img _fcksavedurl="/UserAppearance:detailed see specifications Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:It is an important raw material and intermediate used in Organic Synthesis, Phar
Items Standard Result Assay 99.9%min 99.9% Hangzhou Dingyan Chem is a leading manufacturer and supplier of che
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inquiryEthanethiol Basic information Product Name: Ethanethiol Synonyms: 1-Mercaptoethane;Aethanethiol;Aethylmercaptan;C2H5SH;Etantiolo;Ethaanthiol;Ethyl hydrosulfide;Ethy
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryEnglish Name: Ethanethiol English synonyms: 1-Mercaptoethane;Aethanethiol;Aethylmercaptan;C2H5SH;Etantiolo;Ethaanthiol;Ethyl hydrosulfide;Ethyl sulfhydrate CAS 75-08-1 MF
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inquiryEthanethiol CAS: 75-08-1 Specification Item Standard Test Results Identification A.H-NMR:Comply with the structure Complies B.LC-MS:Comply with the structure Complies
Cas:75-08-1
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inquiryProduct Detail Minimum Order Qty. 10 Gram
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Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:75-08-1
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inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid with a penetrating, Storage:Well-sealed and put in dry and cool conditions. Protected from direct sunlight or high temperature. Package:as per your request Ap
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
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Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
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EthanethiolAppearance:liquid Storage:200MT Package:as your requirement Application:Pharmaceutical Intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/FCL for large
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inquirytrichlorogallium * ethanethiol
diethyl ether
A
galliumtrichloride * diethylether
B
ethanethiol
Conditions | Yield |
---|---|
In benzene under inert gas; 5.88 mmol Et2O added to 5.88 mmol of the Ga compound in benzene; stirring at room temp.; 2 phases sepd.; oily phase stirred with n-pentane and dried in vac.; elem. anal.; | A 99% B n/a |
Conditions | Yield |
---|---|
With NH3 | A 98.5% B n/a |
3α-(1,1-Bisethylthioethyl)-3β-hydroxy-14α-methyl-4-nor-5α-cholest-8-ene
A
3α-(1-Ethylthioethenyl)-3β-hydroxy-14α-methyl-4-nor-5α-cholest-8-ene
B
ethanethiol
Conditions | Yield |
---|---|
With copper(l) chloride In N,N-dimethyl-formamide at 50℃; for 0.166667h; | A 98% B n/a |
With copper(l) chloride In N,N-dimethyl-formamide at 50℃; for 0.166667h; other substrates; | A 98% B n/a |
trichlorogallium * ethanethiol
Trimethyl(methylthio)silane
A
chloro-trimethyl-silane
D
methylthiol
E
ethanethiol
Conditions | Yield |
---|---|
In benzene 4.62 mmol Me3SiSMe added to 4.62 mmol of the Ga compound in benzene; stirring at room temp.; filtration; solvent removed in vac.; elem. anal. (Cl2GaSC2H5); | A n/a B 98% C n/a D n/a E n/a |
trichlorogallium * ethanethiol
lead bis(methylthiolate)
C
methylthiol
D
ethanethiol
Conditions | Yield |
---|---|
In benzene 2.10 mmol Pb(SCH3)2 added to 4.20 mmol of the Ga compound in benzene; stirring at room temp.; filtration; solvent removed in vac.; residue washed with n-pentane and dried in vac.; elem. anal. (Cl2GaSC2H5); | A 98% B n/a C n/a D n/a E n/a |
isopentyl-dithiocarbamic acid ethyl ester
A
isopentyl isothiocyanate
B
ethanethiol
Conditions | Yield |
---|---|
at 250 - 260℃; | A 97% B n/a |
3β-(1,1-Bisethylthioethyl)-3α-hydroxy-14α-methyl-4-nor-5β-cholest-8-ene
A
3β-(1-Ethylthioethenyl)-3-α-hydroxy-14α-methyl-4-nor-5β-cholest-8-ene
B
ethanethiol
Conditions | Yield |
---|---|
