield |
---|---|
In tetrahydrofuran; acetonitrile at 50℃; for 48h; | 100% |
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