With copper(l) chloride In N,N-dimethyl-formamide at 50℃; for 0.166667h; | A 97% B n/a |
(3R,5S,8R,9S,10S,13R,14S,17R)-3-(1,1-Bis-ethylsulfanyl-ethyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol
A
(3R,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(1-ethylsulfanyl-vinyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol
B
ethanethiol
Conditions | Yield |
---|---|
With copper(l) chloride In N,N-dimethyl-formamide at 50℃; for 0.166667h; | A 97% B n/a |
methylthiol
ethene
A
dimethylsulfide
B
Ethyl methyl sulfide
C
diethyl sulphide
D
ethanethiol
Conditions | Yield |
---|---|
With 2,2-dimethoxy-2-phenylacetophenone at 45℃; under 2250.23 - 6750.68 Torr; for 14.1h; UV-irradiation; | A n/a B 97% C n/a D n/a |
trichlorogallium * ethanethiol
dimethylsulfide
A
galliumtrichloride * dimethylsulfide
B
ethanethiol
Conditions | Yield |
---|---|
In benzene under inert gas; 6.30 mmol Et2S added to 6.30 mmol of the Ga compound in benzene; stirring at room temp.; 2 phases sepd.; oily phase stirred with n-pentane and dried in vac.; elem. anal.; | A 97% B n/a |
aluminiumtrichloride*ethanediol
diethyl ether
A
aluminium trichloride-diethyl ether (1/1)
B
ethanethiol
Conditions | Yield |
---|---|
In benzene under inert gas; 4.24 mmol Et2O added to 4.23 mmol of the Al compound in benzene; stirring at room temp.; solvent evapd. in vac., residue washed with n-pentane and dried in vac.; elem. anal.; | A 97% B n/a |
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride In various solvent(s) under 0.0750075 Torr; Reduction; | 96% |
at 496℃; mit Naphtha-Daempfen; | |
With diethyl ether; sodium |
Methyldithiocarbamidsaeure-ethylester
A
methyl thioisocyanate
B
ethanethiol
Conditions | Yield |
---|---|
at 250 - 260℃; | A 96% B n/a |
(3S,5S,8R,9S,10S,13R,14S,17R)-3-(1,1-Bis-ethylsulfanyl-ethyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol
A
(3S,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(1-ethylsulfanyl-vinyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol
B
ethanethiol
Conditions | Yield |
---|---|
With copper(l) chloride In N,N-dimethyl-formamide at 50℃; for 0.166667h; | A 96% B n/a |
aluminiumtrichloride*ethanediol
dimethylsulfide
A
aluminiumtrichloride * dimethylsulfide
B
ethanethiol
Conditions | Yield |
---|---|
In benzene under inert gas; 5.52 mmol Et2S added to 5.53 mmol of the Al compound in benzene; stirring at room temp.; solvent evapd. in vac.; residue washed with n-pentane and dried in vac.; elem. anal.; | A 96% B n/a |
diethyl dimethylphosphoramidodithioite
A
triethyl trithiophosphite
C
ethanethiol
Conditions | Yield |
---|---|
With water at 120 - 130℃; for 0.5h; | A 81% B 72% C 95% |
ethyl cyclohexyldithiocarbamate
A
ethanethiol
B
isothiocyanatocyclohexane
Conditions | Yield |
---|---|
at 250 - 260℃; | A 95% B 92% |
aluminiumtrichloride*ethanediol
trimethylamine
A
aluminiumtrichloride * trimethylamine
B
ethanethiol
Conditions | Yield |
---|---|
In benzene under inert gas; 6.06 mmol Me3N in benzene added to 6.04 mmol of the Al compound in benzene; stirring at room temp.; solvent removed in vac.; residue washed with n-pentane and dried in vac.; elem. anal.; | A 95% B n/a |
3,3-Bis-ethylsulfanyl-2-phenyl-butan-2-ol
A
3-Ethylsulfanyl-2-phenyl-but-3-en-2-ol
B
ethanethiol
Conditions | Yield |
---|---|
With copper(l) chloride In N,N-dimethyl-formamide at 50℃; for 0.166667h; | A 94% B n/a |
Conditions | Yield |
---|---|
In chloroform 1:1 mixt. stirred for 10 min; evapd., washed (Et2O), dried (vac.); NMR; | A 94% B n/a |
Conditions | Yield |
---|---|
at 250 - 260℃; | A 93% B n/a |
Conditions | Yield |
---|---|
at 250 - 260℃; | A 87% B 93% |
ethyl ethylselenosulfenate
ethanethiol
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride In various solvent(s) under 0.0750075 Torr; Reduction; | 92% |
Octyl-dithiocarbamic acid ethyl ester
A
n-octylisothiocyanate
B
ethanethiol
Conditions | Yield |
---|---|
at 250 - 260℃; | A 91% B n/a |
Propyl-dithiocarbamic acid ethyl ester
A
n-Propyl isothiocyanate
B
ethanethiol
Conditions | Yield |
---|---|
at 250 - 260℃; | A 89% B n/a |
triethyl trithiophosphite
benzoic acid
A
S-ethyl thiobenzoate
B
ethanethiol
Conditions | Yield |
---|---|
at 120 - 130℃; under 90 Torr; for 4h; Product distribution; | A 89% B 61% C n/a |
Conditions | Yield |
---|---|
With NH3 -70°C, then warming at room temp. 15 h; | A 89% B n/a |
Conditions | Yield |
---|---|
With ammonia | A 88.5% B n/a |
With NH3 | A 88.5% B n/a |
Hexyl-dithiocarbamic acid ethyl ester
A
n-hexyl isothiocyanate
B
ethanethiol
Conditions | Yield |
---|---|
at 250 - 260℃; | A 85% B n/a |
Conditions | Yield |
---|---|
With sodium hydroxide; water at 25 - 40℃; for 1h; Addition; | 100% |
With water | |
for 2h; Ambient temperature; |
Conditions | Yield |
---|---|
1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione In chloroform at 20℃; | 100% |
With air; iron(III) chloride; sodium iodide In acetonitrile for 0.116667h; Ambient temperature; | 98% |
With oxygen; SiO2-Cl In dichloromethane at 0℃; for 0.166667h; | 98% |
Conditions | Yield |
---|---|
With sodium hydroxide In methanol at 0 - 20℃; for 1h; | 100% |
(i) Na, liq. NH3, (ii) /BRN= 605309/; Multistep reaction; | |
With sodium ethanolate In ethanol |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 25℃; | 100% |
With sodium hydride In tetrahydrofuran |
1,3-Dimethyl-6-chlorouracil
ethanethiol
6-Ethylsulfanyl-1,3-dimethyl-1H-pyrimidine-2,4-dione
Conditions | Yield |
---|---|
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride In dichloromethane; water for 2.5h; Ambient temperature; | 100% |
1,3-diphenylpropanedione
ethanethiol
3-ethylsulfanyl-1,3-diphenylprop-2-en-1-one
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In benzene for 15h; Heating; | 100% |
1,2,4,6-tetra-O-acetyl-3-O-benzyl-β-D-glucopyranose
ethanethiol
ethyl 2,4,6-tri-O-acetyl-3-O-benzyl-1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane for 2h; Ambient temperature; | 100% |
With molecular sieve; boron trifluoride diethyl etherate In dichloromethane for 2h; Ambient temperature; | 91% |
With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve In dichloromethane at 0℃; for 2h; | 79% |
Conditions | Yield |
---|---|
With lithium hydroxide In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; | 100% |
diethyl 2,4-dinitrobenzylidenemalonate
ethanethiol
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran Ambient temperature; | 100% |
cis-2,6-dihydroxy-1,4-dioxathiane
ethanethiol
thiodiglycolaldehyde bis(diethyl dithioacetal)
Conditions | Yield |
---|---|
With hydrogenchloride at 0℃; for 0.5h; | 100% |
(S)-2-formylpyrrolidine-1-carboxylic acid benzyl ester
ethanethiol
benzyl (2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolecarboxylate
Conditions | Yield |
---|---|
Stage #1: (S)-2-formylpyrrolidine-1-carboxylic acid benzyl ester; ethanethiol In chloroform for 0.5h; Inert atmosphere; Stage #2: With chloro-trimethyl-silane In chloroform at 20℃; Inert atmosphere; | 100% |
With chloro-trimethyl-silane In chloroform | 79% |
(3S,4R)-3-Hydroxy-1,4-dimethyl-5-oxo-3-((3aR,5S,7R,7aR)-2,2,7-trimethyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran-5-yl)-pyrrolidine-2,2-dicarboxylic acid dimethyl ester
ethanethiol
(3R,3aS,4S,6aR)-4-((2R,3R)-4,4-Bis-ethylsulfanyl-3-hydroxy-2-methyl-butyl)-3a-hydroxy-1,3-dimethyl-2,6-dioxo-tetrahydro-furo[3,4-b]pyrrole-6a-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With hydrogenchloride | 100% |
ethanethiol
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile -78 deg C to RT; | 100% |
Conditions | Yield |
---|---|
In toluene for 20h; Ambient temperature; | 100% |
5-Methoxy-4-phenyl-5,6-dihydro-4H-[1,3,4]thiadiazine
ethanethiol
Conditions | Yield |
---|---|
Ambient temperature; | 100% |
1,1-dibromo-4-chloro-3,3-dimethyl-2-butanone
ethanethiol
4-chloro-1-(ethylthio)-3,3-dimethyl-2-butanone
Conditions | Yield |
---|---|
With sodium methylate In methanol for 1h; Ambient temperature; | 100% |
With sodium methylate 1.) MeOH, ice-cooling, 5 min, 2.) r.t., 1 h; Yield given; |
(S)-(-)-1,1-dimethylethyl <3-methyl-1-<<(methylsulfonyl)oxy>methyl>butyl>carbamate
ethanethiol
tert-butyl (S)-N-[1-(ethylsulfanylmethyl)-3-methylbutyl]carbamate
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran Heating; | 100% |
(2S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropyl methanesulfonate
ethanethiol
tert-butyl (S)-N-[1-(ethylsulfanylmethyl)-2-phenylethyl]carbamate
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 67℃; for 2h; | 100% |
Stage #1: ethanethiol With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: (2S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropyl methanesulfonate In tetrahydrofuran at 20℃; for 12h; |
(R)-1-<(1,1-dimethylethoxy)carbonyl>-2-pyrrolidinemethanolmethanesulfonate
ethanethiol
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran Heating; | 100% |
(S)-2-[ (tert-butoxycarbonyl)-amino]-3-(4-methoxyphenyl)-propylmethanesulfonate
ethanethiol
[(S)-1-Ethylsulfanylmethyl-2-(4-methoxy-phenyl)-ethyl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran for 2h; Heating; | 100% |
4-((S)-2-tert-Butoxycarbonylamino-3-methanesulfonyloxy-propyl)-imidazole-1-carboxylic acid tert-butyl ester
ethanethiol
[(S)-1-Ethylsulfanylmethyl-2-(1H-imidazol-4-yl)-ethyl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran Heating; | 100% |
ethanethiol
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60℃; | 100% |
ethylene dibromide
ethanethiol
2,2'-ethane-1,2-diylbissulfanyl-bis-ethanol
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 1h; Heating; | 100% |
N-propargyl-2,4-bis(trifluoroacetyl)-1-naphthylamine
ethanethiol
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 24h; Ambient temperature; | 100% |
(-)-(4S,5R,2'S,3'R)-3-(3-hydroxy-2-methylbutanoyl)-4-methyl-5-phenyl-1,3-oxazolidin-2-one
ethanethiol
A
(4S,5R)-4-methyl-5-phenyl-oxazolidin-2-one
B
(+)-S-ethyl (2S,3R)-3-hydroxy-2-methylbutanethioate
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Substitution; | A 100% B 99% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 48h; Addition; Michael addition; | 100% |
ethanethiol
2-{6-[7-(4-benzyl-2-oxo-oxazolidine-3-carbonyl)-4-(tert-butyl-dimethyl-silanyloxy)-1-(4-methoxy-benzyloxy)-5,9-dimethyl-6-oxo-undec-10-ynyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester
Conditions | Yield |
---|---|
With potassium hydride In tetrahydrofuran at 25℃; for 3h; | 100% |
ethanethiol
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve In dichloromethane at 0℃; for 1.08333h; Substitution; | 100% |
Conditions | Yield |
---|---|
Stage #1: ethanethiol With sodium hydroxide In water at 20℃; for 0.5h; Stage #2: 2-chloro-benzaldehyde With tetrabutylammomium bromide In water at 82℃; | 100% |
With tetrabutylammomium bromide; sodium hydroxide In water at 82℃; for 4 - 6h; | 95% |
With sodium carbonate In N,N-dimethyl-formamide at 100℃; for 24h; | 80% |
Stage #1: ethanethiol With sodium hydroxide In water for 1h; Stage #2: 2-chloro-benzaldehyde With tetrabutylammomium bromide In water for 4h; Reflux; |
Conditions | Yield |
---|---|
Stage #1: ethanethiol With sodium tetrahydroborate; sodium hydroxide In water at 5℃; Inert atmosphere; Stage #2: isopropyl bromide; tetrabutylammomium bromide In water at 50℃; Inert atmosphere; | 100% |
With potassium hydroxide In ethanol for 0.5h; Heating; | 51% |
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